Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities
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inquiry533-73-3 Hubei Vanz Pharm Co. Ltd. is the manufacture of APIs, supplements raw powder and some customization products. located in Hubei province, China. We are one of the most professional company in pharm/chemical industry for more than 10 years.
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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inquiryNow we would like to update our product list for you, kindly check the below information: 1. Catalyst series ( such as Noble Metal Catalyst, Phosphorous ligand, etc ) 2. Pharmaceutical Intermediate ( such as diabtes series, Anti
With our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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inquiry1. Product advantages ♦ High purity, all above 98.5%, no impurities after dissolution ♦ We will test each batch to ensure quality ♦ OEM and private brand services designed for free ♦ Various cap colors available ♦ W
Cas:533-73-3
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inquiryName: 1,2,4-Trihydroxybenzene Synonyms: 1,2,4-Benzentril CAS: 533-73-3 MF: C6H6O3 Appearance:White powder or crystalline powder Storage:Store in cool and dry place, away from sun light. Package: 25kgs/drum Application:Agrochemical Intermediates,
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inquiryAppearance:White powder Storage:Room temperature Package:25kg/drum Application:organic synthesis intermediates Transportation:Express/Sea/Air Port:Any port in china
Cas:533-73-3
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inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At present,
1,2,4-Benzenetriol CAS:533-73-3 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermed
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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Min.Order:1 Kilogram
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inquiry1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists of highly qualifie
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Type:Lab/Research institutions
inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Our advantages: 1, High quality with competitive price: 1) Standard:BP/USP/EP/Enterprise standard 2) All Purity≥99% 3) We are manufacturer and can provide high quality products with factory price. 2, Fast and safe delivery 1) Parcel can be
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inquiryEstablished in May 2015, TaiChem Ltd. is initially invested by a British research and development company and started by PhDs back from aboard. The company is registered in China Medical City (CMC), Taizhou, Jiangsu Province, and the production site
Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
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Min.Order:1 Gram
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Type:Lab/Research institutions
inquiryOur Advantages A. International Top level TechnologyOur company owned biomedicine experts are famous at home and abroad with rich experience in research and development in the field of efficient chiral functional molecules research and development an
GMP standard, high purity, competitive price, in stock 1. Quick Response: within 6 hours after receiving your email. 2. Quality Guarantee: All products are strictly tested by our QC, confirmed by QA, and approved by a third-party lab in China, USA,
Conditions | Yield |
---|---|
With hydrogenchloride; water In methanol for 7h; Reagent/catalyst; Reflux; | 98% |
With hydrogenchloride; methanol | |
With acetic acid |
Conditions | Yield |
---|---|
With dihydrogen peroxide at 20℃; for 0.833333h; Dakin Phenol Oxidation; Green chemistry; | 96% |
With dihydrogen peroxide; sodium carbonate In tetrahydrofuran; water at 0 - 20℃; for 3h; | 85% |
(4S,5R,6S)-4,5,6-trihydroxy-2-cyclohexene-1-one
1,2,4-Trihydroxybenzene
Conditions | Yield |
---|---|
In water at 170℃; for 2h; Inert atmosphere; | 93% |
hydrogenchloride
triphenylantimony m-hydroxy-o-phenylenedioxide
A
1,2,4-Trihydroxybenzene
B
triphenylantimony dichloride
Conditions | Yield |
---|---|
heating (3 h, water bath); soln. pouring into Petri dish, solid extraction by benzene; | A 78% B 86% |
Conditions | Yield |
---|---|
With hydrogenchloride; water at 250℃; under 37503.8 Torr; for 3h; Sealed tube; Inert atmosphere; | 57% |
Conditions | Yield |
---|---|
With hydrogenchloride; water at 250℃; under 37503.8 Torr; for 3h; Reagent/catalyst; Sealed tube; Inert atmosphere; | 56% |
Conditions | Yield |
---|---|
With <(Ce2(p-tert-butylcalix(8)arene))(Me2SO)5>*2Me2SO; dihydrogen peroxide In acetonitrile for 5h; Ambient temperature; | 42% |
With 2,6-dichloroquinone-4-chloroimide; sodium acetate; acetic acid | |
With water for 0.166667h; |
Conditions | Yield |
---|---|
With <(Ce2(p-tert-butylcalix(8)arene))(Me2SO)5>*2Me2SO; dihydrogen peroxide In acetonitrile for 5h; Ambient temperature; | 39% |
With sodium hydroxide | |
With oxygen; iron(III) In water pH=2.0; Kinetics; hydroxylation; Electrochemical reaction; | |
With titanium(IV) oxide In water at 30℃; Mechanism; Time; UV-irradiation; | |
Multi-step reaction with 3 steps 1: iodine; dihydrogen peroxide / water; sulfuric acid / 30 - 50 °C 2: sulfuric acid / 0.5 h / 25 - 50 °C 3: hydrogenchloride; water / methanol / 7 h / Reflux View Scheme |
2L-(2,4/3,5)-2,3,4,5-tetrahydroxycyclohexan-1-one
1,2,4-Trihydroxybenzene
Conditions | Yield |
---|---|
With phosphoric acid In water at 125℃; for 12h; | 39% |
In water at 170℃; for 2h; Product distribution / selectivity; Inert atmosphere; Autoclave; | 95 %Chromat. |
Conditions | Yield |
---|---|
With air; methylene blue In methanol for 12h; Product distribution; Mechanism; Irradiation; | A 15% B 35% |
Conditions | Yield |
---|---|
With air; methylene blue In methanol for 12h; Product distribution; Mechanism; Irradiation; | A 15% B 35% |
4,4-bis(ethylthio)-1,3-cyclohexanedione
1,2,4-Trihydroxybenzene
Conditions | Yield |
---|---|
With mercury dichloride In methanol; water for 5h; Ambient temperature; | 32% |
With acetic acid; mercury dichloride 1.) aqueous MeOH, r.t., 2.) reflux, 1 h; Yield given. Multistep reaction; |
5-hydroxymethyl-2-furfuraldehyde
A
furfural
B
1,2,4-Trihydroxybenzene
C
levulinic acid
D
hydroquinone
Conditions | Yield |
---|---|
In water at 330℃; under 210017 Torr; for 0.075h; Further byproducts given. Yields of byproduct given; | A n/a B 25% C n/a D n/a |
5-hydroxymethyl-2-furfuraldehyde
A
furfural
B
1,2,4-Trihydroxybenzene
C
levulinic acid
D
hydroquinone
E
2-hydroxyresorcinol
Conditions | Yield |
---|---|
In water at 330℃; under 210017 Torr; for 0.075h; other temperatures, other reaction times, other educt; | A n/a B 25% C n/a D n/a E n/a |
2L-(2,4/3,5)-2,3,4,5-tetrahydroxycyclohexan-1-one
A
1,2,4-Trihydroxybenzene
B
benzene-1,2-diol
Conditions | Yield |
---|---|
With zinc In acetic acid Product distribution; Further Variations:; Reagents; Temperatures; reductiv dehydration; reflux; | A n/a B 18% |
Conditions | Yield |
---|---|
In water at 330℃; for 0.0513889h; | 9% |
Conditions | Yield |
---|---|
at 200 - 220℃; |
Conditions | Yield |
---|---|
With pyridine hydrochloride at 200 - 220℃; |
Conditions | Yield |
---|---|
at 220℃; |
Conditions | Yield |
---|---|
ueber mehrere Stufen; | |
Multi-step reaction with 2 steps 1: sulfuric acid / 0.5 h / 25 - 50 °C 2: hydrogenchloride; water / methanol / 7 h / Reflux View Scheme | |
Multi-step reaction with 2 steps 1: sulfuric acid; acetic acid / 40 - 50 °C 2: hydrogenchloride; water / methanol / 7 h / Reflux View Scheme |
1,2,4-Tris-(bis-trifluormethyl-aminooxy)-benzol
1,2,4-Trihydroxybenzene
Conditions | Yield |
---|---|
With potassium hydroxide |
5-hydroxymethyl-2-furfuraldehyde
A
furfural
B
5-Methylfurfural
C
5-methyl-2-furanone
D
hydroxyquinone
E
1,2,4-Trihydroxybenzene
F
levulinic acid
Conditions | Yield |
---|---|
With water at 126.9℃; under 206266 Torr; Product distribution; Kinetics; Thermodynamic data; Ea, various water densities; |
Cellobiose
A
formic acid
B
1,2,4-Trihydroxybenzene
C
glycolaldehyde hydrate
D
acetic acid
E
hydroxy-2-propanone
F
2-hydroxyresorcinol
Conditions | Yield |
---|---|
at 300℃; under 1.5 Torr; for 0.5h; Mechanism; also with cellobiitol and other (13)C labeled glucans; |
A
1,2,4-Trihydroxybenzene
C
acetic acid
D
Glycolaldehyde
E
hydroxy-2-propanone
F
2-hydroxyresorcinol
Conditions | Yield |
---|---|
With sodium chloride at 300℃; under 2 Torr; for 1h; Product distribution; other temperatures, other reaction times, or without 1percent aq. NaCl; | A 1.1 % Chromat. B n/a C 3.7 % Spectr. D 12.8 % Spectr. E 1.6 % Spectr. F 0.4 % Chromat. |
4-chloro-phenol
A
4-chloro-1,2-benzenediol
B
hydroxyquinone
C
1,2,4-Trihydroxybenzene
D
hydroquinone
E
p-benzoquinone
Conditions | Yield |
---|---|
With oxygen In water Product distribution; Irradiation; |
benzene
A
[18O]phenol
B
1,2,4-Trihydroxybenzene
C
hydroquinone
D
p-benzoquinone
E
phenol
Conditions | Yield |
---|---|
With dioxygen-(16)O; 4-pentafluorophenyl perfluoro biphenyl; 18O-labeled water In acetonitrile; benzene Product distribution; Mechanism; Irradiation; ratio of C6H518OH to C6H5OH; |
phenol
A
hydroxyquinone
B
1,2,4-Trihydroxybenzene
C
benzene-1,2-diol
D
hydroquinone
E
p-benzoquinone
F
2-hydroxyresorcinol
Conditions | Yield |
---|---|
With oxygen; titanium(IV) oxide In water at 25℃; Product distribution; Quantum yield; Mechanism; Irradiation; various wavelengths, other catalysts; |
1,2,4-Tris-(prop-1-enyloxy)-benzol
1,2,4-Trihydroxybenzene
Conditions | Yield |
---|---|
With hydrogenchloride |
recorcinol
A
1,2,4-Trihydroxybenzene
B
4-nitroso-1,3-benzenediol
C
4-nitroresorcinol
D
2-hydroxyresorcinol
Conditions | Yield |
---|---|
With potassium nitrate In water pH=5.7; Quantum yield; Kinetics; Further Variations:; Reagents; pH-values; wavelength; phototransformation; Irradiation; |
Conditions | Yield |
---|---|
With sodium hydride In tetrahydrofuran at 20℃; for 12h; | 99% |
With sodium hydride In tetrahydrofuran; mineral oil at 0 - 20℃; for 16h; Inert atmosphere; | 96% |
With sodium hydroxide |
1,2,4-Trihydroxybenzene
p-Methoxybenzyl bromide
1,2,4-tris(p-methoxybenzyloxy)benzene
Conditions | Yield |
---|---|
With sodium hydride In N,N-dimethyl-formamide at 0 - 20℃; for 18.3333h; | 97.1% |
With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0 - 20℃; for 18h; Cooling with ice; | 97.1% |
1,2,4-Trihydroxybenzene
ethyl acetoacetate
6,7-dihydroxy-4-methylcoumarin
Conditions | Yield |
---|---|
With trifluoroacetic acid at 100℃; for 0.5h; Pechmann condensation; Microwave irradiation; regioselective reaction; | 97% |
With zirconium(IV) chloride In toluene at 80℃; Pechmann Condensation; Inert atmosphere; | 95% |
With phosphoric acid at 60℃; | 90% |
methyl 3,3,3-trifluoropyruvate
1,2,4-Trihydroxybenzene
3,3,3-Trifluoro-2-hydroxy-2-(2,4,5-trihydroxy-phenyl)-propionic acid methyl ester
Conditions | Yield |
---|---|
In benzene at 80℃; for 1h; | 95% |
1,2,4-Trihydroxybenzene
tert-butyl[(4,4-dimethoxycyclohexyl)oxy]dimethylsilane
Conditions | Yield |
---|---|
With pyridinium p-toluenesulfonate In toluene Inert atmosphere; Schlenk technique; Reflux; | 95% |
1,2,4-Trihydroxybenzene
Conditions | Yield |
---|---|
With piperidine In methanol for 5h; Reflux; | 95% |
Conditions | Yield |
---|---|
With zirconium(IV) chloride In toluene at 80℃; Pechmann Condensation; Inert atmosphere; | 92% |
1,2,4-Trihydroxybenzene
ethyl acetoacetate
4-methyl-5,7-dihydroxycoumarin
Conditions | Yield |
---|---|
With nanosilica molybdic acid 2 In neat (no solvent) at 80℃; for 0.333333h; Pechmann Condensation; Green chemistry; | 91% |
Conditions | Yield |
---|---|
86% |
Conditions | Yield |
---|---|
With hexafluorophosphoric acid In acetic acid at 20℃; for 48h; | 86% |
1,2,4,5-tetrachloro-3,6-dimethyl-benzene
1,2,4-Trihydroxybenzene
Triethyl orthoacetate
Conditions | Yield |
---|---|
86% |
1,2,4-Trihydroxybenzene
2-chloro-5-(dichlorophosphanyloxy)-1,3,2-benzodioxaphosphole
Conditions | Yield |
---|---|
With phosphorus trichloride | 85% |
With phosphorus trichloride In neat (no solvent) Inert atmosphere; | 85% |
With phosphorus trichloride |
Conditions | Yield |
---|---|
With triethylamine at 20℃; | 84.11% |
Conditions | Yield |
---|---|
With dicyclohexyl-carbodiimide In tetrahydrofuran at 0℃; for 20h; | 84% |
With dicyclohexyl-carbodiimide In tetrahydrofuran at 0℃; for 20h; |
ethyl (2-chloroaceto)acetate
1,2,4-Trihydroxybenzene
4-chloromethyl-5,7-dihydroxy-chromen-2-one
Conditions | Yield |
---|---|
With nanosilica molybdic acid 2 In neat (no solvent) at 80℃; for 0.333333h; Pechmann Condensation; Green chemistry; | 84% |
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide for 1h; Williamson reaction; Heating; | 81% |
1,2,4-Trihydroxybenzene
[1,1′-biphenyl]-2,2′,4,4′,5,5′-hexaol
Conditions | Yield |
---|---|
With oxygen; Y2(Sn0.7Ce0.3)2O7 In water at 100℃; for 12h; Reagent/catalyst; Temperature; | 80.2% |
With air In water for 20h; Time; Solvent; Reflux; | |
With oxygen In water at 100℃; for 72h; Green chemistry; | 94.4 %Chromat. |
1,2,4-Trihydroxybenzene
2,2-dimethoxy-propane
2,2-Dimethyl-5-hydroxybenzo[1,3]dioxole
Conditions | Yield |
---|---|
Stage #1: 1,2,4-Trihydroxybenzene With pyridinium p-toluenesulfonate In toluene Reflux; Stage #2: 2,2-dimethoxy-propane In toluene for 1.83333h; | 80% |
With pyridinium p-toluenesulfonate In toluene for 1.83333h; Reflux; | 57% |
Stage #1: 1,2,4-Trihydroxybenzene; 2,2-dimethoxy-propane With toluene-4-sulfonic acid In toluene at 130℃; for 1.5h; Stage #2: With sodium methylate In methanol; toluene at 20℃; | 28.9% |
With pyridinium p-toluenesulfonate In toluene at 110℃; for 2h; | |
With pyridinium p-toluenesulfonate In ethyl acetate at 85℃; Inert atmosphere; |
1,2,4-Trihydroxybenzene
p-methoxybenzylnitrile
1-(2,4,5-trihydroxyphenyl)-2-(4'-methoxyphenyl)ethanone
Conditions | Yield |
---|---|
Stage #1: 1,2,4-Trihydroxybenzene; p-methoxybenzylnitrile With hydrogenchloride; zinc(II) chloride In diethyl ether at 0 - 20℃; Stage #2: With water In methanol Reflux; | 79.6% |
With hydrogenchloride; zinc(II) chloride at 0℃; |
3-Methylbutenoic acid
1,2,4-Trihydroxybenzene
2,2-Dimethyl-6,7-dihydroxy-4-chromanone
Conditions | Yield |
---|---|
With zinc(II) chloride; trichlorophosphate at 50℃; for 5h; | 79% |
1,2,4-Trihydroxybenzene
Conditions | Yield |
---|---|
With triethylamine In toluene (N2); addn. of toluene and triethyl amine (excess) to a mixture of Mo-complex and 1,2,4-benzenetriol; heating to 80°C with vigorous stirring; helding there for 1 h; evapn. to dryness (vac.); adsorption chromy. on silica gel; recrystn. from dichloromethane/hexane; | 79% |
Conditions | Yield |
---|---|
With sulfated montmorillonite K-10 In nitrobenzene at 100℃; | 79% |
With montmorillonite K-10 at 100℃; |
1,2,4-Trihydroxybenzene
Conditions | Yield |
---|---|
With boron trifluoride diethyl etherate In dichloromethane at 20℃; for 0.25h; Inert atmosphere; diastereoselective reaction; | 76% |
1,2,4-Trihydroxybenzene
ethyl 3-oxo-3-phenylpropionate
5,7-dihydroxy-4-phenyl-2H-1-benzopyran-2-one
Conditions | Yield |
---|---|
With nanosilica molybdic acid 2 In neat (no solvent) at 80℃; for 0.333333h; Pechmann Condensation; Green chemistry; | 76% |
1,2,4-Trihydroxybenzene
4-(1H-imidazo[4,5-b]pyridin-2-yl)aniline
Conditions | Yield |
---|---|
Stage #1: 4-(1H-imidazo[4,5-b]pyridin-2-yl)aniline With hydrogenchloride; sodium nitrite In water at 0 - 5℃; Stage #2: 1,2,4-Trihydroxybenzene With sodium hydroxide In water at 0 - 5℃; for 2h; | 76% |
4-cyanomethylphenol
1,2,4-Trihydroxybenzene
1-(2,4,5-trihydroxyphenyl)-2-(4'-hydroxyphenyl)ethanone
Conditions | Yield |
---|---|
Stage #1: 4-cyanomethylphenol; 1,2,4-Trihydroxybenzene With hydrogenchloride; zinc(II) chloride In diethyl ether at 0 - 20℃; Stage #2: With water In methanol Reflux; | 75.4% |
With hydrogenchloride; zinc(II) chloride at 0℃; |
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