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Dayang Chem (Hangzhou) Co.,Ltd.

As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch

2-Hydroxy-4-methoxybenzophenone-5-sulfonic acid Manufacturer/High quality/Best price/In stock

Cas:4065-45-6

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

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Aecochem Corp.

Benzophenone-4 CAS#4056-45-6 Xiamen Aeco Chemical Industrial Co., Ltd. (short as Aecochem) Your Partner in China, a Professional chemical raw material supplier, our main products including the Epxoy Chemical ,Petro Chemical,Pharma Intermedia

Supply high quality Benzophenone-4

Cas:4065-45-6

Min.Order:0 Metric Ton

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Jinan Finer Chemical Co., Ltd

Product description: Product name 2-Hydroxy-4-methoxybenzophenone-5-sulfonic acid CAS number 4065-45-6 Assay ≥99% Appearance White to yellowish powder Capacity 100mt/year Applic

2-Hydroxy-4-methoxybenzophenone-5-sulfonic acid

Cas:4065-45-6

Min.Order:10 Gram

FOB Price: $12.0

Type:Lab/Research institutions

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Qingdao Jade New Material Technology CO.,Ltd

■POLYMER ADDITIVES JADEWIN BP-4 CHEMICAL COMPONENT COMPONENT 2-Hydroxy-4-methoxybenzophenone-5-sulfonic acid CAS 4065-45-6 Molecular C14H12O6S M.W 308 SPECIFICATION AND PHYSICAL PROPERTIES

UV ABSORBER BP-4

Cas:4065-45-6

Min.Order:1 Kilogram

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Type:Trading Company

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Wuhan ZeShanCheng Biomedical Technology Co., Ltd.

UV Absorbers Benzophenone-4 CAS No.:4065-45-6 Other Names:Sulisobenzona MF:C14H12O6S EINECS No.:223-772-2 Grade Standard:Cosmtic Grade Purity:99% Appearance:Light yellow powder Application:raw cosmetic materials Density:1.4±0.1 g/cm3 Boiling

Sulisobenzona

Cas:4065-45-6

Min.Order:0 Metric Ton

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Type:Trading Company

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Simagchem Corporation

Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our

High quality 2-Hydroxy-4-Methoxy-5-Sulphoic Benzophenone Uv284 Bp4 supplier in China

Cas:4065-45-6

Min.Order:1 Kilogram

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Hebei yanxi chemical co.,LTD.

Hebei yanxi chemical co., LTD is a professional research, development and production 2-phenylacetamide enterprise backbone members by local well-known entrepreneurs and professional senior engineers in the party's "low carbon environ

2-Hydroxy-4-methoxybenzophenone-5-sulfonic acid CAS NO.4065-45-6

Cas:4065-45-6

Min.Order:100 Gram

FOB Price: $2.0

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Wuhan Fortuna Chemical Co.,Ltd

Unique advantages Guaranteed purity High quality & competitive price Quality control Fast feedback Prompt shipment Appearance:White or slightly yellow powder Storage:cool dry place Package:1kg/foil bag;25kg/drum Application:UV Absorber Tran

Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Xi'an Xszo Chem Co., Ltd.

1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s

Factory price Cosmetic BENZOPHENONE-4 4065-45-6 Manufacturer

Cas:4065-45-6

Min.Order:1 Gram

FOB Price: $0.1

Type:Manufacturers

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COLORCOM LTD.

Colorcom is a global leader in industrial chemical manufacturing and is continuously innovating and transforming to exceed client expectations and industry standards. Colorcom prides itself on superior customer and technical focus, while focusing on

PEG-120 Methyl Glucose Triisostearate

Cas:4065-45-6

Min.Order:1 Metric Ton

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Type:Manufacturers

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Chemwill Asia Co., Ltd.

Chemwill Asia co.,Ltd is one of the leading manufacturer in CHINA. Product quality, process, price and service 2-Hydroxy-4-methoxybenzophenone-5-sulfonic acid 4065-45-6 Factory PRICE IN STOCK UV 284 COA Benzophenone-4 CAS 4065-45-6 CAS 4065-4

Henan Tianfu Chemical Co., Ltd.

Our company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O

tianfu-chem_UV-284//BP-4,CAS: 4065-45-6

Cas:4065-45-6

Min.Order:1 Kilogram

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Hebei Nengqian Chemical Import and Export Co., LTD

With our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufactu

UV Absorber Benzophenone 4 / UV-284 CAS 4065-45-6

Cas:4065-45-6

Min.Order:1 Kilogram

FOB Price: $1.0 / 10.0

Type:Trading Company

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Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Factory direct supply CAS 4065-45-6 with best quality

Cas:4065-45-6

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

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Henan Sinotech Import&Export Corporation

1. Low MOQ: No worry about the big MOQ. 2. Good Service: Clients are treated as friend. 3. Good Quality: We have strict quality control system .Good reputation in the market. 4. Fast Delivery: Fast response and handling. Appearance:O

2-Hydroxy-4-Methoxy Benzophenone-5-Sulphonic Acid; Benzophenone-4

Cas:4065-45-6

Min.Order:5 Metric Ton

FOB Price: $1.0 / 2.0

Type:Other

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Hangzhou Sartort Biopharma Co., Ltd

Appearance:White powder Storage:Room temperature Package:25kg/drum Application:UV absorber Transportation:Express/Sea/Air Port:Any port in china

Manufacture Benzophenone-4 (BP-4/UV-284) UV ABSORBER

Cas:4065-45-6

Min.Order:1 Kilogram

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Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

2-Hydroxy-4-methoxybenzophenone-5-sulfonic acid 4065-45-6

Cas:4065-45-6

Min.Order:1 Kilogram

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Xi'an Faithful Biotech Co., Ltd.

We are the manufacturers and suppliers of API in China, and warehouse in Germany and USA of California, which can quickly and safely deliver to your address 1.High quality and competitive price. 2.Free sample for your evaluation. 3.Promptly delivery

Qingdao Beluga Import and Export Co., LTD

Beluga chemical professional supply High quality Sulisobenzone CAS 4065-45-6 1. Beluga Chemical has a professional RESEARCH and development team and strong technical force to ensure technical support and research capabilities. 2. Made in China an

High quality Sulisobenzone CAS 4065-45-6

Cas:4065-45-6

Min.Order:1 Gram

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Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

2-Hydroxy-4-methoxybenzophenone-5-sulfonic acid

Cas:4065-45-6

Min.Order:1 Kilogram

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Changchun Artel lmport and Export trade company

Minimum Order Qty. 10 Gram Supply Ability 500 Kilograms/Month Storage store in cool, dry, ventilated place 20℃ Delivery Time 3 business days after payment Payment Term TT,western union,Paypal,MoneyGram Package 10g,20g,50g,100g,500g,1KGS,

2-Hydroxy-4-methoxybenzophenone-5-sulfonic acid CAS NO.4065-45-6

Cas:4065-45-6

Min.Order:10 Gram

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Hubei Jiutian Bio-medical Technology Co., Ltd

1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists

2-Hydroxy-4-methoxybenzophenone-5-sulfonic acid 4065-45-6

Cas:4065-45-6

Min.Order:1 Kilogram

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Hebei Mojin Biotechnology Co.,Ltd

Hebei Mojin Biotechnology Co., Ltd, Our company is a professional in chemical raw materials and chemical reagents research and development production enterprises. Our business covers more than 30 countries, most of the big customers come from Europe,

UV Absorber Bp-4 Benzophenone-4 CAS 4065-45-6 UV-284 Sulisobenzone

Cas:4065-45-6

Min.Order:1 Kilogram

FOB Price: $135.0 / 150.0

Type:Trading Company

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Wuhan Han Sheng New Material Technology Co.,Ltd

Our Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We

Lonwin Chemical Group Limited

2-Hydroxy-4-methoxybenzophenone-5-sulfonic acid CAS: 4065-45-6 Specification Product name 2-Hydroxy-4-methoxybenzophenone-5-sulfonic acid CAS number 4065-45-6 Assay ≥99% Appearance White to yellow

Factory supply 2-Hydroxy-4-methoxybenzophenone-5-sulfonic acid

Cas:4065-45-6

Min.Order:1 Kilogram

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Type:Other

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Leader Biochemical Group

PRODUCT DETAILS 2-Hydroxy-4-methoxybenzophenone-5-sulfonic acid Basic information Produ

China Largest Manufacturer factory Supply ENZOPHENONE-4 CAS 4065-45-6

Cas:4065-45-6

Min.Order:500 Kilogram

FOB Price: $1.0 / 2.0

Type:Lab/Research institutions

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Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

2-Hydroxy-4-methoxybenzophenone-5-sulfonic acid

Cas:4065-45-6

Min.Order:0

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Xiamen Hisunny Chemical Co.,Ltd

Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia

2-Hydroxy-4-Methoxybenzophenone-5-Sulfonic Acid

Cas:4065-45-6

Min.Order:0

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Type:Manufacturers

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Hangzhou Keyingchem Co.,Ltd

Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det

2-Hydroxy-4-methoxybenzophenone-5-sulfonic acid

Cas:4065-45-6

Min.Order:0 Metric Ton

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Synthetic route

Benzophenone-3
131-57-7

Benzophenone-3

2-hydroxy-4-methoxybenzophenone-5-sulfonic acid
4065-45-6

2-hydroxy-4-methoxybenzophenone-5-sulfonic acid

Conditions
ConditionsYield
With sulfur trioxide; acetic acid In 1,2-dichloro-ethane at 25℃; for 3h; Inert atmosphere;98.82%
With chlorosulfonic acid In ethyl acetate at 45℃; Temperature;96%
With chlorosulfonic acid In phthalic acid dimethyl ester
With chlorosulfonic acid at 25℃; for 20h; Inert atmosphere; Autoclave;
4-benzoyloxy-2-methoxybenzenesulfonic acid

4-benzoyloxy-2-methoxybenzenesulfonic acid

2-hydroxy-4-methoxybenzophenone-5-sulfonic acid
4065-45-6

2-hydroxy-4-methoxybenzophenone-5-sulfonic acid

Conditions
ConditionsYield
In methanol at 35℃; for 0.333333h; UVB irradiation;
2-hydroxy-4-methoxybenzophenone-5-sulfonic acid
4065-45-6

2-hydroxy-4-methoxybenzophenone-5-sulfonic acid

chlorobenzene
108-90-7

chlorobenzene

C14H11O6S(1-)*C18H12Cl3S(1+)
817203-48-8

C14H11O6S(1-)*C18H12Cl3S(1+)

Conditions
ConditionsYield
Stage #1: chlorobenzene With thionyl chloride; aluminum (III) chloride at 20 - 150℃; for 5h;
Stage #2: With water at 60℃; for 1h;
Stage #3: 2-hydroxy-4-methoxybenzophenone-5-sulfonic acid In water for 4h;
79%
2-hydroxy-4-methoxybenzophenone-5-sulfonic acid
4065-45-6

2-hydroxy-4-methoxybenzophenone-5-sulfonic acid

3,5-dichloro-2-hydroxy-4-methoxybenzophenone
158547-83-2

3,5-dichloro-2-hydroxy-4-methoxybenzophenone

Conditions
ConditionsYield
With trichloroisocyanuric acid; sodium hydrogencarbonate In water33%
2-hydroxy-4-methoxybenzophenone-5-sulfonic acid
4065-45-6

2-hydroxy-4-methoxybenzophenone-5-sulfonic acid

5-benzoyl-3-chloro-4-hydroxy-2-methoxybenzenesulfonic acid
1631050-95-7

5-benzoyl-3-chloro-4-hydroxy-2-methoxybenzenesulfonic acid

Conditions
ConditionsYield
With hydrogenchloride; sodium hypochlorite In water for 2h; Cooling with ice;18%
2-hydroxy-4-methoxybenzophenone-5-sulfonic acid
4065-45-6

2-hydroxy-4-methoxybenzophenone-5-sulfonic acid

diethyl dicarbonate
1609-47-8

diethyl dicarbonate

2--4-methoxy-5-sulfo-benzophenon
19337-04-3

2--4-methoxy-5-sulfo-benzophenon

2-hydroxy-4-methoxybenzophenone-5-sulfonic acid
4065-45-6

2-hydroxy-4-methoxybenzophenone-5-sulfonic acid

dimethyl sulfate
77-78-1

dimethyl sulfate

sodium 2,4-dimethoxy-5-benzoylbenzenesulfonate

sodium 2,4-dimethoxy-5-benzoylbenzenesulfonate

Conditions
ConditionsYield
With sodium hydroxide Heating;
2-hydroxy-4-methoxybenzophenone-5-sulfonic acid
4065-45-6

2-hydroxy-4-methoxybenzophenone-5-sulfonic acid

5-benzoyl-4-hydroxy-2-methoxy-benzenesulfonyl chloride
121715-18-2

5-benzoyl-4-hydroxy-2-methoxy-benzenesulfonyl chloride

2-[2-[2-chloro-3-[(1,3-dihydro-1,3,3-trimethyl-2H-indol-2-ylidene)ethylidene]-1-cyclohexen-1-yl]ethenyl]-1,3,3-trimethyl-3H-indolium bromide

2-[2-[2-chloro-3-[(1,3-dihydro-1,3,3-trimethyl-2H-indol-2-ylidene)ethylidene]-1-cyclohexen-1-yl]ethenyl]-1,3,3-trimethyl-3H-indolium bromide

2-hydroxy-4-methoxybenzophenone-5-sulfonic acid
4065-45-6

2-hydroxy-4-methoxybenzophenone-5-sulfonic acid

2-[2-[2-chloro-3-[(1,3-dihydro-1,3,3-trimethyl-2H-indol-2-ylidene)ethylidene]-1-cyclohexen-1-yl]ethenyl]-1,3,3-trimethyl-3H-indolium, 2-hydroxy-4-methoxybenzophenone-5-sulfonic acid salt

2-[2-[2-chloro-3-[(1,3-dihydro-1,3,3-trimethyl-2H-indol-2-ylidene)ethylidene]-1-cyclohexen-1-yl]ethenyl]-1,3,3-trimethyl-3H-indolium, 2-hydroxy-4-methoxybenzophenone-5-sulfonic acid salt

Conditions
ConditionsYield
Stage #1: 2-hydroxy-4-methoxybenzophenone-5-sulfonic acid With sodium hydrogencarbonate In 1-methoxy-2-propanol; water
Stage #2: 2-[2-[2-chloro-3-[(1,3-dihydro-1,3,3-trimethyl-2H-indol-2-ylidene)ethylidene]-1-cyclohexen-1-yl]ethenyl]-1,3,3-trimethyl-3H-indolium bromide In 1-methoxy-2-propanol; water at 20℃; for 2.16667h; In the dark;
2-hydroxy-4-methoxybenzophenone-5-sulfonic acid
4065-45-6

2-hydroxy-4-methoxybenzophenone-5-sulfonic acid

3-nitro-aniline
99-09-2

3-nitro-aniline

1-[2-hydroxy-4-methoxy-5-(3-nitrophenylazo)phenyl]-1-phenylmethanone
1243203-31-7

1-[2-hydroxy-4-methoxy-5-(3-nitrophenylazo)phenyl]-1-phenylmethanone

Conditions
ConditionsYield
Stage #1: 3-nitro-aniline With hydrogenchloride In water at 70℃; for 0.5h;
Stage #2: With sodium nitrite In water at 0 - 5℃;
Stage #3: 2-hydroxy-4-methoxybenzophenone-5-sulfonic acid regioselective reaction; Further stages;
10.73 %Chromat.
2-hydroxy-4-methoxybenzophenone-5-sulfonic acid
4065-45-6

2-hydroxy-4-methoxybenzophenone-5-sulfonic acid

2-nitro-aniline
88-74-4

2-nitro-aniline

1-[2-hydroxy-4-methoxy-5-(2-nitrophenylazo)phenyl]-1-phenylmethanone
1243203-29-3

1-[2-hydroxy-4-methoxy-5-(2-nitrophenylazo)phenyl]-1-phenylmethanone

Conditions
ConditionsYield
Stage #1: 2-nitro-aniline With hydrogenchloride In water at 70℃; for 0.5h;
Stage #2: With sodium nitrite In water at 0 - 5℃;
Stage #3: 2-hydroxy-4-methoxybenzophenone-5-sulfonic acid regioselective reaction; Further stages;
5.14 %Chromat.
2-hydroxy-4-methoxybenzophenone-5-sulfonic acid
4065-45-6

2-hydroxy-4-methoxybenzophenone-5-sulfonic acid

2,4-Dinitroanilin
97-02-9

2,4-Dinitroanilin

C20H14N4O7
1446786-84-0

C20H14N4O7

Conditions
ConditionsYield
Stage #1: 2,4-Dinitroanilin With sulfuric acid; sodium nitrite at 0 - 70℃;
Stage #2: 2-hydroxy-4-methoxybenzophenone-5-sulfonic acid With sodium carbonate In ethanol at -20℃; for 2.5h; pH=8 - 9;
Stage #3: With hydrogenchloride In ethanol; water pH=3; regioselective reaction;
9.9 %Chromat.
4-trifluoromethylphenylamine
455-14-1

4-trifluoromethylphenylamine

2-hydroxy-4-methoxybenzophenone-5-sulfonic acid
4065-45-6

2-hydroxy-4-methoxybenzophenone-5-sulfonic acid

C21H15F3N2O3
1446786-85-1

C21H15F3N2O3

Conditions
ConditionsYield
Stage #1: 4-trifluoromethylphenylamine With hydrogenchloride; sodium nitrite In water at 0 - 5℃;
Stage #2: 2-hydroxy-4-methoxybenzophenone-5-sulfonic acid With sodium carbonate In ethanol; water at -20℃; for 2.5h; pH=8 - 9;
Stage #3: With hydrogenchloride In ethanol; water pH=3; regioselective reaction;
13.2 %Chromat.
2-hydroxy-4-methoxybenzophenone-5-sulfonic acid
4065-45-6

2-hydroxy-4-methoxybenzophenone-5-sulfonic acid

4-nitro-aniline
100-01-6

4-nitro-aniline

1-[2-hydroxy-4-methoxy-5-(4-nitrophenylazo)phenyl]-1-phenylmethanone
1243203-30-6

1-[2-hydroxy-4-methoxy-5-(4-nitrophenylazo)phenyl]-1-phenylmethanone

Conditions
ConditionsYield
Stage #1: 4-nitro-aniline With hydrogenchloride In water at 70℃; for 0.5h;
Stage #2: With sodium nitrite In water at 0 - 5℃;
Stage #3: 2-hydroxy-4-methoxybenzophenone-5-sulfonic acid Temperature; Solvent; regioselective reaction; Further stages;
43.94 %Chromat.
2-hydroxy-4-methoxybenzophenone-5-sulfonic acid
4065-45-6

2-hydroxy-4-methoxybenzophenone-5-sulfonic acid

C14H11O6S

C14H11O6S

Conditions
ConditionsYield
In water; acetonitrile Photolysis; Inert atmosphere;
2-hydroxy-4-methoxybenzophenone-5-sulfonic acid
4065-45-6

2-hydroxy-4-methoxybenzophenone-5-sulfonic acid

Benzophenone-3
131-57-7

Benzophenone-3

Conditions
ConditionsYield
With sulfuric acid; water at 110℃; for 5h; Temperature; Reagent/catalyst;85.95 g
magnesium(II) nitrate hexahydrate

magnesium(II) nitrate hexahydrate

zinc(II) nitrate hexahydrate

zinc(II) nitrate hexahydrate

aluminum nitrate hexahydrate

aluminum nitrate hexahydrate

(E)-3-phenylacrylic acid
140-10-3

(E)-3-phenylacrylic acid

2-hydroxy-4-methoxybenzophenone-5-sulfonic acid
4065-45-6

2-hydroxy-4-methoxybenzophenone-5-sulfonic acid

water
7732-18-5

water

sodium hydroxide
1310-73-2

sodium hydroxide

Mg0.499Zn0.221Al0.280(OH)2(cinnamate)0.140(2-hydroxy-4-methoxybenzophenone-5-sulphonate)0.140*1.06H2O

Mg0.499Zn0.221Al0.280(OH)2(cinnamate)0.140(2-hydroxy-4-methoxybenzophenone-5-sulphonate)0.140*1.06H2O

Conditions
ConditionsYield
Stage #1: (E)-3-phenylacrylic acid; 2-hydroxy-4-methoxybenzophenone-5-sulfonic acid; water; sodium hydroxide at 80℃; Inert atmosphere;
Stage #2: magnesium(II) nitrate hexahydrate; zinc(II) nitrate hexahydrate; aluminum nitrate hexahydrate; water at 20℃; for 0.666667h; Inert atmosphere;
Stage #3: (E)-3-phenylacrylic acid With sodium hydroxide at 95℃; for 12h; pH=Ca. 6.62; Inert atmosphere;
magnesium(II) nitrate hexahydrate

magnesium(II) nitrate hexahydrate

zinc(II) nitrate hexahydrate

zinc(II) nitrate hexahydrate

aluminum nitrate hexahydrate

aluminum nitrate hexahydrate

2-hydroxy-4-methoxybenzophenone-5-sulfonic acid
4065-45-6

2-hydroxy-4-methoxybenzophenone-5-sulfonic acid

water
7732-18-5

water

sodium hydroxide
1310-73-2

sodium hydroxide

Mg0.465Zn0.245Al0.291(OH)2(2-hydroxy-4-methoxybenzophenone-5-sulphonate)0.291*1.28H2O

Mg0.465Zn0.245Al0.291(OH)2(2-hydroxy-4-methoxybenzophenone-5-sulphonate)0.291*1.28H2O

Conditions
ConditionsYield
Stage #1: 2-hydroxy-4-methoxybenzophenone-5-sulfonic acid; water; sodium hydroxide at 80℃; Inert atmosphere;
Stage #2: magnesium(II) nitrate hexahydrate; zinc(II) nitrate hexahydrate; aluminum nitrate hexahydrate; water at 20℃; for 0.666667h; Inert atmosphere;
Stage #3: With sodium hydroxide at 95℃; for 12h; pH=Ca. 6.62; Inert atmosphere;
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