Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities
Cas:594-70-7
Min.Order:1 Kilogram
FOB Price: $3.0
Type:Lab/Research institutions
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Cas:594-70-7
Min.Order:5 Kiloliter
FOB Price: $1.2 / 5.0
Type:Manufacturers
inquiryTIANFUCHEM--594-70-7--High purity 2-Methyl-2-nitropropanein stock Our company was built in 2009 with an ISO certificate.In the past 10 years, we have grown up as a famous fine chemicals supplier in China And we had established stable busin
Cas:594-70-7
Min.Order:1 Metric Ton
FOB Price: $2000.0
Type:Lab/Research institutions
inquiryOur advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva
Cas:594-70-7
Min.Order:1 Kilogram
FOB Price: $9.0 / 99.0
Type:Trading Company
inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:594-70-7
Min.Order:10 Gram
FOB Price: $146.0 / 176.0
Type:Trading Company
inquiry1.In No Less 10 years exporting experience. you can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specializ
Cas:594-70-7
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
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Min.Order:0
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Type:Lab/Research institutions
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Cas:594-70-7
Min.Order:0 Metric Ton
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Type:Other
inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Cas:594-70-7
Min.Order:0
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Type:Lab/Research institutions
inquiryZhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed
Cas:594-70-7
Min.Order:1 Kilogram
FOB Price: $2.0
Type:Lab/Research institutions
inquiryLower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe
Hunan chemfish Pharmaceutical co.,Ltd.located in Lugu High-tech industral park ,Hunan province . with its own R&D center and more than 10000㎡manufacture plant . Chemfish owns 40 reactors from 1000L to 8000L. With complete auxiliary equipment as
high quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea
2-Methyl-2-nitropropaneAppearance:detailed see specifications Storage:Keep away of light, cool place Package:25kg/drum;200kg/drum Application:Used in Synthesis, Pharmaceuticals and other fields Transportation:Sea/air/courier
We are committed to providing our customers with the best products and services at the most competitive prices.Appearance:off-white powder Storage:Room temperature with sealed well Package:according to the clients requirement Application:Use as prima
2-Methyl-2-nitropropane cas 594-70-7Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
Price, service, company and transport advantage: 1. Best service, place of origin China, high quality, and reasonable price. 2. It's customers' right to choose the package (EMS, DHL, FEDEX, UPS). 3. It's customers' right
Cas:594-70-7
Min.Order:0
Negotiable
Type:Trading Company
inquiryAt Share Chemical Company, we scrupulously abide by our policy of “Excellent Quality at a Reasonable Price”. We strive to satisfy all of our customers by providing the finest quality products supported by the finest in customer servi
FINETECH INDUSTRY LIMITED is a LONDON based CRO company providing drug discovery & development services to worldwide clients. FINETECH INDUSTRY LIMITED supplies the 2-Methyl-2-nitropropane, CAS:594-70-7 with the most competitive price and the best qu
1.We have rich experience in the development and production 2.Our factory is in Shanghai of China,We have convenient traffic conditions.3.We have advanced testing equipment and shipping line. Package:5g, 10g, 50g, 100g, 1kg Application:Pharmaceutical
Debyesci is here who supplied several kinds of chemical products to global pharmaceutical, drug discovery, agrochemical and biotechnology industries for four yearsOur key scientific leadership team has gained experience in top research and developmen
CFTC?PharmaChem?is?a?service?based?company?in?China,?a?pharmachem?division?of?Changzhou?Foreign?Trade?Corp.,supplying?raw?materials,?intermediates,?APIs?and?fine?chemicals?for?the?pharmaceutical?and?specialty?chemical?industries?worldwide. Applicatio
Conditions | Yield |
---|---|
With dihydrogen peroxide; Na12[WZn3(H2O)2(ZnW9O34)2] at 75℃; for 7h; | 100% |
With potassium permanganate In water 1.) 11 deg C -> room temperature, 8 h, 2.) 55 deg C, 18 h; | 78% |
With sodium permanganate In hexane at 69℃; for 24h; | 76% |
Conditions | Yield |
---|---|
With nitronium tetrafluoborate; silver carbonate In N,N-dimethyl acetamide at 90℃; for 12h; Inert atmosphere; Schlenk technique; regioselective reaction; | 79% |
Conditions | Yield |
---|---|
With iodosylbenzene; meso-tetraphenylporphyrin iron(III) chloride In dichloromethane at 0℃; | 75% |
tert-butylmercury chloride
2-Methyl-2-nitropropane
Conditions | Yield |
---|---|
With potassium nitrite; 18-crown-6 ether In various solvent(s) for 2h; Irradiation; | 70% |
With potassium nitrite; 18-crown-6 ether In dimethyl sulfoxide at 35℃; Irradiation; | 71 % Spectr. |
t-butylnitrite
1-(trimethylsilyl)-2-methyl-1-propenyl triflate
A
2,2,4,4-tetramethyl-1,3-cyclobutanedione
B
dimethylacetylene
C
2-Methyl-2-nitropropane
D
N-tert-butylmethacrylamide
E
N-tert-butylisobutyramide
F
N-tert-butyl-2-hydroxy-2-methylpropanamide
Conditions | Yield |
---|---|
With tetrabutyl ammonium fluoride In 1,2-dimethoxyethane at -20℃; for 0.0333333h; Mechanism; | A 8.3% B 70% C n/a D 6.4% E 8.3% F 5.3% |
t-butyl azide
2-Methyl-2-nitropropane
Conditions | Yield |
---|---|
With HOF* CH3CN In chloroform at -78℃; | 70% |
Conditions | Yield |
---|---|
With N-hydroxyphthalimide; air; Nitrogen dioxide In various solvent(s) at 70℃; under 1520.1 Torr; for 14h; | 61% |
With N-hydroxyphthalimide; air; Nitrogen dioxide In various solvent(s) at 70℃; under 760 Torr; for 14h; | 46% |
With nitric acid at 150℃; |
Conditions | Yield |
---|---|
In methanol at 20℃; Solvent; | A 0.5% B 60% |
sodium 2-nitropropane
1N-methyl-2,4,6-triphenylpyridinium tetrafluoroborate
A
2-Methyl-2-nitropropane
B
2,4,6-triphenylpyridine
Conditions | Yield |
---|---|
In dimethyl sulfoxide at 80℃; | A 57% B n/a |
In dimethyl sulfoxide at 25℃; for 2h; Rate constant; Kinetics; |
N-tert-Butylhydroxylamine
2-Methyl-2-nitropropane
Conditions | Yield |
---|---|
With potassium permanganate In water at 45 - 55℃; | 52% |
Conditions | Yield |
---|---|
In methanol at 20℃; Solvent; | A n/a B 0.65% |
Conditions | Yield |
---|---|
With nitric acid |
Conditions | Yield |
---|---|
With silver(I) nitrite; diethyl ether |
Conditions | Yield |
---|---|
With silver(I) nitrite unter Kuehlung; |
1,1-dibromo-1-nitro-ethane
dimethyl zinc(II)
A
Nitroethane
B
2-nitropropane
C
2-Methyl-2-nitropropane
N-(benzenesulfonyl)-3-phenyloxaziridine
tert-butylamine
A
t-butylnitrite
B
2-Methyl-2-nitropropane
C
N-benzylidene tert-butylamine
D
N-tert-butyl-α-phenylnitrone
Conditions | Yield |
---|---|
In chloroform-d1 for 1h; Product distribution; other primary amines; | A 30 % Spectr. B n/a C 65 % Spectr. D n/a |
tert-butylamine
A
tert-butylnitroso dimer
B
t-butylnitrite
C
2-Methyl-2-nitropropane
Conditions | Yield |
---|---|
With oxaziridinium tetrafluoroborate derived from N-methyl-1,2,3,4-tetrahydroisoquinoline In dichloromethane at 0℃; for 48h; | A 50 % Spectr. B 30 % Spectr. C 20 % Spectr. |
With oxaziridinium tetrafluoroborate derived from N-methyl-1,2,3,4-tetrahydroisoquinoline In dichloromethane for 2h; | A 5 % Spectr. B 65 % Spectr. C 25 % Spectr. |
Conditions | Yield |
---|---|
at 150℃; |
Conditions | Yield |
---|---|
With diethyl ether |
diethyl ether
tertiary butyl chloride
A
tert.-butylnitrite
B
2-Methyl-2-nitropropane
2,2-dimethylpropane
nitric acid
A
nitromethane
B
2-Methyl-2-nitropropane
C
2,2-dimethyl-1-nitro-propane
Conditions | Yield |
---|---|
at 410℃; |
Isobutane
nitric acid
A
2-nitropropane
B
1-nitroisobutane
C
2-Methyl-2-nitropropane
D
acetone
Conditions | Yield |
---|---|
at 420℃; Produkt 5:Nitromethan; |
Conditions | Yield |
---|---|
In tetralin at 154℃; Mechanism; Kinetics; Ea, log A, other solvent, other temperatures; |
2,2-dimethylpropyl nitrate
A
formaldehyd
B
tert.-butylnitrite
C
tetramethyl-2,2,3,3 butane
D
2-methyl-2-butanol nitrate
E
2-Methyl-2-nitropropane
F
pivalaldehyde
Conditions | Yield |
---|---|
In cyclohexane at 175℃; Mechanism; gas phase; |
2-Methyl-2-nitropropane
N-tert-Butylhydroxylamine
Conditions | Yield |
---|---|
With acetic acid; zinc In ethanol at 10 - 20℃; for 3h; | 100% |
With ammonia borane; gold on titanium oxide In ethanol at 20℃; for 0.666667h; Inert atmosphere; | 85% |
Reduction; | 82% |
tetrakis(triphenylphosphine)nickel(0)
2-Methyl-2-nitropropane
C4H9NONi(P(C6H5)3)2
Conditions | Yield |
---|---|
In benzene Kinetics; byproducts: P(C6H5)3, OP(C6H5)3; the soln. of Ni(PPh3)4/benzene was added to the soln. of t-BuNO2/benzene with stirring at under Ar, stirred for 1 h; evapd. in vac., washed with hot hexane, dried in vac.; | 100% |
2-Methyl-2-nitropropane
tetrakis(triethylphosphine)nickel(0)
C4H9NONi(P(C2H5)3)2
Conditions | Yield |
---|---|
In pentane Kinetics; byproducts: P(C2H5)3, OP(C2H5)3; to the soln. of Ni(PEt3)4/butane the soln. of t-BuNO2/pentane was addedwith stirring at -6°C under Ar, stirred for 1 h, warmed to 25°C; butane was added, cooled to -20°C, the liquid was remuved, partially evapd., this procedure repeated five times, crystd. at -78°C; | 100% |
2-Methyl-2-nitropropane
tert-butylamine hydrochloride
Conditions | Yield |
---|---|
Stage #1: 2-Methyl-2-nitropropane With iron(III)-acetylacetonate; hydrazine hydrate In methanol at 150℃; for 0.0333333h; Microwave irradiation; Stage #2: With hydrogenchloride In water; ethyl acetate chemoselective reaction; | 99% |
Stage #1: 2-Methyl-2-nitropropane With C36H56Cl3CrN2O; magnesium; 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane In tetrahydrofuran at 60℃; for 24h; Inert atmosphere; Schlenk technique; Stage #2: With hydrogenchloride In tetrahydrofuran; water; ethyl acetate at 20℃; | 99% |
2-Methyl-2-nitropropane
(1R,3aR,4S,7aR)-octahydro-1-[(1’R,2’E)-4’-acetoxy-1’-methyl-but-2’-en-1’-yl]-7a-methyl-4-triethylsilyloxy-1H-indene
(1R,3aR,4S,7aR)-octahydro-1-[(1’R,2’E)-1’,5’-dimethyl-5’-nitro-hex-2’-en-1’-yl]-7a-methyl-4-triethylsilyloxy-1H-indene
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); caesium carbonate In dimethyl sulfoxide at 20℃; for 16h; | 99% |
2-Methyl-2-nitropropane
ortho-anisaldehyde
C-(2-methoxyphenyl)-N-tert-butylnitrone
Conditions | Yield |
---|---|
With acetic acid; zinc In ethanol for 2h; Ambient temperature; | 97% |
Conditions | Yield |
---|---|
With [Zn(BH4)2(py)] In tetrahydrofuran for 0.67h; Heating; | 96% |
Stage #1: 2-Methyl-2-nitropropane In water; acetonitrile at 20℃; for 0.0833333h; Stage #2: With sodium tetrahydroborate In water; acetonitrile at 20℃; for 0.5h; | 90% |
With palladium on activated charcoal; tetrabutylammomium bromide; water; sodium hydroxide; silicon at 100℃; for 6h; | 86% |
Conditions | Yield |
---|---|
With acetic acid; zinc In ethanol at 20℃; for 66h; | 96% |
Conditions | Yield |
---|---|
With acetic acid; zinc In ethanol at 20℃; for 20h; | 95% |
2-Methyl-2-nitropropane
3-Trifluoromethylbenzaldehyde
C-<3-(α,α,α-trifluoromethyl)phenyl>-N-tert-butylnitrone
Conditions | Yield |
---|---|
With acetic acid; zinc In ethanol for 2h; Ambient temperature; | 93% |
With acetic acid; zinc In ethanol at 0 - 20℃; for 16h; | 39% |
2-Methyl-2-nitropropane
ortho-anisaldehyde
N-tert-butyl-α-(2-methoxy)phenylnitrone
Conditions | Yield |
---|---|
With acetic acid; zinc In ethanol at 0 - 60℃; for 22.5h; Inert atmosphere; Darkness; Molecular sieve; | 92% |
With zinc diacetate; acetic acid In ethanol | 877.2 mg(93%) |
Conditions | Yield |
---|---|
With sodium tetrahydroborate; nickel(II) chloride hexahydrate In water at 20℃; for 3h; Inert atmosphere; Green chemistry; | 92% |
2-Methyl-2-nitropropane
3,4 difluorobenzaldehyde
3,4-difluorophenyl t-butyl nitrone
Conditions | Yield |
---|---|
With acetic acid In ethanol | 91% |
2-Methyl-2-nitropropane
2,5-difluorobenzaldehyde
N-tert-butyl-α-(2,5-difluorophenyl)nitrone
Conditions | Yield |
---|---|
With acetic acid In ethanol | 90% |
Conditions | Yield |
---|---|
Stage #1: 2-Methyl-2-nitropropane With acetic acid; zinc In ethanol at 20℃; for 3h; Cooling with ice; Stage #2: C16H15NO2 In ethanol at 20℃; for 10h; | 90% |
Stage #1: 2-Methyl-2-nitropropane With acetic acid; zinc In ethanol at 20℃; for 3h; Cooling with ice; Stage #2: C16H15NO2 In ethanol at 20℃; for 10h; | 90% |
Conditions | Yield |
---|---|
Stage #1: 2-Methyl-2-nitropropane With acetic acid; zinc In ethanol at 20℃; for 3h; Cooling with ice; Stage #2: C12H13NO2 In ethanol at 20℃; for 16h; | 89% |
Stage #1: 2-Methyl-2-nitropropane With acetic acid; zinc In ethanol at 20℃; for 3h; Cooling with ice; Stage #2: C12H13NO2 In ethanol at 20℃; for 16h; | 89% |
Conditions | Yield |
---|---|
With acetic acid; zinc In ethanol at 20℃; for 29h; | 88% |
2-Methyl-2-nitropropane
N-ethyl-N,N-diisopropylamine
N-ethylidene-1,1-dimethylethanamine N-oxide
Conditions | Yield |
---|---|
With tris(2,2'-bipyridyl)ruthenium(II)chloride hexahydrate In acetonitrile at 50℃; for 9h; Irradiation; | 88% |
2-Methyl-2-nitropropane
butyraldehyde
N-butylidene-1,1-dimethylethanamine N-Oxide
Conditions | Yield |
---|---|
With tris(2,2'-bipyridyl)ruthenium(II)chloride hexahydrate; N,N-bis(1-methylethyl)-2-methyl-1-propanamine In acetonitrile at 50℃; for 9h; Irradiation; | 88% |
4-Trifluoromethylbenzaldehyde
2-Methyl-2-nitropropane
C-<4-(α,α,α-trifluoromethyl)phenyl>-N-tert-butylnitrone
Conditions | Yield |
---|---|
With acetic acid; zinc In ethanol for 2h; Ambient temperature; | 86% |
2-Methyl-2-nitropropane
3-diazo-5-phenyl-3H-1,2,4-triazole
A
t-butylnitrite
B
benzonitrile
Conditions | Yield |
---|---|
at 80℃; Yields of byproduct given; | A 86% B n/a |
2-Methyl-2-nitropropane
benzaldehyde
(Z)-N-benzylidene-2-methylpropan-2-amine oxide
Conditions | Yield |
---|---|
With acetic acid; zinc In ethanol at 20℃; for 21h; | 85% |
With tin(II) chloride dihdyrate; sodium carbonate In tetrahydrofuran for 32h; Reflux; | 82% |
With acetic acid; zinc In ethanol 1.) 10 deg C, 2 h, 2.) 6 deg C, 48 h; | 78% |
Conditions | Yield |
---|---|
With acetic acid; zinc In ethanol at 20℃; for 19h; | 85% |
2-Methyl-2-nitropropane
N,N-bis(1-methylethyl)-2-methyl-1-propanamine
(Z)-2-methyl-N-(2-methylpropylidene)propan-2-amine N-oxide
Conditions | Yield |
---|---|
With tris(2,2'-bipyridyl)ruthenium(II)chloride hexahydrate In acetonitrile at 50℃; for 9h; Irradiation; | 84% |
2-Methyl-2-nitropropane
3-Fluorobenzaldehyde
(Z)-N-3-fluorobenzylidene-t-butanamine oxide
Conditions | Yield |
---|---|
With acetic acid; zinc In ethanol for 2h; Ambient temperature; | 83% |
With acetic acid; zinc In ethanol at 0 - 20℃; |
2-Methyl-2-nitropropane
3-methoxy-benzaldehyde
N-tert-butyl-α-(3-methoxy)phenylnitrone
Conditions | Yield |
---|---|
With acetic acid; zinc In ethanol at 0 - 60℃; for 24h; Inert atmosphere; Darkness; Molecular sieve; | 83% |
2-Methyl-2-nitropropane
β-naphthaldehyde
(Z)‑N‑(tert‑butyl)‑1‑(naphthalen‑2‑yl)methanimine oxide
Conditions | Yield |
---|---|
With tin(II) chloride dihdyrate; sodium carbonate In tetrahydrofuran for 32h; Reflux; | 81% |
With acetic acid; zinc In ethanol at 0 - 20℃; |
2-Methyl-2-nitropropane
4-chlorobenzaldehyde
(Z)‑N‑(tert‑butyl)‑1‑(4‑chlorophenyl)methanimine oxide
Conditions | Yield |
---|---|
With acetic acid; zinc In ethanol for 2h; Ambient temperature; | 80% |
With tin(II) chloride dihdyrate; sodium carbonate In tetrahydrofuran for 32h; Reflux; | 80% |
2-Methyl-2-nitropropane
4-bromo-benzaldehyde
N-<(4-Bromophenyl)methylene>-2-methyl-2-propanamine N-oxide
Conditions | Yield |
---|---|
With acetic acid; zinc In ethanol for 2h; Ambient temperature; | 80% |
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