Dayang Chem (Hangzhou) Co.,Ltd.
Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities
Cas:620-71-3
Min.Order:1 Kilogram
FOB Price: $3.0
Type:Lab/Research institutions
inquiryHenan Tianfu Chemical Co., Ltd.
PROPIONANILIDE at competitive price from Henan Tianfu Chemical: Henan Tianfu Chemical Co.,LTD was built in 2009 with an ISO certificate in the past 5 years, we have grown up as a famous fine chemicals supplier in china and we had established stab
Shanghai Upbio Tech Co.,Ltd
1.In No Less 10 years exporting experience. you can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specializ
Cas:620-71-3
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryWin-Win chemical Co.Ltd
Stock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai
Cas:620-71-3
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryHangzhou Keyingchem Co.,Ltd
Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:620-71-3
Min.Order:0 Metric Ton
Negotiable
Type:Lab/Research institutions
inquiryHangzhou J&H Chemical Co., Ltd.
J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
TAIZHOU ZHENYU BIOTECHNOLOGY CO., LTD
Zhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed
Cas:620-71-3
Min.Order:1 Kilogram
FOB Price: $2.0
Type:Lab/Research institutions
inquiryBluecrystal chem-union
We are a Union of chemistry in China, consists of chemists，engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp
Cas:620-71-3
Min.Order:1 Metric Ton
FOB Price: $1.0
Type:Trading Company
inquiryAntimex Chemical Limied
Our own factory produces direct sales with absolute price advantage Application:Pharmaceutical industry Transportation:By sea Port:Shanghai/tianjin
Hangzhou Fandachem Co.,Ltd
Propanamide, N-phenyl- cas 620-71-3Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
Chemlyte Solutions
factory?direct?sale Application:Fine chemical intermediates, used as the main raw material for the synthesis of various pesticides, medicines, surfactants, polymer monomers, and antifungal agents
ZHEJIANG JIUZHOU CHEM CO.,LTD
factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
Amadis Chemical Co., Ltd.
1.Professional synthesis laboratory and production base. 2.Strong synthesis team and service team. 3.Professional data management system. 4.We provide the professional test date and product information ,ex. HNMR ,CNMR,FNMR, HPLC/G
Cas:620-71-3
Min.Order:10 Milligram
Negotiable
Type:Lab/Research institutions
inquiryHangzhou Share Chemical Co., Ltd
At Share Chemical Company, we scrupulously abide by our policy of “Excellent Quality at a Reasonable Price”. We strive to satisfy all of our customers by providing the finest quality products supported by the finest in customer servi
Shanghai Forever Synthesis Co.,Ltd.
As a professional chemical R&D and synthesis supplier, Shanghai Forever Synthesis Co.,Ltd. is specialized R&D and synthesizing APIs and Impurities. Besides, we value more special service, that is, to customize chemical synthesis according to client’s
Finetech Industry Limited
FINETECH INDUSTRY LIMITED is a LONDON based CRO company providing drug discovery & development services to worldwide clients. FINETECH INDUSTRY LIMITED supplies the PROPIONANILIDE, CAS:620-71-3 with the most competitive price and the best quality. We
Shanghai Run-Biotech Co., Ltd.
1.We have rich experience in the development and production 2.Our factory is in Shanghai of China,We have convenient traffic conditions.3.We have advanced testing equipment and shipping line. Package:5g, 10g, 50g, 100g, 1kg Application:Pharmaceutical
Debye Scientific
Debyesci is here who supplied several kinds of chemical products to global pharmaceutical, drug discovery, agrochemical and biotechnology industries for four yearsOur key scientific leadership team has gained experience in top research and developmen
NovaChemistry
High purity Application:Pharmaceutical intermediates, Material synthesis and analyzing the expectant ingredients
Synthetic route
-
-
23517-42-2
propiophenone oxime
-
-
620-71-3
N-(phenyl)-2-methylacetamide
| Conditions | Yield |
|---|---|
| With sulfuric acid; 3-butyl-1-methyl-1H-imidazol-3-ium hexafluorophosphate for 0.0166667h; Beckmann rearrangement; microwave irradiation; | 100% |
| mercury dichloride In acetonitrile at 80℃; for 8h; Beckmann rearrangement; | 98% |
| With bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; zinc(II) chloride In acetonitrile for 1h; Beckmann rearrangement; Heating; | 97% |
| Conditions | Yield |
|---|---|
| With 1,1'-carbonyldiimidazole; methyl iodide In acetonitrile for 1h; Heating; | 98% |
| With p-toluenesulfonyl chloride; zinc(II) chloride In acetonitrile for 1h; Beckmann rearrangement; Inert atmosphere; Reflux; | 98% |
| With silica gel; caesium carbonate; N-tosylimidazole In N,N-dimethyl-formamide for 2h; Beckmann rearrangement; Reflux; | 98% |
| Conditions | Yield |
|---|---|
| With fluorosulfonyl fluoride; N-ethyl-N,N-diisopropylamine In acetonitrile at 20℃; for 5h; | 98% |
| Stage #1: propionic acid With iodine; triethylamine; phosphorous acid trimethyl ester In dichloromethane for 0.166667h; Cooling with ice; Inert atmosphere; Stage #2: aniline In dichloromethane at 20℃; for 3h; Inert atmosphere; Cooling with ice; | 96% |
| With [((CH3)5Cp)2Zr(H2O)2OSO2C8F17]+[OSO2C8F17]-*THF In neat (no solvent) at 80℃; for 2h; | 94% |
| Conditions | Yield |
|---|---|
| With palladium(II) acetylacetonate In toluene at 100℃; under 30003 Torr; for 20h; Autoclave; Inert atmosphere; regioselective reaction; | 98% |
| With C52H52NO5P; palladium(II) iodide In tetrahydrofuran at 60℃; under 760.051 Torr; for 72h; Autoclave; regioselective reaction; | 93% |
| With Ru-clusters supported on ceria In tetrahydrofuran at 160℃; under 7500.75 Torr; for 24h; Autoclave; | 67% |
| Co/C In water at 150℃; under 53203.6 Torr; for 72h; | 54% |
-
-
369-57-3
benzenediazonium tetrafluoroborate
-
-
107-12-0
propiononitrile
-
-
620-71-3
N-(phenyl)-2-methylacetamide
| Conditions | Yield |
|---|---|
| Stage #1: benzenediazonium tetrafluoroborate; propiononitrile for 0.0166667h; Microwave irradiation; Stage #2: With water In diethyl ether | 97% |
| Conditions | Yield |
|---|---|
| With oxygen; sodium hydroxide In water at 40℃; for 24h; | 97% |
| With oxygen; sodium hydroxide In water at 40℃; for 24h; Green chemistry; | 94% |
| With potassium tert-butylate In 1,4-dioxane at 110℃; for 24h; | 88% |
| Conditions | Yield |
|---|---|
| With tris(pentafluorophenyl)borate In neat (no solvent) at 20℃; for 0.0333333h; Green chemistry; | 96% |
| With sodium dodecyl-sulfate In water | 87% |
| Conditions | Yield |
|---|---|
| With trifluorormethanesulfonic acid; hydroxylamine hydrochloride In formic acid for 7h; Heating; | 96% |
| With sodium azide; sulfuric acid; silica gel at 60℃; for 0.5h; Schmidt reaction; | 95% |
| With zinc(II) chloride; hydroxylamine-O-sulfonic acid In water at 20℃; for 16h; Beckmann Rearrangement; | 93% |
| Conditions | Yield |
|---|---|
| With triphenylphosphine In benzene for 60h; Heating; | 96% |
| With triethylphosphine In benzene at 80℃; for 12h; | 87% |
| Conditions | Yield |
|---|---|
| With hydrogen for 1h; | 94% |
| Conditions | Yield |
|---|---|
| With allylchloro-[1,3-bis(diisopropylphenyl)-imidazole-2-ylidene]palladium(II); water; potassium carbonate In toluene at 110℃; for 16h; Inert atmosphere; | 94% |
| Conditions | Yield |
|---|---|
| With thermally decomposed Ni-Fe-hydrotalcite at 26.84℃; for 0.0166667h; Neat (no solvent); | 89% |
| With pyridine In dichloromethane for 16h; Ambient temperature; | 84% |
| In dichloromethane at 20℃; Schlenk technique; | 47% |
| Conditions | Yield |
|---|---|
| With samarium; titanium tetrachloride In tetrahydrofuran at 65℃; for 0.116667h; | 85% |
-
-
95465-23-9
((C6H11)3P)NiN(C6H5)CO(CH2)2
-
-
620-71-3
N-(phenyl)-2-methylacetamide
| Conditions | Yield |
|---|---|
| 83% | |
| With oxonium In not given hydrolysis; | 83% |
-
-
21262-52-2
2-chloro-N-phenylpropanamide
-
-
620-71-3
N-(phenyl)-2-methylacetamide
| Conditions | Yield |
|---|---|
| With tri-n-butyl-tin hydride; 2,2'-azobis(isobutyronitrile) In toluene for 14h; Heating; | 82% |
| Conditions | Yield |
|---|---|
| With samarium; titanium tetrachloride In tetrahydrofuran at 65℃; for 0.0833333h; | 82% |
| Conditions | Yield |
|---|---|
| In tetrahydrofuran at 20℃; | 82% |
| Conditions | Yield |
|---|---|
| Stage #1: diethyl 1-propionyl-1,4-dihydropyridine-3,5-dicarboxylate With 2,3-dicyano-5,6-dichloro-p-benzoquinone In dichloromethane for 0.5h; Stage #2: aniline With dmap In dichloromethane for 21.5h; | 82% |
| Conditions | Yield |
|---|---|
| In acetonitrile at 20℃; for 16h; | 82% |
| Conditions | Yield |
|---|---|
| With (difluoroboryl)dimethylglyoximatocobalt(II) bis(acetonitrile); 3-cyano-1-methylquinolinium cation In acetonitrile at 20℃; for 5h; Inert atmosphere; Irradiation; Green chemistry; | 81% |
| Conditions | Yield |
|---|---|
| In 1,2-dichloro-ethane at 100℃; for 24h; | 81% |
| Conditions | Yield |
|---|---|
| 80% |
| Conditions | Yield |
|---|---|
| With triethyl phosphite at 100℃; for 0.333333h; Microwave irradiation; neat (no solvent); | 80% |
| Conditions | Yield |
|---|---|
| With carbonylhydrido(tetrahydroborato)[bis(2-diphenylphosphinoethyl)-amino]ruthenium(II); potassium tert-butylate In toluene at 120℃; for 48h; Inert atmosphere; Schlenk technique; Reflux; Green chemistry; | 80% |
| Conditions | Yield |
|---|---|
| With trifluorormethanesulfonic acid; Tri(p-tolyl)phosphine; chloro(1,5-cyclooctadiene)rhodium(I) dimer In 1,2-dichloro-ethane for 3h; Product distribution; Further Variations:; Reagents; Beckmann rearrangement; Heating; | A 2% B 78% |
-
-
620-71-3
N-(phenyl)-2-methylacetamide
| Conditions | Yield |
|---|---|
| With water; benzoic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; iron(II) chloride In 1,2-dichloro-ethane at 60℃; Catalytic behavior; Reagent/catalyst; Schlenk technique; Inert atmosphere; | 78% |
| Conditions | Yield |
|---|---|
| In hexane for 5h; Ambient temperature; | 74% |
| Conditions | Yield |
|---|---|
| Stage #1: N-(phenyl)-2-methylacetamide With n-butyllithium In tetrahydrofuran; hexane at 0℃; for 0.5h; Stage #2: 2-chloro-benzaldehyde In tetrahydrofuran; hexane at 0℃; for 0.5h; | A 15% B n/a |
| Conditions | Yield |
|---|---|
| Stage #1: N-(phenyl)-2-methylacetamide With n-butyllithium In tetrahydrofuran; hexane for 0.75h; Stage #2: With zinc(II) chloride In tetrahydrofuran; hexane Stage #3: 4-methoxy-benzaldehyde In tetrahydrofuran; hexane at 0℃; for 0.25h; | 15% |
| Conditions | Yield |
|---|---|
| Stage #1: N-(phenyl)-2-methylacetamide With n-butyllithium In tetrahydrofuran; hexane at 0℃; for 0.5h; Stage #2: ortho-anisaldehyde In tetrahydrofuran; hexane at 0℃; for 0.5h; | A 16% B n/a |
-
-
620-71-3
N-(phenyl)-2-methylacetamide
-
-
145474-72-2, 145474-74-4
N-<<1-benzyl-5-<(4-methylphenyl)sulfonyloxymethyl>-2-piperidinyl>methyl>-4-fluorobenzamide
-
-
145474-78-8
N-<<1-benzyl-5-<(N-phenyl,N-propionyl)aminomethyl>-2-piperidinyl>methyl>-4-fluorobenzamide
| Conditions | Yield |
|---|---|
| With 18-crown-6 ether; potassium tert-butylate In toluene at 70℃; for 24h; | 17% |
| Conditions | Yield |
|---|---|
| Stage #1: N-(phenyl)-2-methylacetamide With n-butyllithium In tetrahydrofuran; hexane at 0℃; for 0.5h; Stage #2: isobutyraldehyde In tetrahydrofuran; hexane at 0℃; for 0.5h; | A 19% B n/a |
| Conditions | Yield |
|---|---|
| Stage #1: N-(phenyl)-2-methylacetamide With n-butyllithium In tetrahydrofuran; hexane at 0℃; for 0.5h; Stage #2: β-naphthaldehyde In tetrahydrofuran; hexane at 0℃; for 0.5h; | A 24% B n/a |
-
-
620-71-3
N-(phenyl)-2-methylacetamide
-
-
100-51-6
benzyl alcohol
-
-
80818-45-7
N-phenyl methyl-2 phenyl-3 propene-2 amide
| Conditions | Yield |
|---|---|
| With (4-Me)Triaz(NHPiPr2)2Mn(CO)2Br; caesium carbonate In tert-Amyl alcohol at 135℃; for 24h; Inert atmosphere; Schlenk technique; Glovebox; | 24% |
-
-
620-71-3
N-(phenyl)-2-methylacetamide
-
-
75-07-0
acetaldehyde
-
-
90033-14-0, 127603-88-7
(+/-)-(2S,3R)-3-hydroxy-2-methyl-N-phenylbutanamide
-
-
90033-14-0, 127603-88-7
(+/-)-(2S,3S)-3-hydroxy-2-methyl-N-phenylbutanamide
| Conditions | Yield |
|---|---|
| Stage #1: N-(phenyl)-2-methylacetamide With n-butyllithium In tetrahydrofuran; hexane at 0℃; for 0.5h; Stage #2: acetaldehyde In tetrahydrofuran; hexane at 0℃; for 0.5h; | A n/a B 25% |
| Conditions | Yield |
|---|---|
| Stage #1: N-(phenyl)-2-methylacetamide With n-butyllithium In tetrahydrofuran; hexane at 0℃; for 0.5h; Stage #2: furfural In tetrahydrofuran; hexane at 0℃; for 0.5h; | A 26% B n/a |
-
-
73568-25-9
2-chloro-3-quinoline carboxaldehyde
-
-
620-71-3
N-(phenyl)-2-methylacetamide
-
-
76671-67-5
3-Methyl-1-phenyl-1H-benzo[b][1,8]naphthyridin-2-one
| Conditions | Yield |
|---|---|
| With phosphorus (III) oxychloride; N,N-dimethyl-formamide; Acetanilid at 75℃; for 3h; | 27% |
| Conditions | Yield |
|---|---|
| With potassium In 1,4-dioxane at 150℃; under 9120 Torr; for 10h; in autoclave; | 30% |
| Conditions | Yield |
|---|---|
| With Lawessons reagent In toluene at 100 - 110℃; for 4.33333h; Inert atmosphere; | 37% |
| With Lawessons reagent In toluene for 2h; Reflux; Inert atmosphere; |
-
-
591-50-4
iodobenzene
-
-
620-71-3
N-(phenyl)-2-methylacetamide
-
-
7470-52-2
N-([1,1’-biphenyl]-2-yl)propionamide
| Conditions | Yield |
|---|---|
| Stage #1: N-(phenyl)-2-methylacetamide With silver hexafluoroantimonate; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; silver trifluoroacetate In 1,2-dichloro-ethane for 0.0833333h; Sealed tube; Inert atmosphere; Stage #2: iodobenzene In 1,2-dichloro-ethane at 120℃; for 24h; Sealed tube; Inert atmosphere; | 41% |
-
-
6320-02-1
2-bromothiophenol
-
-
620-71-3
N-(phenyl)-2-methylacetamide
-
-
6622-75-9
1-(10H-phenothiazin-10-yl)propan-1-one
| Conditions | Yield |
|---|---|
| Stage #1: o-bromothiophenol; N-(phenyl)-2-methylacetamide With dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; silver(I) acetate; copper(II) bis(trifluoromethanesulfonate) at 100℃; for 18h; Stage #2: With caesium carbonate; N,N`-dimethylethylenediamine at 100℃; for 2h; | 41% |
| Conditions | Yield |
|---|---|
| With ytterbium trifluoromethanesulfonate; lithium perchlorate In nitromethane at 100℃; for 8h; Fries rearrangement; | 43% |
| With aluminium trichloride at 200℃; |
-
-
620-71-3
N-(phenyl)-2-methylacetamide
| Conditions | Yield |
|---|---|
| With [ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2; sodium acetate; silver(I) triflimide In dichloromethane at 60℃; for 36h; Schlenk technique; Inert atmosphere; regioselective reaction; | 44% |
-
-
620-71-3
N-(phenyl)-2-methylacetamide
-
-
100-52-7
benzaldehyde
-
-
84918-79-6
N-phenyl-N-propionylbenzamide
| Conditions | Yield |
|---|---|
| With tert.-butylhydroperoxide; water; iron(II) bromide In 1,2-dichloro-ethane at 60℃; for 16h; Catalytic behavior; Inert atmosphere; Schlenk technique; | 47% |
-
-
591-50-4
iodobenzene
-
-
620-71-3
N-(phenyl)-2-methylacetamide
-
-
32870-22-7
1,4-diphenyl-1H-quinolin-2-one
| Conditions | Yield |
|---|---|
| With 2,5-dimethylpyridine; silver carbonate; palladium dichloride In tert-Amyl alcohol at 140℃; for 24h; | 48% |
| Conditions | Yield |
|---|---|
| With [ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2; silver methanesulfonate; copper(II) acetate monohydrate In toluene at 110℃; for 12h; Inert atmosphere; | 50% |
| Conditions | Yield |
|---|---|
| Stage #1: N-(phenyl)-2-methylacetamide With n-butyllithium In tetrahydrofuran; hexane at 0℃; for 0.5h; Stage #2: 1-naphthaldehyde In tetrahydrofuran; hexane at 0℃; for 0.5h; | A 52% B n/a |
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