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Dayang Chem (Hangzhou) Co.,Ltd.

As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch

4-Methyl-2-nitroaniline Manufacturer/High quality/Best price/In stock

Cas:89-62-3

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

inquiry

Simagchem Corporation

Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our

High quality Fast Red GL base supplier in China

Cas:89-62-3

Min.Order:0 Metric Ton

Negotiable

Type:Manufacturers

inquiry

Hebei yanxi chemical co.,LTD.

hebei yanxi chemical co., LTD who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do research and developm

4-Methyl-2-nitroaniline Manufacturer/High quality

Cas:89-62-3

Min.Order:1 Metric Ton

FOB Price: $1.0 / 3.0

Type:Manufacturers

inquiry

Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply 2-nitro-p-toluidine

Cas:89-62-3

Min.Order:1

Negotiable

Type:Other

inquiry

Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

2-Nitro-p-toluidine (NH2=1) (C.I. 37110)

Cas:89-62-3

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

inquiry

Henan Tianfu Chemical Co., Ltd.

Our company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O

4-Methyl-2-nitroaniline-

Cas:89-62-3

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Henan Sinotech Import&Export Corporation

Product Name: 4-Methyl-2-nitroaniline Synonyms: 4-methyl-2-nitro-Benzenamine;4-Methyl-6-nitroaniline;ai3-09044;Amarthol Fast Red GL Base;Amarthol Fast Red GL Salt;Azoamine Red A;azoaminereda;Azobase NAT

4-Methyl-2-nitroaniline CAS: 89-62-3

Cas:89-62-3

Min.Order:5 Metric Ton

FOB Price: $1.0 / 2.0

Type:Other

inquiry

Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

CAS NO.:89-62-3

Cas:89-62-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

4-Methyl-2-nitroaniline

Cas:89-62-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

High quality Fast Red GL base

Cas:89-62-3

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

inquiry

HANGZHOU YUNUO CHEMICAL CO.,LTD

Superior quality, moderate price & quick delivery. Appearance:orange to orange-brown fine crystalline powder Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:1kg/bag, 1kg/drum or 25kg/drum or as per your re

4-Methyl-2-nitroaniline

Cas:89-62-3

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

inquiry

Zibo Dorne chemical technology co. LTD

Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,

4-Methyl-2-nitroaniline

Cas:89-62-3

Min.Order:1 Metric Ton

Negotiable

Type:Lab/Research institutions

inquiry

Wuhan Fortuna Chemical Co.,Ltd

CAS:89-62-3 EINECS:201-924-9 MW:152.15 MF:C7H8N2O2 Melting point:115-116 °C(lit.) Boiling point:169°C (21 mmHg) Appearance:nacarat crystalline powder Package:25kg/drum Transportation:by sea/air Port:Shanghai

4-Methyl-2-nitroaniline

Cas:89-62-3

Min.Order:0 Metric Ton

Negotiable

Type:Trading Company

inquiry

Hunan chemfish Pharmaceutical co.,Ltd

Appearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea

4-Methyl-2-nitroaniline

Cas:89-62-3

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

SAGECHEM LIMITED

SAGECHEM is a chemical R&D, manufacturing and distribution company in China since 2009, including pharmaceutical intermediates, agrochemical, dyestuff intermediates, organosilicone, API and etc. We also offer a full range of services in custom synthe

SAGECHEM/3-Nitro-4-aminotoluene

Cas:89-62-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Beijing Greenchem Technology Co.,Ltd. ( Panjin Greenchem Technology Co.Ltd .)

Capability on chemical synthesis1. Beijing High-Tech Enterprises2. Strong R&D Team3. 8 years of experiences in R & D of high-tech Catalyst;4. 5000 production techniques, 69 items of national patents, and 360 kinds of products on sales;5. The producti

3-Nitro-4-aminotoluene

Cas:89-62-3

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Changzhou Anchor Biological Technology Co., Ltd.

Our company is engaged in customizing the benzene ring and pyridine derivative organic intermediates, and the quantity is flexible according to customer's needs. It mainly provides high-quality intermediates for domestic and foreign pharmaceutical an

4-Methyl-2-nitroaniline Manufacturer/High quality/Best price/In stock CAS NO.89-62-3

Cas:89-62-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Greenutra Resource Inc

2,5-DichloronitrobenzeneAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air

2,5-Dichloronitrobenzene

Cas:89-62-3

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Kono Chem Co.,Ltd

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou

2,5-Dichloronitrobenzene

Cas:89-62-3

Min.Order:0

Negotiable

Type:Other

inquiry

Hangzhou Dingyan Chem Co., Ltd

R & D enterprises have their own stock in stockAppearance:To be subject to the object Package:Customized Application:pharmaceutical intermediates Transportation:Air Port:Shanghai;Guangzhou

4-Methyl-2-nitroaniline

Cas:89-62-3

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

GIHI CHEMICALS CO.,LIMITED

high purity,in stock Package:25kg/drum,or as per customers'demand Application:API,Pharmaceutical intermediates Transportation:air,sea,courier

3-Nitro-4-aminotoluene

Cas:89-62-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Henan Allgreen Chemical Co.,Ltd

high quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea

4-Methyl-2-nitroaniline

Cas:89-62-3

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Aecochem Corp.

Our clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS

Fast Red GL base

Cas:89-62-3

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Zhuozhou Wenxi import and Export Co., Ltd

Product Description Description & Specification Category Pharmaceutical Raw Materials, Fine Chemicals, Bulk drug Standard Medical standard

factory supply CAS 89-62-3 with competitive price

Cas:89-62-3

Min.Order:1 Kilogram

FOB Price: $112.0

Type:Trading Company

inquiry

Antimex Chemical Limied

Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali

Benzenamine,4-methyl-2-nitro-

Cas:89-62-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Xiamen AmoyChem Co.,Ltd

Amoychem is committed to providing the top-quality chemical products and services Internationally. We offer our customers with friendly, professional service and reliable, high performance products that have been manufactured according to the accredi

4-Methyl-2-Nitroaniline

Cas:89-62-3

Min.Order:0

Negotiable

Type:Other

inquiry

Hubei Langyou International Trading Co., Ltd

4-Methyl-2-nitroaniline/High quality/Best price/In stock CAS NO.89-62-3 Application:4-Methyl-2-nitroaniline/High quality/Best price/In stock CAS NO.89-62-3

Wuhan ZeShanCheng Biomedical Technology Co., Ltd.

1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists of highl

Benzenamine,4-methyl-2-nitro-

Cas:89-62-3

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Hunan Longxianng Runhui Trading Co.,Ltd

4-Methyl-2-nitroaniline/High quality/Best price/In stock CAS NO.89-62-3Appearance:powder Storage:Store at RT. Package:in foil bag or customized Application:Industrial Transportation:By express (Door to door) such as FEDEX, DHL, EMS for small amount.

4-Methyl-2-nitroaniline/High quality/Best price/In stock CAS NO.89-62-3

Cas:89-62-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hunan Russell Chemicals Technology Co.,Ltd

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:any port in China

4-Methyl-2-nitroaniline 89-62-3

Cas:89-62-3

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Synthetic route

4-methyl-2-nitroacetanilide
612-45-3

4-methyl-2-nitroacetanilide

4-methyl-2-nitroaniline
89-62-3

4-methyl-2-nitroaniline

Conditions
ConditionsYield
With Claisen's base99.4%
With water; potassium hydroxide In ethanol for 3h; Reflux;92%
With hydrogenchloride
N-(4-methyl-2-nitrophenyl) benzamide
26242-93-3

N-(4-methyl-2-nitrophenyl) benzamide

4-methyl-2-nitroaniline
89-62-3

4-methyl-2-nitroaniline

Conditions
ConditionsYield
With potassium hydroxide In methanol at 20℃; for 12h;97%
p-toluidine
106-49-0

p-toluidine

4-methyl-2-nitroaniline
89-62-3

4-methyl-2-nitroaniline

Conditions
ConditionsYield
With Oxone; sodium nitrite In nitromethane at 50℃; chemoselective reaction;86%
With 3-methyl-1-sulfonic acid imidazolium nitrate In dichloromethane at 20℃; for 0.25h;81%
With tetrachloromethane; diethyl ether; dinitrogen pentoxide
ethyl p-tolylcarbamate
5255-66-3

ethyl p-tolylcarbamate

4-methyl-2-nitroaniline
89-62-3

4-methyl-2-nitroaniline

Conditions
ConditionsYield
With tert.-butylnitrite; palladium diacetate In 1,4-dioxane at 90℃; Reagent/catalyst;80%
With tert.-butylnitrite; hydrogen; copper dichloride In 1,4-dioxane at 90℃; for 6h; Reagent/catalyst; Temperature;79%
5-methylbenzofuroxan
19164-41-1

5-methylbenzofuroxan

A

5-methyl-2-nitroaniline
578-46-1

5-methyl-2-nitroaniline

B

4-methyl-2-nitroaniline
89-62-3

4-methyl-2-nitroaniline

Conditions
ConditionsYield
With iron(II) sulfate In water; dimethyl sulfoxide Ambient temperature; Title compound not separated from byproducts;A 65%
B 35%
With iron(II) sulfate In dimethyl sulfoxide at 20℃; for 1h;A 60%
B 26%
With HbO2(2+) In phosphate buffer; dimethyl sulfoxide for 1h; pH=7.4;A 38 % Chromat.
B 54 % Chromat.
trinitromethane
517-25-9

trinitromethane

4-methylphenyl isocyanide
7175-47-5

4-methylphenyl isocyanide

A

p-toluidine
106-49-0

p-toluidine

B

3-(2-nitro-4-methylphenyl)-1,2,3,4-oxatriazolium-5-olate

3-(2-nitro-4-methylphenyl)-1,2,3,4-oxatriazolium-5-olate

C

4-methyl-2-nitroaniline
89-62-3

4-methyl-2-nitroaniline

Conditions
ConditionsYield
A 3%
B 48%
C 21%
4-methylphenyl isocyanide
7175-47-5

4-methylphenyl isocyanide

A

p-toluidine
106-49-0

p-toluidine

B

3-(2-nitro-4-methylphenyl)-1,2,3,4-oxatriazolium-5-olate

3-(2-nitro-4-methylphenyl)-1,2,3,4-oxatriazolium-5-olate

C

4-methyl-2-nitroaniline
89-62-3

4-methyl-2-nitroaniline

Conditions
ConditionsYield
With trinitromethaneA 3%
B 48%
C 21%
N-acetonyl-4-methyl-2-nitro-N-p-tolylsulphonylaniline
71467-88-4

N-acetonyl-4-methyl-2-nitro-N-p-tolylsulphonylaniline

A

2,7-dimethylquinoxaline
39859-62-6

2,7-dimethylquinoxaline

B

di(p-tolyl) disulfide
103-19-5

di(p-tolyl) disulfide

C

4-methyl-2-nitroaniline
89-62-3

4-methyl-2-nitroaniline

Conditions
ConditionsYield
With hydrogenchloride; tin(ll) chloride In acetic acid 1.) 65 deg C, 1.5 h, 2.) 100 deg C, 1.5 h;A 42%
B n/a
C n/a
ethanol
64-17-5

ethanol

1,3-bis-(4-methyl-2-nitro-phenyl)-triazene

1,3-bis-(4-methyl-2-nitro-phenyl)-triazene

A

1-methyl-3-nitrobenzene
99-08-1

1-methyl-3-nitrobenzene

B

4-methyl-2-nitroaniline
89-62-3

4-methyl-2-nitroaniline

Conditions
ConditionsYield
at 170℃; im geschlossenen Rohr;
4-methyl-2-nitrophenol
119-33-5

4-methyl-2-nitrophenol

4-methyl-2-nitroaniline
89-62-3

4-methyl-2-nitroaniline

Conditions
ConditionsYield
With ammonia at 170 - 180℃;
With formic acid; ammonia; water at 150℃;
N-(4-methylphenyl)formamide
3085-54-9

N-(4-methylphenyl)formamide

4-methyl-2-nitroaniline
89-62-3

4-methyl-2-nitroaniline

Conditions
ConditionsYield
With sulfuric acid; water; nitric acid und Eintragen des Reaktionsgemisches in Wasser;
N-(4-methylphenyl)benzamide
582-78-5

N-(4-methylphenyl)benzamide

4-methyl-2-nitroaniline
89-62-3

4-methyl-2-nitroaniline

Conditions
ConditionsYield
With nitric acid Erhitzen des entstandenen Benzoylderivats mit konz.Salzsaeure auf 200grad;
With nitric acid Erhitzen des entstandenen Benzoylderivats mit verd. Natronlauge;
Multi-step reaction with 2 steps
1: nitric acid; copper(II) nitrate hydrate; oxygen / acetonitrile; water / 12 h / 100 °C / 760.05 Torr
2: potassium hydroxide / methanol / 12 h / 20 °C
View Scheme
3,4-Dinitrotoluene
610-39-9

3,4-Dinitrotoluene

4-methyl-2-nitroaniline
89-62-3

4-methyl-2-nitroaniline

Conditions
ConditionsYield
With methanol; ammonia at 150℃; unter Druck;
3,4-Dinitrotoluene
610-39-9

3,4-Dinitrotoluene

A

5-methyl-2-nitroaniline
578-46-1

5-methyl-2-nitroaniline

B

4-methyl-2-nitroaniline
89-62-3

4-methyl-2-nitroaniline

Conditions
ConditionsYield
With hydrogenchloride; tin(ll) chloride at 7℃;
With methanol; ammonia at 150℃; unter Druck;
BTB01434
3968-10-3

BTB01434

4-methyl-2-nitroaniline
89-62-3

4-methyl-2-nitroaniline

Conditions
ConditionsYield
With sulfuric acid
With sulfuric acid
acetic anhydride
108-24-7

acetic anhydride

para-methyl anilinium nitrate
32954-54-4

para-methyl anilinium nitrate

A

4-Methylacetanilide
103-89-9

4-Methylacetanilide

B

4-methyl-2-nitroaniline
89-62-3

4-methyl-2-nitroaniline

C

N-nitro-p-toluidine
20020-14-8

N-nitro-p-toluidine

p-toluidine
106-49-0

p-toluidine

A

4-Methyl-3-nitroanilin
119-32-4

4-Methyl-3-nitroanilin

B

4-methyl-2-nitroaniline
89-62-3

4-methyl-2-nitroaniline

Conditions
ConditionsYield
With sulfuric acid; nitric acid wendet man viel Schwefelsaeure an, so entsteht nur 2-Nitro-4-amino-toluol;
With sulfuric acid; nitric acid
2,2,2-trichloro-N,N'-bis(4-methylphenylethane)-1,1-diamine
39809-78-4

2,2,2-trichloro-N,N'-bis(4-methylphenylethane)-1,1-diamine

acetic acid
64-19-7

acetic acid

4-methyl-2-nitroaniline
89-62-3

4-methyl-2-nitroaniline

Conditions
ConditionsYield
With nitric acid Eingeiessen des Produktes in Wasser;
1-chloro-4-methyl-2-nitro-benzene
89-60-1

1-chloro-4-methyl-2-nitro-benzene

4-methyl-2-nitroaniline
89-62-3

4-methyl-2-nitroaniline

Conditions
ConditionsYield
With ammonia at 175℃; im Autoklaven;
4-Methylacetanilide
103-89-9

4-Methylacetanilide

4-methyl-2-nitroaniline
89-62-3

4-methyl-2-nitroaniline

Conditions
ConditionsYield
With nitric acid das entstandenene Acetylderivat verseift man durch Erwaermen mit alkoh.Kali;
With nitric acid; acetic acid
With hydrogenchloride; nitric acid das Acetylderivat entsteht;
N-nitro-p-toluidine
20020-14-8

N-nitro-p-toluidine

4-methyl-2-nitroaniline
89-62-3

4-methyl-2-nitroaniline

Conditions
ConditionsYield
With hydrogenchloride; diethyl ether
1-methyl-3-nitrobenzene
99-08-1

1-methyl-3-nitrobenzene

A

2-Methyl-6-nitroaniline
570-24-1

2-Methyl-6-nitroaniline

B

2-methyl-4-nitro-benzenamine
99-52-5

2-methyl-4-nitro-benzenamine

C

4-methyl-2-nitroaniline
89-62-3

4-methyl-2-nitroaniline

Conditions
ConditionsYield
With potassium tert-butylate; N,N,N-trimethylhydrazinium iodide In dimethyl sulfoxide Ambient temperature; Yield given. Yields of byproduct given;
2-p-tolylisoindoline-1,3-dione
2142-03-2

2-p-tolylisoindoline-1,3-dione

nitric acid
7697-37-2

nitric acid

A

4-Methyl-3-nitroanilin
119-32-4

4-Methyl-3-nitroanilin

B

4-methyl-2-nitroaniline
89-62-3

4-methyl-2-nitroaniline

Conditions
ConditionsYield
und Kochen der entstandenen Nitro-Verbindungen mit 2n-Natronlauge;
hydrogenchloride
7647-01-0

hydrogenchloride

N-(4-methyl-2-nitrophenyl) benzamide
26242-93-3

N-(4-methyl-2-nitrophenyl) benzamide

A

benzoic acid
65-85-0

benzoic acid

B

4-methyl-2-nitroaniline
89-62-3

4-methyl-2-nitroaniline

Conditions
ConditionsYield
at 200℃;
N-(4-methyl-2-nitrophenyl) benzamide
26242-93-3

N-(4-methyl-2-nitrophenyl) benzamide

alkali

alkali

A

benzoic acid
65-85-0

benzoic acid

B

4-methyl-2-nitroaniline
89-62-3

4-methyl-2-nitroaniline

sulfuric acid
7664-93-9

sulfuric acid

nitric acid
7697-37-2

nitric acid

p-toluidine
106-49-0

p-toluidine

A

4-Methyl-3-nitroanilin
119-32-4

4-Methyl-3-nitroanilin

B

4-methyl-2-nitroaniline
89-62-3

4-methyl-2-nitroaniline

tetrachloromethane
56-23-5

tetrachloromethane

diethyl ether
60-29-7

diethyl ether

p-toluidine
106-49-0

p-toluidine

N2O5

N2O5

A

toluene-4-diazonium ; nitrate

toluene-4-diazonium ; nitrate

B

4-methyl-2-nitroaniline
89-62-3

4-methyl-2-nitroaniline

C

N-nitro-p-toluidine
20020-14-8

N-nitro-p-toluidine

D

nitrate p-toluidine

nitrate p-toluidine

hydrogenchloride
7647-01-0

hydrogenchloride

diethyl ether
60-29-7

diethyl ether

N-nitro-p-toluidine
20020-14-8

N-nitro-p-toluidine

4-methyl-2-nitroaniline
89-62-3

4-methyl-2-nitroaniline

4-fluoro-3-nitrotoluene
446-11-7

4-fluoro-3-nitrotoluene

ammonia
7664-41-7

ammonia

4-methyl-2-nitroaniline
89-62-3

4-methyl-2-nitroaniline

4-methyl-2-nitroaniline
89-62-3

4-methyl-2-nitroaniline

2-amino-5-methyl-3-nitrophenyliodide
123158-77-0

2-amino-5-methyl-3-nitrophenyliodide

Conditions
ConditionsYield
With silver(II) sulfate; iodine In ethanol at 20℃; for 36h; Darkness;100%
With iodine; silver sulfate In ethanol at 20℃; for 36h; Darkness;100%
With silver(II) sulfate; iodine for 18h;100%
dimethyl sulfate
77-78-1

dimethyl sulfate

4-methyl-2-nitroaniline
89-62-3

4-methyl-2-nitroaniline

4,N-dimethyl-2-nitroaniline
4600-08-2

4,N-dimethyl-2-nitroaniline

Conditions
ConditionsYield
With sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate In water; toluene at 20℃; Methylation;99%
With tetra(n-butyl)ammonium hydrogensulfate; sodium hydroxide In water; toluene at 20℃;98%
N-phenylacetoacetamide
102-01-2

N-phenylacetoacetamide

4-methyl-2-nitroaniline
89-62-3

4-methyl-2-nitroaniline

pigment yellow 1
2512-29-0

pigment yellow 1

Conditions
ConditionsYield
With hydrogenchloride; sodium nitrite In water at 20℃; for 0.333333h; Time;99%
With hydrogenchloride; sodium nitrite In water at 20℃; for 0.666667h; Green chemistry;99%
Stage #1: 4-methyl-2-nitroaniline With hydrogenchloride; C25H20N6O6S2; sodium nitrite In water at 10℃; for 1h;
Stage #2: N-phenylacetoacetamide With sodium acetate; acetic acid In water at 25 - 90℃; for 2.5h; pH=6;
Stage #1: 4-methyl-2-nitroaniline With hydrogenchloride; sodium nitrite In water at 10℃; for 1h;
Stage #2: N-phenylacetoacetamide With sodium hydroxide; sodium acetate; acetic acid In water at 25 - 90℃; for 2.5h; pH=6;
Stage #1: 4-methyl-2-nitroaniline With hydrogenchloride In water at 75 - 80℃; for 1h;
Stage #2: With sodium nitrite In water at 0 - 5℃; for 0.75h;
Stage #3: N-phenylacetoacetamide Further stages;
edaravone
89-25-8

edaravone

4-methyl-2-nitroaniline
89-62-3

4-methyl-2-nitroaniline

pigment orange 6

pigment orange 6

Conditions
ConditionsYield
Stage #1: 4-methyl-2-nitroaniline With hydrogenchloride; sodium nitrite In water at 20℃; for 0.333333h;
Stage #2: 3-methyl-1-phenylpyrazolin-5-(4H)-one In water at 20℃; for 0.166667h;
99%
2'-methoxyacetoacetanilide
92-15-9

2'-methoxyacetoacetanilide

4-methyl-2-nitroaniline
89-62-3

4-methyl-2-nitroaniline

pigment yellow 203

pigment yellow 203

Conditions
ConditionsYield
Stage #1: 4-methyl-2-nitroaniline With hydrogenchloride; sodium nitrite In water at 20℃; for 0.333333h;
Stage #2: 2'-methoxyacetoacetanilide In water at 20℃; for 1h;
99%
β-naphthol
135-19-3

β-naphthol

4-methyl-2-nitroaniline
89-62-3

4-methyl-2-nitroaniline

((4-methyl-2-nitrophenyl)azo)-2-naphthol
2425-85-6

((4-methyl-2-nitrophenyl)azo)-2-naphthol

Conditions
ConditionsYield
Stage #1: 4-methyl-2-nitroaniline With hydrogenchloride; sodium nitrite In water at 20℃; for 0.333333h;
Stage #2: β-naphthol In water at 60℃; for 1h; Temperature;
99%
Stage #1: 4-methyl-2-nitroaniline With hydrogenchloride; sodium nitrite In water at 20℃; for 0.333333h; Green chemistry;
Stage #2: β-naphthol In water at 60℃; for 1h; Green chemistry;
99%
3-methyl-1-phenylpyrazolin-5(4H)-one
19735-89-8

3-methyl-1-phenylpyrazolin-5(4H)-one

4-methyl-2-nitroaniline
89-62-3

4-methyl-2-nitroaniline

pigment orange 6

pigment orange 6

Conditions
ConditionsYield
Stage #1: 4-methyl-2-nitroaniline With hydrogenchloride; sodium nitrite In water at 20℃; for 0.333333h; Green chemistry;
Stage #2: 3-methyl-1-phenylpyrazolin-5(4H)-one In water at 20℃; for 0.166667h; Green chemistry;
99%
methanol
67-56-1

methanol

4-methyl-2-nitroaniline
89-62-3

4-methyl-2-nitroaniline

5-methylbenzimidazole
614-97-1

5-methylbenzimidazole

Conditions
ConditionsYield
With palladium with copper supported on alumina In water at 179.84℃; under 26252.6 Torr; for 12h; Autoclave;98.7%
4-methyl-2-nitroaniline
89-62-3

4-methyl-2-nitroaniline

2-bromo-4-methyl-6-nitroaniline
827-24-7

2-bromo-4-methyl-6-nitroaniline

Conditions
ConditionsYield
With bromine; acetic acid for 0.5h;98%
Stage #1: 4-methyl-2-nitroaniline In acetic acid at 50℃;
Stage #2: With bromine for 0.5h;
98%
With bromine; acetic acid at 20℃; for 1h;98%
4-(5-chloro-2-methoxybenzamido-N-methylene)benzene sulfonyl chloride

4-(5-chloro-2-methoxybenzamido-N-methylene)benzene sulfonyl chloride

4-methyl-2-nitroaniline
89-62-3

4-methyl-2-nitroaniline

5-chloro-2-methoxy-N-[(N-2-nitro-4-methylphenyl-4-sulfamoyl)benzyl]benzamide

5-chloro-2-methoxy-N-[(N-2-nitro-4-methylphenyl-4-sulfamoyl)benzyl]benzamide

Conditions
ConditionsYield
With sodium carbonate In dichloromethane; water at 20℃; for 24h;98%
1-allyloxy-2-iodobenzene
24892-63-5

1-allyloxy-2-iodobenzene

4-methyl-2-nitroaniline
89-62-3

4-methyl-2-nitroaniline

C16H16N2O3

C16H16N2O3

Conditions
ConditionsYield
With potassium phosphate; silver hexafluoroantimonate; chloro[di(1-adamantyl)-2-dimethylaminophenylphosphine]gold(I) In 1,2-dichloro-ethane at 80℃; chemoselective reaction;98%
ethanol
64-17-5

ethanol

4-methyl-2-nitroaniline
89-62-3

4-methyl-2-nitroaniline

2,5-dimethylbenzimidazole
1792-41-2

2,5-dimethylbenzimidazole

Conditions
ConditionsYield
With palladium with copper supported on alumina In water at 179.84℃; under 26252.6 Torr; for 12h; Autoclave;97.5%
With TiO2-P25 nanoparticles In acetonitrile for 3h; UV-irradiation;
propan-1-ol
71-23-8

propan-1-ol

4-methyl-2-nitroaniline
89-62-3

4-methyl-2-nitroaniline

2-ethyl-5-methyl-1H-benzo[d]imidazole
30411-81-5

2-ethyl-5-methyl-1H-benzo[d]imidazole

Conditions
ConditionsYield
With palladium with copper supported on alumina In water at 179.84℃; under 26252.6 Torr; for 12h; Autoclave;97.5%
4-methyl-2-nitroaniline
89-62-3

4-methyl-2-nitroaniline

4-methyl-1,2-diaminobenzene
496-72-0

4-methyl-1,2-diaminobenzene

Conditions
ConditionsYield
With hydrogen; nickel In methanol at 65 - 75℃; for 1h; Autoclave; Inert atmosphere;97%
With aluminum oxide; hydrazine hydrate; iron(III) chloride at 111℃; for 0.1h; Irradiation; microwave;96%
With hydrazine hydrate In ethanol at 70℃; for 4h; chemoselective reaction;94%
4-methyl-2-nitroaniline
89-62-3

4-methyl-2-nitroaniline

2,3-dibromo-5-methylnitrobenzene
73557-63-8

2,3-dibromo-5-methylnitrobenzene

Conditions
ConditionsYield
With tert.-butylnitrite; bromine; copper(ll) bromide In acetonitrile at 50℃; for 0.5h;97%
Multi-step reaction with 2 steps
1: water; bromine
View Scheme
2-chloro-4,6-dimethylquinoline
3913-18-6

2-chloro-4,6-dimethylquinoline

4-methyl-2-nitroaniline
89-62-3

4-methyl-2-nitroaniline

4,6-dimethyl-2-(4-methyl-2-nitroanilino)quinoline
158470-92-9

4,6-dimethyl-2-(4-methyl-2-nitroanilino)quinoline

Conditions
ConditionsYield
at 150 - 160℃; for 10h;97%
acrylic acid methyl ester
292638-85-8

acrylic acid methyl ester

4-methyl-2-nitroaniline
89-62-3

4-methyl-2-nitroaniline

methyl (E)-3-(4′-methyl-2′-nitrophenyl)acrylate
99843-45-5

methyl (E)-3-(4′-methyl-2′-nitrophenyl)acrylate

Conditions
ConditionsYield
Stage #1: 4-methyl-2-nitroaniline With tert.-butylnitrite In methanol at 0℃; for 0.5h;
Stage #2: acrylic acid methyl ester With methanesulfonic acid; palladium diacetate In methanol at 0 - 25℃; Heck-Matsuda reaction;
97%
With palladium diacetate; toluene-4-sulfonic acid In methanol at 60℃; for 1.5h; Inert atmosphere;77%
Stage #1: 4-methyl-2-nitroaniline With methanesulfonic acid In methanol at 25℃;
Stage #2: With tert.-butylnitrite In methanol at 25℃; for 0.00833333h;
Stage #3: acrylic acid methyl ester With palladium diacetate In tetrahydrofuran; methanol at 25 - 40℃; for 0.278333h; Reagent/catalyst; Time;
75%
With tert.-butylnitrite In methanol at 25℃; for 24h; chemoselective reaction;71%
3-chloro-2,4-dimethoxypyridine

3-chloro-2,4-dimethoxypyridine

4-methyl-2-nitroaniline
89-62-3

4-methyl-2-nitroaniline

C14H15N3O4

C14H15N3O4

Conditions
ConditionsYield
With potassium phosphate; tris-(dibenzylideneacetone)dipalladium(0); C35H38NO4P In 1,4-dioxane at 100℃; for 18h;97%
chloroacetyl chloride
79-04-9

chloroacetyl chloride

4-methyl-2-nitroaniline
89-62-3

4-methyl-2-nitroaniline

2-chloro-N-(4-methyl-2-nitrophenyl)acetamide
72196-97-5

2-chloro-N-(4-methyl-2-nitrophenyl)acetamide

Conditions
ConditionsYield
In N,N-dimethyl-formamide Cooling with ice;96%
With benzene
With triethylamine In dichloromethane at 20℃; for 24h;
benzyl bromide
100-39-0

benzyl bromide

4-methyl-2-nitroaniline
89-62-3

4-methyl-2-nitroaniline

4-methyl-2-nitro-N-benzylaniline
22019-66-5

4-methyl-2-nitro-N-benzylaniline

Conditions
ConditionsYield
In water at 100℃; for 1.5h;96%
With pyridine In dichloromethane for 16h; Reflux;90.3%
With potassium carbonate In N,N-dimethyl-formamide at 110 - 120℃; for 4h;
In water at 110℃; Sealed tube;
1,2-di(4-methylphenyl)-1,2-ethanedione
3457-48-5

1,2-di(4-methylphenyl)-1,2-ethanedione

4-methyl-2-nitroaniline
89-62-3

4-methyl-2-nitroaniline

6-methyl-2,3-di-p-tolylquinoxaline
16107-87-2

6-methyl-2,3-di-p-tolylquinoxaline

Conditions
ConditionsYield
With tin(ll) chloride In ethanol; water for 0.333333h; Reflux;96%
2-hydroxy-6,6-dimethyl-4-oxo-cyclohex-2-enecarboxylic acid ethyl ester
300680-16-4

2-hydroxy-6,6-dimethyl-4-oxo-cyclohex-2-enecarboxylic acid ethyl ester

4-methyl-2-nitroaniline
89-62-3

4-methyl-2-nitroaniline

C18H21N3O6

C18H21N3O6

Conditions
ConditionsYield
Stage #1: 4-methyl-2-nitroaniline With hydrogenchloride; sodium nitrite In water at 0℃; for 1h;
Stage #2: 2-hydroxy-6,6-dimethyl-4-oxo-cyclohex-2-enecarboxylic acid ethyl ester With sodium hydroxide In water for 3h; pH=7.5 - 9;
95.4%
Stage #1: 4-methyl-2-nitroaniline With hydrogenchloride; sodium nitrite In water at 0℃; for 1h;
Stage #2: 2-hydroxy-6,6-dimethyl-4-oxo-cyclohex-2-enecarboxylic acid ethyl ester With sodium hydroxide In water for 3h; pH=7.5 - 9; Alkaline aqueous solution;
95.4%
orthoformic acid triethyl ester
122-51-0

orthoformic acid triethyl ester

4-methyl-2-nitroaniline
89-62-3

4-methyl-2-nitroaniline

5-methylbenzimidazole
614-97-1

5-methylbenzimidazole

Conditions
ConditionsYield
With 10% Pd/C; hydrogen; acetic acid In methanol at 20℃; under 760.051 Torr; for 8h;95%
carbon dioxide
124-38-9

carbon dioxide

4-methyl-2-nitroaniline
89-62-3

4-methyl-2-nitroaniline

5-methylbenzimidazole
614-97-1

5-methylbenzimidazole

Conditions
ConditionsYield
With palladium 10% on activated carbon; phenylsilane; 1,3,4,6,7,8-hexahydro-2H-pyrimido[1,2-a]pyrimidine In acetonitrile at 70℃; under 7500.75 Torr; for 15h;95%
With dimethylamine borane; potassium carbonate In ethanol; water under 15001.5 Torr; for 18h; Catalytic behavior; Autoclave;87%
benzaldehyde
100-52-7

benzaldehyde

4-methyl-2-nitroaniline
89-62-3

4-methyl-2-nitroaniline

5-methyl-2-phenyl-1H-1,3-benzimidazole
2963-65-7

5-methyl-2-phenyl-1H-1,3-benzimidazole

Conditions
ConditionsYield
With hydrogen In ethyl acetate at 60℃; under 7500.75 Torr; for 20h; Autoclave; Green chemistry;95%
benzaldehyde
100-52-7

benzaldehyde

4-methyl-2-nitroaniline
89-62-3

4-methyl-2-nitroaniline

4-methyl-2-nitro-N-benzylaniline
22019-66-5

4-methyl-2-nitro-N-benzylaniline

Conditions
ConditionsYield
Stage #1: benzaldehyde; 4-methyl-2-nitroaniline With sodium tris(acetoxy)borohydride; acetic acid In dichloromethane at 20℃; for 1h;
Stage #2: With sodium hydrogencarbonate In water; ethyl acetate
94%
Triethyl orthoacetate
78-39-7

Triethyl orthoacetate

4-methyl-2-nitroaniline
89-62-3

4-methyl-2-nitroaniline

2,5-dimethylbenzimidazole
1792-41-2

2,5-dimethylbenzimidazole

Conditions
ConditionsYield
With 10% Pd/C; hydrogen; acetic acid In methanol at 20℃; under 760.051 Torr;94%
4-methyl-2-nitroaniline
89-62-3

4-methyl-2-nitroaniline

2.3-butanediol
513-85-9

2.3-butanediol

2,3,6-trimethylquinoxaline
17635-21-1

2,3,6-trimethylquinoxaline

Conditions
ConditionsYield
With sodium hydroxide In toluene at 120℃; for 3h; Inert atmosphere; Sealed tube; Green chemistry;94%

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