CAS No.4125-43-3,1-ALLYLOXY-2-METHOXY-BENZENE Suppliers

Dayang Chem (Hangzhou) Co.,Ltd.

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1-ALLYLOXY-2-METHOXY-BENZENE

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Shandong Mopai Biotechnology Co., LTD

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Antimex Chemical Limied

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2-Allyloxyanisole cas 4125-43-3Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express

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1-methoxy-2-[3-[3-(2-methoxyphenyl)prop-2-enoxy]prop-1-enyl]benzene

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Finetech Industry Limited

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2-methoxy phenyl allyl ether

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2-Allyloxyanisole

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Synthetic route

: 90-05-1
2-methoxy-phenol

: 106-95-6
allyl bromide

: 4125-43-3
O-allyl guaiacol

Conditions

Conditions	Yield
With potassium carbonate In acetone at 20℃; Reflux;	100%
With potassium carbonate; potassium iodide In acetone for 18h; Reflux;	100%
With potassium carbonate	99%

: 35466-83-2
allyl methyl carbonate

: 90-05-1
2-methoxy-phenol

: 4125-43-3
O-allyl guaiacol

Conditions

Conditions	Yield
With triphenylphosphine In water at 80℃; for 2h; Tsuji-Trost Allylation;	92%

: 13052-77-2
sodium 2-methoxyphenolate

: 106-95-6
allyl bromide

: 4125-43-3
O-allyl guaiacol

Conditions

Conditions	Yield
With potassium carbonate In water; acetonitrile at 50℃; for 48h; Reagent/catalyst;	92%

: 90-05-1
2-methoxy-phenol

allyl halide: allyl halide

: 4125-43-3
O-allyl guaiacol

Conditions

Conditions	Yield
With potassium carbonate In acetone	70%

: 529-28-2
4-iodoanisol

: 107-18-6
allyl alcohol

: 4125-43-3
O-allyl guaiacol

Conditions

Conditions	Yield
With caesium carbonate; copper(l) iodide at 110℃; for 22h;	55%
With copper(l) iodide; (11R,12R)-9,10-dihydro-9,10-ethanoanthracene-11,12-dimethanol; caesium carbonate at 82℃; for 36h; Ullmann coupling;	50%

: 7575-57-7
allyl benzenesulfonate

: 13052-77-2
sodium 2-methoxyphenolate

: 4125-43-3
O-allyl guaiacol

Conditions

Conditions	Yield
With ethanol

: 556-56-9
allyl iodid

: 90-05-1
2-methoxy-phenol

: 4125-43-3
O-allyl guaiacol

Conditions

Conditions	Yield
With potassium carbonate

: 90-05-1
2-methoxy-phenol

: 107-05-1
3-chloroprop-1-ene

: 4125-43-3
O-allyl guaiacol

Conditions

Conditions	Yield
With sodium hydroxide
With potassium carbonate; acetone; sodium iodide

: 5633-98-7
potassium guaiacolate

: 106-95-6
allyl bromide

: 4125-43-3
O-allyl guaiacol

Conditions

Conditions	Yield
With methanol; diethyl ether

: 90-05-1
2-methoxy-phenol

: 107-18-6
allyl alcohol

: 4125-43-3
O-allyl guaiacol

Conditions

Conditions	Yield
With dicyclohexyl-carbodiimide

: 51896-39-0
1-Methoxy-2-[((Z)-propenyl)oxy]-benzene

: 4125-43-3
O-allyl guaiacol

Conditions

Conditions	Yield
With potassium tert-butylate In dimethyl sulfoxide at 100.05℃; Equilibrium constant; Further Variations:; Temperatures;

: 90-05-1
2-methoxy-phenol

: 106-96-7
propargyl bromide

: 4125-43-3
O-allyl guaiacol

Conditions

Conditions	Yield
With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 34h; Product distribution / selectivity;

: 120-80-9
benzene-1,2-diol

: 4125-43-3
O-allyl guaiacol

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: potassium carbonate / acetone 2: potassium carbonate / acetone View Scheme

: 90-05-1
2-methoxy-phenol

allyl-X: allyl-X

: 4125-43-3
O-allyl guaiacol

Conditions

Conditions	Yield
With potassium carbonate In acetone

: 4125-43-3
O-allyl guaiacol

: 90-05-1
2-methoxy-phenol

Conditions

Conditions	Yield
With ethylmagnesium chloride; iron(II) chloride In tetrahydrofuran; m-xylene at 20℃; for 1h; Reagent/catalyst; Temperature; Time; Solvent; Concentration;	97%
With palladium diacetate; sodium hydride In N,N-dimethyl acetamide at 20℃; for 4h; Inert atmosphere;	91%
Stage #1: O-allyl guaiacol With C12H37NiP4(1+)*C2F6NO4S2(1-) In tetrahydrofuran at 20℃; for 0.5h; Glovebox; Schlenk technique; Inert atmosphere; Stage #2: With toluene-4-sulfonic acid In tetrahydrofuran for 1.5h; Catalytic behavior; Reagent/catalyst; Time; Glovebox; Schlenk technique; Reflux; Inert atmosphere;	84%

: 4125-43-3
O-allyl guaiacol

: 579-60-2
6-allylguaicol

Conditions

Conditions	Yield
In N,N-dimethyl-formamide at 190℃; for 12h; Claisen rearrangement;	96%
at 180℃; for 24h;	91%
at 180℃; Rearrangement; Claisen rearrangement;	91%

: 4125-43-3
O-allyl guaiacol

: propenyl guaiacol

Conditions

Conditions	Yield
(carbonyl)(chloro)(hydrido)tris(triphenylphosphine)ruthenium(II) In benzene at 50 - 60℃; Isomerization;	90%

: 4125-43-3
O-allyl guaiacol

: 97-53-0
4-allylguaiacol

Conditions

Conditions	Yield
In N,N-dimethyl-formamide at 276 - 300℃; for 0.025h; Irradiation;	87%
With boron trifluoride diacetate at 68℃;

: 4125-43-3
O-allyl guaiacol

A: 97-53-0
4-allylguaiacol

B: 579-60-2
6-allylguaicol

Conditions

Conditions	Yield
at 200℃; for 1.5h; Claisen Rearrangement;	A 10% B 84%
With 1-butyl-2,3-(trimethylene)imidazolium bistriflylimide at 250℃; for 0.025h; Claisen rearrangement; microwave irradiation;	A 18% B 64%
With bismuth(lll) trifluoromethanesulfonate In acetonitrile for 0.25h; Claisen rearrangement; Heating;	A n/a B 60%

: 4125-43-3
O-allyl guaiacol

: 100-52-7
benzaldehyde

: erythro-1-phenyl-2-(2-methoxyphenyl)-3-butenol

Conditions

Conditions	Yield
Stage #1: O-allyl guaiacol With Li(2,2,6,6-tetramethylpiperidide)*Al(iBu)3 In tetrahydrofuran; hexane at 0℃; for 1h; Stage #2: benzaldehyde In tetrahydrofuran; hexane at 20℃; for 16h;	82%

: 4125-43-3
O-allyl guaiacol

A: 29515-39-7
1-methoxy-2-n-propoxybenzene

B: 90-05-1
2-methoxy-phenol

Conditions

Conditions	Yield
With potassium hydroxide In methanol at 20℃; for 48h;	A 6% B 76%

: 64-17-5
ethanol

: 201230-82-2
carbon monoxide

: 4125-43-3
O-allyl guaiacol

: 56359-21-8
ethyl 4-(2-methoxyphenoxy)butanoate

Conditions

Conditions	Yield
With tris-(dibenzylideneacetone)dipalladium(0); 2-methyl-but-2-ene; hydrogen; 1,4-di(diphenylphosphino)-butane In chloroform at 120℃; under 31029.7 Torr; for 36h; Schlenk technique; Inert atmosphere; Autoclave; regioselective reaction;	69%

...Expand

: 4125-43-3
O-allyl guaiacol

: 115395-29-4
C20H24Cl2O4S

Conditions

Conditions	Yield
With sulfur dichloride In dichloromethane 1.) 2 h, -40 deg C; 2.) 4 h, room temp.;	37%

: 42516-72-3
Ru(1,5-cyclooctadiene)(1,3,5-cyclooctatriene)

: 4125-43-3
O-allyl guaiacol

: 594-09-2
trimethylphosphane

: Ru(C3H5)(OC6H4OCH3)(P(CH3)3)3

Conditions

Conditions	Yield
In hexane stirring (50°C, 40 h); crystallization (hexane), washing (pentane), drying (vac.);	15%

...Expand

: 693-03-8
n-butyl magnesium bromide

: 60-29-7
diethyl ether

: 4125-43-3
O-allyl guaiacol

A: 592-76-7
1-Heptene

B: 90-05-1
2-methoxy-phenol

Conditions

Conditions	Yield
at 60℃;

...Expand

: 79-21-0
peracetic acid

: 4125-43-3
O-allyl guaiacol

: 2210-74-4
2-(2-methoxy-phenoxymethyl)-oxirane

Conditions

Conditions	Yield
With diethyl ether

: 4125-43-3
O-allyl guaiacol

: 7799-39-5
2,4-diallyl-6-methoxy-phenol

Conditions

Conditions	Yield
With borontrifluoride acetic acid at 68℃;
Multi-step reaction with 3 steps 1: 230 °C 2: K2CO3; acetone 3: 230 °C View Scheme

: 60-29-7
diethyl ether

: 4125-43-3
O-allyl guaiacol

: 591-51-5
phenyllithium

A: 120-80-9
benzene-1,2-diol

B: 90-05-1
2-methoxy-phenol

Conditions

Conditions	Yield
at 38℃;

...Expand

: 4125-43-3
O-allyl guaiacol

: 121-69-7
N,N-dimethyl-aniline

: 579-60-2
6-allylguaicol

: 4125-43-3
O-allyl guaiacol

A: 3345-11-7
2,3-Dihydro-7-methoxy-2-methylbenzofuran

B: 97-53-0
4-allylguaiacol

C: 579-60-2
6-allylguaicol

Conditions

Conditions	Yield
With Y-zeolite 1.) n-pentane, r.t., 24 h, 2.) microwave irradiation, 5 min; Yield given. Multistep reaction. Yields of byproduct given;

...Expand

: 4125-43-3
O-allyl guaiacol

: 501-19-9
chavibetol

Conditions

Conditions	Yield
for 1h; Heating;

: 4125-43-3
O-allyl guaiacol

A: 61248-75-7
(R)-guaifenesin

B: 61248-76-8
(S)-guaifenesin

Conditions

Conditions	Yield
With AD-mix-β In water; tert-butyl alcohol at 0℃; Title compound not separated from byproducts;
With osmium(VIII) oxide; potassium carbonate; 1,4-bis(9-O-dihydroquinidine)phthalazine; K2Fe(CN)6 In water; toluene; tert-butyl alcohol at 0℃; Sharpless asymmetric dihydroxylation; Title compound not separated from byproducts;

: 4125-43-3
O-allyl guaiacol

A: 2,6,10-Tris-allyloxy-3,7,11-trimethoxy-triphenylene

B: 2,6,11-Tris-allyloxy-3,7,10-trimethoxy-triphenylene

Conditions

Conditions	Yield
With tetrabutylammonium tetrafluoroborate; triethylamine 1.) acetonitrile, anodic oxidation, 2.) acetonitrile or pentane, Et3N, room temperature, 2 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;

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