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inquiryHubei Vanz Pharm Co. Ltd. is located in Wuhan, Hubei province. We are one of the most professional company in pharm/chmecial industry for more than 10 years. We export to many countries and area with very competitive price, high quality, good ser
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inquiryHigh quality Methyl 2-bromomethyl-3-nitrobenzoate Cas 98475-07-1 with low price Company profile Wuhan Fortuna Chemical Co.,Ltd established in 2006, is a big integrative chemical enterprise being engaged in Pharmaceutical & its intermediates,
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inquiryName:Methyl 2-bromomethyl-3-nitrobenzoate CAS NO: 98475-07-1 Grade:Medical scientific research and export Molecular formula: C9H8BrNO4 Molecular weight:274.07 Product Quality 12 years of chemical raw materials Mature operation of the i
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inquiryProduct Description Product name Methyl 2-bromomethyl-3-nitrobenzoate CAS 98475-07-1 Assay 99% Appearance
Cas:98475-07-1
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inquiryOur Advantage Rich Experience Our products are sold all over Europe,North&South America, Sino-East, Asia and pacific area as well as Africa,we establish long term. Quality service Company cooperates with research institutes. We strictly con
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inquiryAppearance:White to Light yellow powder Storage:under inert gas (nitrogen or Argon) at 2-8°C Package:25kg/drum Application:chemicals Transportation:Express/Sea/Air Port:Shanghai
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inquiryHangzhou Huarong Pharm Co., Ltd. established since 2009 , has been always focusing on supplying products and services to our clients in the field of small molecule drug. Huarong Pharm has built platforms for the research, development and manufac
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inquiryAdvantage : LIDE PHARMACEUTICALS LTD. is a mid-small manufacturing-type enterprise, engaged in pharmaceutical intermediates of R&D, custom-made and production, and also involving trading chemicals for export. We have established the
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inquiryProduct Name: Methyl 2-bromomethyl-3-nitrobenzoate CAS: 98475-07-1 MF: C9H8BrNO4 MW: 274.07 EINECS: 619-354-8 Mol File: 98475-07-1.mol Methyl 2-bromomethyl-3-nitrobenzoate Structure Methyl 2-bromomethyl-3-nitrobenzoate Chemical Pr
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inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At prese
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inquiryMethyl 2-bromomethyl-3-nitrobenzoate CAS:98475-07-1 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high qual
Cas:98475-07-1
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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Cas:98475-07-1
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inquiryMethyl 2-bromomethyl-3-nitrobenzoate CAS: 98475-07-1 Specification Item Specification Appearance White Crystals Assay 99%min Density 1.624±0.06 g/cm3(Predicted) Boiling point 72-
Cas:98475-07-1
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inquiry1. Timely and efficient service to ensure communication with customers 2. Produce products of different specifications and sizes according to your requirements. 3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures s
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inquiryProduct Detail Minimum Order Qty. 10 Gram
Cas:98475-07-1
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inquiry2-methyl-3-nitro-benzoic acid methyl ester
2-bromomethyl-3-nitro-benzoic acid methyl ester
Conditions | Yield |
---|---|
With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) In tetrachloromethane Reflux; | 100% |
With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) In dichloromethane for 16h; Heating; | 98% |
With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) In acetic acid methyl ester at 57℃; for 18h; | 98% |
methyl 2-methyl-4-nitrobenzoate
2-bromomethyl-3-nitro-benzoic acid methyl ester
Conditions | Yield |
---|---|
With azobisisobutyronitrile In tetrachloromethane; hexane; dichloromethane | 98% |
diethyl ether
2-methyl-3-nitro-benzoic acid methyl ester
2-bromomethyl-3-nitro-benzoic acid methyl ester
Conditions | Yield |
---|---|
With N-Bromosuccinimide; dibenzoyl peroxide In tetrachloromethane | 88.3% |
2-bromomethyl-3-nitro-benzoic acid methyl ester
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: CH2Cl2 2: benzoyl peroxide; bromine / CCl4 / 46 h / Irradiation; heating View Scheme |
2-methyl-3-nitro-benzoic acid methyl ester
dibenzoyl peroxide
2-bromomethyl-3-nitro-benzoic acid methyl ester
Conditions | Yield |
---|---|
In tetrachloromethane; ethyl acetate |
n-Butyl chloride
2-methyl-3-nitro-benzoic acid methyl ester
2-bromomethyl-3-nitro-benzoic acid methyl ester
Conditions | Yield |
---|---|
With N-Bromosuccinimide; dibenzoyl peroxide In tetrachloromethane; cyclohexane |
2-methyl-3-nitrobenzic acid
2-bromomethyl-3-nitro-benzoic acid methyl ester
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: thionyl chloride / 5 h / Reflux 2: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / Reflux View Scheme | |
Multi-step reaction with 2 steps 1.1: thionyl chloride / dichloromethane / Reflux 1.2: Reflux 2.1: bromine / tetrachloromethane / 20 °C View Scheme | |
Multi-step reaction with 2 steps 1: bis(trichloromethyl) carbonate / N,N-dimethyl-formamide / 6 h / Reflux 2: N-Bromosuccinimide; dibenzoyl peroxide / 8 h / Reflux View Scheme | |
Multi-step reaction with 2 steps 1: sulfuric acid / 24 h / Inert atmosphere; Reflux 2: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / benzene / 24 h / Inert atmosphere; Reflux View Scheme |
methylamine
2-bromomethyl-3-nitro-benzoic acid methyl ester
2-methyl-4-nitroisoindolin-1-one
Conditions | Yield |
---|---|
In tetrahydrofuran; water at 20℃; for 18h; Inert atmosphere; | 100% |
In tetrahydrofuran; water at 20 - 60℃; for 8h; | 91.9% |
In methanol at 20℃; for 3h; | 50% |
rac-α-aminoglutarimide hydrochloride
2-bromomethyl-3-nitro-benzoic acid methyl ester
3-(4-nitro-1-oxoisoindolin-2-yl)piperidine-2,6-dione
Conditions | Yield |
---|---|
Stage #1: rac-α-aminoglutarimide hydrochloride With triethylamine In dimethyl sulfoxide for 0.166667h; Inert atmosphere; Stage #2: 2-bromomethyl-3-nitro-benzoic acid methyl ester In dimethyl sulfoxide at 50 - 55℃; for 12.3333h; Inert atmosphere; | 99.73% |
With sodium carbonate at 100℃; for 0.75h; Reagent/catalyst; Temperature; Inert atmosphere; | 98.5% |
With sodium carbonate In acetonitrile at 70℃; for 8h; Solvent; Reagent/catalyst; Temperature; | 98.8% |
triphenylphosphine
2-bromomethyl-3-nitro-benzoic acid methyl ester
Conditions | Yield |
---|---|
In chloroform for 1h; Heating; | 99% |
In chloroform for 1.5h; Reflux; |
4-methoxy-benzylamine
2-bromomethyl-3-nitro-benzoic acid methyl ester
Conditions | Yield |
---|---|
In tetrahydrofuran at 50℃; for 24h; Inert atmosphere; | 99% |
propylamine
2-bromomethyl-3-nitro-benzoic acid methyl ester
Conditions | Yield |
---|---|
With potassium carbonate In acetonitrile at 20℃; for 5h; Inert atmosphere; | 97% |
2-bromomethyl-3-nitro-benzoic acid methyl ester
4-nitro-2,3-dihydro-1H-isoindol-1-one
Conditions | Yield |
---|---|
With ammonium hydroxide at 90℃; for 2h; | 96.04% |
With ammonia In methanol at 20℃; for 2.5h; | 90% |
With ammonia In methanol at 20℃; for 2h; | 81% |
aniline
2-bromomethyl-3-nitro-benzoic acid methyl ester
Conditions | Yield |
---|---|
at 40℃; for 0.0833333h; | 96.03% |
2-bromomethyl-3-nitro-benzoic acid methyl ester
(+/-)-α-aminoglutarimide
3-(4-nitro-1-oxoisoindolin-2-yl)piperidine-2,6-dione
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide for 3h; Reflux; | 96% |
Stage #1: 2-bromomethyl-3-nitro-benzoic acid methyl ester; (+/-)-α-aminoglutarimide With sodium carbonate In acetonitrile at 5℃; Inert atmosphere; Reflux; Large scale; Stage #2: With hydrogenchloride In water at 20 - 62℃; for 4h; pH=< 6; Large scale; | 79.5% |
With triethylamine In N,N-dimethyl-formamide at 25 - 100℃; for 7h; Inert atmosphere; | |
With potassium hydrogencarbonate In acetonitrile Reflux; | |
With triethylamine In N,N-dimethyl-formamide at 75℃; for 20h; |
benzylamine
2-bromomethyl-3-nitro-benzoic acid methyl ester
2-benzyl-4-nitro-2,3-dihydroisoindol-1-one
Conditions | Yield |
---|---|
With potassium carbonate In acetonitrile at 20℃; for 5h; Inert atmosphere; | 95% |
1,3-dihydro-1-(1-methylethenyl)-2H-benzimidazol-2-one
2-bromomethyl-3-nitro-benzoic acid methyl ester
2-(3-isopropenyl-2-oxo-2,3-dihydro-benzoimidazol-1-ylmethyl)-3-nitro-benzoic acid methyl ester
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 20 - 80℃; for 2h; | 94% |
p-toluidine
2-bromomethyl-3-nitro-benzoic acid methyl ester
2-(p-tolyl)-4-nitro-2,3-dihydroisoindol-1-one
Conditions | Yield |
---|---|
With potassium carbonate In acetonitrile at 20℃; for 5h; Inert atmosphere; | 94% |
2-bromomethyl-3-nitro-benzoic acid methyl ester
Conditions | Yield |
---|---|
With thiourea In methanol; ethyl acetate | 93% |
With thiourea In methanol |
2-bromomethyl-3-nitro-benzoic acid methyl ester
Conditions | Yield |
---|---|
With triethylamine In N,N-dimethyl-formamide at 75℃; for 20h; Inert atmosphere; | 93% |
2-bromomethyl-3-nitro-benzoic acid methyl ester
Conditions | Yield |
---|---|
With triethylamine In N,N-dimethyl-formamide at 75℃; for 20h; Inert atmosphere; | 93% |
2-bromomethyl-3-nitro-benzoic acid methyl ester
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 22℃; for 17h; | 93% |
4-chloro-aniline
2-bromomethyl-3-nitro-benzoic acid methyl ester
2-(4-chlorophenyl)-4-nitro-2,3-dihydroisoindol-1-one
Conditions | Yield |
---|---|
With potassium carbonate In acetonitrile at 20℃; for 5h; Inert atmosphere; | 90% |
2-bromomethyl-3-nitro-benzoic acid methyl ester
2-(azidomethyl)-3-nitrobenzoic acid methyl ester
Conditions | Yield |
---|---|
With sodium azide In DMF (N,N-dimethyl-formamide); water | 89.6% |
With sodium azide In DMF (N,N-dimethyl-formamide); water | 89.6% |
2-bromomethyl-3-nitro-benzoic acid methyl ester
2-aminocaprolactam
Conditions | Yield |
---|---|
With triethylamine In N,N-dimethyl-formamide at 50℃; for 18h; | 89% |
2-methoxyethylamine
2-bromomethyl-3-nitro-benzoic acid methyl ester
2-(2-methoxyethyl)-4-nitro-2,3-dihydro-isoindol-1-one
Conditions | Yield |
---|---|
In toluene for 1h; Product distribution / selectivity; Reflux; | 88% |
3-iodobenzylamine
2-bromomethyl-3-nitro-benzoic acid methyl ester
2-(3-iodobenzyl)-4-nitroisoindolin-1-one
Conditions | Yield |
---|---|
With triethylamine In metahnol at 20℃; Reflux; | 87% |
glutamic acid dimethyl ether
2-bromomethyl-3-nitro-benzoic acid methyl ester
2-(4-nitro-1-oxo-1,3-dihydroisoindol-2-yl)glutaric acid dimethyl ester
Conditions | Yield |
---|---|
With sodium carbonate In N,N-dimethyl-formamide at 45℃; for 16h; Reagent/catalyst; Solvent; | 86.3% |
With sodium hydrogencarbonate In acetonitrile Heating / reflux; | 78% |
(R)-2-aminopropan-1-ol
2-bromomethyl-3-nitro-benzoic acid methyl ester
2-((R)-2-hydroxy-1-methyl-ethyl)-4-nitro-2,3-dihydroisoindol-1-one
Conditions | Yield |
---|---|
In toluene at 20 - 50℃; for 24h; Product distribution / selectivity; | 86% |
p-methoxybenzylmercaptan
2-bromomethyl-3-nitro-benzoic acid methyl ester
Conditions | Yield |
---|---|
Stage #1: p-methoxybenzylmercaptan With triethylamine In dichloromethane at 20℃; for 0.5h; Stage #2: 2-bromomethyl-3-nitro-benzoic acid methyl ester In dichloromethane at 20℃; | 86% |
2-bromomethyl-3-nitro-benzoic acid methyl ester
Conditions | Yield |
---|---|
With triethylamine In acetonitrile at 75℃; Inert atmosphere; | 83% |
2-bromomethyl-3-nitro-benzoic acid methyl ester
3-(4-nitro-1-oxoisoindolin-2-yl)(piperidine-3,5,5-d3)-2,6-dione
Conditions | Yield |
---|---|
With sodium carbonate In N,N-dimethyl acetamide at 20℃; for 18h; | 81% |
Conditions | Yield |
---|---|
With triethylamine In acetonitrile at 75℃; Inert atmosphere; | 81% |
2-amino-3-tert-butoxypropionic acid
2-bromomethyl-3-nitro-benzoic acid methyl ester
3-(4-nitro-1-oxoisoindolin-2-yl)piperidine-2,6-dione
Conditions | Yield |
---|---|
Stage #1: 2-amino-3-tert-butoxypropionic acid; 2-bromomethyl-3-nitro-benzoic acid methyl ester With sodium hydrogencarbonate In acetonitrile at 5 - 20℃; Reflux; Stage #2: With hydrogenchloride In water at 58 - 62℃; for 4.16667h; pH=< 6; Temperature; Time; | 79.5% |
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