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inquiryItems Standard Result Assay (Ursolic acid) 98%min 98.22% ----------------------------------------------------------------
Cas:6065-82-3
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inquiryProduct description: Product Name Ethyl diethoxyacetate CAS No. 6065-82-3 Appearance Colorless transparent liquid Assay ≥99% Capacity 100mt/year Application Pharmaceutical in
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inquiryEthyl diethoxyacetate Basic information Product Name: Ethyl diethoxyacetate Synonyms: GLYOXALIC ACID ETHYL ESTER DIETHYL ACETAL;GLYOXYLIC ACID ETHYL ESTER DIETHYL ACETAL;ETHYL GLYOXALATE
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inquiryProduct name:Ethyl diethoxyacetate Cas No.:6065-82-3 Einecs No.:227-999-8 MF:C8H16O4 Purity:99.0%min Appearance:Colorless Clear Liquid Storage:Preserve in well-closed, light-resistant and airtight containers. Package:25KG/Drum Application:Synthes
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inquiryProduct Name: Ethyl diethoxyacetate Synonyms: Diethoxyacetic acid ethyl ester~Ethyl glyoxylate diethyl acetal~Glyoxylic acid ethyl ester diethyl acetal;2,6 DEA;Ethyldiethoxyacetate,98%;ethyl glyoxylate diethyl acetal;Acetic acid, diethoxy-, ethyl
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inquiryBest quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
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Cas:6065-82-3
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inquiryProduct name: Ethyl Diethoxyacetate CAS No.:6065-82-3 Molecule Formula: C8H16O4 Molecule Weight:176.21 Purity: 99.0% Package: 25kg/drum Description:Colorless transparent liquid Manufacture Standards:Enterprise Standard TESTING IT
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inquiryOur Advantages A. International Top level TechnologyOur company owned biomedicine experts are famous at home and abroad with rich experience in research and development in the field of efficient chiral functional molecules research and development an
Ethyl diethoxyacetate Chemical Properties Melting point 198-200 Boiling point 199 °C(lit.) density 0.985 g/mL at 25 °C(lit.) refractive index n20/D 1.410(lit.) Fp 73°C solubility Soluble in Dichloromethane, Ethyl A
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inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
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Conditions | Yield |
---|---|
Stage #1: Glyoxilic acid In water at 70℃; under 37.5038 Torr; Stage #2: ethanol; sulfuric acid In water Product distribution / selectivity; Heating / reflux; | 90% |
at 120℃; | |
With hydrogenchloride unter Entfernen von Wasser; | |
In water; benzene Heating; |
Conditions | Yield |
---|---|
sulfuric acid Product distribution / selectivity; Heating / reflux; | 90% |
Conditions | Yield |
---|---|
With hydrogenchloride at 0 - 5℃; | 85% |
ethanol
3,6-diethoxy-2,5-piperazinedione
A
ethyl 2-(diethoxyacetylamino)-2-ethoxyacetate
B
Ethyl diethoxyacetate
Conditions | Yield |
---|---|
With hydrogen bromide for 1.5h; Product distribution; Heating; | A 42% B 31% |
ethanol
ethyl 2-(diethoxyacetylamino)-2-ethoxyacetate
Ethyl diethoxyacetate
Conditions | Yield |
---|---|
With hydrogenchloride for 3h; Heating; | 39% |
With hydrogenchloride In ethanol for 3h; Product distribution; Heating; | 39% |
ethanol
ethyl N-(2-diethoxyacetyl)glycinate
A
glycine ethyl ester hydrochloride
B
Ethyl diethoxyacetate
Conditions | Yield |
---|---|
With hydrogenchloride for 3h; Heating; | A 35% B 38% |
With hydrogenchloride for 3h; Product distribution; Heating; | A 35% B 38% |
diethoxycarbonium fluoroborate
A
pentaethoxyethane
B
ethyl 2,2,3,3-tetraethoxypropanoate
C
Ethyl diethoxyacetate
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In dichloromethane at -10℃; | A 11% B 35% C 2% |
With N-ethyl-N,N-diisopropylamine In dichloromethane at -10℃; | A 11% B 35% C 2% |
ethanol
3,6-Dibromo-piperazine-2,5-dione
A
ethyl N-(2-diethoxyacetyl)glycinate
B
3,6-diethoxy-2,5-piperazinedione
C
N-(1-ethoxy-1-ethoxycarbonylmethyl)oxamide
D
ethyl 2-(diethoxyacetylamino)-2-ethoxyacetate
E
Ethyl diethoxyacetate
Conditions | Yield |
---|---|
In dichloromethane Ambient temperature; other nucleophiles and reactions products; | A 13% B 3.3% C 1.6% D 24.8% E 4.2% |
Conditions | Yield |
---|---|
Veresterung mit alkoh. Schwefelsaeure; | |
Veresterung mit alkoh. Salzsaeure; | |
Behandlung des Silbersalzes mit Aethyljodid; | |
folgende Veresterung mit alkoh. HCl; |
dichloro-acetic acid
sodium ethanolate
A
ethyl 2-ethoxyglycolate
B
Ethyl diethoxyacetate
Conditions | Yield |
---|---|
und Veresterung des Reaktionsproduktes; |
ethanol
ethyl 2,2-diethoxyethanimidate
A
2,2-diethoxyacetonitrile
B
diethoxyacetamide
C
pentaethoxyethane
D
Ethyl diethoxyacetate
Conditions | Yield |
---|---|
With ethanol |
sodium ethanolate
ethyl 1,1-dichloroacetate
A
2,2-diethoxy-3-chloro-succinic acid diethyl ester
B
Ethyl diethoxyacetate
Conditions | Yield |
---|---|
With tert-butylhypochlorite |
Conditions | Yield |
---|---|
(i) Mor, (ii) /BRN= 1718733/, HCl; Multistep reaction; |
Conditions | Yield |
---|---|
With pyridine; triethylamine In benzene |
ethanol
ethyl 2-bromo-2-ethoxy-acetate
A
2-Ethoxy-3-ethoxycarbonyl-bernsteinsaeurediethylester
B
Ethyl diethoxyacetate
Conditions | Yield |
---|---|
With sodium 1.) RT; 2.) 70 deg C, 3 h; Yield given. Multistep reaction; |
ethanol
3,6-Dibromo-piperazine-2,5-dione
A
ethyl N-(2-diethoxyacetyl)glycinate
B
3,6-diethoxy-2,5-piperazinedione
C
ethyl 2-(diethoxyacetylamino)-2-ethoxyacetate
D
Ethyl diethoxyacetate
Conditions | Yield |
---|---|
In dichloromethane Ambient temperature; Yield given. Further byproducts given. Yields of byproduct given; |
ethanol
Glyoxilic acid
A
3,6-Diethoxy-[1,4]dioxane-2,5-dione
B
diethoxy-4,5-dioxolanne-1,3 carboxylate-2 d'ethyle
C
Ethoxy-(ethoxy-ethoxycarbonyl-methoxy)-acetic acid ethyl ester
D
Ethyl diethoxyacetate
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid 1.) benzene, reflux, 3 h; 2.) reflux, 16 h; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts; |
Conditions | Yield |
---|---|
With pyridine |
Conditions | Yield |
---|---|
at 100 - 130℃; |
Conditions | Yield |
---|---|
With hydrogenchloride |
Ethyl diethoxyacetate
Conditions | Yield |
---|---|
With water Electrolysis.an Platin-Elektroden; |
2,3-diethoxy-3-oxopropionic acid
water
A
ethyl 2-ethoxyglycolate
B
ethanol
C
Ethyl diethoxyacetate
Conditions | Yield |
---|---|
das Kaliumsalz liefert an Platin-Elektroden; Pr.5: Acetaldehyd, Pr.6: Formaldehyd, Pr.7: Oxalsaeure.Electrolysis; |
Ethyl diethoxyacetate
ethyl 2-chloro-2-ethoxyacetate
Conditions | Yield |
---|---|
With iodine; acetyl chloride at 50℃; for 22h; | 100% |
With iodine; acetyl chloride at 50℃; for 24h; Product distribution / selectivity; | 100% |
With acetyl chloride; iodine at 50℃; for 1h; | 82% |
With phosphorus pentachloride at 80 - 140℃; | |
With iodine; acetyl chloride |
Ethyl diethoxyacetate
diethoxyacetamide
Conditions | Yield |
---|---|
With ammonia In ethanol for 48h; Ambient temperature; | 100% |
With ammonia; water for 40h; | 99% |
With ammonium hydroxide at 25 - 30℃; | 95% |
Conditions | Yield |
---|---|
With titanium(IV) iodide In acetonitrile at -78℃; | 100% |
Conditions | Yield |
---|---|
With iodine | 100% |
Ethyl propionate
Ethyl diethoxyacetate
ethyl 4,4-diethoxy-2-methyl-3-oxobutanoate
Conditions | Yield |
---|---|
With lithium diisopropyl amide In tetrahydrofuran at -78 - 20℃; Claisen condensation; | 99% |
With sodium at 80℃; | |
With sodium ethanolate |
Ethyl diethoxyacetate
Conditions | Yield |
---|---|
With boron trifluoride diethyl etherate In dichloromethane; toluene at 20℃; for 96h; Inert atmosphere; | 99% |
(trimethylsilyl)methylmagnesium chloride
Ethyl diethoxyacetate
1,1-Diethoxy-3-trimethylsilanyl-2-trimethylsilanylmethyl-propan-2-ol
Conditions | Yield |
---|---|
With cerium(III) chloride | 98% |
With cerium(III) chloride In tetrahydrofuran at -78℃; | 90% |
Ethyl diethoxyacetate
Conditions | Yield |
---|---|
With sodium hydroxide In ethanol; water for 5h; Heating; | 97% |
benzylmagnesium chloride
Ethyl diethoxyacetate
1,1-diethoxy-3-phenylpropane-2-one
Conditions | Yield |
---|---|
In tetrahydrofuran at -78℃; for 2h; | 96% |
In tetrahydrofuran at -78℃; for 12h; | 93% |
In tetrahydrofuran at -78℃; for 2h; | 91.8% |
Conditions | Yield |
---|---|
With potassium carbonate In neat (no solvent) at 100℃; for 6h; | 96% |
p-toluamidoxime
Ethyl diethoxyacetate
Conditions | Yield |
---|---|
With potassium carbonate In neat (no solvent) at 100℃; for 6h; | 96% |
Ethyl diethoxyacetate
2,2-diethoxy acetic acid
Conditions | Yield |
---|---|
With water; sodium hydroxide at 70℃; for 0.5h; Industrial scale; | 95.1% |
Stage #1: Ethyl diethoxyacetate With water; sodium hydroxide In ethanol at 20℃; for 1h; Stage #2: With hydrogenchloride In water | 88% |
With sodium hydroxide In ethanol at 20℃; for 3h; | 85% |
dimethyl amine
Ethyl diethoxyacetate
2,2-diethoxy-N,N-dimethylacetamide
Conditions | Yield |
---|---|
With sodium methylate In methanol at 45 - 50℃; for 4h; Product distribution / selectivity; | 95% |
With calcium chloride at 15 - 100℃; | |
With n-butyllithium; hexane 1.) -78 deg C, 15 min, THF, 2.) 3 h, from -78 deg C to room temperature; 1 h, room temperature; Yield given. Multistep reaction; |
Conditions | Yield |
---|---|
With titanium tetrachloride In nitromethane at 20℃; for 12h; Cooling with ice; | 95% |
1.3-propanedithiol
Ethyl diethoxyacetate
ethyl 1,3-dithiane-2-carboxylate
Conditions | Yield |
---|---|
With boron trifluoride diethyl etherate In chloroform for 1.5h; Heating / reflux; | 94% |
With boron trifluoride diethyl etherate In dichloromethane for 14h; Ambient temperature; | 60% |
Stage #1: 1.3-propanedithiol With boron trifluoride diethyl etherate In chloroform at -70℃; Stage #2: Ethyl diethoxyacetate In chloroform at 70℃; for 1h; | 47% |
N'-hydroxy-3-methylbenzimidamide
Ethyl diethoxyacetate
Conditions | Yield |
---|---|
With potassium carbonate In neat (no solvent) at 100℃; for 6h; | 94% |
Conditions | Yield |
---|---|
Stage #1: ethyl acetate; Ethyl diethoxyacetate With sodium at 20 - 60℃; for 20h; Inert atmosphere; Stage #2: With hydrogenchloride In ethanol; water pH=6; | 93% |
With sodium at 20 - 60℃; for 19h; Claisen Condensation; Inert atmosphere; | 89% |
With sodium hydride In tetrahydrofuran at 20℃; for 20.5h; Heating / reflux; | 81% |
Conditions | Yield |
---|---|
Stage #1: chloro-trimethyl-silane; C17H24N2O5 In 1,2-dichloro-ethane at 20℃; for 2h; Reflux; Stage #2: Ethyl diethoxyacetate With trimethylsilyl trifluoromethanesulfonate In 1,2-dichloro-ethane at 20℃; for 16h; stereoselective reaction; | 93% |
2-bromo-5-fluoropyridine
Ethyl diethoxyacetate
Conditions | Yield |
---|---|
Stage #1: 2-bromo-5-fluoropyridine With lithium diisopropyl amide In tetrahydrofuran at -78℃; for 1.5h; Inert atmosphere; Stage #2: Ethyl diethoxyacetate In tetrahydrofuran at -78℃; for 2h; | 92% |
Stage #1: 2-bromo-5-fluoropyridine With lithium diisopropyl amide In tetrahydrofuran at -78℃; for 1.5h; Inert atmosphere; Stage #2: Ethyl diethoxyacetate In tetrahydrofuran at -78℃; for 2h; Inert atmosphere; | 92% |
Stage #1: 2-bromo-5-fluoropyridine With lithium diisopropyl amide In tetrahydrofuran at -78℃; for 1.5h; Inert atmosphere; Stage #2: Ethyl diethoxyacetate In tetrahydrofuran at -78℃; for 2h; | 92% |
Stage #1: 2-bromo-5-fluoropyridine With lithium diisopropyl amide In tetrahydrofuran at -78℃; for 1.5h; Inert atmosphere; Stage #2: Ethyl diethoxyacetate In tetrahydrofuran at -78℃; for 2h; | 92% |
Conditions | Yield |
---|---|
With potassium carbonate In neat (no solvent) at 100℃; for 6h; | 92% |
4-fluoro-benzamidoxime
Ethyl diethoxyacetate
Conditions | Yield |
---|---|
With potassium carbonate In neat (no solvent) at 100℃; for 6h; | 92% |
Conditions | Yield |
---|---|
With hydrogenchloride In 1,4-dioxane at 0℃; for 48h; | 91% |
Ethyl diethoxyacetate
2,2-dihydroxyacetic acid
glyoxylic acid ethyl ester
Conditions | Yield |
---|---|
Stage #1: Ethyl diethoxyacetate; 2,2-dihydroxyacetic acid With toluene-4-sulfonic acid at 90℃; for 27h; Stage #2: With phosphorus pentoxide at 90 - 100℃; for 2h; | 90% |
3-bromo-N'-hydroxybenzenecarboximidamide
Ethyl diethoxyacetate
Conditions | Yield |
---|---|
With potassium carbonate In neat (no solvent) at 100℃; for 6h; | 90% |
4-methoxy-N-[(E)-phenylmethylidene]aniline
Ethyl diethoxyacetate
3,3-diethoxy-1-(4-methoxyphenyl)-4-phenyl-2-azetidinone
Conditions | Yield |
---|---|
With lithium diisopropyl amide In tetrahydrofuran; hexane at -70 - 20℃; for 19.5h; Cycloaddition; | 89% |
phenylmagnesium bromide
Ethyl diethoxyacetate
hydroxy-diphenyl-acetaldehyde
Conditions | Yield |
---|---|
Stage #1: phenylmagnesium bromide; Ethyl diethoxyacetate In tetrahydrofuran at 20 - 90℃; for 0.666667h; Inert atmosphere; Stage #2: With hydrogenchloride In water; acetone at 70℃; for 1h; Inert atmosphere; | 89% |
Conditions | Yield |
---|---|
With sodium tetrahydroborate In dimethoxyethane, 1,2; ethanol at 50℃; for 7h; Heating / reflux; | 88.7% |
[4-(benzylideneamino)phenyl]methanol
Ethyl diethoxyacetate
3,3-diethoxy-1-(4-methoxyphenyl)-4-phenyl-2-azetidinone
Conditions | Yield |
---|---|
With potassium tert-butylate In N,N-dimethyl-formamide for 12h; Ambient temperature; | 88% |
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