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Methyl isopropyl ether CAS NO.598-53-8 Application:Methyl isopropyl ether CAS NO.598-53-8
2,6-di-tert-butyl-4-methylpyridine
methyltriphenylbismuthonium tetrafluoroborate
isopropyl alcohol
A
isopropyl methyl ether
B
2,6-di-tert-butyl-4-methylpyridinium tetrafluoroborate
C
triphenylbismuthane
Conditions | Yield |
---|---|
In chloroform-d1 alcohol was added to mixt. (Ph3BiMe)(BF4) and 2,6-di-tert-butyl-4-methylpyridine in CDCl3 and allowed to react at 23°C for 4-7 h; detn. by NMR; | A 82% B 100% C 100% |
methanol
isopropyloxy(diphenyl)-λ6-sulfanenitrile
A
isopropyl methyl ether
B
S,S-diphenylsulphoximine
Conditions | Yield |
---|---|
at 45℃; for 114h; | A 99% B n/a |
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide for 48h; Heating; | 66% |
ethyl methyl ether
diazomethane-d2
A
diethyl ether
B
isopropyl methyl ether
C
ethene
D
Dimethyl ether
E
methyl propyl ether
Conditions | Yield |
---|---|
Product distribution; Mechanism; Ambient temperature; Irradiation; deuterium distribution; | A 29.7% B 17.9% C n/a D 37.2% E 15.2% |
diazomethane
ethyl methyl ether
A
diethyl ether
B
isopropyl methyl ether
C
ethene
D
methyl propyl ether
Conditions | Yield |
---|---|
Product distribution; Mechanism; Ambient temperature; Irradiation; | A 34% B 33.2% C n/a D 32.8% |
diazomethane
aluminum isopropoxide
isopropyl methyl ether
Conditions | Yield |
---|---|
With isopropyl alcohol |
diazomethane
aluminum isopropoxide
isopropyl alcohol
isopropyl methyl ether
diazomethane
isopropyl alcohol
A
isopropyl methyl ether
B
ethene
C
iso-butanol
D
tert-butyl alcohol
Conditions | Yield |
---|---|
bei der Einw. von Sonnenlicht; |
Conditions | Yield |
---|---|
With 1,2-dimethoxyethane; naphthalene; sodium Behandlung der Loesung mit Dimethylsulfat unterhalb 20grad; |
Conditions | Yield |
---|---|
With sodium hydride | |
With sodium hydride 1.) ether, 4 h, reflux, 2.) 0.5 h at 20 deg C, reflux, 1 h; Multistep reaction; | |
With diethylene glycol dimethyl ether; sodium hydride | |
Stage #1: isopropyl alcohol With sodium hydride In dimethyl sulfoxide Stage #2: methyl iodide In dimethyl sulfoxide at 20℃; for 5h; Further stages.; |
methanol
Methyltriisopropoxyphosphonium tetrafluoroborate
isopropyl methyl ether
Conditions | Yield |
---|---|
at 25℃; for 12h; | 90 % Spectr. |
Conditions | Yield |
---|---|
Thermodynamic data; Mechanism; calculated (BEBO and equibonding method) activation energies for hydrogen atom transfer reaction, anodic methoxylation; |
Conditions | Yield |
---|---|
With sodium hydroxide; tetra-(n-butyl)ammonium iodide In chlorobenzene 1.) ice bath, 1h, 2.) water bath, 2h; |
Tetramethyl-[1,2,4,5]tetroxan
A
methanol
B
biphenyl
C
isopropyl methyl ether
D
acetic acid methyl ester
E
acetone
F
toluene
Conditions | Yield |
---|---|
In benzene at 135.5 - 165℃; Rate constant; Product distribution; Mechanism; ΔH(excit.), ΔS(excit.); dependence of kexp from ACDP initial conc. at different temperatures; |
Conditions | Yield |
---|---|
beim Zersetzen des bildenden Anlagerungsprodukts mit Natronlage; |
1-(4-ethoxycarbonylphenyl)-3-methyltriazene
isopropyl alcohol
A
isopropyl methyl ether
B
p-aminoethylbenzoate
Conditions | Yield |
---|---|
copper(II) ion at 35℃; Rate constant; Mechanism; |
acetic acid methyl ester
isopropyl alcohol
A
propene
B
isopropyl methyl ether
C
di-isopropyl ether
D
Isopropyl acetate
Conditions | Yield |
---|---|
With sodium oxide; aluminum oxide at 280℃; Product distribution; Further Variations:; different persentage compositions of reactans; |
propene
propane
Dimethyl ether
1,2-propanediene
prop-1-yne
A
methanol
B
isopropyl methyl ether
C
di-isopropyl ether
D
isopropyl alcohol
E
acetone
Conditions | Yield |
---|---|
With hydrogen; hydrogenation catalyst from SCI of Louisville, Ky., USA at 209℃; under 16801.7 Torr; |
methanol
1,2-propanediene
2,2-dimethoxy-propane
prop-1-yne
A
propene
B
isopropyl methyl ether
C
propane
D
methyl propyl ether
E
acetone
Conditions | Yield |
---|---|
Zn-Si catalyst prepared from silicagel and zinc acetate, content of zinc amounts to 20percent converting to ZnO Product distribution / selectivity; |
Conditions | Yield |
---|---|
With hydrogen In methanol at 210℃; under 37503.8 - 180018 Torr; for 12h; | 98 %Chromat. |
methanol
propene
propane
1,2-propanediene
prop-1-yne
A
isopropyl methyl ether
B
methyl propyl ether
C
acetone
Conditions | Yield |
---|---|
Stage #1: methanol at 170℃; under 5250.53 Torr; for 0.25h; Stage #2: propene; propane; 1,2-propanediene; prop-1-yne; Zn-Si catalyst prepared from silicagel and zinc acetate, content of zinc amounts to 20percent converting to ZnO at 175 - 220℃; under 5250.53 Torr; for 506h; Product distribution / selectivity; |
Conditions | Yield |
---|---|
Stage #1: isopropyl alcohol With methane; dinitrogen monoxide Stage #2: methylene chloride Kinetics; Thermodynamic data; Gas phase; |
isopropyl methyl ether
(1R,3R,4S,9R)-6-bromo-5,8-dimethoxy-9-methyl-2,3-dihydro-1,4-(epoxymethano)naphthalene-3,4(1H)-diol
(3aR,5S,9bR,10R)-8-bromo-6,9-dimethoxy-2,2,10-trimethyl-4,5-dihydro-3aH-5,9b-(epoxymethano)naphtho[1,2-d][1,3]dioxole
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In tetrahydrofuran at 0 - 20℃; for 12h; | 91% |
isopropyl methyl ether
Conditions | Yield |
---|---|
With pyridinium p-toluenesulfonate In acetone at 20℃; for 3h; Inert atmosphere; Combinatorial reaction / High throughput screening (HTS); | 90% |
isopropyl methyl ether
Conditions | Yield |
---|---|
With pyridinium p-toluenesulfonate In acetone at 20℃; for 3h; Inert atmosphere; Combinatorial reaction / High throughput screening (HTS); | 88% |
isopropyl methyl ether
2-<(R)-3-benzyloxytetradecanamido>-2-deoxy-D-glucopyranose
2-<(R)-3-(benzyloxy)tetradecanamido>-2-deoxy-4,6-O-isopropylidene-D-glucopyranose
Conditions | Yield |
---|---|
With 4 A molecular sieve; toluene-4-sulfonic acid In N,N-dimethyl-formamide for 1h; Ambient temperature; | 60% |
1-methoxy-2-methyl-1-trimethylsiloxy-1-propene
isopropyl methyl ether
methyl 2,2,3-trimethylbut-3-enoate
Conditions | Yield |
---|---|
With gallium(III) bromide In 1,2-dichloro-ethane at 80℃; for 2h; | 58% |
Conditions | Yield |
---|---|
With sodium tetrahydroborate; acetic acid In 1,2-dichloro-ethane at 20℃; for 16h; Inert atmosphere; | 53% |
isopropyl methyl ether
isopropyl methyl ether hydrotrioxide
Conditions | Yield |
---|---|
With ozone In acetone at -78℃; Oxidation; | 40% |
isopropyl methyl ether
2-O-benzoyl-myo-inositol
2-O-benzoyl-1,6:3,4-di-O-isopropylidene-myo-inositol
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In N,N-dimethyl-formamide at 50℃; for 1.5h; Inert atmosphere; | 35% |
1,2,3,4-tetrahydrocarbazole
isopropyl methyl ether
A
1-propyl-1,2,3,4-tetrahydrocarbazole
B
1-ethyl-1,2,3,4-tetrahydrocarbazole
Conditions | Yield |
---|---|
With n-butyllithium; potassium tert-butylate In hexane Ambient temperature; | A n/a B 27% C n/a D n/a |
isopropyl methyl ether
2-chlorobenzalaniline
(2-Methoxy-2-methyl-1-phenyl-propyl)-phenyl-amine
Conditions | Yield |
---|---|
With sodium |
isopropyl methyl ether
2-chlorobenzalaniline
[1-(2-Chloro-phenyl)-2-methoxy-2-methyl-propyl]-phenyl-amine
Conditions | Yield |
---|---|
With sodium |
isopropyl methyl ether
phenyl(bromodichloromethyl)mercury
1,1-dichloro-2-methoxy-2-methyl-propane
Conditions | Yield |
---|---|
In benzene |
isopropyl methyl ether
2-methoxy-propane-2-sulfinic acid
Conditions | Yield |
---|---|
With sulfur dioxide Irradiation; |
isopropyl methyl ether
5-phenyl-3,4-dihydro-2H-pyrrole perchlorate
A
2-(1-Methoxy-1-methyl-ethyl)-2-phenyl-pyrrolidine
Conditions | Yield |
---|---|
In acetonitrile Irradiation; |
isopropyl methyl ether
(2S,5S)-1,6-bis[(tert-butyldiphenylsilyl)oxy]hexane-2,5-diol
1,6-di-O-(tert-butyldiphenyl)silyl-2,5-di-O-isopropylidene-3,4-dideoxy-D-threo-hexitol
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In tetrahydrofuran at 0℃; for 2h; | 4.11 g |
isopropyl methyl ether
(3aR,4R,5R,6aS)-4-((1E,5Z)-(S)-3-Hydroxy-octa-1,5-dienyl)-5-(tetrahydro-pyran-2-yloxy)-hexahydro-cyclopenta[b]furan-2-one
(3aR,4R,5R,6aS)-4-[(1E,5Z)-(S)-3-(1-Methoxy-1-methyl-ethoxy)-octa-1,5-dienyl]-5-(tetrahydro-pyran-2-yloxy)-hexahydro-cyclopenta[b]furan-2-one
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In dichloromethane for 0.166667h; Ambient temperature; |
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