Diethylamine hydrochloride supplier

Name
Diethylamine hydrochloride
EINECS 211-541-9
CAS No. 660-68-4
Article Data96
CAS DataBase
Density 1.0 g/mL at 20 °C
Solubility soluble in water
Melting Point 227-230 °C(lit.)
Formula C₄H₁₁N^.HCl
Boiling Point 57.3 °C at 760 mmHg
Molecular Weight 109.599
Flash Point 320-330°C
Transport Information UN 1993 3/PG 3
Appearance white to off-white crystals or crystalline powder
Safety 26-39-7-24/25-36
Risk Codes 10-36/37/38
Molecular Structure
Hazard Symbols Xn,Xi
Synonyms Diethyl ammonium chloride;Di-Ethyl Amine Hydrochloride;Diethylammonium chloride;Ethanamine, N-ethyl-, hydrochloride;diethyl amine hydrochloride;N-Ethylethanamine hydrochloride;diethylazanium chloride;N-ethylethanamine;
PSA 12.03000
LogP 1.80870

Synthetic route

: 109-89-7
diethylamine

: 660-68-4
diethyl amine hydrochloride

Conditions

Conditions	Yield
With hydroxylamine hydrochloride In ethanol for 2h; Reflux;	100%
With methanol; acetyl chloride In diethyl ether at 0℃; for 1h; Inert atmosphere;	93%

: 36288-37-6
N-hydroxy-4-methylbenzenecarboximidoyl chloride

: 109-89-7
diethylamine

A: 660-68-4
diethyl amine hydrochloride

B: 188118-36-7
N,N-Diethyl-N'-hydroxy-4-methyl-benzamidine

Conditions

Conditions	Yield
In diethyl ether for 48h; Ambient temperature;	A n/a B 99%

...Expand

: 109-89-7
diethylamine

: 1011-84-3
4-nitrobenzohydroximoyl chloride

A: 660-68-4
diethyl amine hydrochloride

B: 188118-39-0
N,N-Diethyl-N'-hydroxy-4-nitro-benzamidine

Conditions

Conditions	Yield
In diethyl ether for 48h; Ambient temperature;	A n/a B 99%

...Expand

: 2-(diethylamino)-1-(4-hydroxyphenyl)ethanone hydrochloride

A: 156-38-7
4-hydroxyphenylacetate

B: 660-68-4
diethyl amine hydrochloride

Conditions

Conditions	Yield
In aq. buffer pH=4 - 7.4; pH-value; Irradiation;	A 99% B 99%

: bis(diethylamino)-(-)-menthylphosphine(pentacarbonyl)molybdenum(0)

A: chlorodiethylamino-(-)-menthylphosphine(pentacarbonyl)molybdenum(0)

B: 660-68-4
diethyl amine hydrochloride

Conditions

Conditions	Yield
With hydrogenchloride In pentane Under stirring a strong stream of hydrogenhalogenide is bubbled for 20 min through the soln. of phosphine complex at room temp.(inert atmosphere).; Solvent is evapd. at room temp. in vac., residue is digested with pentane, dialkylamminhydrohalogenide is filtered off, filtrate is dried to dryness in vac., chromy., elem. anal.;	A 98% B n/a

: bis(diethylamino)-(-)-menthylphosphine(pentacarbonyl)tungsten(0)

A: chlorodiethylamino-(-)-menthylphosphine(pentacarbonyl)tungsten(0)

B: 660-68-4
diethyl amine hydrochloride

Conditions

Conditions	Yield
With hydrogenchloride In pentane Under stirring a strong stream of hydrogenhalogenide is bubbled for 3-10 min through the cooled (-50-0°C) soln. of phosphine complex (inert atmosphere).; Solvent is evapd. at room temp. in vac., residue is digested with pentane, dialkylamminhydrohalogenide is filtered off, filtrate is dried to dryness in vac., recrystn. from pentane (-78°C), not purely isolated.;	A 96% B n/a

Yield

With hydrogenchloride In pentane Under stirring a strong stream of hydrogenhalogenide is bubbled for 3-10 min through the cooled (-50-0°C) soln. of phosphine complex (inert atmosphere).; Solvent is evapd. at room temp. in vac., residue is digested with pentane, dialkylamminhydrohalogenide is filtered off, filtrate is dried to dryness in vac., recrystn. from pentane (-78°C), not purely isolated.;

A 96%
B n/a

: 84534-89-4
bis(diethylamino)phenylphosphine(pentacarbonyl)molybdenum(0)

A: 126289-60-9
chlorodiethylaminophenylphosphine(pentacarbonyl)molybdenum(0)

B: 660-68-4
diethyl amine hydrochloride

Conditions

Conditions	Yield
With hydrogenchloride In benzene Under stirring a strong stream of hydrogenhalogenide is bubbled for 10 min through the cooled (0°C) soln. of phosphine complex (inert atmosphere).; Solvent is evapd. at room temp. in vac., residue is digested with pentane, dialkylamminhydrohalogenide is filtered off, filtrate is dried to dryness in vac., recrystn. from pentane (-78°C), elem. anal.;	A 95% B n/a

: 126306-20-5
bis(diethylamino)phenylphosphine(pentacarbonyl)tungsten(0)

A: 126289-63-2
chlorodiethylaminophenylphosphine(pentacarbonyl)tungsten(0)

B: 660-68-4
diethyl amine hydrochloride

Conditions

Conditions	Yield
With hydrogenchloride In pentane Under stirring a strong stream of hydrogenhalogenide is bubbled for 3-10 min through the cooled (-50-0°C) soln. of phosphine complex (inert atmosphere).; Solvent is evapd. at room temp. in vac., residue is digested with pentane, dialkylamminhydrohalogenide is filtered off, filtrate is dried to dryness in vac., recrystn. from pentane (-78°C), not purely isolated.;	A 93% B n/a

Yield

A 93%
B n/a

: 31355-55-2, 39210-30-5
trichlorotris(tetrahydrofuran)molybdenum(III)

: 4648-54-8
trimethylsilylazide

: 76276-42-1
diethylammonium O,O-dimethyl phosphorodithioate

: 82621-45-2
[MoN(S2P(OCH3)2)2]4

B: 660-68-4
diethyl amine hydrochloride

Conditions

Conditions	Yield
In tetrahydrofuran byproducts: (CH3)3SiCl; (N2); mixt. of complex/(CH3)3SiN3/THF warmed at 45-50°C for 1 h,evapd., (C2H5)2NH2(S2P(OCH3)2) and THF added, stirred for 3 h; concd., filtered, filtrate treated with MeOH, concd., MeOH added, ppt. filtered, washed with MeOH, dried, recrystd. (MeOH/THF); elem. anal.;	A 61% B 93%

...Expand

: 771-99-3
4-phenylpiperidine

: 24424-99-5
di-tert-butyl dicarbonate

A: 660-68-4
diethyl amine hydrochloride

B: 123387-49-5
tert-butyl 4-phenylpiperidine-1-carboxylate

Conditions

Conditions	Yield
With diethylamine In 1,2-dichloro-ethane at 20℃;	A n/a B 90.6%

...Expand

: 126306-21-6
bis(diethylamino)-t-butylphosphine(pentacarbonyl)tungsten(0)

A: 126289-65-4
chlorodiethylamino-t-butylphosphine(pentacarbonyl)tungsten(0)

B: 660-68-4
diethyl amine hydrochloride

Conditions

Conditions	Yield
With hydrogenchloride In pentane Under stirring a strong stream of hydrogenhalogenide is bubbled for 3-10 min through the cooled (-50-0°C) soln. of phosphine complex (inert atmosphere).; Solvent is evapd. at room temp. in vac., residue is digested with pentane, dialkylamminhydrohalogenide is filtered off, filtrate is dried to dryness in vac., recrystn. from pentane (-78°C), not purely isolated.;	A 87% B n/a

Yield

A 87%
B n/a

: 126306-22-7
bis(diethylamino)-t-butylphosphine(pentacarbonyl)molybdenum(0)

A: 126289-62-1
chlorodiethylamino-t-butylphosphine(pentacarbonyl)molybdenum(0)

B: 660-68-4
diethyl amine hydrochloride

Conditions

Conditions	Yield
With hydrogenchloride In pentane Under stirring a strong stream of hydrogenhalogenide is bubbled for 20 min through the soln. of phosphine complex at room temp.(inert atmosphere).; Solvent is evapd. at room temp. in vac., residue is digested with pentane, dialkylamminhydrohalogenide is filtered off, filtrate is dried to dryness in vac., chromy., elem. anal.;	A 85% B n/a

: 97548-95-3, 93304-25-7
[H(C5H5)Mo(CO)2(P(OC(CH3)2CH2)2NH)](1+)*Cl(1-)=[H(C5H5)Mo(CO)2(P(OC(CH3)2CH2)2NH)]Cl

: 109-89-7
diethylamine

A: 97466-39-2, 93304-24-6, 97466-40-5
H(C5H5)Mo(CO)2(P(OC(CH3)2CH2)2N)

B: 660-68-4
diethyl amine hydrochloride

Conditions

Conditions	Yield
In not given 1 equiv. of Et2NH;	A 80% B 85%

...Expand

: 421-58-9
(trifluoromethyl)phosphonous dichloride

: 109-89-7
diethylamine

A: 21941-40-2
Diethylamino-chlor-trifluormethyl-phosphin

B: 660-68-4
diethyl amine hydrochloride

Conditions

Conditions	Yield
In hexane under Ar; warming up from -40°C to 20°C;	A 83% B n/a

...Expand

: C19H37N3P(1+)*Cl(1-)

A: 660-68-4
diethyl amine hydrochloride

B: diethylamidophenyl(N-diethylaminomethyl)phosphinate

Conditions

Conditions	Yield
With water In acetonitrile	A n/a B 81%

: bis(diethylamino)-(-)-menthylphosphine(pentacarbonyl)chromium(0)

A: chlorodiethylamino-(-)-menthylphosphine(pentacarbonyl)chromium(0)

B: 660-68-4
diethyl amine hydrochloride

Conditions

Conditions	Yield
With hydrogenchloride In pentane Under stirring a strong stream of hydrogenhalogenide is bubbled for 10 min through the cooled (0°C) soln. of phosphine complex (inert atmosphere).; Solvent is evapd. at room temp. in vac., residue is digested with pentane, dialkylamminhydrohalogenide is filtered off, filtrate is dried to dryness in vac., recrystn. from pentane (-78°C), elem. anal.;	A 81% B n/a

: 105502-26-9
bis(diethylamino)phenylphosphine(pentacarbonyl)chromium(0)

A: 126306-25-0
chlorodiethylaminophenylphosphine(pentacarbonyl)chromium(0)

B: 660-68-4
diethyl amine hydrochloride

Conditions

Conditions	Yield
With hydrogenchloride In pentane Under stirring a strong stream of hydrogenhalogenide is bubbled for 10 min through the cooled (0°C) soln. of phosphine complex (inert atmosphere).; Solvent is evapd. at room temp. in vac., residue is digested with pentane, dialkylamminhydrohalogenide is filtered off, filtrate is dried to dryness in vac., recrystn. from pentane (-78°C), elem. anal.;	A 77% B n/a

: 107531-53-3
(2-vinylphenyl)bis(diethylamino)phosphine

A: 660-68-4
diethyl amine hydrochloride

B: 107531-51-1
(2-vinylphenyl)dichlorophosphine

Conditions

Conditions	Yield
With hydrogenchloride In Petroleum ether at -90℃; for 3h;	A n/a B 75%

: 109-89-7
diethylamine

: 698-16-8
benzohydroximoyl chloride

A: 69305-79-9
N,N-diethylamino benzamidoxime

B: 660-68-4
diethyl amine hydrochloride

Conditions

Conditions	Yield
In diethyl ether for 48h; Ambient temperature;	A 73% B n/a

...Expand

: 126306-17-0
bis(diethylamino)cyclohexylphosphine(pentacarbonyl)chromium(0)

A: 126306-29-4
chlorodiethylaminocyclohexylphosphine(pentacarbonyl)chromium(0)

B: 660-68-4
diethyl amine hydrochloride

Conditions

Conditions	Yield
With hydrogenchloride In pentane Under stirring a strong stream of hydrogenhalogenide is bubbled for 10 min through the cooled (0°C) soln. of phosphine complex (inert atmosphere).; Solvent is evapd. at room temp. in vac., residue is digested with pentane, dialkylamminhydrohalogenide is filtered off, filtrate is dried to dryness in vac., recrystn. from pentane (-78°C), elem. anal.;	A 73% B n/a

: 1066-45-1
trimethyltin(IV)chloride

: 109-89-7
diethylamine

: 536-74-3
phenylacetylene

A: 1199-95-7
1-(trimethylstannyl)-2-phenylethyne

B: 660-68-4
diethyl amine hydrochloride

Conditions

Conditions	Yield
The reaction mixture is heated to 35-40 °C. A white precipitate is observed to separate almost immediately. Then heating to slight boiling for 2 h, filter the mixture while it is cooling.; The precipitate is washed with small portions of absolue ether. The filtrate is evaporated and vacuum-distilled.;	A 71% B n/a

...Expand

: 2742-65-6
N,N-diethyl-N'-p-tolyl-thiourea

: 70-11-1
α-bromoacetophenone

A: 34587-31-0
5-phenyl-2-p-tolylimino-1,3-oxathiole

B: 660-68-4
diethyl amine hydrochloride

Conditions

Conditions	Yield
In acetone Heating;	A 70% B n/a

...Expand

: 109-89-7
diethylamine

: 28123-63-9
4-chlorobenzohydroximoyl chloride

A: 660-68-4
diethyl amine hydrochloride

B: 188118-38-9
4-Chloro-N,N-diethyl-N'-hydroxy-benzamidine

Conditions

Conditions	Yield
In diethyl ether for 48h; Ambient temperature;	A n/a B 70%

...Expand

: 124-38-9
carbon dioxide

: 109-89-7
diethylamine

: manganese(ll) chloride

A: [Mn(II)6(O2CNEt2)12]

B: 660-68-4
diethyl amine hydrochloride

Conditions

Conditions	Yield
In toluene under Ar or N2;soln. of NHEt2 (excess) satd. with CO2 at room temp., addn. of anhydrous MnCl2, heating for 4 d at 50 ° C with periodic cooling to room temp. and restoration of the pressure of CO2, dialkylammonium chloride filtered off; soln. evapd., solid dissolved in boiling n-heptane, filtration, cooling first to room temp. and then to -30 ° C for 24 h, pptn., elem. anal.;	A 66% B n/a

...Expand

: 31480-07-6
allylbis(diethylamino)phosphine

A: 31078-91-8
Allylphosphonsaeuredichlorid

B: 660-68-4
diethyl amine hydrochloride

Conditions

Conditions	Yield
With hydrogenchloride In Petroleum ether at -90℃; for 3h;	A 65% B n/a

: 107531-54-4
(2-allylphenyl)bis(diethylamino)phosphine

A: 660-68-4
diethyl amine hydrochloride

B: 107531-52-2
(2-Allylphenyl)dichlorphosphan

Conditions

Conditions	Yield
With hydrogenchloride In Petroleum ether at -90℃; for 3h;	A n/a B 65%

: 109-89-7
diethylamine

: 5032-90-6
chlorobis(pentafluorophenyl)phosphane

A: 660-68-4
diethyl amine hydrochloride

B: 13917-53-8
Bis-(Pentafluorphenyl)-diaethylaminophosphin

Conditions

Conditions	Yield
In diethyl ether byproducts: HCl; in presence of a HCl-trap;	A n/a B 63%
In diethyl ether byproducts: HCl; in presence of a HCl-trap;	A n/a B 63%

...Expand

: 109-89-7
diethylamine

: 38435-51-7
N-hydroxy-4-methoxy-benzenecarboximidoyl chloride

A: 660-68-4
diethyl amine hydrochloride

B: 188118-37-8
N,N-Diethyl-N'-hydroxy-4-methoxy-benzamidine

Conditions

Conditions	Yield
In diethyl ether for 48h; Ambient temperature;	A n/a B 62%

...Expand

: 109-89-7
diethylamine

: tris(dimethylamino)isothiocyanatophosphonium chloride

A: 660-68-4
diethyl amine hydrochloride

B: C11H28N5PS

Conditions

Conditions	Yield
for 6h;	A n/a B 60%

...Expand

: 109-89-7
diethylamine

: 5032-91-7
pentafluorophenyl dichlorophosphine

A: 660-68-4
diethyl amine hydrochloride

B: 13648-83-4
bis(diethylamino)-2,3,4,5,6-pentafluorophenylphosphane

Conditions

Conditions	Yield
In diethyl ether byproducts: HCl; in presence of a trap for HCl;	A n/a B 60%
In diethyl ether byproducts: HCl; in presence of a trap for HCl;	A n/a B 60%

...Expand

: 50-00-0
formaldehyd

: 67883-62-9
2-methylallyltributyltin

: 660-68-4
diethyl amine hydrochloride

: 62751-20-6
4-(diethylamino)-2-methyl-1-butene

Conditions

Conditions	Yield
In ethanol; chloroform; water for 4h; Ambient temperature;	100%

...Expand

: 2270-20-4
5-Phenylpentanoic acid

: 660-68-4
diethyl amine hydrochloride

: 5-phenyl-pentanoic acid diethylamide

Conditions

Conditions	Yield
Stage #1: 5-Phenylpentanoic acid With chloroformic acid ethyl ester; triethylamine In dichloromethane for 0.5h; Stage #2: diethyl amine hydrochloride In dichloromethane Heating;	100%

: 130004-33-0, 145926-28-9, 376354-47-1
(2,2'-bis(diphenylphosphino)-1,1'-binaphathalene)chloro(p-cymene)ruthenium chloride

: 660-68-4
diethyl amine hydrochloride

: [(RuCl((C6H5)2PC10H6C10H6P(C6H5)2))2Cl3](1-)*[(CH3CH2)2NH2](1+)=[(RuCl((C6H5)2PC10H6C10H6P(C6H5)2))2Cl3][(CH3CH2)2NH2]

Conditions

Conditions	Yield
In tetrahydrofuran (Ar); heating a soln. of ruthenium complex with ammonium salt in THF for 6 h; evapn., washing;	100%

: 153305-67-0, 100165-88-6, 99646-28-3
(+)-(R)-2,2'bis(di-para-tolylphosphanyl)-1,1'binaphthyl

: 52462-29-0
[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2

: 660-68-4
diethyl amine hydrochloride

: (RuCl(CH3C6H4)2PC10H6C10H6P(CH3C6H4)2)2Cl3(1-)*(CH3CH2)2NH2(1+)=[(RuCl(CH3C6H4)2PC10H6C10H6P(CH3C6H4)2)2Cl3](CH3CH2)2NH2

Conditions

Conditions	Yield
In toluene (Ar); heating a soln. of ruthenium complex with ammonium salt and phosphine in toluene at 50°C for 2 h with stirring, refluxing for 12 hwith stirring; cooling, evapn.;	100%

...Expand

: 50-00-0
formaldehyd

: 660-68-4
diethyl amine hydrochloride

: 11-methylpyridol[2,3-b]acridine-5,12-dione

: 11-[2'-(diethylamino)ethyl]pyrido[2,3-b]acridine-5,12-dione

Conditions

Conditions	Yield
In acetic acid at 110℃; for 0.333333h; Alkylation;	99%

...Expand

: 28917-43-3
3,5-dibenzyloxybenzoic acid

: 660-68-4
diethyl amine hydrochloride

: 859103-01-8
(3,5-di-benzyloxy)-N,N-diethylbenzamide

Conditions

Conditions	Yield
With WSC*HCl; benzotriazol-1-ol; triethylamine In dichloromethane for 10h;	99%

: 167323-74-2
(η(5)-C2B9H11)Zr(NEt2)2(NHEt2)

: 660-68-4
diethyl amine hydrochloride

: 167323-77-5
(η(5)-C2B9H11)ZrCl2(NHEt2)2

Conditions

Conditions	Yield
In dichloromethane N2-atmosphere; stirring (23°C, 2 h); evapn. (vac.), drying (vac., 1 h); elem. anal.;	99%

: 660-68-4
diethyl amine hydrochloride

: 154419-32-6
9-phenyl-1,2-dihydro-3H-pyrrolo[3,4-b]quinolin-3-one

: 342011-77-2
N,N-diethyl-3-hydroxymethyl-4-phenylquinoline-2-carboxamide

Conditions

Conditions	Yield
Stage #1: diethyl amine hydrochloride With trimethylaluminum In hexane; dichloromethane at 20℃; for 0.25h; Stage #2: 9-phenylfurol<3,4-b>quinolin-3(1H)-one In hexane; dichloromethane at 25 - 41℃; Weinreb amidation; Further stages.;	98%

: 34374-88-4
2,4,6-triformylphloroglucinol

: 660-68-4
diethyl amine hydrochloride

: C21H33N3O3

Conditions

Conditions	Yield
In d(4)-methanol at 20℃; for 16h;	98%

: 660-68-4
diethyl amine hydrochloride

: 616-38-6
carbonic acid dimethyl ester

: 29508-45-0
dimethyldiethylammonium chloride

Conditions

Conditions	Yield
With 1-ethyl-3-methylimidazolium bromide at 169.84℃; for 8h;	97.4%

: 660-68-4
diethyl amine hydrochloride

: 95835-64-6
4-chloro-6-methyl-3-nitro-2-pyridone

: 4-(diethylamino)-6-methyl-3-nitropyridin-2(1H)-one

Conditions

Conditions	Yield
With N-ethyl-N,N-diisopropylamine In acetonitrile for 2.5h; Inert atmosphere; Reflux;	97%

: 6089-09-4
4-pentynoic acid

: 660-68-4
diethyl amine hydrochloride

: 13991-17-8
N,N-diethylpent-4-ynamide

Conditions

Conditions	Yield
	95%

: [(pyrrolidine)dimethylaluminum]2

: 660-68-4
diethyl amine hydrochloride

: 570401-19-3
Al(CH3)2Cl(C4H8NH)

Conditions

Conditions	Yield
In tetrahydrofuran suspn. of NH2Et2Cl in THF was treated with Al-complex, stirred for 2 h under N2; solvent was removed in vacuo; elem. anal.;	95%

: 1422953-19-2
4-bromo-3-methoxy-5-(methoxymethoxy)benzoic acid

: 660-68-4
diethyl amine hydrochloride

: 1422953-20-5
4-bromo-N,N-diethyl-3-methoxy-5-(methoxymethoxy)benzamide

Conditions

Conditions	Yield
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 0 - 25℃; for 12h; Inert atmosphere;	95%

: 96-48-0
4-butanolide

: 660-68-4
diethyl amine hydrochloride

: 86452-59-7
N,N-Diethyl-4-hydroxy-butyramide

Conditions

Conditions	Yield
Stage #1: diethyl amine hydrochloride With diisobutylaluminium hydride In tetrahydrofuran; toluene Stage #2: 4-butanolide In tetrahydrofuran at 20℃; for 0.5h;	94%

: 660-68-4
diethyl amine hydrochloride

: 7550-45-0
titanium tetrachloride

: [NH2Et2]2[TiCl6]

Conditions

Conditions	Yield
In dichloromethane at 24.84℃; for 3h; Inert atmosphere;	94%

: 660-68-4
diethyl amine hydrochloride

: 10026-11-6
zirconium(IV) chloride

: bis(diethylammonium) hexachlorozirconate(IV),

Conditions

Conditions	Yield
In acetonitrile	93%

: 18386-03-3
3-(3-bromophenoxy)propanoic acid

: 660-68-4
diethyl amine hydrochloride

: C13H18BrNO2

Conditions

Conditions	Yield
Stage #1: 3-(3-bromophenoxy)propionic acid With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate In tetrahydrofuran; acetonitrile at 20℃; for 0.5h; Stage #2: diethyl amine hydrochloride In tetrahydrofuran; acetonitrile at 20℃;	93%

: 3066-75-9
allyl diethyl phosphate

: 201230-82-2
carbon monoxide

: 660-68-4
diethyl amine hydrochloride

: 17093-17-3
N, N-diethylbut-3-enamide

Conditions

Conditions	Yield
With dmap; hexarhodium hexadecacarbonyl; triethylamine In dimethyl sulfoxide at 50℃; under 15200 Torr; for 6h;	92%

...Expand

: 660-68-4
diethyl amine hydrochloride

: 103-71-9
phenyl isocyanate

: 1014-72-8
1-phenyl-3,3-diethylurea

Conditions

Conditions	Yield
With triethylamine In dichloromethane at 0 - 20℃;	92%

: 660-68-4
diethyl amine hydrochloride

: 100-51-6
benzyl alcohol

: 1696-17-9
N,N-diethylbenzamide

Conditions

Conditions	Yield
With tert.-butylhydroperoxide; tris(bipyridine)ruthenium(II) dichloride hexahydrate; calcium carbonate In water; ethyl acetate at 20℃; for 72h; Inert atmosphere; Irradiation;	92%
With tert.-butylhydroperoxide; calcium carbonate In water; acetonitrile at 80℃; for 4h;	60%

Diethylamine hydrochloride Chemical Properties

IUPAC Name:N-ethylethanamine hydrochloride
Molecular Formula:C₄H₁₁N·ClH
Molecular Weight:109.62
EINECS:211-541-9
Melting Point:227-230 °C
Boiling Point:320-330 °C
Solubility:Soluble
Density:1.0 g/mL at 20 °C
Sensitive:Hygroscopic
Appearance:Off-white solid
Diethylammonium Chloride's(660-68-4) Synonyms: Diethyl-ammonium;Ethanamine,N-ethyl-,hydrochloride;n-ethylethanaminehydrochloride;n-ethyl-ethanaminhydrochloride;TETRAMETHYLTHIONINE CHLORIDE;NEISSER'S METHYLENE BLUE;NEISSER'S SOLUTION IA;SWISS BLUE
Diethylammonium Chloride's(660-68-4) Molecular Structure:

Diethylamine hydrochloride Toxicity Data With Reference

1.	orl-rat LD50:9900 mg/kg	GISAAA Gigiena i Sanitariya. 49 (1)(1984),71.
2.	orl-mus LD50:4860 mg/kg	GTPZAB Gigiena Truda i Professionalnye Zabolevaniia. Labor Hygiene and Occupational Diseases. 31 (1)(1987),49.
3.	ipr-mus LD50:960 mg/kg	JJPAAZ Japanese Journal of Pharmacology. 17 (1967),475.
4.	scu-mus LD50:1130 mg/kg	AIPTAK Archives Internationales de Pharmacodynamie et de Therapie. 112 (1957),36.
5.	ivn-mus LD50:320 mg/kg	AIPTAK Archives Internationales de Pharmacodynamie et de Therapie. 112 (1957),36.

Diethylamine hydrochloride Consensus Reports

EPA Genetic Toxicology Program. Reported in EPA TSCA Inventory.

Diethylamine hydrochloride Safety Profile

Poison by intravenous route. Moderately toxic by subcutaneous and intraperitoneal routes. When heated to decomposition it emits toxic fumes of NO_x, NH₃, and HCl.

Safety Information of Diethylammonium Chloride(660-68-4)
Hazard Codes Xn,Xi
Risk Statements 10-36/37/38
10 Flammable
36/37/38 Irritating to eyes, respiratory system and skin
Safety Statements 26-39-7-24/25-36
RIDADR UN 1993 3/PG 3
WGK Germany 3
RTECS SP5740000
F 21
HS Code 29211200

Diethylamine hydrochloride Specification

Stability and Reactivity of Diethylammonium Chloride(660-68-4)
【Disposal Code】3
【Incompatibilities】Oxidizing agents.
【Stability】Stable under normal temperatures and pressures.
【Decomposition】Hydrogen chloride, nitrogen oxides, carbon monoxide, irritating and toxic fumes and gases, carbon dioxide, nitrogen.

Product Name

Diethylamine hydrochloride

Synthetic route

Diethylamine hydrochloride Chemical Properties

Diethylamine hydrochloride Toxicity Data With Reference

Diethylamine hydrochloride Consensus Reports

Diethylamine hydrochloride Safety Profile

Diethylamine hydrochloride Specification

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