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inquiryConditions | Yield |
---|---|
With copper(l) iodide; potassium carbonate; L-proline In ethyl methyl ether at 90 - 110℃; Inert atmosphere; | 75% |
Conditions | Yield |
---|---|
Stage #1: 2-acetylphenothiazine With sodium hydride In N,N-dimethyl-formamide at 20℃; for 0.5h; Stage #2: 3-(Dimethylamino)propyl chloride In N,N-dimethyl-formamide at 50℃; for 5h; | 22% |
With sodium hydride |
2-acetyl-phenothiazine-10-carboxylic acid 3-dimethylamino-propyl ester
acetopromazine
Conditions | Yield |
---|---|
oder unter vermindertem Druck; | |
With copper; 1,3-Dimethoxybenzene |
2-acetyl-10-(3'-chloropropyl)-10H-phenothiazine
dimethyl amine
acetopromazine
Conditions | Yield |
---|---|
In ethanol |
Conditions | Yield |
---|---|
Stage #1: 2-chloro-benzaldehyde; acetopromazine With sodium ethanolate In ethanol Cooling with ice; Sonication; Stage #2: With hydrogenchloride pH=5 - 7; | 81% |
Conditions | Yield |
---|---|
Stage #1: 4-chlorobenzaldehyde; acetopromazine With sodium ethanolate In ethanol Cooling with ice; Sonication; Stage #2: With hydrogenchloride pH=5 - 7; | 78% |
Conditions | Yield |
---|---|
Stage #1: acetopromazine; benzaldehyde With sodium ethanolate In ethanol Cooling with ice; Sonication; Stage #2: With hydrogenchloride pH=5 - 7; | 68% |
Conditions | Yield |
---|---|
Stage #1: acetopromazine; 2,4-dichlorobenzaldeyhde With sodium ethanolate In ethanol Cooling with ice; Sonication; Stage #2: With hydrogenchloride pH=5 - 7; | 62% |
Conditions | Yield |
---|---|
Stage #1: 2-Trifluoromethylbenzaldehyde; acetopromazine With sodium ethanolate In ethanol Cooling with ice; Sonication; Stage #2: With hydrogenchloride pH=5 - 7; | 58% |
Conditions | Yield |
---|---|
Stage #1: 4-fluorobenzaldehyde; acetopromazine With sodium ethanolate In ethanol Cooling with ice; Sonication; Stage #2: With hydrogenchloride pH=5 - 7; | 57% |
Conditions | Yield |
---|---|
Stage #1: 3,4,5-trimethoxy-benzaldehyde; acetopromazine With sodium ethanolate In ethanol Cooling with ice; Sonication; Stage #2: With hydrogenchloride pH=5 - 7; | 51% |
Conditions | Yield |
---|---|
Stage #1: m-bromobenzoic aldehyde; acetopromazine With sodium ethanolate In ethanol Cooling with ice; Sonication; Stage #2: With hydrogenchloride pH=5 - 7; | 51% |
Conditions | Yield |
---|---|
Stage #1: acetopromazine; 3-methoxy-benzaldehyde With sodium ethanolate In ethanol Cooling with ice; Sonication; Stage #2: With hydrogenchloride pH=5 - 7; | 43% |
Conditions | Yield |
---|---|
Stage #1: 2-chloro-6-fluorobenzaldehyde; acetopromazine With sodium ethanolate In ethanol Cooling with ice; Sonication; Stage #2: With hydrogenchloride pH=5 - 7; | 43% |
Conditions | Yield |
---|---|
Stage #1: acetopromazine; 4-methoxy-benzaldehyde With sodium ethanolate In ethanol Cooling with ice; Sonication; Stage #2: With hydrogenchloride pH=5 - 7; | 41% |
Conditions | Yield |
---|---|
Stage #1: p-benzyloxybenzaldehyde; acetopromazine With sodium ethanolate In ethanol Cooling with ice; Sonication; Stage #2: With hydrogenchloride pH=5 - 7; | 40% |
Conditions | Yield |
---|---|
Stage #1: acetopromazine; 4-dimethylamino-benzaldehyde With sodium ethanolate In ethanol Cooling with ice; Sonication; Stage #2: With hydrogenchloride pH=5 - 7; | 39% |
7-chloro-4-hydrazinoquinoline
acetopromazine
Conditions | Yield |
---|---|
With acetic acid In ethanol for 24h; Reflux; | 35% |
acetopromazine
1-[10-(3-dimethylamino-propyl)-phenothiazin-2-yl]-ethanol
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride; diethyl ether |
methyllithium
acetopromazine
2-[10-(3-dimethylamino-propyl)-10H-phenothiazin-2-yl]-propan-2-ol
Conditions | Yield |
---|---|
In diethyl ether |
sodium acetylide
acetopromazine
2-[10-(3-dimethylamino-propyl)-10H-phenothiazin-2-yl]-but-3-yn-2-ol
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at -14 - 20℃; for 2.5h; |
5-methyl-indole-2,3-dione
acetopromazine
2-[10-(3-dimethylamino-propyl)-10H-phenothiazin-2-yl]-6-methyl-quinoline-4-carboxylic acid
Conditions | Yield |
---|---|
With potassium hydroxide In 1,4-dioxane; ethanol; water for 24h; Heating; |
5-fluoro-1H-indole-2,3-dione
acetopromazine
2-[10-(3-dimethylamino-propyl)-10H-phenothiazin-2-yl]-6-fluoro-quinoline-4-carboxylic acid
Conditions | Yield |
---|---|
With potassium hydroxide In 1,4-dioxane; ethanol; water for 24h; Heating; |
5-methoxyisatine
acetopromazine
2-[10-(3-dimethylamino-propyl)-10H-phenothiazin-2-yl]-6-methoxy-quinoline-4-carboxylic acid
Conditions | Yield |
---|---|
With potassium hydroxide In 1,4-dioxane; ethanol; water for 24h; Heating; |
indole-2,3-dione
acetopromazine
2-[10-(3-dimethylamino-propyl)-10H-phenothiazin-2-yl]-quinoline-4-carboxylic acid
Conditions | Yield |
---|---|
With potassium hydroxide In 1,4-dioxane; ethanol; water for 24h; Heating; |
5-chloroindole 2,3-dione
acetopromazine
6-chloro-2-[10-(3-dimethylamino-propyl)-10H-phenothiazin-2-yl]-quinoline-4-carboxylic acid
Conditions | Yield |
---|---|
With potassium hydroxide In 1,4-dioxane; ethanol; water for 24h; Heating; |
Conditions | Yield |
---|---|
With pyridine |
Conditions | Yield |
---|---|
With pyridine |
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