Product description: Product name 2,6-Dichloro-4-nitroaniline CAS number 99-30-9 Assay ≥99% Appearance Yellow powder Capacity 500mt/year Application Dye intermediates
Cas:99-30-9
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Cas:99-30-9
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Cas:99-30-9
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inquiryName: 2,6-Dichloro-4-nitroaniline Synonyms: dicloran CAS:99-30-9 MF: C6H4Cl2N2O2 Appearance: white powder Storage:Store in cool and dry place, away from sun light. Package: 25kgs/drum Application:Dye Intermediates Transportation:By sea or by air
Cas:99-30-9
Min.Order:1 Kilogram
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inquiryAppearance:yellow powder Storage:room temperature Package:25kg/drum Application:Dichloran is a component for pesticide formulations. Transportation:Express/Sea/Air Port:Shanghai
Cas:99-30-9
Min.Order:1 Kilogram
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Min.Order:1 Gram
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Min.Order:1 Kilogram
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Min.Order:1 Gram
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Cas:99-30-9
Min.Order:10 Gram
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inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
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Min.Order:1 Gram
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inquiryProduct name: 2,6-Dichloro-4-Nitroaniline CAS No.:99-30-9 Molecule Formula:C6H4Cl2N2O2 Molecule Weight:207.01 Purity: 94.0% Package: 25kg/drum Description:Yellow powder Manufacture Standards:Enterprise Standard TES
Cas:99-30-9
Min.Order:1 Kilogram
Negotiable
Type:Trading Company
inquiryProduct Name: 2,6-Dichloro-4-nitroaniline Synonyms: Resisan;Resissan;u-2069;DICLORAN, 1GM, NEAT;DICHLORAN PESTANAL (2,6-DICHLORO- 4-NITR;2,6-Dichloro-4-nitroaniline, tech., 97%;2,6-Dichloro-4-nitro-1-aminobenzene;dichloran (canada) CAS: 99-3
Cas:99-30-9
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
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Min.Order:1 Kilogram
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Min.Order:0 Metric Ton
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Cas:99-30-9
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inquiryhigh purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
Conditions | Yield |
---|---|
With hydrogenchloride; dihydrogen peroxide In water at -8 - 20℃; for 2h; Temperature; Reagent/catalyst; | 99.5% |
With N-chloro-N-(benzenesulfonyl)benzenesulfonamide In acetonitrile at 20 - 25℃; for 0.133333h; Green chemistry; | 99% |
Stage #1: 4-nitro-aniline With hydrogenchloride In water at 63℃; for 0.5h; Stage #2: With chlorine In water for 0.166667h; Temperature; Time; | 98.65% |
Conditions | Yield |
---|---|
With 1,9-diperoxynonanedioic acid In acetonitrile at 50℃; for 0.5h; | 92% |
2,6-dichloro-4-aminonitrobenzene
4-nitro-2,6-dichloroaniline
Conditions | Yield |
---|---|
With nickel(II) tetrafluoroborate hexahydrate; ammonia; hydrogen; bis(2-diphenylphosphinoethyl)phenylphosphine In 2,2,2-trifluoroethanol at 120℃; under 37503.8 Torr; for 24h; chemoselective reaction; | 90% |
Conditions | Yield |
---|---|
With N-chloro-N-(benzenesulfonyl)benzenesulfonamide In 1,4-dioxane at 20 - 25℃; Solvent; Green chemistry; | A n/a B 50% |
With hydrogenchloride; sodium chlorate In water; acetic acid at 20℃; for 40h; | A 9% B 32% |
Chlorierung; | |
With methanol; chlorine |
4-amino-3,5-dichloro-benzenesulfonamide
4-nitro-2,6-dichloroaniline
Conditions | Yield |
---|---|
With ammonium nitrate; sulfuric acid at 0 - 5℃; for 0.25h; | 21% |
4-nitro-aniline
A
4-nitro-2,6-dichloroaniline
B
2-Chloro-4-nitroaniline
C
bis(4-nitrophenyl)diazene
Conditions | Yield |
---|---|
With sodium hydroxide; sodium hypochlorite In ethanol at 25℃; for 0.0833333h; | A n/a B 15% C 9% |
Conditions | Yield |
---|---|
With nitric acid; acetic acid |
1,3-dichloro-2,5-dinitro-benzene
4-nitro-2,6-dichloroaniline
Conditions | Yield |
---|---|
With ethanol; ammonia in der Kaelte; |
N,N-dichloro-4-nitro-aniline
4-nitro-2,6-dichloroaniline
Conditions | Yield |
---|---|
With hydrogenchloride; diethyl ether | |
With diethyl ether | |
With acetic anhydride |
N,N-dichloro-4-nitro-aniline
acetic anhydride
4-nitro-2,6-dichloroaniline
Conditions | Yield |
---|---|
With benzene | |
With acetic acid | |
With tert-butyl alcohol |
acetic acid-(2,4,N-trichloro-anilide)
2-Chloro-4-nitroaniline
4-nitro-2,6-dichloroaniline
Conditions | Yield |
---|---|
With chloroform |
Conditions | Yield |
---|---|
With hydrogenchloride; chlorine | |
With hydrogenchloride; dihydrogen peroxide In water at 30 - 40℃; Green chemistry; |
2,6-dichloro-N-nitroaniline
4-nitro-2,6-dichloroaniline
Conditions | Yield |
---|---|
With trifluoroacetic acid-d1 In chloroform-d1 at 30℃; Rate constant; Mechanism; kinetic isotope effect; |
hydrogenchloride
chlorine
2-Chloro-4-nitroaniline
4-nitro-2,6-dichloroaniline
Conditions | Yield |
---|---|
bei 2.5-stdg. Behandeln; |
hydrogenchloride
4-nitro-aniline
A
4-nitro-2,6-dichloroaniline
B
2-Chloro-4-nitroaniline
hydrogenchloride
ethanol
dihydrogen peroxide
4-nitro-aniline
A
4-nitro-2,6-dichloroaniline
B
bis(4-nitrophenyl)diazene
4-bromo-2,6-dichloro-N-nitro-aniline
sulfuric acid
acetic acid
4-nitro-2,6-dichloroaniline
hydrogenchloride
diethyl ether
N,N-dichloro-4-nitro-aniline
4-nitro-2,6-dichloroaniline
Conditions | Yield |
---|---|
at -20℃; |
N,N-dichloro-4-nitro-aniline
A
4-nitro-2,6-dichloroaniline
B
bis(4-nitrophenyl)diazene
2,4,6-trichloro-N-nitroaniline
A
4-nitro-2,6-dichloroaniline
B
2,4,6-trichloroaniline
Conditions | Yield |
---|---|
With silica gel at 140℃; for 2h; Product distribution; Further Variations:; Reagents; | A n/a B 20 % Chromat. |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: chloroform 2: glacial acetic acid; nitric acid View Scheme |
Conditions | Yield |
---|---|
With sulfuric acid; nitric acid Heating; |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: sulfuric acid; nitric acid / 0 - 5 °C / Green chemistry 2: ammonia / water / Autoclave; Heating; Green chemistry 3: hydrogenchloride; dihydrogen peroxide / water / 30 - 40 °C / Green chemistry View Scheme |
4-nitro-2,6-dichloroaniline
3,4,5-trichloronitrobenzen
Conditions | Yield |
---|---|
Stage #1: 4-nitro-2,6-dichloroaniline With sulfuric acid; sodium nitrite at 50 - 70℃; for 1h; Stage #2: With acetic acid at 5℃; for 1h; Stage #3: With hydrogenchloride; copper(l) chloride In water at 15 - 70℃; for 2h; | 98.5% |
Stage #1: 4-nitro-2,6-dichloroaniline With sulfuric acid; sodium nitrite at 5 - 70℃; for 0.333333h; Stage #2: With acetic acid for 0.5h; Stage #3: With hydrogenchloride; copper(l) chloride In water at 25 - 70℃; for 1h; | 75% |
With copper(I) chloride; hydrogenchloride; sulfuric acid In acetic acid for 1h; | 47% |
With methyl nitrite; sulfuric acid; acetic acid Diazotization.Behandeln mit Kupfer(I)-chlorid in konz. Salzsaeure; | |
Stage #1: 4-nitro-2,6-dichloroaniline With sulfuric acid; sodium nitrite at 50℃; for 0.666667h; Sandmeyer Reaction; Stage #2: With acetic acid at 5℃; for 1h; Sandmeyer Reaction; Stage #3: With hydrogenchloride; copper(l) chloride at 15 - 70℃; for 1.83333h; Sandmeyer Reaction; |
4-nitro-2,6-dichloroaniline
1-bromo-2,6-dichloro-4-nitrobenzene
Conditions | Yield |
---|---|
With tert.-butylnitrite; copper(I) bromide In acetonitrile at 20℃; for 6h; Cooling with ice; | 97% |
With tert.-butylnitrite; copper(ll) bromide In acetonitrile at 20℃; for 10h; Cooling with ice; | 92% |
With hydrogen bromide; acetic acid; sodium nitrite |
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 20 - 60℃; | 94% |
4-nitro-2,6-dichloroaniline
nitratocarbonylbis(triphenylphosphine)rhodium
Conditions | Yield |
---|---|
With KOH In methanol; acetone to an acetone soln. of Rh complex were added equimolar quantity of nitroaniline (in acetone) and KOH in MeOH; solvents were evpd. in vac., red residue extd. with benzene and filtered from KNO3; solvent removed in vac., crystals pptd. with hexane, filtered, washed with hexane and dried in air; elem. anal.; | 92% |
4-nitro-2,6-dichloroaniline
4-azido-5-fluoro-pyridine-3-carbaldehyde
[1-(4-azido-5-fluoropyridin-3-yl)-meth-(E)-ylidene]-(2,6-dichloro-4-nitrophenyl)-amine
Conditions | Yield |
---|---|
With titanium tetrachloride; triethylamine In dichloromethane at 0 - 20℃; for 4h; Inert atmosphere; | 92% |
Conditions | Yield |
---|---|
Stage #1: 4-nitro-2,6-dichloroaniline With sulfuric acid; sodium nitrite In 1,2-dimethoxyethane; water at 0 - 5℃; for 1.25h; Stage #2: phenol With sodium carbonate In water at 0 - 70℃; for 7h; pH=9 - 10; | 84.5% |
4-nitro-2,6-dichloroaniline
Benzophenone-3
1-[2-hydroxy-4-methoxy-5-(2,6-dichloro-4-nitrophenylazo)phenyl]-1-phenylmethanone
Conditions | Yield |
---|---|
Stage #1: 4-nitro-2,6-dichloroaniline With hydrogenchloride; sodium nitrite In water at 0 - 5℃; Stage #2: Benzophenone-3 In water at 0 - 20℃; Alkaline conditions; | 84% |
4-nitro-2,6-dichloroaniline
Conditions | Yield |
---|---|
Stage #1: 4-nitro-2,6-dichloroaniline With hydrogenchloride In water at 40 - 60℃; for 2h; Stage #2: With sodium nitrite In water at 0℃; for 2h; Stage #3: N-cyclohexyl-2-(phenylamino)-2-(p-tolyl)acetamide With acetic acid In methanol; water at 0 - 20℃; for 24h; | 84% |
cis,trans-2,5-dimethoxytetrahydrofuran
4-nitro-2,6-dichloroaniline
N-(2,6-dichloro-4-nitrophenyl)pyrrole
Conditions | Yield |
---|---|
With acetic acid Heating; | 82% |
4-nitro-2,6-dichloroaniline
2-(2-bromophenyl)-N-cyclohexyl-2-(phenylamino)acetamide
Conditions | Yield |
---|---|
Stage #1: 4-nitro-2,6-dichloroaniline With hydrogenchloride In water at 40 - 60℃; for 2h; Stage #2: With sodium nitrite In water at 0℃; for 2h; Stage #3: 2-(2-bromophenyl)-N-cyclohexyl-2-(phenylamino)acetamide With acetic acid In methanol; water at 0 - 20℃; for 24h; | 81% |
4-nitro-2,6-dichloroaniline
m-acetylamino-N,N-diethylanilne
N,N-diethyl-4-(2,6-dichloro-4-nitrophenylazo)-3-acetylaminoaniline
Conditions | Yield |
---|---|
Stage #1: 4-nitro-2,6-dichloroaniline With tert.-butylnitrite; naphthalene-1,5-disulfonate In 1,2-dimethoxyethane at 25℃; for 0.5h; Stage #2: m-acetylamino-N,N-diethylanilne With sodium carbonate; naphthalene-1,5-disulfonate In water at 0℃; for 0.166667h; pH=4 - 6; | 78.77% |
Stage #1: 4-nitro-2,6-dichloroaniline With naphthalene-1,5-disulfonate In ethyl acetate at 50℃; for 0.166667h; Stage #2: With tert.-butylnitrite In ethyl acetate at 25℃; for 0.333333h; Stage #3: m-acetylamino-N,N-diethylanilne With hydrogenchloride In water at 0 - 5℃; for 0.316667h; |
formic acid
4-nitro-2,6-dichloroaniline
N-(2,6-dichloro-4-nitrophenyl)formamide
Conditions | Yield |
---|---|
Stage #1: formic acid With acetic anhydride at 70 - 80℃; for 1h; Stage #2: 4-nitro-2,6-dichloroaniline for 3h; Heating; | 78% |
Stage #1: formic acid With acetic anhydride at 55 - 60℃; for 0.333333h; Stage #2: 4-nitro-2,6-dichloroaniline at 55℃; for 6.33333h; | 65% |
4-nitro-2,6-dichloroaniline
2-(2'-anthraquinonylamino-3'-hydroxy)-4-anilino-6-chloro-s-triazine
C29H17Cl2N7O5
Conditions | Yield |
---|---|
In nitrobenzene at 60 - 65℃; for 5h; | 76% |
Conditions | Yield |
---|---|
Stage #1: 4-nitro-2,6-dichloroaniline With sulfuric acid; sodium nitrite In 1,2-dimethoxyethane; water at 0 - 5℃; for 1.25h; Stage #2: α-naphthol With sodium carbonate In water at 0 - 70℃; for 7h; pH=9 - 10; | 75.61% |
Conditions | Yield |
---|---|
With hydrogenchloride; tin(ll) chloride | 75% |
With ethanol; ammonium chloride; zinc | |
With ethanol; nickel Hydrogenation; |
4-nitro-2,6-dichloroaniline
10-undecenoic acid
Undec-10-enoic acid (2,6-dichloro-4-nitro-phenyl)-amide
Conditions | Yield |
---|---|
With triethylamine; trichlorophosphate In dichloromethane | 75% |
4-nitro-2,6-dichloroaniline
β-naphthol
1-(2,6-dichloro-4-nitro-phenylazo)-[2]naphthol
Conditions | Yield |
---|---|
Stage #1: 4-nitro-2,6-dichloroaniline With sulfuric acid; sodium nitrite In 1,2-dimethoxyethane; water at 0 - 5℃; for 1.25h; Stage #2: β-naphthol With sodium carbonate In water at 0 - 70℃; for 7h; pH=9 - 10; | 73.28% |
4-nitro-2,6-dichloroaniline
(1R,2R)-N,N-dimethylcyclohexane-1,2-diamine
1,1'-carbonyldiimidazole
C15H20Cl2N4O3
Conditions | Yield |
---|---|
Stage #1: 4-nitro-2,6-dichloroaniline With potassium hydride In tetrahydrofuran at 0℃; for 0.25h; Inert atmosphere; Stage #2: 1,1'-carbonyldiimidazole In tetrahydrofuran; 1,4-dioxane at 0 - 20℃; Inert atmosphere; Stage #3: (1R,2R)-N,N-dimethylcyclohexane-1,2-diamine In tetrahydrofuran; 1,4-dioxane at 20℃; for 20h; Inert atmosphere; | 73% |
4-nitro-2,6-dichloroaniline
ethyl 2-phenyldiazoacetate
Conditions | Yield |
---|---|
With C43H37Br2CuN3P2(1+)*ClO4(1-) In dichloromethane at 0 - 20℃; for 5h; Schlenk technique; Inert atmosphere; chemoselective reaction; | 71% |
Conditions | Yield |
---|---|
With indium; acetic acid In toluene for 12h; Inert atmosphere; Reflux; | 67% |
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