As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
Cas:584-12-3
Min.Order:1 Kilogram
FOB Price: $3.0
Type:Lab/Research institutions
inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
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Min.Order:1 Kilogram
FOB Price: $139.0 / 210.0
Type:Trading Company
inquiryOur Advantage Rich Experience Our products are sold all over Europe,North&South America, Sino-East, Asia and pacific area as well as Africa,we establish long term. Quality service Company cooperates with research institutes. We strictly con
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Min.Order:1 Kilogram
FOB Price: $15.0 / 50.0
Type:Trading Company
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Min.Order:1 Gram
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Type:Lab/Research institutions
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2-Bromofuran CAS:584-12-3 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermediates,
Cas:584-12-3
Min.Order:1 Gram
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
2-Bromofuran Basic information Product Name: 2-Bromofuran Synonyms: BUTTPARK 98\57-03;2-BROMOFURAN;2-Bromofuran96%;2-Bromofurane;2-BROMOETHYLAMIN
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Min.Order:1 Metric Ton
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inquiry2-Bromofuran Chemical Properties Melting point 116 °C Boiling point 52 °C density 1.662 refractive index 1.4960 to 1.5000 Fp 3°C Sensitive Light Sensitive λmax 216nm(EtOH)(lit.) CAS DataBase Reference
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inquiryhigh purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
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Acmec is a leading manufacturer and supplier of biochemical reagents and life science products. We have over 40,000 items in stock (real-time inventory) and offer discounted prices to registered members of the online store ( www.acmec.com.cn ) Appea
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Min.Order:1 bottle
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inquirybulk productiongoods in stockswe have the best competitive price in the marketmeantime,we are committed to service to our every customer Chemsigma International Co.,Ltd. is a chemical manufacturer, specialize in custom synthesis and organic chemical
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high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:any port in China
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Conditions | Yield |
---|---|
With bromine; ethyllithium In diethyl ether 1.) 25 deg C, 1 h, 2.) -80 deg C; | 83% |
With 2,4,4,6-Tetrabromo-2,5-cyclohexadien-1-one for 0.0222222h; microwave irradiation; | 78% |
With hexabromocyclopenta-1,3-diene In acetonitrile Heating; | 75% |
Conditions | Yield |
---|---|
With copper In quinoline Heating; | 81% |
With quinoline; copper at 210℃; | 75% |
With quinoline; copper | |
With water; mercury dichloride |
Conditions | Yield |
---|---|
With bromine In N,N-dimethyl-formamide at 30 - 35℃; for 1.5h; | A 72% B 8% |
With N-Bromosuccinimide; p-toluenesulfonic acid monohydrate In benzene |
Conditions | Yield |
---|---|
With bromine In N-methyl-acetamide; (2S)-N-methyl-1-phenylpropan-2-amine hydrate | 23% |
1,4-dioxane
furan
bromocyane
A
2-bromofuran
B
2-furancarbonitrile
Conditions | Yield |
---|---|
With 1,4-dioxane anschliessend Erhitzen mit wss. Natronlauge und Natriumsulfit; |
Conditions | Yield |
---|---|
With 1,4-dioxane Erhitzen des Reaktionsgemisches mit wss. Natronlauge und Natriumsulfit; |
2-bromofuran
Conditions | Yield |
---|---|
With hydrogenchloride |
Conditions | Yield |
---|---|
With 1,10-Phenanthroline; oxygen; potassium carbonate In dimethyl sulfoxide at 140℃; under 3750.38 Torr; for 18h; Autoclave; Molecular sieve; | 57 %Chromat. |
Conditions | Yield |
---|---|
With 1,10-Phenanthroline; oxygen; potassium carbonate In dimethyl sulfoxide at 140℃; under 3750.38 Torr; for 18h; Autoclave; Molecular sieve; | 72 %Chromat. |
2-bromofuran
tert-Butyldimethyl(prop-2-ynyloxy)silane
Conditions | Yield |
---|---|
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine at 70℃; Inert atmosphere; | 100% |
Conditions | Yield |
---|---|
With copper(l) iodide; potassium carbonate; N,N`-dimethylethylenediamine at 110℃; for 24h; | 99% |
With copper(l) iodide; potassium carbonate; N,N`-dimethylethylenediamine In 1,4-dioxane at 110℃; for 24h; | 82% |
2-bromofuran
3,4-dimethylphenylmagnesium bromide
2-(3,4-dimethylphenyl)furan
Conditions | Yield |
---|---|
1,2-bis(diphenylphosphino)ethane nickel(II) chloride In diethyl ether for 16h; Ambient temperature; | 98% |
Conditions | Yield |
---|---|
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride In diethyl ether 1.) -30 deg C; 2.) RT, 5h; | 98% |
Conditions | Yield |
---|---|
With tetrabutylammomium bromide In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide 2:1 substrate/Me2SiCl2 ratio, electrochemical conditions (Mg anode, 2.2 F.mol-1); | 98% |
Conditions | Yield |
---|---|
With palladium diacetate; sodium t-butanolate; nixantphos In N,N-dimethyl-formamide at 24℃; for 12h; Heck Reaction; Inert atmosphere; | 98% |
With potassium carbonate In dimethyl sulfoxide at 100℃; for 8h; Green chemistry; | 56 %Chromat. |
Conditions | Yield |
---|---|
1,2-bis(diphenylphosphino)ethane nickel(II) chloride In diethyl ether for 16h; Ambient temperature; | 97% |
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In water; N,N-dimethyl-formamide at 75 - 85℃; Suzuki coupling; Inert atmosphere; | 97% |
With bis-triphenylphosphine-palladium(II) chloride; potassium carbonate In water; N,N-dimethyl-formamide at 75 - 85℃; Suzuki coupling; Inert atmosphere; | 56% |
With sodium carbonate; tetrakis(triphenylphosphine) palladium(0) In 1,2-dimethoxyethane; ethanol; water |
Conditions | Yield |
---|---|
With potassium carbonate In ethanol; water at 20℃; for 16h; Suzuki-Miyaura Coupling; | 97% |
With potassium carbonate In ethanol; water at 90℃; for 0.5h; Suzuki Coupling; Microwave irradiation; | 92% |
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In water; N,N-dimethyl-formamide at 75 - 85℃; Suzuki coupling; Inert atmosphere; | 77% |
With bis-triphenylphosphine-palladium(II) chloride; potassium carbonate In water; N,N-dimethyl-formamide at 75 - 85℃; Suzuki coupling; Inert atmosphere; | 57% |
Conditions | Yield |
---|---|
Inert atmosphere; | 97% |
Conditions | Yield |
---|---|
With tetrabutylammomium bromide In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide electrochemical conditions (Mg anode, 2.2 F.mol-1); | 96% |
Conditions | Yield |
---|---|
Stage #1: 2-bromofuran With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 1h; Inert atmosphere; Stage #2: With zinc(II) chloride In tetrahydrofuran; hexane at -78 - 20℃; Inert atmosphere; Stage #3: 4-bromoisoquinoline With methanesulfonic acid(2-dicyclohexylphosphino-2′,4′,6′-triisopropyl-1,1′-biphenyl)[2-(2′-amino-1,1′-biphenyl)]palladium(II); XPhos In tetrahydrofuran; hexane at 20℃; for 12h; Negishi Coupling; Inert atmosphere; | 96% |
Conditions | Yield |
---|---|
With tetrabutylammomium bromide In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide electrochemical conditions (Mg anode, 2.2 F.mol-1); | 95% |
Conditions | Yield |
---|---|
With potassium carbonate In ethanol; water at 80℃; for 0.333333h; Suzuki-Miyaura Coupling; | 95% |
With potassium phosphate; tetraphosphine N,N,N′,N′-tetra(diphenylphosphinomethyl)-pyridine-2,6-diamine; palladium dichloride In o-xylene at 90℃; for 24h; Concentration; Suzuki-Miyaura Coupling; Inert atmosphere; Schlenk technique; | 93% |
With C30H18Cl2N2O4Pd; tetrabutylammomium bromide; potassium carbonate In ethanol at 60℃; Suzuki-Miyaura Coupling; Sealed tube; Microwave irradiation; | 93% |
2-bromofuran
2-formylthiophene-3-boronic acid
3-(furan-2-yl)thiophene-2-carbaldehyde
Conditions | Yield |
---|---|
With bis-triphenylphosphine-palladium(II) chloride; sodium carbonate In water; acetonitrile at 150℃; for 0.1h; Suzuki coupling; Microwave irradiation; | 95% |
2-bromofuran
1-methyl-5-(pent-4-ynyl)-3,4-dihydropyridin-2(1H)-one
5-(5-(furan-2-yl)pent-4-ynyl)-1-methyl-3,4-dihydropyridin-2(1H)-one
Conditions | Yield |
---|---|
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine In dichloromethane at 20℃; for 24h; Sonogashira coupling; Inert atmosphere; | 95% |
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In water; N,N-dimethyl-formamide at 75 - 85℃; Suzuki coupling; Inert atmosphere; | 95% |
With bis-triphenylphosphine-palladium(II) chloride; potassium carbonate In water; N,N-dimethyl-formamide at 75 - 85℃; Suzuki coupling; Inert atmosphere; | 80% |
Conditions | Yield |
---|---|
With tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; sodium t-butanolate In toluene at 100℃; | 95% |
2-bromofuran
dichloromethylphenylsilane
di(2-furyl)(methyl)phenylsilane
Conditions | Yield |
---|---|
With tetrabutylammomium bromide In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide 2:1 substrate/PhMeSiCl2 ratio, electrochemical conditions (Mg anode, 2.2 F.mol-1); | 94% |
Conditions | Yield |
---|---|
With {1,3-bis[2,6-bis(propan-2-yl)phenyl]-1,3-dihydro-2H-imidazol-2-ylidene}dichloro(pyridine)palladium; caesium carbonate In neat (no solvent) at 100℃; for 12h; Heck Reaction; | 93% |
Conditions | Yield |
---|---|
With palladium diacetate; caesium carbonate; triphenylphosphine In 1-methyl-pyrrolidin-2-one at 90℃; for 1h; | 92% |
2-bromofuran
tert-butylisonitrile
furan-2-carboxylic acid tert-butylamide
Conditions | Yield |
---|---|
With 4,5-dimethyl-1,3-bis-(2,4,6-trimethylphenyl)-3H-imidazol-1-ium chloride; water; nickel dibromide; sodium t-butanolate In toluene at 150℃; for 20h; Schlenk technique; Inert atmosphere; Sealed tube; | 92% |
2-bromofuran
tris-(4-ethoxy-phenyl)-bismuthine
2-(4-ethoxyphenyl)furan
Conditions | Yield |
---|---|
With palladium diacetate; caesium carbonate; triphenylphosphine In 1-methyl-pyrrolidin-2-one at 90℃; for 1h; | 91% |
Conditions | Yield |
---|---|
With [PhCOPd(PtBu3)I]; dtbpf In 2-methyltetrahydrofuran at 80℃; for 18h; Inert atmosphere; | 91% |
Conditions | Yield |
---|---|
With tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; sodium t-butanolate In toluene at 100℃; | 90% |
Conditions | Yield |
---|---|
Stage #1: 2-bromofuran; 1-(2′-naphthyl)-4,4,4-trifluorobut-2-yn-1-one In dichloromethane at 20℃; for 6h; Diels-Alder Cycloaddition; Stage #2: With diiron nonacarbonyl In toluene at 80℃; for 2h; regioselective reaction; | 89% |
Conditions | Yield |
---|---|
With tetrabutylammomium bromide In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide electrochemical conditions; | 88% |
Stage #1: 2-bromofuran With n-butyllithium In diethyl ether at 0 - 20℃; for 3.33333h; Inert atmosphere; Stage #2: chloro-trimethyl-silane In diethyl ether at 0℃; Inert atmosphere; | 51% |
Conditions | Yield |
---|---|
Stage #1: 2-bromofuran With n-butyllithium; Triisopropyl borate In tetrahydrofuran; hexane at -78℃; for 1h; Inert atmosphere; Stage #2: 5-bromo-1H-indole With potassium phosphate; chloro-(2-dicyclohexylphosphino-2,4,6-triisopropyl-1,1-biphenyl)[2-(2-amino-1,1-biphenyl)]palladium(II) In tetrahydrofuran; hexane; water at 40℃; for 2h; Suzuki-Miyaura Coupling; Inert atmosphere; | 88% |
Conditions | Yield |
---|---|
With tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; sodium t-butanolate In toluene at 105℃; for 24h; Inert atmosphere; | 87.2% |
Conditions | Yield |
---|---|
With tetrabutylammomium bromide In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide 1:20 substrate/Me2SiCl2 ratio, electrochemical conditions (Mg anode, 2.2 F.mol-1); | 87% |
Stage #1: 2-bromofuran With magnesium; ethylene dibromide In tetrahydrofuran Inert atmosphere; Reflux; Stage #2: dimethylsilicon dichloride In tetrahydrofuran; diethyl ether at 20℃; for 20h; |
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