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TRIS(DIMETHYLAMINO)ANTIMONY Basic information Product Name: TRIS(DIMETHYLAMINO)ANTIMONY Synonyms: TRIS(DIMETHYLAMINO)ANTIMONY;ANTIMONY TRIS(DIMETHYLAMIDE);TRIS(DIMETHYLAMINO)ANTIMONY, 99.99%;TRIS(DIMETHYLAMINO)ANTIMONY (99.99%-SB) SPECTRO;Tri

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Synthetic route

: 10025-91-9
antimony(III) chloride

: 3585-33-9
lithium dimethylamide

: 7289-92-1
tris(dimethylamino)stibine

Conditions

Conditions	Yield
In diethyl ether under Ar; from a 1:3 stoich. react. of SbCl3 and Me2NLi in Et2O; according to A. Kiennemann et al., J. Organomet. Chem., 1972, 35, 143; purifn. by distn.;

: 463-51-4
Ketene

: 7289-92-1
tris(dimethylamino)stibine

: 113359-20-9
tris(dimethylcarbamoylmethyl)stibine

Conditions

Conditions	Yield
In diethyl ether under N2 or Ar, ketene passed into ethereal soln. of Sb(NMe2)3 at -20°C; after removal of solvent residue dried under reduced pressure (ca. 1E-2 Pa) for 4 h;	98%

: 1116-70-7
tri(n-butyl)aluminium

: 7289-92-1
tris(dimethylamino)stibine

A: {(C4H9)2AlN(CH3)2}2

B: 2155-73-9
tributylstibine

Conditions

Conditions	Yield
In neat (no solvent) under N2; Al-compd. added slowly over a period of 2 h to Sb-compd. at 0°C with stirring, warmed slowly to room temp., stirred for 4 h, heated for 12 h at 120°C;; monitored by NMR, fractional distn., Al-compd. isolated by distn.;;	A 95% B 87%
In benzene-d6 addn. of Al-compd. to soln. of Sb-compd. in a NMR tube;; not isolated, monitored by 1H-, 13C-NMR spectroscopy;;

...Expand

: 100-99-2
triisobutylaluminum

: 7289-92-1
tris(dimethylamino)stibine

A: [(C4H9)2Al(N(CH3)2)2Al(C4H9)2]

B: 42966-06-3
triisobutylantimony

Conditions

Conditions	Yield
In neat (no solvent) under N2; Al-compd. added slowly over a period of 2 h to Sb-compd. at 0°C with stirring, warmed slowly to room temp., stirred for 4 h, heated for 12 h at 120°C;; monitored by NMR, fractional distn., Al-compd. isolated by sublimation; elem. anal.;;	A 95% B 63%
In benzene-d6 addn. of Al-compd. to soln. of Sb-compd. in a NMR tube;; not isolated, monitored by 1H-, 13C-NMR spctroscopy;;

...Expand

: 75-24-1
trimethylaluminum

: 7289-92-1
tris(dimethylamino)stibine

A: 22450-81-3
tetramethylbis[μ-(N-mrthylmethanaminato)]dialuminum

B: 594-10-5
trimethylantimony

Conditions

Conditions	Yield
In neat (no solvent) under N2; Al-compd. added slowly over a period of 2 h to Sb-compd. at 0°C with stirring, warmed slowly to room temp., stirred for 4 h, heated for 12 h at 120°C;; monitored by NMR, fractional distn., Al-compd. isolated by sublimation;;	A 93% B 82%
In benzene-d6 addn. of Al-compd. to soln. of Sb-compd. in a NMR tube;; not isolated, monitored by 1H-, 13C-NMR spectroscopy;;

...Expand

: 1121-53-5
benzyl sodium

: 110-18-9
N,N,N,N,-tetramethylethylenediamine

: 7289-92-1
tris(dimethylamino)stibine

: 822-68-4
cyclohexylphosphine

: Sb7Na3((CH3)2NCH2CH2N(CH3)2)3(C4H8O)3

Conditions

Conditions	Yield
In tetrahydrofuran; hexane; toluene under Ar; Sb(NMe2)3 in toluene added to chilled soln. of C6H11PH2 (1:1)in hexane; warmed to room temp.; stirred for 10 min; added to soln. prepared from PhCH2Na and CyPH2 in hexane-THF at -20°C; excess TMEDAadded; warmed to 25°C; reflux; filtered while warm; stored at -35°C;	93%

...Expand

: 102-67-0
tri-n-propylaluminum

: 7289-92-1
tris(dimethylamino)stibine

A: {(C3H7)2AlN(CH3)2}2

B: 5613-69-4
tripropylstibine

Conditions

Conditions	Yield
In neat (no solvent) under N2; Al-compd. added slowly over a period of 2 h to Sb-compd. at 0°C with stirring, warmed slowly to room temp., stirred for 4 h, heated for 12 h at 120°C;; monitored by NMR, fractional distn., Al-compd. isolated by distn.;;	A 91% B 83%
In benzene-d6 addn. of Al-compd. to soln. of Sb-compd. in a NMR tube;; not isolated, monitored by 1H-, 13C-NMR spectroscopy;;

...Expand

: 124-38-9
carbon dioxide

: 7289-92-1
tris(dimethylamino)stibine

: 473302-00-0
tris(N,N-dimethylcarbamato)antimony(III)

Conditions

Conditions	Yield
In hexane through soln. Sb(NMe2)3 in hexane CO2 was bubbled for 30 min; solvent was removed in vacuo, residue was recrystd. from toluene at -20°C; elem. anal.;	91%

: 97-93-8
triethylaluminum

: 7289-92-1
tris(dimethylamino)stibine

A: [(C2H5)2Al(N(CH3)2)2Al(C2H5)2]

B: 617-85-6
triethylantimony

Conditions

Conditions	Yield
In neat (no solvent) under N2; Al-compd. added slowly over a period of 2 h to Sb-compd. at 0°C with stirring, warmed slowly to room temp., stirred for 4 h, heated for 12 h at 120°C; monitored by NMR, fractional distn., Al-compd. isolated by distn.;;	A 89% B 83%
In benzene-d6 addn. of Al-compd. to soln. of Sb-compd. in a NMR tube; not isolated, monitored by 1H-, 13C-NMR spectroscopy;;

...Expand

: 110-54-3
hexane

: 7289-92-1
tris(dimethylamino)stibine

: 166302-06-3
5,11,17,23,29-penta-tert-butyl-31-n-benzoxy-32,33,34,35-tetrahydroxycalix<5>arene

: [Sb2O(monobenzyl-para-t-butylcalix[5]arene(4-))]*1.5(hexane)

Conditions

Conditions	Yield
In benzene (N2) soln. Sb(NMe2)3 in benzene was added dropwise to soln. t-BuC5(Bn)(H)4 in benzene and stirred for 48 h at room temp.; soln. was evapd., residue was crystd. by hexane diffusion into soln. in benzene; elem. anal.;	89%

...Expand

: 109-72-8, 29786-93-4
n-butyllithium

: 7289-92-1
tris(dimethylamino)stibine

: 108-91-8
cyclohexylamine

: Li[(((CH3)2N)Sb(NC6H11)2)2Sb]

Conditions

Conditions	Yield
With ((CH3)2CH)2NH In hexane; toluene under Ar; adding n-BuLi in hexanes to soln. of i-Pr2NH in hexane, heating briefly to reflux, cooling to room temp., adding this to mixt. of Sb(NMe2)3 (in toluene) and C6H11NH2 (previously briefly refluxed and cooledto room temp.); filtration, reducing filtrate under vac. until ppt. appeared, warming ppt. back into soln., crystn. by storage at 25°C (24 h);	88%

...Expand

: 7289-92-1
tris(dimethylamino)stibine

: 620177-71-1
2,2'-((4-bromophenyl)methylene)bis(3-methyl-1H-indole)

: 1401085-50-4
Di-(3-methylindol-2-yl)dimethylamidoantimony-4-bromophenylmethane

Conditions

Conditions	Yield
In toluene at -78 - 25℃; for 3h;	88%

: 7289-92-1
tris(dimethylamino)stibine

: 148808-60-0
HSeSi(Si(CH3)3)3

: Sb(3+)*3SeSi(Si(CH3)3)3(1-)=Sb[SeSi(Si(CH3)3)3]3

Conditions

Conditions	Yield
In hexane N2-atmosphere; stirring Sb-compd. with 3 equiv. of Se-compd. (-78°C, 10 min), warming to room temp., stirring for 2 h; evapn. (reduced pressure), extn. into O(SiMe3)2, filtration, concn., crystn. (-40°C, several d), filtration; elem. anal.;	87%

: 576-26-1
2.6-dimethylphenol

: 7289-92-1
tris(dimethylamino)stibine

: Sb(OC6H3Me2-2,6)3

Conditions

Conditions	Yield
In hexane 2,6-dimethylphenol in hexane was added slowly to soln. tris(dimethylamino)antimony(III) in hexane and stirred overnight; solvent was removed in vacuo, residue was dissolved in toluene; elem. anal.;	84%

: 7289-92-1
tris(dimethylamino)stibine

: 163631-37-6
(2,6-iPr2C6H3)N(SiMe3)Si(OH)3

: 934165-80-7
[Sb(SiO3((2,6-iPr2C6H3)NSiMe3))]4

Conditions

Conditions	Yield
In tetrahydrofuran; hexane byproducts: HNMe2; under dry oxygen-free N2; metal compd. added dropwise to suspn. of Si compd. (1:1) at room temp., stirred for 24 h at room temp., refluxed for 1h, coooled, concd.; crystd. in 4 d, elem. anal.;	83%

: 109-99-9
tetrahydrofuran

: 7289-92-1
tris(dimethylamino)stibine

: 96107-95-8
calix[6]arene

: [Sb2(calix[6]arene(6-))]*1.5THF*1.5pentane

Conditions

Conditions	Yield
In toluene (N2) soln. Sb(NMe2)3 in toluene was added dropwise to suspn. HC6(H)6 in toluene and stirred for 48 h; ppt. was centrifugated and washed with toluene; elem. anal.;	83%

...Expand

: 109-99-9
tetrahydrofuran

: 1192283-08-1
H2(CH2C6H2(C(CH3)3)O)5(CH2C6H5)Si(CH3)2

: 7289-92-1
tris(dimethylamino)stibine

: Sb(N(CH3)2)(CH2C6H2(C(CH3)3)O)5(CH2C6H5)Si(CH3)2*OC4H8

Conditions

Conditions	Yield
In toluene (N2) soln. Sb(NMe2)3 in toluene was added dropwise to soln. ligand in tiluene, stirred for 24 h at room temp.; solvent was removed in vacuo, residue was dissolved in pentane and centrifuged, THF was added and placed in freezer at -35°C for 4 days; elem. anal.;	83%

...Expand

: 10025-91-9
antimony(III) chloride

: 7289-92-1
tris(dimethylamino)stibine

: dimethylaminochloroethoxostibane

Conditions

Conditions	Yield
With ethanol In diethyl ether exclusion of air and moisture; dropwise addn. of SbCl3 in ether to a soln. of Sb(NMe2)3 in ether (molar ratio amide:chloride = 2:1) at -78°C with stirring; after 2 h dropwise addn. of EtOH in ether, stirring for 12 h; ppt. is filtd. at -78°C, dried in vac.; elem. anal.;	82%

: 10025-91-9
antimony(III) chloride

: 7289-92-1
tris(dimethylamino)stibine

: dimethylaminodichlorostibane

Conditions

Conditions	Yield
In diethyl ether; hexane exclusion of air and moisture; dropwise addn. of Sb(NMe2)3 in hexane toa soln. of SbCl3 (molar ratio amide:chloride = 1:2) in ether at -78°C with stirring; mixt. stirred for 12 h at this temp.; solid is filtd. at -78°C, washed (ether); elem. anal.;	81%

: 109-72-8, 29786-93-4
n-butyllithium

: 7289-92-1
tris(dimethylamino)stibine

: 108-91-8
cyclohexylamine

: ((C6H11NLi)3Sb)2

Conditions

Conditions	Yield
In hexane; toluene 20°C; filtering, pptn. on concg. (vac.);	80%

...Expand

: 10025-91-9
antimony(III) chloride

: 7289-92-1
tris(dimethylamino)stibine

: bis(dimethylamino)chlorostibane

Conditions

Conditions	Yield
In diethyl ether; hexane exclusion of air and moisture; dropwise addn. of SbCl3 in ether to a soln. of Sb(NMe2)3 in hexane (molar ratio amide:chloride = 2:1) at -78°C with stirring, reaction time 24 h; solid is filtd. at -78°C; elem. anal.;	77%

: 7289-92-1
tris(dimethylamino)stibine

: 133100-98-8
tris(trimethylsilyl)silyltellurol

: Sb(3+)*3TeSi(Si(CH3)3)3(1-)=Sb[TeSi(Si(CH3)3)3]3

Conditions

Conditions	Yield
In hexane N2-atmosphere; stirring Sb-compd. with 3 equiv. of Te-compd. (-78°C, 15 min), warming to room temp., stirring for 60 min; evapn. (reduced pressure), extn. into O(SiMe3)2, filtration, concn., crystn. (-40°C, 24 h), filtration; elem. anal.;	75%

: 10025-91-9
antimony(III) chloride

: 7289-92-1
tris(dimethylamino)stibine

: dimethylaminochloromethoxostibane

Conditions

Conditions	Yield
With methanol In diethyl ether exclusion of air and moisture; dropwise addn. of SbCl3 in ether to a soln. of Sb(NMe2)3 in ether (molar ratio amide:chloride = 2:1) at -78°C with stirring; after 2 h dropwise addn. of MeOH in ether, stirring for 12 h; ppt. is filtd. at -78°C, dried in vac.; elem. anal.;	74%

: 205517-60-8
((CH3)3SiNHC6H4)2NH

: 7289-92-1
tris(dimethylamino)stibine

: C18H26N3SbSi2

Conditions

Conditions	Yield
Stage #1: ((CH3)3SiNHC6H4)2NH; tris(dimethylamino)stibine In hexane at -30 - 20℃; for 24h; Schlenk technique; Glovebox; Inert atmosphere; Stage #2: In hexane under 0.00750075 Torr; for 20h; Schlenk technique; Glovebox; Inert atmosphere;	72%

: 189832-67-5
5,11,17,23,29,35-hexakis(tert-butyl)-37,38,39,40,41-hexakis(hydroxy)calix[6]arene

: 7289-92-1
tris(dimethylamino)stibine

: 1185419-79-7
[Sb2(para-tert-butylcalix[6]arene(6-))]

Conditions

Conditions	Yield
In benzene (N2) soln. Sb(NMe2)3 in benzene was added dropwise to suspn. t-BuC6(H)6 in benzene and stirred for 48 h; ppt. was filtered and washed with benzene; elem. anal.;	71%

: 109-72-8, 29786-93-4
n-butyllithium

: 2501-94-2
tert-butylphosphine

: 7289-92-1
tris(dimethylamino)stibine

A: Sb7(3-)

: 511242-27-6
(((CH3)3CP)3Sb)2

Conditions

Conditions	Yield
In tetrahydrofuran; hexane; toluene byproducts: Sb; (Ar); react. of a soln. of phosphine in THF with a soln. of lithium compd. in hexanes at 0°C, addn. of a soln. of antimony compd. in toluene, warming to room temp., refluxing for 10 min; storage at room temp. for 7 d; elem. anal.;	A 0% B 69%

...Expand

: 113748-54-2
(2,6-diisopropylphenylimino)(2,2,6,6-tetramethylpiperidino)borane

: 7289-92-1
tris(dimethylamino)stibine

: 117499-86-2
{(2,6-diisopropylphenyl)(dimethylamino(2,2,6,6-tetramethylpiperidino)boryl)amino}bis(dimethylamino)stibane

Conditions

Conditions	Yield
In hexane; pentane (N2 or Ar); to suspn. of borane in pentane was dropped soln. of As(OCH3)3 in hexane with stirring, after stirring for 12 h solvents were removed in vac.; residue was recrystd. from hexane; elem. anal.;	68%

: 317322-17-1
[Ga(2-((2,6-diisoproylphenyl)amino)-4-((2,6-diisopropylphenyl)imino)-2-pentene)]

: 7289-92-1
tris(dimethylamino)stibine

: C62H94Ga2N6Sb2

Conditions

Conditions	Yield
In toluene at 75℃; for 24h; Inert atmosphere; Schlenk technique; Glovebox;	64%

: [((2,6-(isopropyl)2C6H3)NC(CH3)CHC(CH3)N(2,6-(isopropyl)2C6H3))Al(methyl)OH]

: 7289-92-1
tris(dimethylamino)stibine

: [HC(CMeN(C6H3(i-Pr)2))2Al(Me)(μ-O)]2Sb(NMe2)

Conditions

Conditions	Yield
In toluene toluene soln. of Al compd. added dropwise to toluene soln. of Sb compd. (2:1 molar ratio) at 0°C, react. mixt. warmed to room temp., stirred overnight; evapd., extd. (n-hexane), elem. anal.;	60%

: 7289-92-1
tris(dimethylamino)stibine

: 108-91-8
cyclohexylamine

: benzyl rubidium

: [Sb3(NC6H11)4(NHC6H11)2Rb(C4H8O)2]

Conditions

Conditions	Yield
In tetrahydrofuran; toluene byproducts: toluene, dimethylamine; (argon); addn. of cyclohexylamine in toluene at -78°C to RbCH2C6H5 in toluene, warming to room temp. and stirring 5 min, cooling to -78°C, addn. of Sb(NMe2)3 in THF, stirring (20 min), warming to room temp.; filtration (Celite), removal of solvents (vac.), addn. of Et2O and THF, crystn. upon storage (-15°C, 12 h); elem. anal.;	59%

...Expand

: 7289-92-1
tris(dimethylamino)stibine

: 89201-97-8
(tert-butylimino)(2,2,6,6-tetramethylpiperidino)borane

: 117499-82-8
{t-butyl(dimethylamino(2,2,6,6-tetramethylpiperidino)boryl)amino}bis(dimethylamino)stibane

Conditions

Conditions	Yield
In hexane (N2 or Ar); to soln. of borane was dropped Sb(NMe2)3 soln. with stirring, after stirring for 12 h solvent was removed in vac.; residue was recrystd. from hexane; elem. anal.;	58%

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L-Leucine,N-[(1,1-dimethylethoxy)carbonyl]-L-a-glutamyl-L-a-glutamyl-,3-methyl ester (9CI)

72904-85-9

a-D-Galactopyranoside, methyl4,6-O-[(R)-phenylmethylene]-

72905-86-3

Octadecanoic acid, 2,3-dihydroxypropyl ester, ester with boric acid(H3BO3)

72905-88-5

Aluminum,amidoimidodiphosphate phosphoramidate ammonium complexes

72906-24-2

1,5-Naphthalenedisulfonic acid, 3,3-((3-methyl-1,2-phenylene)bis(imino(6-chloro-1,3,5-triazine-4,2-diyl)imino(2-(acetylamino)-5-methoxy-4,1-phenylene)azo))bis-, tetrasodium salt

72908-87-3

Pyrrolo[2,3-c]azepine-4,8(1H,5H)-dione,6,7-dihydro-

72909-34-3

1H-Pyrrolo[2,3-f]quinoline-2,7,9-tricarboxylicacid, 4,5-dihydro-4,5-dioxo-

7291-22-7

Pyridine-2,3,4,5,6-d5

7291-33-0

Acetamide,2,2,2-trichloro-N,N-dimethyl-

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