CAS No.7784-35-2,ARSENIC TRIFLUORIDE Suppliers,MSDS download

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Arsenic trifluoride

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arsenic trifluoride

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Synthetic route

: 12793-14-5
niobocene dichloride

: 7784-36-3
arsenic pentafluoride

A: (η5-C5H5)2niobium(V)(Cl2) hexafluoroarsenate

B: 7784-35-2
arsenic(III) fluoride

Conditions

Conditions	Yield
In liquid sulphur dioxide under Ar; recrystn. (SO2), elem. anal.;	A 100% B n/a

...Expand

: 10544-50-0
sulfur

: 7726-95-6
bromine

: 7784-36-3
arsenic pentafluoride

A: S3Br3(1+)*AsF6(1-) = [S3Br3]AsF6

B: 7784-35-2
arsenic(III) fluoride

Conditions

Conditions	Yield
In sulfur dioxide 1 d; slow removal of solvent, cooling to 0°C;	A 99.7% B n/a

...Expand

: 116-14-3
polytetrafluoroethylene

: 12536-35-5
Te4(2+)*2AsF6(1-)=Te4(AsF6)2

A: 76-16-4
Hexafluoroethane

B: 41055-97-4
bis(pentafluoroethyl)tellurium

C: 41055-98-5
bis(pentafluoroethyl) ditelluride

D: 55620-41-2
pentafluoroethyl(nonafluorobutyl)tellurium

E: 7784-35-2
arsenic(III) fluoride

Conditions

Conditions	Yield
at 100°C for 11 d, at 15 atm in a Monel reactor;	A n/a B 87% C 12.2% D 0.5% E n/a
at 100°C for 11 d, at 15 atm in a Monel reactor;	A n/a B 87% C 12.2% D 0.5% E n/a
at 100°C for 11 d, at 15 atm in a Monel reactor;	A n/a B 87% C 12.2% D 0.5% E n/a

...Expand

: 7784-36-3
arsenic pentafluoride

: 7784-33-0
arsenic(III) bromide

A: 119484-31-0
AsBr4(1+)*AsF6(1-)={AsBr4}{AsF6}

B: 7784-35-2
arsenic(III) fluoride

Conditions

Conditions	Yield
With bromine Condensing of AsF5 onto Br2 and AsBr3 at -196°C, warming to -5°C until a clear soln. is formed (1 min), cooling (-196°C), repeating of process in excess of 10 times.; Evapn. of volatiles in vac (-5°C, 10 min).;	A 60% B n/a

...Expand

: 1279123-63-5
potassium hydrogenfluoride

: 7784-34-1
arsenic trichloride

: 7784-35-2
arsenic(III) fluoride

Conditions

Conditions	Yield
In neat (no solvent) byproducts: KAsF4, HCl; dropping AsCl3 to KF*HF over 1 h while heating to 50-60°C; and 1 h while heating to 170°C;; distn.; elem. anal.;;	28.3%

: 15606-93-6
triamyl arsenite

: 455-32-3
benzoyl fluoride

: 7784-35-2
arsenic(III) fluoride

Conditions

Conditions	Yield
In neat (no solvent) byproducts: C6H5COOC5H11; stirring mixt. of (C5H11O)3As and C6H5COF for 0.5 h at room temp. and 1 h while heating to 170°C;; distn. of fraction during heating process; reapeated fractionated distn.; elem. anal.;;	15.1%

: 7782-49-2
selenium

: 7784-36-3
arsenic pentafluoride

: 7553-56-2
iodine

A: 59544-89-7
SeI3(1+)*AsF6(1-)=(SeI3)(AsF6)

B: 7784-35-2
arsenic(III) fluoride

...Expand

: AsF3*3SO3

: sodium fluoride

: 7784-35-2
arsenic(III) fluoride

Conditions

Conditions	Yield
byproducts: NaSO3F; in cold very vigorous reaction;
byproducts: NaSO3F; in cold very vigorous reaction;

: arsenic

: 7782-41-4
fluorine

: 7784-36-3
arsenic pentafluoride

B: 7784-35-2
arsenic(III) fluoride

Conditions

Conditions	Yield
In neat (no solvent) from As and gaseous F2 with inflammation;; small amount of AsF5;;
In neat (no solvent) from gaseous F2 and As; vigorous reaction; in a sufficiently rapid flow of F2 also AsF5 is formed;;
In neat (no solvent) from gaseous F2 and As; vigorous reaction; in a sufficiently rapid flow of F2 also AsF5 is formed;;

...Expand

: calcium fluoride

: arsenic(III) trioxide

: 7784-35-2
arsenic(III) fluoride

Conditions

Conditions	Yield
In sulfuric acid on heating mixture of As2O3, CaF2 and concd. H2SO4;;

: arsenic(III) trioxide

: 7782-41-4
fluorine

: 7784-35-2
arsenic(III) fluoride

Conditions

Conditions	Yield
In neat (no solvent) violent reaction with inflammation;;

: 1279123-63-5
potassium hydrogenfluoride

: arsenic(III) trioxide

: 7784-35-2
arsenic(III) fluoride

Conditions

Conditions	Yield
In neat (no solvent) heating a mixture of As2O3 and KHF2;;
In neat (no solvent) heating a mixture of As2O3 and KHF2;;

: 1279123-63-5
potassium hydrogenfluoride

: 15606-93-6
triamyl arsenite

A: potassium fluoride

B: 7784-35-2
arsenic(III) fluoride

Conditions

Conditions	Yield
In neat (no solvent) byproducts: C5H11OH; heating equimolar mixt. of (C5H11O)3As and KF*HF;;	A 0% B 0%

...Expand

: 7784-36-3
arsenic pentafluoride

: 7553-56-2
iodine

A: 84493-41-4
I4(2+)*2AsF6(1-) = I4(AsF6)2

B: 7784-35-2
arsenic(III) fluoride

Conditions

Conditions	Yield
In sulfur dioxide A soln. of I2 and AsF5 was stirred in SO2 at room temp. for 48 h, volatile components were slowly removed producing dark crystals, which form a red powder by grinding.; The red powder was dissolved in SO2, the crystals were obtained by slowly removal of the solvent.;
In further solvent(s) A soln. of I2 and AsF5 was stirred in SO2ClF at room temp. for 48 h, volatile components were slowly removed producing a red powder.; The red powder was dissolved in SO2, the crystals were obtained by slowly removal of the solvent.;

...Expand

: 7784-36-3
arsenic pentafluoride

: 7726-95-6
bromine

: 7784-33-0
arsenic(III) bromide

A: 119484-31-0
AsBr4(1+)*AsF6(1-)={AsBr4}{AsF6}

B: 7784-35-2
arsenic(III) fluoride

Conditions

Conditions	Yield
AsF5 condensed at -196°C onto a mixture of Br2 and AsBr3, warmed to -5°C, recooled to -196°C (repeated for more than 10 times); AsF3 removed at -5°C under dynamic vac.;

...Expand

: ammonium fluoride

: 7784-33-0
arsenic(III) bromide

: 7784-35-2
arsenic(III) fluoride

Conditions

Conditions	Yield
In neat (no solvent) heating;;
In neat (no solvent) heating;;

: 12083-48-6
bis(cyclopentadienyl)vanadium dichloride

: 7784-36-3
arsenic pentafluoride

A: bis(η5-cyclopentadienyl)dichlorovanadium(V)hexafluoroarsenate

B: 2C5H5(1-)*V(4+)*Cl(1-)*AsF6(1-)=(C5H5)2VCl(AsF6)

C: 7784-35-2
arsenic(III) fluoride

Conditions

Conditions	Yield
With ClF3 In trichlorofluoromethane byproducts: Cl2, (ClF2)(AsF6); 25°C, 8h;	A 0% B n/a C n/a

...Expand

: 2083-91-2
N,N-Dimethyltrimethylsilylamine

: 7784-36-3
arsenic pentafluoride

A: 420-56-4
trimethylsilyl fluoride

B: 14722-43-1
dimethyl-N-fluoroamine

C: 7784-35-2
arsenic(III) fluoride

Conditions

Conditions	Yield
In solid matrix onto a frozen soln. of Me3SiNMe2 in SO2 in an NMR-tube AsF5 is condensed at -196°C, warming to room temp.; monitored by NMR-spectroscopy;

...Expand

: 109-63-7
boron trifluoride diethyl etherate

: arsenic(III) trioxide

A: boron trioxide

B: 7784-35-2
arsenic(III) fluoride

Conditions

Conditions	Yield
In neat (no solvent) byproducts: (C2H5)2O; heating equimolar mixt. of BF3*(C2H5)2O and As2O3;;	A 0% B 0%

...Expand

: 15606-93-6
triamyl arsenite

: 109-63-7
boron trifluoride diethyl etherate

A: 621-78-3
tri-n-amylborate

B: 7784-35-2
arsenic(III) fluoride

Conditions

Conditions	Yield
In neat (no solvent) byproducts: (C2H5)2O; heating equimolar mixt. of BF3*(C2H5)2O and (C5H11O)3As;;	A 0% B 0%

...Expand

: 432-02-0
tris(trifluoromethyl)arsine

A: 75-73-0
carbon tetrafluoride

B: 76-19-7
freon-218

C: 76-16-4
Hexafluoroethane

D: 7784-35-2
arsenic(III) fluoride

Conditions

Conditions	Yield
Kinetics; byproducts: higher satd. perfluorohydrocarbons; thermal decompn. at 350-410°C; in platinum vessel;	A <1 B n/a C n/a D n/a

...Expand

: 432-02-0
tris(trifluoromethyl)arsine

: 7784-23-8
aluminium(III) iodide

A: arsenic

B: 75-73-0
carbon tetrafluoride

C: 76-16-4
Hexafluoroethane

D: 7784-35-2
arsenic(III) fluoride

Conditions

Conditions	Yield
quick react. at 150°C (1 h);
quick react. at 150°C (1 h);

...Expand

: 10026-18-3
cobalt(III) fluoride

: 432-02-0
tris(trifluoromethyl)arsine

A: 75-73-0
carbon tetrafluoride

B: 359-54-6
bis(trifluoromethyl)fluoroarsine

C: 7784-35-2
arsenic(III) fluoride

Conditions

Conditions	Yield
in N2 stream at 100°C; fractionated condensation;
100°C, 3.5 h; leading of N2 stream containing (CF3)As over CoF3;

...Expand

: 10026-18-3
cobalt(III) fluoride

: 432-02-0
tris(trifluoromethyl)arsine

A: 75-73-0
carbon tetrafluoride

B: 7784-35-2
arsenic(III) fluoride

Conditions

Conditions	Yield
160°C;	A >99 B >99

...Expand

: 432-02-0
tris(trifluoromethyl)arsine

: 7782-41-4
fluorine

: 7784-35-2
arsenic(III) fluoride

Conditions

Conditions	Yield
In not given

: 432-02-0
tris(trifluoromethyl)arsine

: 7782-41-4
fluorine

A: 75-73-0
carbon tetrafluoride

B: 7784-35-2
arsenic(III) fluoride

Conditions

Conditions	Yield
between -66 and -28°C;

...Expand

: 359-69-3
Tris(pentafluoraethyl)arsan

: 7782-41-4
fluorine

: 7784-35-2
arsenic(III) fluoride

Conditions

Conditions	Yield
In not given byproducts: As(C2F5)3F2; 120°C;

: C8AsF5

A: 7784-35-2
arsenic(III) fluoride

B: 7784-36-3
arsenic pentafluoride

Conditions

Conditions	Yield
at 20°C under vac., 1 min; monitored by IR spectroscopy;

: arsenic

: 7783-54-2
nitrogen trifluoride

A: 7727-37-9
nitrogen

B: 7784-35-2
arsenic(III) fluoride

Conditions

Conditions	Yield
In neat (no solvent) react. of NF3 and As on heating with inflammation;;
In neat (no solvent) react. of NF3 and As on heating with inflammation;;

...Expand

: ammonium hydrogen fluoride

: 15606-93-6
triamyl arsenite

: 7784-35-2
arsenic(III) fluoride

Conditions

Conditions	Yield
With hydrogenchloride In neat (no solvent) byproducts: amyl alcohol, NH4Cl; passing dry HCl into mixt. containing (C5H11O)3As and NH4F*HF for 2 h at 110°C;; not isolated; mass spectroscopy; low yield;;

: 309-89-7
titanocene difluoride

: 7784-35-2
arsenic(III) fluoride

: {Ti(η-C5H5)2F2}*AsF3

Conditions

Conditions	Yield
In liquid sulphur dioxide under inert atm.; stirring at room temp. for 1 h;; evapn.; elem. anal.;	96%

: tetrachloro(cyclopentadienyl)niobium(V)

: 7784-35-2
arsenic(III) fluoride

: tetrafluoro(η5-cyclopentadienyl)niobium

Conditions

Conditions	Yield
In toluene addn. of AsF3 to Nb compd. soln. under N2; stirring, room temp., 2h; filtration; washing twice (toluene and n-hexane); drying; heating in oil pump vac. (100°C), 2h;	95%

: (η-5-ethyltetramethylcyclopentadienyl)titanium trichloride

: 7784-35-2
arsenic(III) fluoride

: (η5-ethyltetramethylcyclopentadienyl)titanium trifluoride

Conditions

Conditions	Yield
In neat (no solvent) addn. of AsF3 to (C2H5(CH3)4C5)TiCl3 at room temperature; heating for 3 h with stirring on reflux at 60°C; cooling down; evaporation of excess AsF3 in vac.;; sublimation at 1E-3 mbar and 80°C; elem. anal.;;	88%

: dichloroborylferrocene

: 7784-35-2
arsenic(III) fluoride

: (ferrocenyl)difluoroborane

Conditions

Conditions	Yield
In pentane 0°C;	86%

: 12129-06-5
Cp*TiCl3

: 7784-35-2
arsenic(III) fluoride

: (η5-pentamethylcyclopentadienyl)titanium trifluoride

Conditions

Conditions	Yield
In neat (no solvent) addn. of AsF3 to Ti-compound at room temperature; stirring and heating for 3 h on reflux at 60°C; cooling to room temperature; separation of excess AsF3 in vac.;; sublimation of formed ((C5(CH3)5)TiF3)2*2AsF3 at 1E-3 mbar and 110°C; elem. anal.;;	85%

: 6779-72-2
Bis(pentafluorphenyl)-trichlorphosphoran

: 7784-35-2
arsenic(III) fluoride

: 22474-71-1
Bis(pentafluorphenyl)-trifluorphosphoran

Conditions

Conditions	Yield
1.5 h;	76%
1.5 h;	76%

: 31954-57-1
phosphorus(V) chloride * TaCl5

: 7784-35-2
arsenic(III) fluoride

: 7784-34-1
arsenic trichloride

A: TaCl4F

B: 7647-19-0, 874483-74-6
phosphorus pentafluoride

Conditions

Conditions	Yield
heating, excess of AsF3; cooling, washing with cold AsCl3;	A 70% B n/a

...Expand

: 10544-50-0
sulfur

: 7784-35-2
arsenic(III) fluoride

: 7782-50-5
chlorine

: 27075-96-3
{SCl3}(1+)*{AsF6}(1-)=SCl3AsF6

Conditions

Conditions	Yield
In neat (no solvent) byproducts: AsCl3; absence of moisture; condensing AsF3 and then Cl2 onto sulfur, slow warming to room temp. (over 1 h), stirring overnight; removal of volatiles, dissoln. in liquid AsF3 at -15°C, filtration, evapn. (vac.);	65.4%
byproducts: AsCl3, S2Cl2; warmed from -196.degree C to room temp. in vac.; solvents evapd. in high vac. at 100°C overnight;

...Expand

: 7784-35-2
arsenic(III) fluoride

: 13175-72-9
Difluor-pentafluorphenyl-phosphin

: 22474-70-0
Pentafluorphenyl-tetrafluorphosphoran

Conditions

Conditions	Yield
With chlorine in a steel cylinder first at -196°C then heating (15 h) to 20°C finally 5 h at 100-110°C; pptn.;	65%
With Cl2 in a steel cylinder first at -196°C then heating (15 h) to 20°C finally 5 h at 100-110°C; pptn.;	65%
15 h refluxing at 100-110°C in a steel autoclave; fractionation was impossible;

: 113748-54-2
(2,6-diisopropylphenylimino)(2,2,6,6-tetramethylpiperidino)borane

: 7784-35-2
arsenic(III) fluoride

: 113748-71-3
((fluoro(2,2,6,6-tetramethylpiperidino)boryl)(2,6-diisopropylphenyl)amino)arsenic difluoride

Conditions

Conditions	Yield
In hexane oxygen and moisture exclusion, mixing of solns. (0°C or room temp.), stirring (12 h); conc. (pptn.), washing (hexane), drying (high vacuum); elem. anal.;	63%

: 214750-04-6
(Cl2BC5H4)Co(C5H4BCl3)

: 7784-35-2
arsenic(III) fluoride

: 214750-10-4
Co(C5H4BF2)(μ-OH)

Conditions

Conditions	Yield
In nitromethane N2-atmosphere; stirring (room temp., 3 h); evapn. (vac.), hexane addn., chromy. (SiO2, hexane, MeNO2), crystn. on concg. (-30°C); elem. anal.;	60%

: 79-38-9
Chlorotrifluoroethylene

: 7783-70-2
antimony pentafluoride

: 7784-35-2
arsenic(III) fluoride

A: 34699-05-3, 42407-79-4, 42407-80-7
Bis(2-chlor-terafluoraethyl)-fluorarsan

B: 41920-41-6, 42407-76-1, 42407-77-2
bis(1-chlorotetrafluoroethyl)chloroarsine

Conditions

Conditions	Yield
at 20°C, 6 h;	A 58% B 14%
at 20°C, 6 h;	A 58% B 14%

...Expand

: pentamethylcyclopentadienyl tantalum(V) tetrachloride

: 7784-35-2
arsenic(III) fluoride

: di-μ-fluoro-bis{trifluoro(η5-pentamethylcyclopentadienyl)tantalum(V)}-trifluoroarsenic (1/2)

Conditions

Conditions	Yield
In neat (no solvent) byproducts: AsCl3; refluxing for 1 h; cooling to 0°C, standing for 15 h, filtn. and recrystn. from AsF3;	45%

: 116-14-3
polytetrafluoroethylene

: 7783-70-2
antimony pentafluoride

: 7784-35-2
arsenic(III) fluoride

: 359-69-3
Tris(pentafluoraethyl)arsan

Conditions

Conditions	Yield
20°C, under pressure;	39%
20°C, under pressure;	39%

...Expand

: 80432-35-5
pentamethylcyclopentadienyl niobium(V) tetrachloride

: 7784-35-2
arsenic(III) fluoride

: tetrafluoro(η5-pentamethylcycopentadienyl)niobium*AsF3

Conditions

Conditions	Yield
In neat (no solvent) addn. of AsF3 to Nb compd. under N2; exothermic react.; refluxing with stirring, 1h; cooling to room temp.; storage at 5°C; pptn.; elem. anal.;	39%

: 38117-54-3
cyclopentadienyl iron(II) dicarbonyl dimer

: 7784-35-2
arsenic(III) fluoride

: [((C5H5)Fe(CO)2)2As(OH)2](1+)*[AsF4](1-)=[((C5H5)Fe(CO)2)2As(OH)2][AsF4]

Conditions

Conditions	Yield
With (CH3)2CO In neat (no solvent) (N2); complex soln. in AsF3 stirred for 6 h at 50°C, (CH3)2CO added; filtered, washed with pentane, recrystd. (acetone); elem. anal.;	35%

: 7783-70-2
antimony pentafluoride

: 7784-35-2
arsenic(III) fluoride

A: 32395-49-6
Bis(pentafluoraethyl)-fluorarsan

B: 359-69-3
Tris(pentafluoraethyl)arsan

Conditions

Conditions	Yield
20°C, under pressure;	A 30% B n/a
20°C, under pressure;	A 30% B n/a

...Expand

: [(η(5)-C5H4Me)Fe(CO)2]2

: 143-66-8
sodium tetraphenyl borate

: 7784-35-2
arsenic(III) fluoride

: [((CH3C5H4)Fe(CO)2)2As(OCH3)2](1+)*[B(C6H5)4](1-)=[((CH3C5H4)Fe(CO)2)2As(OCH3)2][B(C6H5)4]

Conditions

Conditions	Yield
With CH3OH In neat (no solvent) (N2); (a) complex in AsF3 stirred for 3 h at 50°C, (b) evapd., dissolved in hot MeOH, NaB(C6H5)4/MeOH added; recrystd. (acetone/MeOH); elem. anal.;	18%

...Expand

: 38117-54-3
cyclopentadienyl iron(II) dicarbonyl dimer

: 7784-35-2
arsenic(III) fluoride

: [((C5H5)Fe(CO)2)2AsF2](1+)*[AsF4](1-)*(CH3)2CO=[((C5H5)Fe(CO)2)2AsF2][AsF4]*(CH3)2CO

Conditions

Conditions	Yield
With (CH3)2CO In neat (no solvent) (N2); complex soln. in AsF3 stirred for 6 h at 50°C, (CH3)2CO added; filtered, washed with pentane, dried; elem. anal.;	18%

: [(η(5)-C5H4Me)Fe(CO)2]2

: 143-66-8
sodium tetraphenyl borate

: 7784-35-2
arsenic(III) fluoride

: [((CH3C5H4)Fe(CO)2)2As(F)(OC2H5)](1+)*[B(C6H5)4](1-)=[((CH3C5H4)Fe(CO)2)2As(F)(OC2H5)][B(C6H5)4]

Conditions

Conditions	Yield
With C2H5OH In neat (no solvent) (N2); (a) complex in AsF3 stirred for 3 h at 50°C, (b) evapd., dissolved in EtOH, NaB(C6H5)4/EtOH added; immediately cooled and filtered; elem. anal.;	11%

...Expand

: 7782-49-2
selenium

: 7784-36-3
arsenic pentafluoride

: 7553-56-2
iodine

: 7784-35-2
arsenic(III) fluoride

A: (Se7I)4Se4(6+)*6AsF6(1-)=(Se7I)4Se4(AsF6)6

B: catena-poly{cyclohexaselenium(1+)-4:1-μ-iodo}*n(hexafluoroarsenate)

Conditions

Conditions	Yield
Condensing of AsF5 onto a mixt. of Se, I2 and AsF3, an immediate reat. takes place.; Storing at room temp for 3 months, filtn.;	A 0% B 10%

...Expand

: [(η(5)-C5H4Me)Fe(CO)2]2

: 7784-35-2
arsenic(III) fluoride

: [((CH3C5H4)Fe(CO)2)2AsF2](1+)*[AsF4](1-)=[((CH3C5H4)Fe(CO)2)2AsF2][AsF4]

Conditions

Conditions	Yield
In neat (no solvent) (N2); complex in AsF3 stirred for 3 h at 50°C; evapd. (vac.), recrystd. (acetone);	10%

: [(η(5)-C5H4Me)Fe(CO)2]2

: 143-66-8
sodium tetraphenyl borate

: 7784-35-2
arsenic(III) fluoride

: [((CH3C5H4)Fe(CO)2)2As(OC2H5)2](1+)*[B(C6H5)4](1-)=[((CH3C5H4)Fe(CO)2)2As(OC2H5)2][B(C6H5)4]

Conditions

Conditions	Yield
With C2H5OH In neat (no solvent) (N2); (a) complex in AsF3 stirred for 3 h at 50°C, (b) evapd., dissolved in EtOH, NaB(C6H5)4/EtOH added; cooled, kept for 1 wk at -20°C; elem. anal.;	3%

...Expand

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