DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe
Cas:24666-56-6
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inquiryItems Standard Result Appearance White to off-white powder Complies Water 1.0% max
Cas:24666-56-6
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inquiryProduct description: Product name 3-Amino-2,6-piperidinedione hydrochloride CAS number 24666-56-6 Assay ≥99% Appearance White crystalline powder Capacity 20mt/year Application
Cas:24666-56-6
Min.Order:100 Gram
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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inquiry1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
Cas:24666-56-6
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inquiryhebei yanxi chemical co., LTD who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do research and developm
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Min.Order:5 Kiloliter
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inquiryOur company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O
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inquiryWith our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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Type:Trading Company
inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by email in time prod
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Min.Order:1 Kilogram
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Min.Order:10 Gram
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inquiryProduct:Pemetrexed Intermediate Chemical name:2,6-Piperidinedione,3-amino-, monohydrochloride Batch NO: 20210326 Analysis Date: 2021-03-26 Expiry Date: 2023-03-25 HANGZHOU THINK CHEMICAL CO., LTD. (THINKCHEM) is an integrative corpora
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Type:Other
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Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiry2,6-Dioxopiperidine-3-ammonium chloride CAS:24666-56-6 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high q
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Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Product Name: 2,6-Dioxopiperidine-3-ammonium chloride Synonyms: 3-amino piperdine-2,6-dion hydrochloride;3-Amino-2,6-piperidinedione hydrochloride;2,6-Piperidinedione, 3-amino-, hydrochloride;Glutamic acid imide hydrochloride;3-Amino-2,6-dioxo-pi
Cas:24666-56-6
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiry3-Amino-2,6-piperidinedione hydrochloride CAS: 24666-56-6 Specification Product name 3-Amino-2,6-piperidinedione hydrochloride CAS number 24666-56-6 Assay ≥99% Appearance White crystalline powder
Cas:24666-56-6
Min.Order:1 Kilogram
Negotiable
Type:Other
inquiryProduct Detail Minimum Order Qty. 10 Gram
Cas:24666-56-6
Min.Order:10 Gram
Negotiable
Type:Trading Company
inquiryLorcaserin(856681-05-5)is an orally administered agent and a selective 5-HT2C receptor agonist for the treatment of obesity. It had been approved for marketing in US by FDA on 27 June in 2012. In clinical studies, lorcaserin h
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Min.Order:100 Gram
Negotiable
Type:Lab/Research institutions
inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
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inquiryA substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
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Min.Order:100 Kilogram
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Min.Order:1 Gram
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Type:Lab/Research institutions
inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
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inquiryWe are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov
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Type:Lab/Research institutions
inquiry3-(benzyloxycarbonyl)-amino-2,6-dioxopiperidine
rac-α-aminoglutarimide hydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride; hydrogen; 5% palladium over charcoal In methanol; water under 3102.97 Torr; for 4h; | 100% |
With hydrogenchloride In dimethyl sulfoxide | 92% |
Stage #1: 3-(benzyloxycarbonyl)-amino-2,6-dioxopiperidine With palladium 10% on activated carbon; hydrogen In methanol; water at 25 - 30℃; under 2250.23 - 2625.26 Torr; Stage #2: With hydrogenchloride In methanol; water at 25 - 30℃; | 90% |
With hydrogenchloride; palladium 10% on activated carbon; hydrogen In methanol at 25℃; for 5h; | 90.5% |
With hydrogenchloride; hydrogen; palladium on activated charcoal In ethyl acetate under 2585.74 - 3102.89 Torr; |
(RS)-(2,6-dioxopiperidin-3-yl)carbamic acid tert-butyl ester
rac-α-aminoglutarimide hydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride In methanol; water for 2h; | 99% |
rac-α-aminoglutarimide hydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride; hydrogen; palladium 10% on activated carbon In methanol under 760.051 Torr; for 23h; | 96% |
Glutamic acid
rac-α-aminoglutarimide hydrochloride
Conditions | Yield |
---|---|
Stage #1: Glutamic acid With ammonium hydroxide In water at 15℃; for 0.5h; Stage #2: In water at 60℃; for 2h; Stage #3: With hydrogenchloride In ethanol at 30℃; Temperature; | 82.6% |
rac-α-aminoglutarimide hydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride; palladium Hydration; |
Cbz-L-Gln
rac-α-aminoglutarimide hydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: CDI / tetrahydrofuran / Heating 2: H2, aq. HCl / 10 percent Pd/C / ethyl acetate / 2585.74 - 3102.89 Torr View Scheme | |
Multi-step reaction with 2 steps 1: dmap; 1,1'-carbonyldiimidazole / 1,4-dioxane / 15 h / 100 °C 2: palladium 10% on activated carbon; hydrogen; hydrogenchloride / methanol / 5 h / 25 °C View Scheme |
N-benzyloxycarbonyl-L-isoglutamine
rac-α-aminoglutarimide hydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: dmap; 1,1'-carbonyldiimidazole / tetrahydrofuran / 20 h / Reflux 2: hydrogenchloride; hydrogen / palladium 10% on activated carbon / methanol / 23 h / 760.05 Torr View Scheme |
L-glutamic acid
rac-α-aminoglutarimide hydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: water / 2 h / 0 °C 2: urea / dimethyl sulfoxide / 2 h / 150 °C 3: hydrogenchloride / dimethyl sulfoxide View Scheme |
N-benzyloxycarbonyl-L-glutamic acid
rac-α-aminoglutarimide hydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: urea / dimethyl sulfoxide / 2 h / 150 °C 2: hydrogenchloride / dimethyl sulfoxide View Scheme |
Nα-benzyloxycarbonyl-glutamine
rac-α-aminoglutarimide hydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: dmap; 1,1'-carbonyldiimidazole / 1,4-dioxane / 17.17 h / 20 °C / Heating / reflux 2: hydrogenchloride; hydrogen / 5% palladium over charcoal / methanol; water / 4 h / 3102.97 Torr View Scheme |
rac-α-aminoglutarimide hydrochloride
2-bromomethyl-3-nitro-benzoic acid methyl ester
3-(4-nitro-1-oxoisoindolin-2-yl)piperidine-2,6-dione
Conditions | Yield |
---|---|
Stage #1: rac-α-aminoglutarimide hydrochloride With triethylamine In dimethyl sulfoxide for 0.166667h; Inert atmosphere; Stage #2: 2-bromomethyl-3-nitro-benzoic acid methyl ester In dimethyl sulfoxide at 50 - 55℃; for 12.3333h; Inert atmosphere; | 99.73% |
With sodium carbonate at 100℃; for 0.75h; Reagent/catalyst; Temperature; Inert atmosphere; | 98.5% |
With sodium carbonate In acetonitrile at 70℃; for 8h; Solvent; Reagent/catalyst; Temperature; | 98.8% |
3-bromophthalic anhydride
rac-α-aminoglutarimide hydrochloride
Conditions | Yield |
---|---|
With potassium acetate; acetic acid at 90℃; for 16h; | 99% |
With potassium acetate; acetic acid at 90℃; for 16h; Inert atmosphere; | 99% |
With sodium acetate; acetic acid for 3h; Reflux; | 94.1% |
rac-α-aminoglutarimide hydrochloride
Conditions | Yield |
---|---|
Stage #1: 4-[4,4-difluoro-5-[4-[3-[[5-(5-methylpyrido[4,3-b]indol-7-yl)-2-pyridyl]oxy]cyclobutoxy]-1-piperidyl]pentoxy]phthalic acid With sodium acetate; acetic acid at 25℃; for 1h; Stage #2: rac-α-aminoglutarimide hydrochloride at 120℃; for 11h; | 98% |
3-acetylaminophthalic acid
rac-α-aminoglutarimide hydrochloride
N-(2-(2,6-dioxopiperidin-3-yl)-1,3-dioxoisoindolin-4-yl)acetamide
Conditions | Yield |
---|---|
With potassium acetate In 1,4-dioxane at 100℃; for 24h; Reagent/catalyst; Solvent; Temperature; | 97.5% |
3-hydroxyphthalic anhydride
rac-α-aminoglutarimide hydrochloride
4-Hydroxythalidomide
Conditions | Yield |
---|---|
With potassium acetate In acetic acid for 24h; Reflux; | 96% |
With sodium acetate; acetic acid at 100℃; for 2h; | 96% |
With pyridine at 110℃; | 93% |
4-fluorophthalic anhydride
rac-α-aminoglutarimide hydrochloride
2-(2,6-dioxopiperidin-3-yl)-5-fluoro-2,3-dihydro-1H-isoindole-1,3-dione
Conditions | Yield |
---|---|
With sodium acetate; acetic acid at 120℃; for 12h; | 96% |
With sodium acetate; acetic acid at 135℃; | 92% |
With sodium acetate In acetic acid for 12h; Reflux; | 90% |
rac-α-aminoglutarimide hydrochloride
Conditions | Yield |
---|---|
Stage #1: benzyl (4-(2-((1,3-dioxo-1,3-dihydroisobenzofuran-4-yl)oxy)acetamido)butyl)carbamate; rac-α-aminoglutarimide hydrochloride With triethylamine In tetrahydrofuran for 3h; Reflux; Inert atmosphere; Stage #2: With 1,1'-carbonyldiimidazole In tetrahydrofuran Reflux; Inert atmosphere; | 96% |
Conditions | Yield |
---|---|
With acetic acid; triethylamine for 3h; Temperature; Reagent/catalyst; Concentration; Reflux; | 95% |
3-acetylaminophthalic anhydride
rac-α-aminoglutarimide hydrochloride
N-(2-(2,6-dioxopiperidin-3-yl)-1,3-dioxoisoindolin-4-yl)acetamide
Conditions | Yield |
---|---|
With sodium acetate; acetic acid at 105℃; for 24h; Reagent/catalyst; Temperature; | 95% |
3-hydroxy-1,8-naphthalic acid anhydride
rac-α-aminoglutarimide hydrochloride
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran for 120h; Reflux; | 95% |
With triethylamine In tetrahydrofuran for 120h; Reflux; | 3.44 g |
rac-α-aminoglutarimide hydrochloride
3-aminophthalic acid hydrochloride
pomalidomide
Conditions | Yield |
---|---|
Stage #1: rac-α-aminoglutarimide hydrochloride; 3-aminophthalic acid hydrochloride In acetonitrile for 0.25h; Stage #2: With triethylamine In water; acetonitrile at 15 - 87℃; for 49.0833 - 50.8333h; Product distribution / selectivity; | 94% |
Stage #1: rac-α-aminoglutarimide hydrochloride; 3-aminophthalic acid hydrochloride In acetonitrile for 0.25h; Stage #2: With 1H-imidazole In water; acetonitrile at 15 - 87℃; for 7.08333 - 10.8333h; Product distribution / selectivity; | 92% |
Stage #1: rac-α-aminoglutarimide hydrochloride; 3-aminophthalic acid hydrochloride With acetic acid In acetonitrile for 0.25h; Stage #2: With 1H-imidazole In water; acetonitrile at 15 - 87℃; for 7.08333 - 10.8333h; Product distribution / selectivity; | 85% |
Stage #1: rac-α-aminoglutarimide hydrochloride; 3-aminophthalic acid hydrochloride With acetic acid In acetonitrile for 0.25h; Stage #2: With triethylamine In water; acetonitrile at 15 - 87℃; for 7.08333 - 10.8333h; Product distribution / selectivity; | 84% |
With acetic acid; triethylamine In acetone at 80 - 85℃; for 6h; | 68.5% |
4,5-difluorophthalic anhydride
rac-α-aminoglutarimide hydrochloride
Conditions | Yield |
---|---|
With potassium acetate; acetic acid at 90℃; | 94% |
With potassium acetate; acetic acid at 110℃; | |
With triethylamine In toluene at 100℃; for 4h; |
rac-α-aminoglutarimide hydrochloride
3-(4-nitro-1-oxoisoindolin-2-yl)piperidine-2,6-dione
Conditions | Yield |
---|---|
With triethylamine In acetonitrile at 80℃; for 10h; | 93.2% |
4-bromophthalic anhydride
rac-α-aminoglutarimide hydrochloride
5-bromo-2-(2,6-dioxopiperidin-3-yl)-2,3-dihydro-1H-isoindole-1,3-dione
Conditions | Yield |
---|---|
With sodium acetate; acetic acid Heating / reflux; | 93% |
With sodium acetate In acetic acid at 20 - 80℃; for 16h; | 92% |
With sodium acetate; acetic acid at 115℃; for 16h; | 91.6% |
With potassium acetate; acetic acid at 90℃; for 12h; | 60% |
With sodium acetate; acetic acid at 120℃; for 5h; |
C20H15NO5
rac-α-aminoglutarimide hydrochloride
4-(2-phenoxyphenylamino)-2-(2,6-dioxopiperidin-3-yl)isoindole-1,3-dione
Conditions | Yield |
---|---|
With pyridine for 16h; Heating / reflux; | 93% |
3-(4-tert-butylphenylamino)phthalic acid
rac-α-aminoglutarimide hydrochloride
4-(4-tert-butylphenylamino)-2-(2,6-dioxopiperidin-3-yl)isoindole-1,3-dione
Conditions | Yield |
---|---|
With pyridine for 16h; Heating / reflux; | 92% |
3-(naphthalen-2-ylamino)phthalic acid
rac-α-aminoglutarimide hydrochloride
2-(2,6-Dioxopiperidin-3-yl)-4-(naphthalen-2-ylamino)isoindole-1,3-dione
Conditions | Yield |
---|---|
With pyridine for 16h; Heating / reflux; | 92% |
3-(2-methoxyphenylamino)phthalic acid
rac-α-aminoglutarimide hydrochloride
4-(2-Methoxyphenylamino)-2-(2,6-dioxopiperidin-3-yl)isoindole-1,3-dione
Conditions | Yield |
---|---|
With pyridine for 16h; Heating / reflux; | 92% |
3-fluorophthalic anhydride
rac-α-aminoglutarimide hydrochloride
Conditions | Yield |
---|---|
With sodium acetate; acetic acid at 135℃; | 92% |
With sodium acetate; acetic acid for 12h; Reflux; | 90% |
With sodium acetate In acetic acid for 12h; Reflux; | 90% |
Indole-2-carboxylic acid
rac-α-aminoglutarimide hydrochloride
Conditions | Yield |
---|---|
Stage #1: Indole-2-carboxylic acid With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate In N,N-dimethyl-formamide at 20℃; for 1h; Inert atmosphere; Stage #2: rac-α-aminoglutarimide hydrochloride In N,N-dimethyl-formamide at 20℃; Inert atmosphere; | 92% |
rac-α-aminoglutarimide hydrochloride
Conditions | Yield |
---|---|
With 1,1'-carbonyldiimidazole In acetonitrile for 16h; | 91.7% |
With 1,1'-carbonyldiimidazole In acetonitrile at 80℃; for 16h; Inert atmosphere; | 27% |
3-nitrophthalic acid anhydride
rac-α-aminoglutarimide hydrochloride
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran at 20℃; for 0.5h; Reagent/catalyst; Green chemistry; | 91% |
With triethylamine In tetrahydrofuran at 20℃; for 0.5h; | 91% |
With triethylamine In tetrahydrofuran at 20℃; for 0.5h; | 91% |
Conditions | Yield |
---|---|
With sodium acetate; acetic acid at 105 - 115℃; Large scale; | 90% |
With sodium acetate; acetic acid In water at 116 - 118℃; for 16h; | 86.2% |
With 1,1'-carbonyldiimidazole In acetonitrile at 20 - 80℃; Inert atmosphere; | 28.2 g |
rac-α-aminoglutarimide hydrochloride
2-Nitrobenzenesulfonyl chloride
Conditions | Yield |
---|---|
Stage #1: rac-α-aminoglutarimide hydrochloride With N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃; for 0.5h; Stage #2: 2-Nitrobenzenesulfonyl chloride In N,N-dimethyl-formamide at 0 - 20℃; | 90% |
2-Iodobenzoic acid
rac-α-aminoglutarimide hydrochloride
Conditions | Yield |
---|---|
Stage #1: 2-Iodobenzoic acid With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate In N,N-dimethyl-formamide for 0.166667h; Stage #2: rac-α-aminoglutarimide hydrochloride In N,N-dimethyl-formamide at 20℃; for 2h; | 90% |
Stage #1: 2-Iodobenzoic acid With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate In N,N-dimethyl-formamide at 20℃; for 1h; Inert atmosphere; Stage #2: rac-α-aminoglutarimide hydrochloride In N,N-dimethyl-formamide at 20℃; Inert atmosphere; | 73% |
3-nitrophthalic acid anhydride
rac-α-aminoglutarimide hydrochloride
4-NT
Conditions | Yield |
---|---|
With sodium acetate; acetic acid at 25 - 118℃; for 18h; | 89.7% |
With formic acid; ammonium formate at 80℃; for 0.166667h; Temperature; | 89% |
With sodium acetate; acetic acid In water at 116 - 118℃; for 17h; | 88.3% |
3-(4-isopropylphenylamino)phthalic acid
rac-α-aminoglutarimide hydrochloride
4-(4-isopropylphenylamino)-2-(2,6-dioxopiperidin-3-yl)isoindole-1,3-dione
Conditions | Yield |
---|---|
With pyridine for 16h; Heating / reflux; | 89% |
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