Located in Hangzhou National Hi-Tech Industrial Development Zone, zhongqichem is a technical company mainly focus on the Custom synthesis, manufacturing, sales of chemicals to various industries. Benefiting from the outstanding customer service and
Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
Cas:1192-62-7
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inquiryProduct description: Product name 2-Acetylfuran CAS number 1192-62-7 Assay ≥99% Appearance Yellowish liquid or solid Capacity 500mt/year Application Flavor and pharmaceutical
Cas:1192-62-7
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
Cas:1192-62-7
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inquiryCangzhou Enke Pharma Tech Co.,ltd. is located in Cangzhou City, Hebei province ,where is a famous petroleum chemical industry city in China. Enke Pharma a high-tech enterprise ,and we are dedicated to developing and manufacturing new ap
1、Our factory passed ISO 9001, ISO 14001, ISO 22000 system certification; HALAL 、KOSHER、FCC AND FDA certificate are available. We can provide customers with better prices, and the supply is stable. 2、We founded in 2004,10% of the staff have more tha
Cas:1192-62-7
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inquiryColorcom is a global leader in industrial chemical manufacturing and is continuously innovating and transforming to exceed client expectations and industry standards. Colorcom prides itself on superior customer and technical focus, while focusing on
As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem’s R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis
Cas:1192-62-7
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inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Our company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O
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inquiryOur Advantage Rich Experience Our products are sold all over Europe,North&South America, Sino-East, Asia and pacific area as well as Africa,we establish long term. Quality service Company cooperates with research institutes. We strictly con
Cas:1192-62-7
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:1192-62-7
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inquiryAdvantage : LIDE PHARMACEUTICALS LTD. is a mid-small manufacturing-type enterprise, engaged in pharmaceutical intermediates of R&D, custom-made and production, and also involving trading chemicals for export. We have established the R&
Cas:1192-62-7
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inquiryProduct Name 2-Acetylfuran CAS 1192-62-7 Appearance Colorless liquid Appearance:Colorless to yellowish liquid Storage: Preserve in well-closed, light-resistan
1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
Cas:1192-62-7
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inquiryWe are the manufacturers and suppliers of API in China, and warehouse in Germany and USA of California, which can quickly and safely deliver to your address 1.High quality and competitive price. 2.Free sample for your evaluation. 3.Promptly delivery
Cas:1192-62-7
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Type:Trading Company
inquiryProduct Name: 2-Acetylfuran CAS: 1192-62-7 MF: C6H6O2 MW: 110.11 EINECS: 214-757-1 Mol File: 1192-62-7.mol 2-Acetylfuran Structure 2-Acetylfuran Chemical Properties Melting point 26-28 °C(lit.) Boiling point 67 °C1
Packing: According to customer requirements Delivery time: In stock or depands Port of shipment: Ningbo/Shanghai/Qingdao OEM/ODM:Welcome Sample:We can offer our existing samples at once Appearance:light yello powder / Refer to COA Storage:2-8°C
Our company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At present
Cas:1192-62-7
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Type:Trading Company
inquiry2-Acetylfuran CAS:1192-62-7 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermediate
Cas:1192-62-7
Min.Order:1 Gram
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Hebei yanxi chemical co., LTD who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do research and developmen
Cas:1192-62-7
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Type:Trading Company
inquiry1. Timely and efficient service to ensure communication with customers 2. Produce products of different specifications and sizes according to your requirements. 3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures s
Cas:1192-62-7
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Type:Lab/Research institutions
inquiry2-Acetyl furan CAS: 1192-62-7 Specification Item Standard Structural data confirmation 1.H-NMR: The data of structure are identical with reference standard 2.HPLC/GC-MS: Ensur
Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
Donglian as a factory and supplier of aroma chemicals in China, We can provide different quantities of custom synthesis chemicals in food flavor scale more than fourteen years.in addition, our company has researched and developed four series
1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists of highly qualifie
Cas:1192-62-7
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:1192-62-7
Min.Order:0 Metric Ton
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Type:Lab/Research institutions
inquiryConditions | Yield |
---|---|
With indium(III) triflate; lithium perchlorate In nitromethane at 20℃; | 99% |
With scandium tris(trifluoromethanesulfonate) In acetonitrile for 0.25h; Friedel-Crafts Acylation; Inert atmosphere; Microwave irradiation; Heating; Green chemistry; | 99% |
With nano-sulfated titania at 50℃; for 40h; Friedel Crafts acylation; neat (no solvent); | 95% |
Conditions | Yield |
---|---|
With methanesulfonic acid; oxygen; palladium diacetate; [(NH4)5H6PMo4V7.8O40]*xH2O; sodium chloride In methanol; water at 20℃; for 3.5h; | 98.2% |
With tert.-butylhydroperoxide; C21H19N5Pd(2+)*2BF4(1-) In decane; acetonitrile at 45℃; for 12h; Wacker Oxidation; | 90% |
With dihydrogen peroxide In water; acetonitrile at 55℃; for 12h; Wacker Oxidation; | 80% |
Conditions | Yield |
---|---|
With methanesulfonic acid; pyrographite at 0 - 10℃; for 0.333333h; Friedel-Crafts acylation; | 98% |
With pyrographite; toluene-4-sulfonic acid at 20℃; for 0.5h; Friedel-Crafts reaction; | 97% |
With trifluoroacetic anhydride; Duolite ES 467 H+ phosphonic resin In nitromethane at 25℃; for 0.5h; | 95% |
Conditions | Yield |
---|---|
With nickel(II) triflate; cyclohexanone; 1,2-bis-(dicyclohexylphosphino)ethane In toluene at 110℃; for 12h; Schlenk technique; | 98% |
With oxygen; sodium hydride In tetrahydrofuran at 0 - 20℃; for 6h; | 97% |
With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; potassium tert-butylate; copper(I) triflate; 5-[(2S)-pyrrolidine-2-yl]-1H-tetrazole In N,N-dimethyl-formamide at 25℃; for 0.5h; Catalytic behavior; | 97% |
Conditions | Yield |
---|---|
With manganese triacetate In benzene for 2h; Heating; | 94% |
Conditions | Yield |
---|---|
With zinc trifluoromethanesulfonate at 25 - 100℃; for 3h; Reagent/catalyst; Temperature; | 94% |
Conditions | Yield |
---|---|
With manganese triacetate In benzene for 2h; Heating; | 93% |
Conditions | Yield |
---|---|
With hydrogenchloride; methyllithium | 92% |
Conditions | Yield |
---|---|
With potassium hydroxide In dimethyl sulfoxide at 20 - 35℃; for 2.5h; Etherification; Alkylation; Hydrolysis; | A 12.1% B 87% |
Conditions | Yield |
---|---|
With [BPy][BF4]; ytterbium(III) triflate at 50℃; for 3h; Friedel-Crafts acylation; | 87% |
With zinc trifluoromethanesulfonate In nitromethane at 20℃; for 4h; Friedel-Crafts acylation; | 85% |
1-(2-furyl)-1-ethanone
Conditions | Yield |
---|---|
With 4Na(1+)*6H(1+)*NiMo6O24(10-)=Na4H6NiMo6O24; oxygen In water; acetonitrile at 20℃; under 760.051 Torr; for 12h; Irradiation; | 86% |
With (NH4)4[ZnMo6O18(OH)6]; oxygen In water; acetonitrile at 60℃; under 760.051 Torr; for 12h; | 85% |
1-(2-furyl)-1-ethanone
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide In methanol; water Heating; | 85% |
Conditions | Yield |
---|---|
With methyllithium; lithium bromide In tetrahydrofuran; diethyl ether at -78℃; for 0.25h; | 83% |
Conditions | Yield |
---|---|
With FeH6Mo6O24(3-)*3H3N*3H(1+)*7H2O; tetrabutylammomium bromide; dihydrogen peroxide In 1,4-dioxane at 70℃; for 24h; | 83% |
With tert.-butylhydroperoxide; phosphomolybdic acid; copper diacetate In water; acetonitrile at 90℃; | 66% |
With tert.-butylhydroperoxide; phosphomolybdic acid; copper(II) acetate monohydrate In water; acetonitrile at 90℃; for 10h; Sealed tube; | 66% |
With tert.-butylhydroperoxide In water; acetonitrile at 25℃; for 30h; UV-irradiation; | 65% |
With oxygen; Langlois reagent In acetonitrile at 25℃; under 760.051 Torr; for 12h; Irradiation; Green chemistry; | 51 %Chromat. |
2-ethynylfuran
1-(2-furyl)-1-ethanone
Conditions | Yield |
---|---|
With Perfluorooctanesulfonic acid; C8AgF17O3S*H2O In water at 100℃; for 8h; Darkness; regioselective reaction; | 80% |
With silver tetrafluoroborate; water In acetic acid at 110℃; for 10h; regioselective reaction; | 76% |
1-(2-furyl)-1-(trimethylsilyloxy)ethylene
A
1-(2-furyl)-1-ethanone
B
2-chloroacetylfuran
C
2,2‐dichloro‐1‐(furan‐2‐yl)ethan‐1‐one
Conditions | Yield |
---|---|
With tert-butylhypochlorite; silica gel In hexane at 0℃; for 1h; | A 10 % Chromat. B 77% C 10 % Chromat. D 1 % Chromat. |
Conditions | Yield |
---|---|
trans benzyl(chloro)bis(triphenylphosphine)palladium(II) In benzene for 0.5h; Ambient temperature; | 70% |
Conditions | Yield |
---|---|
With PPA at 60 - 80℃; for 2h; Acylation; Friedel-Crafts acylation; | 70% |
palladium diacetate
saccharin
ethyl-diphenyl-phosphane
1-(2-furyl)-1-ethanone
Conditions | Yield |
---|---|
Stage #1: palladium diacetate; saccharin In water; acetonitrile at 20℃; for 0.5h; Stage #2: ethyl-diphenyl-phosphane In methanol; water; acetonitrile Reflux; | 66% |
2-N-methylanilinoacetylfuran
A
1-(2-furyl)-1-ethanone
B
1,3-diphenylimidazolidine
C
3-(2-furyl)-1-phenylazetidin-3-ol
Conditions | Yield |
---|---|
In diethyl ether for 3h; Irradiation; | A 13% B 9% C 45% |
(1-(furan-2-yl)ethoxy)trimethylsilane
1-(2-furyl)-1-ethanone
Conditions | Yield |
---|---|
With 2,3-dicyano-5,6-dichloro-p-benzoquinone In dichloromethane; acetonitrile for 3h; Irradiation; | 43% |
Conditions | Yield |
---|---|
With trifluorormethanesulfonic acid at 80℃; Inert atmosphere; | 39% |
1-(2,5-dimethoxy-2,5-dihydrofuran-2-yl)ethanol from 2-Acetylfuran
1-(2-furyl)-1-ethanone
Conditions | Yield |
---|---|
at 130℃; for 2h; | 26% |
Conditions | Yield |
---|---|
With diethyl ether |
methyl magnesium iodide
Brenzschleimsaeurenitril
1-(2-furyl)-1-ethanone
Conditions | Yield |
---|---|
With diethyl ether |
Conditions | Yield |
---|---|
With sulfuric acid |
1-(2-furyl)ethanol
A
1-(2-furyl)-1-ethanone
B
(R)-(+)-1-(2-furyl)ethanol
Conditions | Yield |
---|---|
With baker's yeast; pH 5 phosphate buffer In 1,2-dimethoxyethane at 32℃; for 192h; kinetic resolution of other 1-substituted ethanols with Baker's yeast; other solvents, time; | A 79 % Chromat. B 21 % Chromat. |
In 1,2-dimethoxyethane at 32℃; for 192h; Baker's yeast, pH 5 phosphate buffer; | A 79 % Chromat. B 21 % Chromat. |
In 1,2-dimethoxyethane at 32℃; for 168h; Baker's yeast, pH 5 phosphate buffer; | A 68 % Chromat. B 32 % Chromat. |
Conditions | Yield |
---|---|
With lanthanum(lll) triflate 1.) THF, -78 deg C then up to 0 deg C, 2.) -78 up to 0 deg C, 30 min; Yield given. Multistep reaction; |
2-(furan-2-yl)pent-4-en-2-ol
1-(2-furyl)-1-ethanone
Conditions | Yield |
---|---|
at 500℃; Product distribution; flash thermolysis; |
1-(2-furyl)-1-ethanone
ethyl trifluoroacetate,
4,4,4-trifluoro-1-(2-furanyl)-1,3-butanedione
Conditions | Yield |
---|---|
Stage #1: 1-(2-furyl)-1-ethanone; ethyl trifluoroacetate, With lithium hexamethyldisilazane In tetrahydrofuran at 0 - 20℃; Stage #2: With hydrogenchloride In water; ethyl acetate | 100% |
With sodium In ethanol at 20℃; | 82.6% |
With potassium tert-butylate In benzene for 15h; Ambient temperature; | 54% |
1-(2-furyl)-1-ethanone
(R)-(+)-1-(2-furyl)ethanol
Conditions | Yield |
---|---|
With formic acid; C38H40ClN2O2RhS; triethylamine In neat (no solvent) at 24 - 30℃; for 8h; Reagent/catalyst; Inert atmosphere; enantioselective reaction; | 100% |
With dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; sodium formate; (R,R)-N-(p-toluenesulfonyl)-1,2-diphenylethylenediamine In water at 40℃; for 1.5h; enantioselective reaction; | 99% |
With dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; sodium formate; 4-methyl-N-((1R,2R)-2-{[(4-methylphenyl)sulfonyl]amino}-1,2-diphenylethyl)benzenesulfonamide In water at 40℃; for 1.5h; enantioselective reaction; | 99% |
pyridine
1-(2-furyl)-1-ethanone
1-(2-furan-2-yl-2-oxo-ethyl)-pyridinium iodide
Conditions | Yield |
---|---|
With iodine | 100% |
With iodine at 140℃; for 3h; | 100% |
With iodine at 140℃; for 3h; | 100% |
Conditions | Yield |
---|---|
With hydroxylamine hydrochloride; sodium acetate In ethanol; water Reflux; | 100% |
With hydroxylamine hydrochloride; sodium acetate In ethanol; water Heating; | |
With hydroxylamine hydrochloride; sodium acetate In ethanol; water Reflux; |
1-(2-furyl)-1-ethanone
2-Hydroxybenzoylhydrazine
(E)-N'-(1-(furan-2-yl)ethylidene)-2-hydroxybenzohydrazide
Conditions | Yield |
---|---|
at 194℃; under 4650.47 Torr; for 0.0416667h; Microwave irradiation; neat (no solvent); | 100% |
Conditions | Yield |
---|---|
With sodium hydroxide at 20℃; for 24h; | 100% |
With sodium hydroxide In methanol; water at 15 - 20℃; for 15h; Claisen-Schmidt Condensation; | 90% |
With lithium hydroxide monohydrate In ethanol at 40℃; for 7h; Claisen-Schmidt Condensation; | 15% |
With sodium hydroxide In ethanol at 25℃; for 3h; | |
With potassium hydroxide In ethanol at 20℃; |
1-(2-furyl)-1-ethanone
oxalic acid diethyl ester
ethyl 4-(furan-2-yl)-2,4-dioxobutyrate
Conditions | Yield |
---|---|
99% | |
With potassium tert-butylate In tetrahydrofuran; 1,2-dimethoxyethane at 0 - 20℃; for 1h; | 88% |
With potassium tert-butylate In tetrahydrofuran; 1,2-dimethoxyethane for 3h; Knoevenagel Condensation; | 70% |
1-(2-furyl)-1-ethanone
benzaldehyde
1-(2-furyl)-3-phenylpropen-1-one
Conditions | Yield |
---|---|
With potassium fluoride modified clay In methanol at 20℃; for 0.333333h; Catalytic behavior; Solvent; Claisen-Schmidt Condensation; | 99% |
With potassium hydroxide In water at 20℃; for 4h; Claisen-Schmidt Condensation; | 87% |
With sodium hydroxide In ethanol; water at 20℃; | 87% |
Conditions | Yield |
---|---|
With ethanol; (ethylenebis(bicyclohexylphosphane))Ni(cis,cis-1,5-cyclooctadiene) In neat (no solvent) at 130℃; for 36h; Catalytic behavior; | 99% |
With sodium tetrahydroborate In methanol at 0℃; | 98% |
Stage #1: 1-(2-furyl)-1-ethanone With n-butyllithium; 1-(2-hydroxyethyl)-3-methyl-1H-imidazol-3-ium trifluoromethanesulfonate; iron(II) acetate In tetrahydrofuran at 65℃; for 1h; Inert atmosphere; Stage #2: With water; sodium hydroxide In tetrahydrofuran; methanol at 20℃; for 2h; Inert atmosphere; | 98% |
1-(2-furyl)-1-ethanone
(S)-1-(2-furanyl)ethanol
Conditions | Yield |
---|---|
diethylzinc; (+)-N,N'-Bis<(R)-1-phenylethyl>-1,2-ethylendiamin | 99% |
With formic acid; [RuCl2(hexamethylbenzene)]2; (S)-2-piperidinemethanethiol hydrochloride; triethylamine at 30℃; for 24h; Inert atmosphere; optical yield given as %ee; enantioselective reaction; | 99% |
With formic acid; [RuCl2(hexamethylbenzene)]2; (S)-2-piperidinemethanethiol hydrochloride; triethylamine at 30℃; for 24h; Inert atmosphere; optical yield given as %ee; enantioselective reaction; | 99% |
Conditions | Yield |
---|---|
With montmorillonite K10 In acetone at 20℃; for 0.833333h; Catalytic behavior; Green chemistry; | 99% |
With [(3,5-di-tert-Bu,2-OH)-C6H2-CH=N-CH2]2*Ti(O-i-Pr)4; N,N-dimethylaniline N-oxide In dichloromethane at 23℃; for 25h; | 94% |
phosphotungstic acid at 20℃; | 93% |
Conditions | Yield |
---|---|
With hydrogen In water at 160℃; under 30003 Torr; for 2.5h; Autoclave; | 99% |
With hydrogen In water at 160℃; under 30003 Torr; for 2.5h; Autoclave; | 82% |
With water; hydrogen at 160℃; under 30003 Torr; for 4h; Autoclave; |
Conditions | Yield |
---|---|
In diethyl ether at 10 - 20℃; for 1h; Inert atmosphere; | 99% |
1-(2-furyl)-1-ethanone
2-iodo-5-methoxybenzaldehyde
Conditions | Yield |
---|---|
Stage #1: 1-(2-furyl)-1-ethanone With sodium hydroxide In ethanol; water at 0℃; for 0.0833333h; Inert atmosphere; Stage #2: 2-iodo-5-methoxybenzaldehyde In ethanol; water at 10℃; Inert atmosphere; | 99% |
Stage #1: 1-(2-furyl)-1-ethanone With sodium hydroxide In ethanol; water at 0℃; for 0.0833333h; Stage #2: 2-iodo-5-methoxybenzaldehyde In ethanol; water at 0 - 10℃; | 99% |
Conditions | Yield |
---|---|
With potassium carbonate; 1,3-bis(mesityl)imidazolium chloride In N,N-dimethyl acetamide at 80℃; for 6h; | 99% |
1-(2-furyl)-1-ethanone
4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane
Conditions | Yield |
---|---|
With C84H110N10Zn2 In neat (no solvent) at 20℃; for 6h; Sealed tube; Inert atmosphere; Schlenk technique; Glovebox; | 99% |
at 140℃; for 2.5h; | 98% |
With C44H60N5PrSi2 In chloroform-d1 at 20℃; for 0.133333h; Inert atmosphere; | 90 %Spectr. |
1-(2-furyl)-1-ethanone
ketene t-butyldimethylsilyl methyl acetal
Conditions | Yield |
---|---|
Stage #1: 1-(2-furyl)-1-ethanone With bis(trifluoromethanesulfonyl)amide In diethyl ether at -78 - 23℃; Mukaiyama Aldol Addition; Schlenk technique; Inert atmosphere; Stage #2: ketene t-butyldimethylsilyl methyl acetal In diethyl ether at -20℃; for 0.5h; Mukaiyama Aldol Addition; Schlenk technique; Inert atmosphere; | 99% |
1-(2-furyl)-1-ethanone
1-Bromonaphthalene
1-(furan-2-yl)-2-(naphthalen-1-yl)ethan-1-one
Conditions | Yield |
---|---|
With methanesulfonic acid(2-dicyclohexylphosphino-2′,4′,6′-triisopropyl-1,1′-biphenyl)[2-(2′-amino-1,1′-biphenyl)]palladium(II); sodium t-butanolate In tetrahydrofuran at 80℃; Inert atmosphere; | 99% |
Conditions | Yield |
---|---|
With methanesulfonic acid(2-dicyclohexylphosphino-2′,4′,6′-triisopropyl-1,1′-biphenyl)[2-(2′-amino-1,1′-biphenyl)]palladium(II); sodium t-butanolate In tetrahydrofuran at 80℃; Inert atmosphere; | 99% |
1-(2-furyl)-1-ethanone
para-bromoacetophenone
2‐acetyl‐5‐(4‐acetylphenyl)furan
Conditions | Yield |
---|---|
With potassium acetate; dichloro-[1-(isobutyl)-3-(benzyl)benzimidazole-2-ylidene](pyridine)palladium(II) In N,N-dimethyl acetamide at 150℃; for 2h; Reagent/catalyst; Inert atmosphere; Schlenk technique; regioselective reaction; | 99% |
With tetrabromo[1,1'-butylene-3,3'-bis(N-2-(diisopropylaminoethyl)benzimidazol-2-ylidene)]dipyridinedipalladium(II); potassium acetate In N,N-dimethyl acetamide at 120℃; for 2h; Reagent/catalyst; Inert atmosphere; Schlenk technique; | 92% |
With cis-[Pd(saccharine)2(PPhEt2)2]; potassium acetate In N,N-dimethyl acetamide at 120℃; for 2h; Catalytic behavior; Reagent/catalyst; Schlenk technique; Inert atmosphere; | 98 %Chromat. |
With trans‐dibromo[1‐(2,2‐diethoxyethyl)‐3‐(3,5‐di‐tert‐butylbenzyl)benzimidazole‐2‐ylidene]‐(pyridine)‐palladium(II); potassium acetate In N,N-dimethyl acetamide at 120℃; for 2h; Reagent/catalyst; Schlenk technique; | 80 %Chromat. |
With potassium acetate; dibromo[1‑(4‑phenoxybutyl)‑3‑(2,3,5,6‑tetramethylbenzyl)imidazolidin‑2‑ylidene](pyridine)palladium(II) In N,N-dimethyl acetamide at 120℃; for 2h; Catalytic behavior; Reagent/catalyst; Inert atmosphere; | 97 %Chromat. |
Conditions | Yield |
---|---|
With C84H110N10Zn2 In neat (no solvent) at 20℃; for 12h; Sealed tube; Inert atmosphere; Schlenk technique; Glovebox; | 99% |
1-(2-furyl)-1-ethanone
benzaldehyde
(E)-1-(furan-2-yl)-3-phenylprop-2-en-1-one
Conditions | Yield |
---|---|
With sodium hydroxide at 20℃; for 15h; | 98% |
With 4 A molecular sieve; NAP-MgO In toluene for 18h; Claisen-Schmidt condensation; Heating; | 97% |
With fly-ash:H2SO4 Aldol condensation; Microwave irradiation; Neat (no solvent); | 95% |
Conditions | Yield |
---|---|
With potassium hydroxide In water; acetonitrile at 60℃; for 2h; | 98% |
1-(2-furyl)-1-ethanone
4-chlorobenzaldehyde
3-(4-chlorophenyl)-1-(furan-2-yl)prop-2-en-1-one
Conditions | Yield |
---|---|
With potassium fluoride modified clay In methanol at 20℃; for 0.333333h; Claisen-Schmidt Condensation; | 98% |
With sodium hydroxide at 20℃; Claisen-Schmidt condensation; Neat (no solvent); Grinding; | 90% |
With sodium hydroxide In methanol; water for 2h; Ambient temperature; | 88% |
1-(2-furyl)-1-ethanone
2-acetylfuran azine
Conditions | Yield |
---|---|
With hydrazine hydrate; acetic acid for 40h; Heating; | 98% |
With hydrazine hydrate; acetic acid In ethanol at 75℃; |
1-(2-furyl)-1-ethanone
triisopropylsilyl trifluoromethanesulfonate
[[1-(2-furyl)ethenyl]oxy]tri-isopropylsilane
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In dichloromethane at 0 - 20℃; | 98% |
With N-ethyl-N,N-diisopropylamine In dichloromethane cooling; |
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