methoxycarbonylamino acetic acid methyl ester
2-aminoethanoic acid hydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride; formic acid In water at 125℃; for 24h; | 98% |
(3R)-3-<(1S,5R)-3-benzyl-7-oxo-4-oxa-2,6-diazabicyclo<3.2.0>hept-2-en-6-yl>-3,4,4-trimethylthietan-2-one
A
phenylacetic acid
B
2-aminoethanoic acid hydrochloride
C
(2-RS)-2-amino-3-mercapto-2,3-dimethylbutanoic acid hydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride for 15h; Heating; | A 96% B n/a C n/a |
Ethyl N-(trichloroacetyl)-2-aminoacetate
2-aminoethanoic acid hydrochloride
Conditions | Yield |
---|---|
With potassium hydroxide In methanol Ambient temperature; | 95% |
Conditions | Yield |
---|---|
With hydrogenchloride In water at 60℃; for 8h; | 91% |
With hydrogenchloride at 50℃; under 11400.9 Torr; Equilibrium constant; Thermodynamic data; Kinetics; various temperatures, protonation; | |
With hydrogenchloride In water |
Conditions | Yield |
---|---|
With hydrogenchloride; tin(ll) chloride In water at 20 - 25℃; for 16h; | 61% |
Conditions | Yield |
---|---|
With hydrogenchloride |
N-(Trichloroacetyl)glycine
2-aminoethanoic acid hydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride Heating; |
Conditions | Yield |
---|---|
With hydrogenchloride; potassium hydroxide 1.) methanol, 2 h, r. t.; Yield given. Multistep reaction; |
Conditions | Yield |
---|---|
With hydrogenchloride; water |
flurazepam dihydrochloride
A
2-aminoethanoic acid hydrochloride
Conditions | Yield |
---|---|
Product distribution; |
hydrogenchloride
2-aminoacetonitrile
B
2-aminoethanoic acid hydrochloride
2-aminoethanoic acid hydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride |
Conditions | Yield |
---|---|
at 100℃; im geschlossenen Rohr; |
desmocyclopeptide
A
2-aminoethanoic acid hydrochloride
B
L-phenylalanine hydrochloride
C
L-alanine hydrochloride
D
L-isoleucine hydrochloride
E
L-proline hydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride In water at 110℃; for 24h; |
versicoloritide B
A
2-aminoethanoic acid hydrochloride
B
L-phenylalanine hydrochloride
C
L-proline hydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride; water at 110℃; for 20h; |
propan-1-ol
2-aminoethanoic acid hydrochloride
glycine 1-propyl ester hydrochloride
Conditions | Yield |
---|---|
With thionyl chloride at 20 - 70℃; for 15h; Inert atmosphere; | 98% |
Conditions | Yield |
---|---|
Stage #1: formaldehyd; 2-aminoethanoic acid hydrochloride With trimethyl phosphite at 30 - 40℃; for 1h; Stage #2: With phosphorus trichloride at 10℃; for 24h; | 96% |
1-dodecyl alcohol
2-aminoethanoic acid hydrochloride
dodecyloxycarbonylmethylammonium chloride
Conditions | Yield |
---|---|
With hydrogenchloride at 110 - 120℃; for 8h; | 95% |
With hydrogenchloride at 110 - 120℃; for 8h; | 91% |
bis(N-salicylaldimino)nickel(II)
2-aminoethanoic acid hydrochloride
A
bis(N-salicylideneglycinato)Ni(II)
Conditions | Yield |
---|---|
In methanol stirring the soln. for 30 min between room temp. and 60°C, pptn.; filtration, washing with water, recrystn. from acetone; | A 90% B n/a |
Conditions | Yield |
---|---|
With thionyl chloride at -20℃; for 2h; Inert atmosphere; Reflux; | 90% |
ethanol
2-aminoethanoic acid hydrochloride
glycine ethyl ester hydrochloride
Conditions | Yield |
---|---|
With thionyl chloride at -20℃; for 2h; Reflux; Inert atmosphere; | 90% |
Conditions | Yield |
---|---|
Stage #1: 2-Hydroxy-4-methoxybenzaldehyde; 2-aminoethanoic acid hydrochloride With sodium hydroxide In water at 20℃; for 3h; pH=9; Stage #2: With sodium tetrahydroborate; sodium hydroxide In water for 1h; Cooling with ice; | 90% |
Conditions | Yield |
---|---|
With triethylamine In acetone for 10h; Reagent/catalyst; Solvent; Reflux; | 90% |
1-Decanol
2-aminoethanoic acid hydrochloride
decyloxycarbonylmethylammonium chloride
Conditions | Yield |
---|---|
With hydrogenchloride at 120 - 130℃; | 89% |
With hydrogenchloride at 110 - 120℃; for 8h; | 89% |
Conditions | Yield |
---|---|
With hydrogenchloride at 110 - 120℃; for 8h; | 86% |
Conditions | Yield |
---|---|
With phosphotungstic acid 44-hydrate; alloxan monohydrate In N,N-dimethyl-formamide at 110℃; | 86% |
Conditions | Yield |
---|---|
With hydrogenchloride at 110 - 120℃; for 8h; | 85% |
Conditions | Yield |
---|---|
With sodium hydroxide In water at 37℃; for 72h; pH=10.5; Polyethylene glycol; | 85% |
chenodeoxycholic acid
2-aminoethanoic acid hydrochloride
ethyl glycochenodeoxycholate
Conditions | Yield |
---|---|
With triethylamine In acetone for 10h; Reflux; | 85% |
formaldehyd
oxyde de dioctyl phosphine
2-aminoethanoic acid hydrochloride
N,N-bis(methylenedioctylphosphoryl)aminoethanoic acid
Conditions | Yield |
---|---|
In acetonitrile for 3h; Reflux; | 84% |
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran at 20℃; for 12h; | 80% |
2-aminoethanoic acid hydrochloride
(+/-)-(5-methyl-5-hexyl-2-oxothiophen-4-yloxy)acetic acid
(+/-)-(5-methyl-5-hexyl-2-oxothiophen-4-yloxy)acetyl methyl glycinate
Conditions | Yield |
---|---|
With tris(1,3-dihydro-2-oxobenzoxazolin-3-yl) phosphine oxide; triethylamine In acetonitrile at 20℃; for 0.333333h; | 80% |
2-aminoethanoic acid hydrochloride
N,N-dimethyl-formamide
Conditions | Yield |
---|---|
Stage #1: N,N-dimethyl-formamide With trichlorophosphate at 10 - 15℃; for 1h; Stage #2: 2-aminoethanoic acid hydrochloride at 80℃; for 4h; Stage #3: With hexafluorophosphoric acid In water at 0℃; | 78% |
Molecular Structure of 2-Aminoacetic acid hydrochloride (CAS NO.6000-43-7):
IUPAC Name: 2-Aminoacetic acid hydrochloride
CAS: 6000-43-7
Formula: C2H6ClNO2
Molecular Weight: 111.53
EINECS: 227-841-8
H bond acceptors: 3
H bond donors: 3
Freely Rotating Bonds: 2
Polar Surface Area: 29.54 Å2
Flash Point: 99.5 °C
Storage temp: 2-8°C
Water Solubility: Slightly soluble
Sensitive: Hygroscopic
Merck: 14,4491
BRN: 3909617
Melting Point: 176-180 °C(lit.)
Enthalpy of Vaporization: 52.63 kJ/mol
Boiling Point: 240.9 °C at 760 mmHg
Vapour Pressure: 0.0123 mmHg at 25°C
InChI
InChI=1/C2H5NO2.ClH/c3-1-2(4)5;/h1,3H2,(H,4,5);1H
Smiles
C(CN)(O)=O.Cl
Product Categories: alpha-amino acids; amino acids; biochemistry; omega-aminocarboxylic acids; omega-functional alkanols, carboxylic acids, amines & halides; alphabetic; amino acids, peptides and proteins; amino acidsanalytical standards; g;life sciences standards
1. | orl-rat LD50:3340 mg/kg | JPMSAE Journal of Pharmaceutical Sciences. 62 (1973),49. |
Reported in EPA TSCA Inventory.
Moderately toxic by ingestion. When heated to decomposition it emits very toxic fumes of Cl− and NOx.
Safety Statements about 2-Aminoacetic acid hydrochloride (CAS NO.6000-43-7):
S24/25: Avoid contact with skin and eyes.
F10: Keep under argon.
RIDADR: UN 1789 8/PG 3
WGK Germany: 2
RTECS: MC0560000
The chemical synonyms of 2-Aminoacetic acid hydrochloride (CAS NO.6000-43-7) are Aminoethanoic acid hydrochloride ; Aminoacetic acid hydrochloride ; Glycocoll hydrochloride ; Glycine hcl ; Glycine-hcl buffer ; Glycine hydrochloride ; Glycine hydrochloride solution ; Aminoaceticacid.hcl=h-gly-oh.hcl . It shoud avoid breathing dust, vapor, mist, or gas and should be stored in a cool, dry place. Ingestion of large amounts may cause gastrointestinal irritation. Low hazard for usual industrial handling. It can be used to improve the bitter taste of beer, but also can be used in behalf of salts, nutritional supplements, flavor enhancer.
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