Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities
Cas:491-36-1
Min.Order:1 Kilogram
FOB Price: $3.0
Type:Lab/Research institutions
inquiryHigh quality 4-Hydroxyquinazoline CAS 491-36-1 with factory price Company profile Wuhan Fortuna Chemical Co.,Ltd established in 2006, is a big integrative chemical enterprise being engaged in Pharmaceutical & its intermediates, Food/Feed add
Cas:491-36-1
Min.Order:10 Kilogram
FOB Price: $10.0
Type:Trading Company
inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Founded in 2008, East Chemsources Limited is a professional manufacturer and supplier in food and chemical field in China. Through more than ten years development, our company has developed from single product at first to provide solution to final
17-year experience in Phytochemicals Each product has passed very strict tests (NMR\MS\HPLC) Agents in 13 countries Certified by ISO 9001:2008 quality management system Leader Supplier of Botanical Reference Materials in China
Product description: Product name 4-Hydroxyquinazoline CAS number 491-36-1 Assay ≥99% Appearance White solid Capacity 100mt/year Application Pesticide/pharmaceutical intermed
Cas:491-36-1
Min.Order:10 Gram
FOB Price: $12.0
Type:Lab/Research institutions
inquiry1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
Cas:491-36-1
Min.Order:1 Gram
FOB Price: $0.1
Type:Manufacturers
inquiryADVANTAGE: 1. More than 3,000 Chinese medicine reference substances / standard products available from stock, issued on the same day, multiple cities can be delivered the next day 2. The products are provided with COA, HPLC, NMR, quality assurance,
Cas:491-36-1
Min.Order:1 Metric Ton
FOB Price: $1.0
Type:Manufacturers
inquiryProduct Name: 4-Hydroxyquinazoline Synonyms: 4(3H)-Quinazolone;4-Oxoquinazoline;4-Quinazolinone;Quinazolone, 4-;quinazolidin-4-one;QUINAZOLIN-4(3H)-ONE;QUINAZOLIN-4-OL;QUINAZOLONE CAS: 491-36-1 MF: C8H6N2O MW: 146.15
Cas:491-36-1
Min.Order:1 Gram
FOB Price: $8900.0
Type:Lab/Research institutions
inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:491-36-1
Min.Order:1 Kilogram
FOB Price: $139.0 / 210.0
Type:Trading Company
inquiryProduct Name 4-Hydroxyquinazoline Synonyms 4-Hydroxyquinazoline;Quinazolidin-4-one CAS: 491-36-1 MF: - MW: - EINECS: -
Cas:491-36-1
Min.Order:5 Metric Ton
FOB Price: $1.0 / 2.0
Type:Other
inquiry1. Guaranteed purity; 2. Large quantity in stock; 3. Largest manufacturer; 4. Best service after shipment with email; 5. High quality & competitive price; Appearance:powder Storage:Store in sealed containers at cool & dry pla
Cas:491-36-1
Min.Order:100 Gram
Negotiable
Type:Other
inquiry1.In No Less 10 years exporting experience. you can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specializ
Cas:491-36-1
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:491-36-1
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
We have two GMP facilities in Hubei Province and cooperative factories in Zhejiang Province We are concentrating on the R&D and technical service of APIs and pharmaceutical intermediates Appearance:white powder Storage:room temperature Pa
1. Timely and efficient service to ensure communication with customers 2. Produce products of different specifications and sizes according to your requirements. 3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures
Cas:491-36-1
Min.Order:1 Kilogram
FOB Price: $30.0 / 50.0
Type:Lab/Research institutions
inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
Cas:491-36-1
Min.Order:4 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryProduct name: 4-Hydroxyquinazoline CAS No.:491-36-1 Molecule Formula:C8H6N2O Molecule Weight:146.14 Purity: 98.0% Package: 25kg/drum Description:White crystalline powder Manufacture Standards:Enterprise Standard TESTING ITEMS
Cas:491-36-1
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiry4-Hydroxyquinazoline Chemical Properties Melting point 216-219 °C (lit.) Boiling point 265.75°C (rough estimate) density 1.2312 (rough estimate) refractive index 1.4900 (estimate) storage temp. Desiccate at RT form Cry
Cas:491-36-1
Min.Order:1 Gram
FOB Price: $66.0
Type:Lab/Research institutions
inquiryWe Huarong Pharm can provide Customized Synthesis & Process R&D & APIs and intermediates Production & Quality Research & Registration Application, especially our GMP validation service which complies with SFDA, FDA, WHO and EU EMPA. O
1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
Cas:491-36-1
Min.Order:1 Metric Ton
FOB Price: $7.0 / 8.0
Type:Trading Company
inquiryAppearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea
Superior quality, moderate price & quick delivery. Appearance:white crystalline powder Storage:stored in a cool, dry and ventilated place to provent sun and rain Package:25kg/drum, or as per your request. Application:Used as Pharmaceutical
Stock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai
Cas:491-36-1
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiry4-HydroxyquinazolineAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
R & D enterprises have their own stock in stockAppearance:To be subject to the object Package:Customized Application:pharmaceutical intermediates Transportation:Air Port:Shanghai;Guangzhou
Conditions | Yield |
---|---|
With ammonium acetate In methanol at 120℃; for 3h; | 98% |
Conditions | Yield |
---|---|
for 8h; Heating; | 97% |
With iodine; oxygen; dimethyl sulfoxide at 110℃; for 4h; | 55% |
anthranilic acid amide
N,N-dimethyl-formamide
4-Hydroxyquinazoline
Conditions | Yield |
---|---|
With Imidazole hydrochloride at 150℃; for 13h; Temperature; | 97% |
With toluene-4-sulfonic acid at 120℃; for 10h; Sealed tube; | 87% |
With Triethoxysilane; carbon dioxide; tris(pentafluorophenyl)borate at 120℃; for 24h; | 99 %Spectr. |
anthranilic acid amide
orthoformic acid triethyl ester
4-Hydroxyquinazoline
Conditions | Yield |
---|---|
In ethanol for 43h; Heating; | 96% |
With antimony(III) chloride In neat (no solvent) for 0.0333333h; Solvent; Microwave irradiation; Green chemistry; | 95% |
With 1-methyl-3-(propyl-3-sulfonyl)imidazolium trifluoromethanesulfonate at 45 - 46℃; for 0.416667h; Ionic liquid; Sonication; neat (no solvent); chemoselective reaction; | 91% |
Conditions | Yield |
---|---|
With ammonium hydroxide; Glyoxilic acid In water at 110 - 120℃; for 0.133333h; | 96% |
With aluminum potassium sulfate dodecahydrate; ammonium acetate; orthoformic acid triethyl ester for 0.1h; Microwave irradiation; neat (no solvent); | 92% |
With formamidine acetic acid In ethanol for 3h; Heating; | 81% |
With formamide at 120 - 125℃; for 1.5h; | 81% |
formamide
anthranilic acid amide
4-Hydroxyquinazoline
Conditions | Yield |
---|---|
With acetic acid; diethylamine at 150℃; for 2h; Product distribution / selectivity; | 96% |
With antimony(III) chloride for 0.0833333h; Niementowski Quinazolone Synthesis; Microwave irradiation; Green chemistry; | 95% |
With ytterbium(III) triflate In 1,3,5-trimethyl-benzene at 120℃; for 6h; Reagent/catalyst; Temperature; Inert atmosphere; | 79% |
With acetic acid |
4-amino-o-xylene
anthranilic acid amide
orthoformic acid triethyl ester
A
4-Hydroxyquinazoline
Conditions | Yield |
---|---|
With Preyssler heteropolyacid In acetonitrile for 2h; Reflux; | A n/a B 96% |
With H6[PMo9V3O40] In acetonitrile for 2h; Reflux; | A 5% B 95% |
Conditions | Yield |
---|---|
With ammonium hydroxide; palladium dichloride at 90℃; for 0.166667h; Microwave irradiation; Green chemistry; | 96% |
Conditions | Yield |
---|---|
With ammonium hydroxide; palladium dichloride at 90℃; for 0.166667h; Microwave irradiation; Green chemistry; | 96% |
anthranilic acid
formamide
4-Hydroxyquinazoline
Conditions | Yield |
---|---|
Heating; | 95.4% |
95.4% | |
for 0.25h; Irradiation; | 95% |
Conditions | Yield |
---|---|
With diphenyl-phosphinic acid; oxygen In 1,4-dioxane at 130℃; under 760.051 Torr; for 18h; Schlenk technique; | 95% |
p-toluidine
anthranilic acid amide
orthoformic acid triethyl ester
A
4-Hydroxyquinazoline
B
N-(p-tolyl)quinazolin-4-amine
Conditions | Yield |
---|---|
With Preyssler heteropolyacid In acetonitrile for 2h; Reflux; | A n/a B 94% |
With H6[PMo9V3O40] In acetonitrile for 2h; Reflux; | A 7% B 93% |
4-amino-o-xylene
anthranilic acid amide
trimethyl orthoformate
A
4-Hydroxyquinazoline
Conditions | Yield |
---|---|
With H6[PMo9V3O40] In acetonitrile Reflux; | A n/a B 94% |
Conditions | Yield |
---|---|
With copper 8-hydroxyquinolinate; sodium hydroxide In water at 100℃; for 0.5h; Microwave irradiation; | 94% |
Conditions | Yield |
---|---|
With ammonium hydroxide; palladium dichloride at 90℃; for 0.166667h; Microwave irradiation; Green chemistry; | 94% |
Conditions | Yield |
---|---|
With ammonium hydroxide; palladium dichloride at 90℃; for 0.166667h; Microwave irradiation; Green chemistry; | 94% |
Conditions | Yield |
---|---|
With ammonium acetate for 0.1h; microwave irradiation; | 93% |
With ammonium acetate; antimony(III) chloride In neat (no solvent) for 0.0833333h; Microwave irradiation; Green chemistry; | 93% |
With ammonium acetate In ethanol at 110℃; for 0.333333h; Microwave irradiation; |
Conditions | Yield |
---|---|
With iron(III) chloride In water for 1h; Heating; | 92% |
With [Cp*Ir(2,2′-bpyO)(H2O)]; caesium carbonate In toluene at 130℃; for 2h; Microwave irradiation; | 82% |
With bis(acetylacetonate)oxovanadium; oxygen In 1,2-dichloro-ethane at 80℃; under 760.051 Torr; for 6h; | 80% |
Conditions | Yield |
---|---|
With oxygen; copper(II) acetate monohydrate; caesium carbonate at 110℃; for 6h; Catalytic behavior; Reagent/catalyst; Temperature; Time; | 92% |
With [Cp*Ir(2,2′-bpyO)(H2O)]; caesium carbonate at 130℃; for 2h; Catalytic behavior; Reagent/catalyst; Temperature; Microwave irradiation; Green chemistry; | 88% |
With [Cp*Ir(2,2'-bpyO)(H2O)]; caesium carbonate at 130℃; for 2h; Temperature; Reagent/catalyst; Microwave irradiation; Inert atmosphere; | 88% |
Conditions | Yield |
---|---|
With N-hydroxyphthalimide; cobalt(III) acetylacetonate; cobalt acetylacetonate In benzonitrile; trifluoroacetic acid at 70℃; for 12h; Product distribution; Further Variations:; Reagents; | 91% |
p-toluidine
anthranilic acid amide
trimethyl orthoformate
A
4-Hydroxyquinazoline
B
N-(p-tolyl)quinazolin-4-amine
Conditions | Yield |
---|---|
With H6[PMo9V3O40] In acetonitrile Reflux; | A n/a B 91% |
anthranilic acid amide
orthoformic acid triethyl ester
aniline
A
4-Hydroxyquinazoline
B
4-(phenylamino)quinazoline
Conditions | Yield |
---|---|
With H6[PMo9V3O40] In acetonitrile for 2h; Reflux; | A 9% B 91% |
With Preyssler heteropolyacid In acetonitrile for 2h; Reflux; | A n/a B 91% |
Conditions | Yield |
---|---|
With ammonium acetate In neat (no solvent) at 120℃; for 5h; Temperature; Green chemistry; | 91% |
With ammonium acetate; Thiamine hydrochloride In ethanol for 4h; Reflux; | 85% |
Conditions | Yield |
---|---|
With copper(l) iodide; oxygen; caesium carbonate at 20℃; for 10h; Reagent/catalyst; Irradiation; | 91% |
With 2,3-dicyano-5,6-dichloro-p-benzoquinone In chloroform at 20℃; for 1h; Schlenk technique; Sealed tube; | 11.1 mg |
With tetrabutylammonium perchlorate; toluene-4-sulfonic acid In acetonitrile at 20℃; for 1.5h; Electrolysis; | 40 mg |
With cobalt(II) nitrate hexahydrate; tris(2-diphenylphosphinoethyl)phosphine; caesium carbonate In methanol at 150℃; for 3h; Reagent/catalyst; Inert atmosphere; Sealed tube; |
Conditions | Yield |
---|---|
In ethanol for 16h; Reflux; | 90.7% |
anthranilic acid amide
4,4-dimethyl-Δ2-oxazolinium chloride
4-Hydroxyquinazoline
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide for 1h; Heating; | 90% |
4-chloro-aniline
anthranilic acid amide
orthoformic acid triethyl ester
A
4-Hydroxyquinazoline
Conditions | Yield |
---|---|
With Preyssler heteropolyacid In acetonitrile for 2h; Reflux; | A n/a B 90% |
With H6[PMo9V3O40] In acetonitrile for 2h; Reflux; | A 11% B 89% |
4-Hydroxyquinazoline
Conditions | Yield |
---|---|
With 8-quinolinol; sodium hydroxide; copper dichloride In water at 20℃; for 0.333333h; Reagent/catalyst; Microwave irradiation; | 90% |
tert-butylisonitrile
anthranilic acid amide
4-Hydroxyquinazoline
Conditions | Yield |
---|---|
With chloro-trimethyl-silane In acetonitrile at 70℃; for 24h; | 90% |
4-Hydroxyquinazoline
4-(3H-[1,2,3]triazolo[4,5-b]pyridin-3-yloxy)quinazoline
Conditions | Yield |
---|---|
With 1,8-diazabicyclo[5.4.0]undec-7-ene In acetonitrile at 20℃; for 1h; | 99% |
4-Hydroxyquinazoline
methyl 1-phenylprop-2-enyl carbonate
Conditions | Yield |
---|---|
With chloro(1,5-cyclooctadiene)rhodium(I) dimer; (R)-(+)-(6,6'-dimethoxybiphenyl-2,2'-diyl)bis[bis(3,5-di-tert-butylphenyl)phosphine] In 1,2-dichloro-ethane at 80℃; for 24h; Reagent/catalyst; Temperature; Solvent; Schlenk technique; Inert atmosphere; enantioselective reaction; | 99% |
4-Hydroxyquinazoline
Conditions | Yield |
---|---|
Stage #1: 4-Hydroxyquinazoline; diethyl 4-(sec-butyl)-2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylate With trifluoroacetic acid In 2,2,2-trifluoroethanol at 35℃; for 4h; Irradiation; Inert atmosphere; Sealed tube; Stage #2: In 2,2,2-trifluoroethanol for 4h; Reagent/catalyst; Solvent; Irradiation; Inert atmosphere; | 99% |
Stage #1: 4-Hydroxyquinazoline; diethyl 4-(sec-butyl)-2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylate With trifluoroacetic acid In 2,2,2-trifluoroethanol at 20℃; for 4h; Sealed tube; Irradiation; Inert atmosphere; Stage #2: In 2,2,2-trifluoroethanol at 20℃; for 4h; Solvent; Reagent/catalyst; Wavelength; | 97% |
4-Hydroxyquinazoline
Conditions | Yield |
---|---|
With chloro(1,5-cyclooctadiene)rhodium(I) dimer; (R)-(+)-(6,6'-dimethoxybiphenyl-2,2'-diyl)bis[bis(3,5-di-tert-butylphenyl)phosphine] In 1,2-dichloro-ethane at 80℃; for 24h; Schlenk technique; Inert atmosphere; enantioselective reaction; | 98% |
4-Hydroxyquinazoline
Conditions | Yield |
---|---|
With chloro(1,5-cyclooctadiene)rhodium(I) dimer; (R)-(+)-(6,6'-dimethoxybiphenyl-2,2'-diyl)bis[bis(3,5-di-tert-butylphenyl)phosphine] In 1,2-dichloro-ethane at 80℃; for 24h; Schlenk technique; Inert atmosphere; enantioselective reaction; | 98% |
4-Hydroxyquinazoline
Conditions | Yield |
---|---|
With chloro(1,5-cyclooctadiene)rhodium(I) dimer; (R)-(+)-(6,6'-dimethoxybiphenyl-2,2'-diyl)bis[bis(3,5-di-tert-butylphenyl)phosphine] In 1,2-dichloro-ethane at 80℃; for 24h; Schlenk technique; Inert atmosphere; enantioselective reaction; | 98% |
4-Hydroxyquinazoline
Conditions | Yield |
---|---|
With chloro(1,5-cyclooctadiene)rhodium(I) dimer; (R)-(+)-(6,6'-dimethoxybiphenyl-2,2'-diyl)bis[bis(3,5-di-tert-butylphenyl)phosphine] In 1,2-dichloro-ethane at 80℃; for 24h; Schlenk technique; Inert atmosphere; enantioselective reaction; | 98% |
4-Hydroxyquinazoline
Conditions | Yield |
---|---|
Stage #1: 4-Hydroxyquinazoline; diethyl 2,6-dimethyl-4-(pentan-3-yl)-1,4-dihydropyridine-3,5-dicarboxylate With trifluoroacetic acid In 2,2,2-trifluoroethanol at 20℃; for 4h; Sealed tube; Irradiation; Inert atmosphere; Stage #2: In 2,2,2-trifluoroethanol at 20℃; for 4h; | 98% |
Stage #1: 4-Hydroxyquinazoline; diethyl 2,6-dimethyl-4-(pentan-3-yl)-1,4-dihydropyridine-3,5-dicarboxylate With trifluoroacetic acid In 2,2,2-trifluoroethanol at 35℃; for 4h; Irradiation; Inert atmosphere; Sealed tube; Stage #2: In 2,2,2-trifluoroethanol for 4h; Irradiation; Inert atmosphere; | 98% |
With [4,4’-bis(1,1-dimethylethyl)-2,2’-bipyridine-N1,N1‘]bis [3,5-difluoro-2-[5-(trifluoromethyl)-2-pyridinyl-N]phenyl-C]iridium(III) hexafluorophosphate; oxygen; trifluoroacetic acid In dimethyl sulfoxide at 20℃; for 24h; Minisci Aromatic Substitution; Irradiation; | 89% |
4-Hydroxyquinazoline
4-cyclohexyl-2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylic acid diethyl ester
2‐cyclohexylquinazolin‐4(3H)‐one
Conditions | Yield |
---|---|
Stage #1: 4-Hydroxyquinazoline; 4-cyclohexyl-2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylic acid diethyl ester With trifluoroacetic acid In 2,2,2-trifluoroethanol at 20℃; for 4h; Sealed tube; Irradiation; Inert atmosphere; Stage #2: In 2,2,2-trifluoroethanol at 20℃; for 4h; | 98% |
Stage #1: 4-Hydroxyquinazoline; 4-cyclohexyl-2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylic acid diethyl ester With trifluoroacetic acid In 2,2,2-trifluoroethanol at 35℃; for 4h; Irradiation; Inert atmosphere; Sealed tube; Stage #2: In 2,2,2-trifluoroethanol for 4h; Irradiation; Inert atmosphere; | 98% |
With [4,4’-bis(1,1-dimethylethyl)-2,2’-bipyridine-N1,N1‘]bis [3,5-difluoro-2-[5-(trifluoromethyl)-2-pyridinyl-N]phenyl-C]iridium(III) hexafluorophosphate; oxygen; trifluoroacetic acid In dimethyl sulfoxide at 20℃; for 24h; Minisci Aromatic Substitution; Irradiation; | 78% |
Conditions | Yield |
---|---|
With ammonium sulfate; 1,1,1,3,3,3-hexamethyl-disilazane at 125℃; for 2h; | 97% |
4-Hydroxyquinazoline
Conditions | Yield |
---|---|
With chloro(1,5-cyclooctadiene)rhodium(I) dimer; (R)-(+)-(6,6'-dimethoxybiphenyl-2,2'-diyl)bis[bis(3,5-di-tert-butylphenyl)phosphine] In 1,2-dichloro-ethane at 80℃; for 24h; Schlenk technique; Inert atmosphere; enantioselective reaction; | 97% |
4-Hydroxyquinazoline
1-(4'-bromophenyl)-prop-2-enyl methyl carbonate
Conditions | Yield |
---|---|
With chloro(1,5-cyclooctadiene)rhodium(I) dimer; (R)-(+)-(6,6'-dimethoxybiphenyl-2,2'-diyl)bis[bis(3,5-di-tert-butylphenyl)phosphine] In 1,2-dichloro-ethane at 80℃; for 24h; Schlenk technique; Inert atmosphere; enantioselective reaction; | 97% |
4-Hydroxyquinazoline
Conditions | Yield |
---|---|
With chloro(1,5-cyclooctadiene)rhodium(I) dimer; (R)-(+)-(6,6'-dimethoxybiphenyl-2,2'-diyl)bis[bis(3,5-di-tert-butylphenyl)phosphine] In 1,2-dichloro-ethane at 80℃; for 24h; Schlenk technique; Inert atmosphere; enantioselective reaction; | 97% |
Conditions | Yield |
---|---|
With potassium carbonate In dimethyl sulfoxide at 100℃; for 12h; Temperature; | 96.4% |
With potassium carbonate In dimethyl sulfoxide at 100℃; for 12h; Reagent/catalyst; Temperature; | 96.4% |
With potassium carbonate In dimethyl sulfoxide at 100℃; for 12h; Temperature; | 96.4% |
With potassium carbonate In dimethyl sulfoxide at 100℃; for 12h; Temperature; | 96.4% |
Conditions | Yield |
---|---|
Stage #1: 4-Hydroxyquinazoline With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; caesium carbonate In tetrahydrofuran at 20℃; for 0.833333h; Inert atmosphere; Stage #2: 4-methoxy-phenol With caesium carbonate In tetrahydrofuran at 20℃; for 0.5h; | 96% |
With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; 1,8-diazabicyclo[5.4.0]undec-7-ene In acetonitrile at 20 - 60℃; for 52h; | 75% |
Conditions | Yield |
---|---|
Stage #1: 4-Hydroxyquinazoline With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; caesium carbonate In tetrahydrofuran at 20℃; for 0.833333h; Inert atmosphere; Stage #2: benzyl alcohol With caesium carbonate at 20℃; for 1.16667h; | 96% |
Conditions | Yield |
---|---|
With ammonium sulfate; 1,1,1,3,3,3-hexamethyl-disilazane at 125℃; for 2h; | 96% |
Conditions | Yield |
---|---|
With potassium carbonate; sodium iodide In acetone for 24h; Reflux; | 96% |
4-Hydroxyquinazoline
Conditions | Yield |
---|---|
With potassium carbonate; sodium iodide In acetone for 24h; Reflux; | 96% |
4-Hydroxyquinazoline
1-(4'-chlorophenyl)-prop-2-enyl methyl carbonate
Conditions | Yield |
---|---|
With chloro(1,5-cyclooctadiene)rhodium(I) dimer; (R)-(+)-(6,6'-dimethoxybiphenyl-2,2'-diyl)bis[bis(3,5-di-tert-butylphenyl)phosphine] In 1,2-dichloro-ethane at 80℃; for 24h; Schlenk technique; Inert atmosphere; enantioselective reaction; | 96% |
4-Hydroxyquinazoline
(hex-1-en-3-yl)methyl carbonate
Conditions | Yield |
---|---|
With chloro(1,5-cyclooctadiene)rhodium(I) dimer; (R)-(+)-(6,6'-dimethoxybiphenyl-2,2'-diyl)bis[bis(3,5-di-tert-butylphenyl)phosphine] In 1,2-dichloro-ethane at 80℃; for 24h; Schlenk technique; Inert atmosphere; enantioselective reaction; | 96% |
4-Hydroxyquinazoline
Conditions | Yield |
---|---|
With chloro(1,5-cyclooctadiene)rhodium(I) dimer; (R)-(+)-(6,6'-dimethoxybiphenyl-2,2'-diyl)bis[bis(3,5-di-tert-butylphenyl)phosphine] In 1,2-dichloro-ethane at 80℃; for 24h; Schlenk technique; Inert atmosphere; enantioselective reaction; | 96% |
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