As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
Cas:685-91-6
Min.Order:1 Kilogram
FOB Price: $3.0
Type:Lab/Research institutions
inquiryUnique advantages for Diethylacetamide Cas685-91-6 Guaranteed the purity High quality & competitive price Quality control Fast feedback Prompt shipment Appearance:Colorless transparent liquid Package:25kg/drum;200kg/drum Application:Pharma
Cas:685-91-6
Min.Order:25 Kilogram
Negotiable
Type:Trading Company
inquiryColorcom is a global leader in industrial chemical manufacturing and is continuously innovating and transforming to exceed client expectations and industry standards. Colorcom prides itself on superior customer and technical focus, while focusing on
Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Cas:685-91-6
Min.Order:5 Kiloliter
FOB Price: $1.2 / 5.0
Type:Manufacturers
inquiryOur company was built in 2009 with an ISO certificate.In the past 6 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O
Cas:685-91-6
Min.Order:1 Kilogram
FOB Price: $1000.0
Type:Lab/Research institutions
inquiryOur advantages: 1. High quality and competitive price: 1) Standard: BP/USP/EP/ enterprise standard 2) All purity ≥99% 3) We are manufacturers and can provide high quality products at factory prices. 2. Fast and safe delivery 1) The package c
Cas:685-91-6
Min.Order:1 Kilogram
FOB Price: $5.0 / 10.0
Type:Trading Company
inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:685-91-6
Min.Order:1 Kilogram
FOB Price: $139.0 / 210.0
Type:Trading Company
inquiryAbout Product Details
Cas:685-91-6
Min.Order:1 Kilogram
FOB Price: $1.0 / 2.0
Type:Lab/Research institutions
inquiryWe are leading fine chemicals supplier in China and Our main business covers the fields below: 1.Noble Metal Catalysts (Pt.Pd...) 2.Organic Phosphine Ligands (Tert-butyl-phosphine.Cyclohexyl-phosphine...) 3.OLED intermediat
Cas:685-91-6
Min.Order:1 Kilogram
FOB Price: $4.0 / 5.0
Type:Lab/Research institutions
inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
Cas:685-91-6
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryProduct Detail Minimum Order Qty. 10 Gram Supply Ability 500 Kilograms/Month Storage store in cool, dry, ventilated place 20℃ Delivery Time 3 business days after payment Payment Term TT,western union,Paypal,
Cas:685-91-6
Min.Order:20 Metric Ton
Negotiable
Type:Trading Company
inquiryOur advantages: Sales term: Has a strong chemical professional quality and strong sense of responsibilit.In the sales field of fine chemicals and the market development of new products, we have a strong foresight and pertinen
Cas:685-91-6
Min.Order:1 Kilogram
FOB Price: $3.0 / 4.0
Type:Lab/Research institutions
inquiryProduct Name: Diethylacetamide Synonyms: N,N-DIETHYLACETAMIDE FOR SYNTHESIS;685-91-6;acetamide,n,n-diethyl-;acetamine,n,n-diethyl-;aceticacid,amide,n,n-diethyl;CH3CON(C2H5)2;n,n-diaethylacetamid;n,n-diethyl-acetamid CAS: 685-91-6 MF: C6H13NO
Cas:685-91-6
Min.Order:100 Gram
Negotiable
Type:Lab/Research institutions
inquiryBest quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
Our Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists of highly qualifie
Cas:685-91-6
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:685-91-6
Min.Order:0 Metric Ton
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Type:Lab/Research institutions
inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Cas:685-91-6
Min.Order:0 Metric Ton
Negotiable
Type:Other
inquiryWe are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov
Cas:685-91-6
Min.Order:100 Gram
FOB Price: $100.0 / 2000.0
Type:Lab/Research institutions
inquiryProduct name: Diethylacetamide CAS No.:685-91-6 Molecule Formula:C6H13NO Molecule Weight:115.17 Purity: 99.0% Package: 200kg/drum Description:Colorless or light yellow liquid Manufacture Standards:Enterprise Standard
Cas:685-91-6
Min.Order:1 Kilogram
Negotiable
Type:Trading Company
inquiryGMP standard, high purity, competitive price, in stock 1. Quick Response: within 6 hours after receiving your email. 2. Quality Guarantee: All products are strictly tested by our QC, confirmed by QA, and approved by a third-party lab in China, USA,
Diethylacetamide Basic information Product Name: Diethylacetamide Synonyms: n,n-diaethylacetamid;n,n-diethyl-acetamid;diethylacetamide;ACETIC ACID DIETHYLAMIDE;ACETYL DIETHYLAMINE;N-ACETYLDIETHYLAMINE;N,N-DIETHYLACETAMIDE;N,N-Diethylacetamide,
factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
Cas:685-91-6
Min.Order:1 Kilogram
FOB Price: $18.0 / 20.0
Type:Trading Company
inquiryHangzhou Huarong Pharm Co., Ltd.established since 2006 , has been actively developing specialty products for Finished Dosages, APIs, Intermediates, and Fine chemicals markets in North America, Europe, Korea, Japan, Mid-East and all over the World. Hu
Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
Cas:685-91-6
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiry1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
Cas:685-91-6
Min.Order:1 Metric Ton
FOB Price: $7.0 / 8.0
Type:Trading Company
inquiryGOLDEN PHARMA CO.,LIMITED.is a professional pharmaceutical company,our team have more than 20years expereince in pharmaceutical production and sales. we are a professional technical enterprise specializing in the R & D, production,QA regulation
We are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp
Cas:685-91-6
Min.Order:1 Metric Ton
FOB Price: $1.0
Type:Trading Company
inquiryChemical Name: Diethylacetamide CAS: 685-91-6 Molecular Fomula: C6H13NO Molecular weight: 115.17 Appearance:Colorless Transparent Liquid Assay: 99% Appearance:Colorless Clear to light yellow Liquid Storage:Preserve in well-closed, light-resi
ethyl 2,4-dinitrophenylacetoacetate
diethylamine
A
diethylacetamide
B
α-(2,4-dinitrophenyl)ethyl acetate
Conditions | Yield |
---|---|
In chloroform at 80℃; for 48h; | A 100% B n/a |
Conditions | Yield |
---|---|
With tetrachloromethane; potassium carbonate In dichloromethane for 9h; Inert atmosphere; Irradiation; | 100% |
Conditions | Yield |
---|---|
With immobilization of Candida cylindracea lipase In hexane at 55℃; for 12h; | 99% |
Conditions | Yield |
---|---|
With Cu 20%, Co 6%, Mn 4%, Mo 5%, Ag 0000.2%, alkaline earth metal 5%, rare earth metal 2% at 30 - 50℃; Temperature; | 98.5% |
Conditions | Yield |
---|---|
With nickel dichloride at 20℃; for 0.166667h; Neat (no solvent); | 97% |
at 100℃; for 3h; Condensation; | 91% |
ZSM-35 zeolite In acetonitrile for 2h; Heating; | 89.2% |
Conditions | Yield |
---|---|
In tetrahydrofuran at 25℃; for 13.5h; Inert atmosphere; | 96.5% |
Conditions | Yield |
---|---|
With aluminium trichloride In dichloromethane at 25℃; for 3.5h; | 94% |
Conditions | Yield |
---|---|
With [Zn(BH4)2(py)] In tetrahydrofuran for 0.25h; Heating; | 94% |
trans-PdMe(I)(PMePh2)2
carbon monoxide
diethylamine
A
diethylacetamide
B
N,N-diethyl-2-oxo-propanamide
Conditions | Yield |
---|---|
In tetrahydrofuran 10 atm CO pressure, magnetically stirred at room temp. for 1 day, totalyield: 95%; | A 7% B 93% |
In tetrahydrofuran 1 atm CO pressure, magnetically stirred at room temp. for 1 day, total yield: 51%; | A 21% B 79% |
Conditions | Yield |
---|---|
With aluminium trichloride In dichloromethane at 90℃; for 20h; | 92% |
S,S-diethyl-N-diethylamidodithiophosphite
acetic anhydride
A
diethylacetamide
B
O-acetyl S,S-diethyl phosphorodithioite
Conditions | Yield |
---|---|
for 20h; Product distribution; Ambient temperature; | A 91% B 88% |
Conditions | Yield |
---|---|
With hydrogen In water at 120 - 140℃; under 22502.3 - 37503.8 Torr; | 90% |
With nickel In tetrahydrofuran at 20℃; for 2h; | 90 % Spectr. |
With potassium iodide; potassium carbonate In tetrahydrofuran | |
With hydrogen; triethylamine In methanol; water at 120℃; under 22502.3 Torr; for 95h; Autoclave; | 90 %Chromat. |
Conditions | Yield |
---|---|
Stage #1: diethyl amine hydrochloride With diisobutylaluminium hydride In tetrahydrofuran; toluene Stage #2: acetic acid butyl ester In tetrahydrofuran at 20℃; for 2h; | 90% |
N-Hydroxymethyldiethylamine-acetate
bis(diethylamino)phenylphosphine
A
diethylacetamide
Conditions | Yield |
---|---|
at 20℃; for 20h; | A 80% B 89.5% |
Conditions | Yield |
---|---|
With hydroxyapatite supported copper(I) oxide In acetonitrile at 50℃; for 0.25h; | 89% |
With iodine at 20℃; for 0.0166667h; Neat (no solvent); | 86.3% |
With pyridine In dichloromethane for 1h; | 76% |
Conditions | Yield |
---|---|
In dichloromethane for 0.25h; Ambient temperature; | 89% |
dipropyl diethylphosphoramidodithioite
acetic anhydride
A
diethylacetamide
B
O-acetyl S,S-dipropyl phosphorodithioite
Conditions | Yield |
---|---|
Product distribution; Ambient temperature; | A 88% B 82% |
Conditions | Yield |
---|---|
for 4h; Reflux; | 88% |
O-acetyl-α-hydroxyisobutyric acid
A
diethylacetamide
B
2,3-dimethyl-2,3-butane diol
C
Essigsaeure-2-hydroxy-1,1,2-trimethylpropylester
D
acetic anhydride
Conditions | Yield |
---|---|
With triethylamine In acetonitrile Ambient temperature; electrolysis; Further byproducts given; | A 47% B 86.8% C 4.7% D n/a |
O-acetyl-α-hydroxyisobutyric acid
triethylamine
A
diethylacetamide
B
2,3-dimethyl-2,3-butane diol
C
Essigsaeure-2-hydroxy-1,1,2-trimethylpropylester
D
acetic anhydride
Conditions | Yield |
---|---|
In acetonitrile Ambient temperature; electrolysis; Further byproducts given; | A 47% B 86.8% C 4.7% D n/a |
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; water In acetonitrile at 70℃; for 1h; | 85% |
Acetic 4-methylthiobenzoic thioanhydride
Diethylamino-trimethyl-stannan
A
diethylacetamide
B
4,4'-Dimethyl-bis-thiobenzoyldisulfid
C
trimethyltin 4-methylbenzenecarbodithioate
Conditions | Yield |
---|---|
In hexane at 0℃; for 1h; | A 70% B 7% C 84% |
Acetyl bromide
S,S-diethyl-N-diethylamidodithiophosphite
A
diethylacetamide
B
diethyl phosphorobromidodithioite
Conditions | Yield |
---|---|
Product distribution; -70 deg C to room temperature; | A 82% B 65% |
Acetyl bromide
dipropyl diethylphosphoramidodithioite
A
diethylacetamide
Conditions | Yield |
---|---|
Product distribution; | A 78% B 77% |
Conditions | Yield |
---|---|
In tetrahydrofuran at 20℃; | 78% |
dipropyl diethylphosphoramidodithioite
acetic acid
A
diethylacetamide
B
tripropyl phosphorotrithioite
C
O-acetyl S,S-dipropyl phosphorodithioite
Conditions | Yield |
---|---|
for 1h; Ambient temperature; | A 76% B n/a C n/a |
Conditions | Yield |
---|---|
tetraphosphorus decasulfide; triphenyl antimony oxide In benzene at 60℃; for 12h; | 75% |
With tetrachlorosilane; benzene |
Conditions | Yield |
---|---|
triphenyl antimony oxide In benzene at 20℃; for 8h; | 75% |
mixed anhydride of O,O-diisobutyl hydrogen phosphorothioate and tetraethylphosphorodiamidous acid
acetyl chloride
A
diethylacetamide
B
diethylphosphoramidous dichloride
Conditions | Yield |
---|---|
at 48 - 52℃; for 0.5h; | A 65% B 68% C 75% |
dipropyl diethylphosphoramidodithioite
acetyl chloride
A
diethylacetamide
B
dipropyl phosphorochloridodithioite
Conditions | Yield |
---|---|
Product distribution; | A 73% B 69% |
Conditions | Yield |
---|---|
Stage #1: diethylacetamide With sec.-butyllithium In tetrahydrofuran; cyclohexane at -78℃; for 1h; Stage #2: With zinc(II) chloride In tetrahydrofuran; cyclohexane at 20℃; for 0.166667h; Stage #3: 4-bromobenzenecarbonitrile With monophosphine 1,2,3,4,5-pentaphenyl-1'-(di-tert-butylphosphino)ferrocene; bis(dibenzylideneacetone)-palladium(0) In tetrahydrofuran; cyclohexane at 20℃; for 24h; | 98% |
Conditions | Yield |
---|---|
With tri-tert-butyl phosphine; potassium tert-butylate; nickel diacetate In 1,4-dioxane; toluene at 80℃; for 12h; Inert atmosphere; Glovebox; Schlenk technique; | 98% |
With C19H26ClIrNOP; potassium tert-butylate In toluene at 80℃; for 12h; Schlenk technique; Inert atmosphere; Sealed tube; Green chemistry; | 84% |
With C29H55IrN3P2(1+)*Cl(1-); potassium tert-butylate In toluene at 120℃; for 15h; Schlenk technique; Inert atmosphere; Glovebox; | 78% |
With C22H34Cl2CoF3N5P2; potassium tert-butylate In tetrahydrofuran at 100℃; for 24h; Inert atmosphere; Sealed tube; Glovebox; | 76% |
With C23H21MnN2O3P(1+)*Br(1-); potassium tert-butylate In 1,4-dioxane at 130℃; for 15h; Schlenk technique; Inert atmosphere; Green chemistry; | 56% |
Conditions | Yield |
---|---|
Stage #1: diethylacetamide With sec.-butyllithium In tetrahydrofuran; cyclohexane at -78℃; for 1h; Stage #2: With zinc(II) chloride In tetrahydrofuran; cyclohexane at 20℃; for 0.166667h; Stage #3: 4-methoxycarbonylphenyl bromide With monophosphine 1,2,3,4,5-pentaphenyl-1'-(di-tert-butylphosphino)ferrocene; bis(dibenzylideneacetone)-palladium(0) In tetrahydrofuran; cyclohexane at 20℃; for 24h; | 97% |
Conditions | Yield |
---|---|
Stage #1: diethylacetamide With sec.-butyllithium In tetrahydrofuran; cyclohexane at -78℃; for 1h; Stage #2: With zinc(II) chloride In tetrahydrofuran; cyclohexane at 20℃; for 0.166667h; Stage #3: 2,4,6-trimethylphenyl bromide With monophosphine 1,2,3,4,5-pentaphenyl-1'-(di-tert-butylphosphino)ferrocene; bis(dibenzylideneacetone)-palladium(0) In tetrahydrofuran; cyclohexane at 20℃; for 24h; | 96% |
diethylacetamide
1-bromo-4-methoxy-benzene
N,N-diethyl-2-(4-methoxyphenyl)acetamide
Conditions | Yield |
---|---|
With N-(dicyclohexylphosphino)-2-(2'-methylphenyl)-1H-indole; palladium diacetate; lithium tert-butoxide In toluene at 110℃; Inert atmosphere; Sealed tube; Microwave irradiation; chemoselective reaction; | 95% |
Stage #1: diethylacetamide With sec.-butyllithium In tetrahydrofuran; cyclohexane at -78℃; for 1h; Stage #2: With zinc(II) chloride In tetrahydrofuran; cyclohexane at 20℃; for 0.166667h; Stage #3: 1-bromo-4-methoxy-benzene With monophosphine 1,2,3,4,5-pentaphenyl-1'-(di-tert-butylphosphino)ferrocene; bis(dibenzylideneacetone)-palladium(0) In tetrahydrofuran; cyclohexane at 20℃; for 24h; | 93% |
Conditions | Yield |
---|---|
Stage #1: diethylacetamide With sec.-butyllithium In tetrahydrofuran; cyclohexane at -78℃; for 1h; Stage #2: With zinc(II) chloride In tetrahydrofuran; cyclohexane at 20℃; for 0.166667h; Stage #3: 2-Bromo-6-methoxynaphthalene With monophosphine 1,2,3,4,5-pentaphenyl-1'-(di-tert-butylphosphino)ferrocene; bis(dibenzylideneacetone)-palladium(0) In tetrahydrofuran; cyclohexane at 20℃; for 24h; | 95% |
Conditions | Yield |
---|---|
In diethyl ether; water | 95% |
diethylacetamide
1-bromo-4-tert-butylbenzene
2,2-bis(4-(tert-butyl)phenyl)-N,N-diethylacetamide
Conditions | Yield |
---|---|
With N-(dicyclohexylphosphino)-2-(2'-methylphenyl)-1H-indole; palladium diacetate; sodium hexamethyldisilazane In toluene at 110℃; Inert atmosphere; Sealed tube; Microwave irradiation; chemoselective reaction; | 95% |
Conditions | Yield |
---|---|
With N-(dicyclohexylphosphino)-2-(2'-methylphenyl)-1H-indole; palladium diacetate; lithium tert-butoxide In toluene at 110℃; Inert atmosphere; Sealed tube; Microwave irradiation; chemoselective reaction; | 94% |
Stage #1: diethylacetamide With sec.-butyllithium In tetrahydrofuran; cyclohexane at -78℃; for 1h; Stage #2: With zinc(II) chloride In tetrahydrofuran; cyclohexane at 20℃; for 0.166667h; Stage #3: 1-bromo-4-tert-butylbenzene With monophosphine 1,2,3,4,5-pentaphenyl-1'-(di-tert-butylphosphino)ferrocene; bis(dibenzylideneacetone)-palladium(0) In tetrahydrofuran; cyclohexane at 20℃; for 24h; | 93% |
Stage #1: diethylacetamide With bis(2,2,6,6-tetramethyl-1-piperidyl)zinc In toluene at 20℃; for 2h; Stage #2: 1-bromo-4-tert-butylbenzene With tri-tert-butyl phosphine; tris(dibenzylideneacetone)dipalladium (0) In toluene at 20℃; for 24h; Negishi coupling; | 81 % Spectr. |
bromochlorobenzene
diethylacetamide
2-(4-chlorophenyl)-N,N-diethylacetamide
Conditions | Yield |
---|---|
Stage #1: diethylacetamide With sec.-butyllithium In tetrahydrofuran; cyclohexane at -78℃; for 1h; Stage #2: With zinc(II) chloride In tetrahydrofuran; cyclohexane at 20℃; for 0.166667h; Stage #3: bromochlorobenzene With monophosphine 1,2,3,4,5-pentaphenyl-1'-(di-tert-butylphosphino)ferrocene; bis(dibenzylideneacetone)-palladium(0) In tetrahydrofuran; cyclohexane at 20℃; for 24h; | 94% |
With N-(dicyclohexylphosphino)-2-(2'-methylphenyl)-1H-indole; palladium diacetate; lithium tert-butoxide In toluene at 110℃; Inert atmosphere; Sealed tube; Microwave irradiation; chemoselective reaction; | 87% |
Conditions | Yield |
---|---|
With N-(dicyclohexylphosphino)-2-(2'-methylphenyl)-1H-indole; palladium diacetate; sodium hexamethyldisilazane In toluene at 110℃; Inert atmosphere; Sealed tube; Microwave irradiation; chemoselective reaction; | 94% |
diethylacetamide
meta-bromotoluene
N,N-diethyl-2,2-di-m-tolylacetamide
Conditions | Yield |
---|---|
With N-(dicyclohexylphosphino)-2-(2'-methylphenyl)-1H-indole; palladium diacetate; sodium hexamethyldisilazane In toluene at 110℃; Inert atmosphere; Sealed tube; Microwave irradiation; chemoselective reaction; | 94% |
Conditions | Yield |
---|---|
Stage #1: diethylacetamide With bis(2,2,6,6-tetramethyl-1-piperidyl)zinc In toluene at 20℃; for 2h; Stage #2: p-formylacetophenone In toluene at 20℃; for 4h; aldol reaction; | 93% |
Conditions | Yield |
---|---|
With morpholine In toluene byproducts: C6H6; mixt. of N,N-diethylamide, morpholine (1 equiv) and ZnPh2 (3.0 equiv) intoluene heated to 50°C for 24 h; | 93% |
With morpholine In toluene byproducts: C6H6; mixt. of N,N-diethylamide, morpholine (1 equiv) and ZnPh2 (2.0 equiv) intoluene heated to 50°C for 24 h; | 91% |
With piperidine In toluene byproducts: C6H6; mixt. of N,N-diethylamide, piperidine and ZnPh2 in toluene heated to 50°C for 24 h; | 90% |
diethylacetamide
2-ethylsulfanyl-benzoic acid methyl ester
N,N-diethyl-3-(2-ethylsulfanylphenyl)-3-oxopropanamide
Conditions | Yield |
---|---|
With lithium diisopropyl amide In tetrahydrofuran at -78℃; for 0.5h; Inert atmosphere; | 93% |
diethylacetamide
2-methylphenyl bromide
N,N-diethyl-2-(2-methylphenyl)acetamide
Conditions | Yield |
---|---|
With N-(dicyclohexylphosphino)-2-(2'-methylphenyl)-1H-indole; palladium diacetate; lithium tert-butoxide In toluene at 110℃; Inert atmosphere; Sealed tube; Microwave irradiation; chemoselective reaction; | 93% |
Conditions | Yield |
---|---|
Stage #1: diethylacetamide With sec.-butyllithium In tetrahydrofuran; cyclohexane at -78℃; for 1h; Stage #2: With zinc(II) chloride In tetrahydrofuran; cyclohexane at 20℃; for 0.166667h; Stage #3: o-fluorobromobenzene With monophosphine 1,2,3,4,5-pentaphenyl-1'-(di-tert-butylphosphino)ferrocene; bis(dibenzylideneacetone)-palladium(0) In tetrahydrofuran; cyclohexane at 20℃; for 24h; | 92% |
Conditions | Yield |
---|---|
Stage #1: diethylacetamide With sec.-butyllithium In tetrahydrofuran; cyclohexane at -78℃; for 1h; Stage #2: With zinc(II) chloride In tetrahydrofuran; cyclohexane at 20℃; for 0.166667h; Stage #3: (4-bromophenyl)(phenyl)methanone With monophosphine 1,2,3,4,5-pentaphenyl-1'-(di-tert-butylphosphino)ferrocene; bis(dibenzylideneacetone)-palladium(0) In tetrahydrofuran; cyclohexane at 20℃; for 24h; | 92% |
Conditions | Yield |
---|---|
Stage #1: diethylacetamide With sec.-butyllithium In tetrahydrofuran; cyclohexane at -78℃; for 1h; Stage #2: With zinc(II) chloride In tetrahydrofuran; cyclohexane at 20℃; for 0.166667h; Stage #3: para-bromoacetophenone With monophosphine 1,2,3,4,5-pentaphenyl-1'-(di-tert-butylphosphino)ferrocene; bis(dibenzylideneacetone)-palladium(0) In tetrahydrofuran; cyclohexane at 20℃; for 24h; | 92% |
diethylacetamide
1-Bromo-4-fluorobenzene
N,N-diethyl-2-(4-fluorophenyl)acetamide
Conditions | Yield |
---|---|
With N-(dicyclohexylphosphino)-2-(2'-methylphenyl)-1H-indole; palladium diacetate; lithium tert-butoxide In toluene at 110℃; Inert atmosphere; Sealed tube; Microwave irradiation; chemoselective reaction; | 92% |
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