Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities
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inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
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inquiryhebei yanxi chemical co., LTD who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do research and developm
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inquiryhigh quality Appearance:White or off-white Solid Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea Port:shanghai
The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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Cas:56718-71-9
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inquiryCangzhou Enke Pharma Tech Co.,ltd. is located in Cangzhou City, Hebei province ,where is a famous petroleum chemical industry city in China. Enke Pharma a high-tech enterprise ,and we are dedicated to developing and manufacturing new api, intermedi
Cas:56718-71-9
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inquiryColorcom is a global leader in industrial chemical manufacturing and is continuously innovating and transforming to exceed client expectations and industry standards. Colorcom prides itself on superior customer and technical focus, while focusing on
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inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Cas:56718-71-9
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inquiryName:4-(2-Methoxyethyl)phenol CAS NO: 56718-71-9 Grade:Medical scientific research and export Molecular formula:C9H12O2 Molecular weight:152.1904 Product Quality 12 years of chemical raw materials Mature operation of the industry System st
Cas:56718-71-9
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inquiryOur company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O
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inquiryOur advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva
Cas:56718-71-9
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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inquiryOur Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
Cas:56718-71-9
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inquiryEnglish name p-(2-Methoxyethyl) phenol English alias 4-(2-Methoxyethyl)-phenol CAS RN 56718-71-9 Molecular formula C9H12O2 Molecular weight 152.19 Content 98% Appearance:Wh
Cas:56718-71-9
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inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
Cas:56718-71-9
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inquiryp-(2-Methoxyethyl) phenol CAS:56718-71-9 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic
Cas:56718-71-9
Min.Order:1 Gram
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:56718-71-9
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inquiryHebei Mojin Biotechnology Co., Ltd, Our company is a professional chemical raw materials and chemical reagents research and development production enterprises. Our business covers more than 30 countries, most of the big customers come from Europe, Am
Cas:56718-71-9
Min.Order:1 Kilogram
FOB Price: $170.0 / 180.0
Type:Trading Company
inquiryProduct Name: p-(2-Methoxyethyl) phenol Synonyms: Metoprolol-2;Imp. B (EP):4-(2-Methoxyethyl)phenol;Metoprolol-EP-Imp-B;P-ethyl ether;P-Methyl ether;Metoprolol Tartrate EP IMpurity-B;Metoprolol EP IMpurity B;Phenol,4-(2-Methoxyethyl)- CAS: 567
Cas:56718-71-9
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inquiryP-(2-Methoxyethyl) Phenol CAS: 56718-71-9 Specification Item Standard Identification A.H-NMR:Comply with the structure B.LC-MS:Comply with the structure C.The I
Cas:56718-71-9
Min.Order:1 Kilogram
Negotiable
Type:Other
inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Cas:56718-71-9
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inquiryBest quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
Appearance:white powder Storage:Store in a cool,dry place and keep away from direct strong light Package:As customer request Application:Used for research and industrial manufacture. Transportation:Common products:Sea/Air/Courie
Cas:56718-71-9
Min.Order:100 Metric Ton
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inquiryOur Services 1. New Molecules R&D 2. Own test center HPLC NMR GC LC-MS 3. API and Intermediates from China reputed manufacturers 4. Documents support COA MOA MSDS DMF open part Our advantages 1. Government awarded company. Top 100 enter
Cas:56718-71-9
Min.Order:1 Gram
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inquiry1. Timely and efficient service to ensure communication with customers 2. Produce products of different specifications and sizes according to your requirements. 3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures
Cas:56718-71-9
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:56718-71-9
Min.Order:0 Metric Ton
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Cas:56718-71-9
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inquirylower price and high quality Appearance:white Storage:Preserve In Well-Closed, Light-Resistant and Tight Containers. Store In Cool & Dry Place Package:1g,5g,10g...1kg,5kg...more Application:Pharmaceutical Intermediate Transportation:shipping,land,a
Cas:56718-71-9
Min.Order:1 Gram
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inquiryMassive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and
Cas:56718-71-9
Min.Order:1 Gram
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Type:Lab/Research institutions
inquiryalpha-methoxy-4-hydroxyacetophenone
4-(2-methoxyethyl)phenol
Conditions | Yield |
---|---|
With hydrogen; palladium on activated charcoal In ethanol under 2327.2 Torr; for 4h; | 96% |
With hydrogen under 3000.3 Torr; Pressure; Heating; | 80% |
With hydrogen; acetic acid; palladium on activated charcoal | |
With H2; acetic acid; palladium-carbon | 0.54 g (3.6 mmol=61%) |
4-(2-methoxyethyl)phenol
Conditions | Yield |
---|---|
palladium-carbon In hydrogenchloride; methanol | 70% |
With hydrogen; palladium-carbon In hydrogenchloride; methanol | 59% |
With hydrogen; palladium-carbon In methanol | 53% |
With hydrogenchloride; hydrogen; palladium-carbon In methanol | 47% |
p-hydroxyphenethyl alcohol
4-(2-methoxyethyl)phenol
Conditions | Yield |
---|---|
With sulfuric acid In methanol | 40% |
In methanol | 31% |
Multi-step reaction with 3 steps 1: ethanol / 9 h / Heating 2: 1.) NaH / 1.) THF, reflux, 30 min; 2.) THF, reflux, 6 h 3: H2 / 10percent Pd/C / ethanol / 24 h / 3102.9 Torr / Ambient temperature View Scheme |
4-(2-methoxyethyl)phenol
Conditions | Yield |
---|---|
With hydrogen In ethyl acetate at 50℃; under 30402 Torr; for 16h; | 10 g |
Conditions | Yield |
---|---|
With sodium methylate at 50℃; for 7h; Reagent/catalyst; | 92% |
1-(benzyloxy)-4-(2-methoxyethyl)benzene
4-(2-methoxyethyl)phenol
Conditions | Yield |
---|---|
With palladium on activated charcoal; hydrogen In tetrahydrofuran at 20℃; under 3000.3 Torr; for 24h; | 82% |
With hydrogen; palladium on activated charcoal In ethanol under 3102.9 Torr; for 24h; Ambient temperature; | |
With palladium 10% on activated carbon; hydrogen under 37503.8 Torr; for 3h; | 38.6 g |
2-(4'-hydroxyphenyl)ethyl methyl carbonate
carbonic acid dimethyl ester
4-(2-methoxyethyl)phenol
Conditions | Yield |
---|---|
With Amberlyst 15 for 36h; Reflux; | 95% |
p-hydroxyphenethyl alcohol
sodium hydrogencarbonate
4-(2-methoxyethyl)phenol
Conditions | Yield |
---|---|
In methanol | 65% |
Conditions | Yield |
---|---|
at 20℃; for 2h; Inert atmosphere; UV-irradiation; | 57% |
Conditions | Yield |
---|---|
In methanol at 20℃; for 3h; | 79% |
With methanol |
p-hydroxyphenethyl alcohol
A
2-(4-Methoxyphenyl)ethanol
B
4-(2-methoxyethyl)phenol
Conditions | Yield |
---|---|
With potassium carbonate In acetonitrile for 24h; Heating; | A 82% B 9% |
L-tyrosine
4-(2-methoxyethyl)phenol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: ammonia; [bis(acetoxy)iodo]benzene / methanol / 2 h / 0 - 20 °C / Inert atmosphere 2: 2 h / 20 °C / Inert atmosphere; UV-irradiation View Scheme |
L-<15N>tyrosine
4-(2-methoxyethyl)phenol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: ammonia; [bis(acetoxy)iodo]benzene; potassium hydroxide / methanol / 2 h / 0 °C 2: 2 h / 20 °C / Inert atmosphere; UV-irradiation View Scheme |
2-(4-benzyloxyphenyl)ethanol
4-(2-methoxyethyl)phenol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 1.) NaH / 1.) THF, reflux, 30 min; 2.) THF, reflux, 6 h 2: H2 / 10percent Pd/C / ethanol / 24 h / 3102.9 Torr / Ambient temperature View Scheme | |
Multi-step reaction with 2 steps 1: potassium hydroxide / dimethyl sulfoxide / 20 °C 2: palladium on activated charcoal; hydrogen / tetrahydrofuran / 24 h / 20 °C / 3000.3 Torr View Scheme |
phenol
4-(2-methoxyethyl)phenol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 50 percent / AlCl3 / various solvent(s) / 5 h / 70 °C 2: 90 percent / methanol / 24 h / Ambient temperature 3: 96 percent / H2 / 10percent Pd/C / ethanol / 4 h / 2327.2 Torr View Scheme | |
Multi-step reaction with 3 steps 1: aluminum (III) chloride 2: methanol / pH 8 3: hydrogen / 3000.3 Torr / Heating View Scheme |
2-bromo-1-(4'-hydroxyphenyl)-1-ethanone
4-(2-methoxyethyl)phenol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: methanol 2: H2; AcOH / Pd/C View Scheme |
4-Hydroxyacetophenone
4-(2-methoxyethyl)phenol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: CuBr2 / ethyl acetate 2: methanol 3: H2; AcOH / Pd/C View Scheme |
p-hydroxyphenacyl chloride
4-(2-methoxyethyl)phenol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 90 percent / methanol / 24 h / Ambient temperature 2: 96 percent / H2 / 10percent Pd/C / ethanol / 4 h / 2327.2 Torr View Scheme |
Acetic acid 4-(2-methoxy-ethyl)-phenyl ester
4-(2-methoxyethyl)phenol
Conditions | Yield |
---|---|
With sodium hydroxide In ethanol for 4h; Heating; | |
With sodium hydroxide |
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 2: NaOH 3: H2O2, HCOOH 4: NaOH View Scheme | |
Multi-step reaction with 6 steps 1: 207 g / pyridine / benzene / 5 h / 25 - 30 °C 2: 218 g / aluminium chloride / CH2Cl2 / 6 h / Ambient temperature 3: 71 g / sodium hydroxide / ethanol / 5 h / Heating 4: sodium hydroxide / dimethylsulfoxide / 4 h / 50 - 60 °C 5: 88 percent formic acid, cc. sulfuric acid, 35 percent hydrogen peroxide / acetic anhydride / 3 h / 40 - 50 °C 6: sodium hydroxide / ethanol / 4 h / Heating View Scheme |
1-<4-(1-hydroxyethyl)phenyl>ethanone
4-(2-methoxyethyl)phenol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: NaOH 2: H2O2, HCOOH 3: NaOH View Scheme | |
Multi-step reaction with 3 steps 1: sodium hydroxide / dimethylsulfoxide / 4 h / 50 - 60 °C 2: 88 percent formic acid, cc. sulfuric acid, 35 percent hydrogen peroxide / acetic anhydride / 3 h / 40 - 50 °C 3: sodium hydroxide / ethanol / 4 h / Heating View Scheme |
4-methoxyethylacetophenone
4-(2-methoxyethyl)phenol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: H2O2, HCOOH 2: NaOH View Scheme | |
Multi-step reaction with 2 steps 1: 88 percent formic acid, cc. sulfuric acid, 35 percent hydrogen peroxide / acetic anhydride / 3 h / 40 - 50 °C 2: sodium hydroxide / ethanol / 4 h / Heating View Scheme |
4-chloro-phenol
4-(2-methoxyethyl)phenol
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: potassium carbonate / N,N-dimethyl-formamide / 1 h / 80 °C 1.2: 1 h / 105 °C 2.1: magnesium; iodine / 2-methyltetrahydrofuran / 2 h / Reflux 3.1: sodium hydroxide / toluene; water / 2 h 3.2: 2 h 4.1: palladium 10% on activated carbon; hydrogen / 3 h / 37503.8 Torr View Scheme | |
Multi-step reaction with 4 steps 1.1: sulfuric acid / toluene / 16 h / -10 - 0 °C 2.1: magnesium / tetrahydrofuran / 16 h / 65 - 72 °C / Inert atmosphere 2.2: 0 - 10 °C / Inert atmosphere 3.1: thionyl chloride; N,N-dimethyl-formamide / toluene / 2 h / 55 - 60 °C 4.1: sodium methylate / 7 h / 50 °C View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 1.) Et3N, 2.) H2 / 1/2.) 5percent Pd/C / 1.) toluene, 120 deg C, 16 h, 2.) toluene, 85 deg C, 150 psi, 45 min 2: 1.) NaNO2, 50percent H2SO4, 2.) urea / 1.) H20, 5 deg C, 15 min, 2.) H2O, 100 - 105 deg C, 1 h View Scheme |
β-(4-acetylphenyl)ethyl acetate
4-(2-methoxyethyl)phenol
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: 71 g / sodium hydroxide / ethanol / 5 h / Heating 2: sodium hydroxide / dimethylsulfoxide / 4 h / 50 - 60 °C 3: 88 percent formic acid, cc. sulfuric acid, 35 percent hydrogen peroxide / acetic anhydride / 3 h / 40 - 50 °C 4: sodium hydroxide / ethanol / 4 h / Heating View Scheme |
acetic acid phenethyl ester
4-(2-methoxyethyl)phenol
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: 218 g / aluminium chloride / CH2Cl2 / 6 h / Ambient temperature 2: 71 g / sodium hydroxide / ethanol / 5 h / Heating 3: sodium hydroxide / dimethylsulfoxide / 4 h / 50 - 60 °C 4: 88 percent formic acid, cc. sulfuric acid, 35 percent hydrogen peroxide / acetic anhydride / 3 h / 40 - 50 °C 5: sodium hydroxide / ethanol / 4 h / Heating View Scheme |
4-chlorophenyl benzyl ether
4-(2-methoxyethyl)phenol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: magnesium; iodine / 2-methyltetrahydrofuran / 2 h / Reflux 2.1: sodium hydroxide / toluene; water / 2 h 2.2: 2 h 3.1: palladium 10% on activated carbon; hydrogen / 3 h / 37503.8 Torr View Scheme |
4-tert-butoxychlorobenzene
4-(2-methoxyethyl)phenol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: magnesium / tetrahydrofuran / 16 h / 65 - 72 °C / Inert atmosphere 1.2: 0 - 10 °C / Inert atmosphere 2.1: thionyl chloride; N,N-dimethyl-formamide / toluene / 2 h / 55 - 60 °C 3.1: sodium methylate / 7 h / 50 °C View Scheme |
4-tert-butoxybromobenzene
4-(2-methoxyethyl)phenol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: magnesium / tetrahydrofuran / 6 h / 65 - 72 °C / Inert atmosphere 1.2: 0 - 10 °C / Inert atmosphere 2.1: thionyl chloride; N,N-dimethyl-formamide / toluene / 2 h / 55 - 60 °C 3.1: sodium methylate / 7 h / 50 °C View Scheme |
4-bromo-phenol
4-(2-methoxyethyl)phenol
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: sulfuric acid / toluene / 16 h / -10 - 0 °C 2.1: magnesium / tetrahydrofuran / 6 h / 65 - 72 °C / Inert atmosphere 2.2: 0 - 10 °C / Inert atmosphere 3.1: thionyl chloride; N,N-dimethyl-formamide / toluene / 2 h / 55 - 60 °C 4.1: sodium methylate / 7 h / 50 °C View Scheme |
4-(2-methoxyethyl)phenol
4-[(4-chloro-2-pyrimidinyl)amino]benzonitrile
4-{4-[4-(2-methoxylethyl)phenoxy]pyrimidin-2-ylamino}benzonitrile
Conditions | Yield |
---|---|
Stage #1: 4-(2-methoxyethyl)phenol With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 0.166667h; Inert atmosphere; Stage #2: 4-[(4-chloro-2-pyrimidinyl)amino]benzonitrile In N,N-dimethyl-formamide at 80℃; Inert atmosphere; | 98.4% |
succinic acid
4-(2-methoxyethyl)phenol
isopropylamine
epichlorohydrin
Conditions | Yield |
---|---|
Stage #1: 4-(2-methoxyethyl)phenol; epichlorohydrin With sodium hydroxide In water at 30 - 40℃; for 5h; Stage #2: isopropylamine In water at 20 - 30℃; for 5h; Stage #3: succinic acid In acetone at 20 - 35℃; Temperature; Solvent; | 97.8% |
3-hydroxy-3-phenyl-2,3-dihydro-isoindol-1-one
4-(2-methoxyethyl)phenol
Conditions | Yield |
---|---|
Stage #1: 3-hydroxy-3-phenyl-2,3-dihydro-isoindol-1-one With methanesulfonic acid In cyclohexane at 25℃; for 0.166667h; Betti Reaction; Stage #2: 4-(2-methoxyethyl)phenol In cyclohexane at 80℃; for 16h; Betti Reaction; | 97% |
4-(2-methoxyethyl)phenol
4-{6-methyl-4-[4-(2-methoxylethyl)phenoxy]pyrimidin-2-ylamino}benzonitrile
Conditions | Yield |
---|---|
Stage #1: 4-(2-methoxyethyl)phenol With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 0.166667h; Inert atmosphere; Stage #2: 4-(4-chloro-6-methyl-pyrimidin-2-ylamino)-benzonitrile In N,N-dimethyl-formamide at 80℃; Inert atmosphere; | 96.2% |
4-(2-methoxyethyl)phenol
epichlorohydrin
2-[4-(2'-methoxyethyl)phenoxymethyl]oxirane
Conditions | Yield |
---|---|
With sodium hydroxide at 85 - 90℃; pH=8; Temperature; pH-value; Flow reactor; | 95.2% |
With sodium hydroxide at 90 - 115℃; under 1500.15 - 2250.23 Torr; pH=9; Flow reactor; | 95.2% |
With sodium hydroxide In water at 40 - 45℃; for 3 - 5h; | 93% |
4-(2-methoxyethyl)phenol
allyl bromide
3-[4-(2-methoxyethyl)phenoxy]propylene
Conditions | Yield |
---|---|
With potassium carbonate In acetone Reflux; | 87% |
With potassium carbonate In acetone for 7h; Heating; | 85% |
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); sodium acetate; acetic anhydride at 20℃; for 12h; Inert atmosphere; | 87% |
4-(2-methoxyethyl)phenol
Conditions | Yield |
---|---|
With DBN In acetonitrile at 80℃; for 4h; | 84% |
1,1,1,2,3,3-hexafluoro-2-(heptafluoropropoxy)-3-[(trifluorovinyl)oxy]propane
4-(2-methoxyethyl)phenol
Conditions | Yield |
---|---|
With potassium hydroxide Addition; | 78% |
Conditions | Yield |
---|---|
With palladium diacetate; acetic anhydride; triethylamine; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene In toluene at 80℃; for 12h; Inert atmosphere; | 78% |
(S)-epichlorohydrin
4-(2-methoxyethyl)phenol
A
(2S)-2-{[4-(2-Methoxyethyl)phenoxy]methyl}oxirane
B
(R)-2-{[4-(2-methoxyethyl)phenoxy]methyl}oxirane
Conditions | Yield |
---|---|
With potassium carbonate In acetonitrile for 14h; Reflux; optical yield given as %ee; | A n/a B 75% |
4-(2-methoxyethyl)phenol
(S)-5-((4-(2-methoxyethyl)phenoxy)methyl)oxazolidin-2-one
Conditions | Yield |
---|---|
With potassium hydroxide In 4-methyl-2-pentanone at 110 - 115℃; for 2 - 3h; Large scale reaction; | 75% |
(R)-(-)-epichlorohydrin
4-(2-methoxyethyl)phenol
A
(2S)-2-{[4-(2-Methoxyethyl)phenoxy]methyl}oxirane
B
(R)-2-{[4-(2-methoxyethyl)phenoxy]methyl}oxirane
Conditions | Yield |
---|---|
With potassium carbonate In acetonitrile for 14h; Reflux; optical yield given as %ee; | A 73% B n/a |
4-(2-methoxyethyl)phenol
(4S)-N-tert-butoxycarbonyl-4-[[(4'-methylbenzenesulfonyl)oxy]methyl]-2,2-dimethyl-1,3-oxazolidine
4(R)-4-((4-(2-methoxyethyl)phenoxy)methyl)-2,2-dimethyloxazolidine-3-carboxylic acid tert-butyl ester
Conditions | Yield |
---|---|
Stage #1: 4-(2-methoxyethyl)phenol With sodium hydride In N,N-dimethyl-formamide at 20℃; Stage #2: (4S)-N-tert-butoxycarbonyl-4-[[(4'-methylbenzenesulfonyl)oxy]methyl]-2,2-dimethyl-1,3-oxazolidine In N,N-dimethyl-formamide at 40℃; for 1h; | 71% |
With sodium hydride In N,N-dimethyl-formamide at 60 - 80℃; | |
Stage #1: 4-(2-methoxyethyl)phenol With sodium hydride In N,N-dimethyl-formamide at 20℃; for 0.166667h; Stage #2: (4S)-N-tert-butoxycarbonyl-4-[[(4'-methylbenzenesulfonyl)oxy]methyl]-2,2-dimethyl-1,3-oxazolidine In N,N-dimethyl-formamide at 60 - 80℃; for 2h; Further stages.; |
1-(6-chloro-5-nitro-pyrimidin-4-yl)-piperidine-4-carboxylic acid ethyl ester
4-(2-methoxyethyl)phenol
1-{6-[4-(2-methoxyethyl)-phenoxy]-5-nitropyrimidin-4-yl}-piperidine-4-carboxylic acid ethyl ester
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 90℃; for 15h; | 71% |
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