As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
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inquiryProduct description: Product name 3-Hydroxyphenylacetic acid CAS number 621-37-4 Assay ≥99% Appearance Off-white solid Capacity 200mt/year Application Pharmaceutical intermed
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inquiryProduct name: 3-Hydroxyphenylacetic acid CAS: 621-37-4 purity:99%min appearance:White powder Appearance: white powder Storage:Store in cool and dry place, away from sun light. Package: 25KG/drum Application: Pharmaceutical Intermediates Tra
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inquiry3-Hydroxyphenylacetic acid CAS:621-37-4 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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Cas:621-37-4
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inquirysuperior quality moderate price & quick delivery Appearance:white powder Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:1kg/bag, 1kg/drum or 25kg/drum or as per your request. Application:Used to make other
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
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inquiryadvantage: 1. The best price, satisfactory quality; 2. customers have the right to choose the delivery of parcels (EMS, DHL, FedEx, UPS); 3. customers have the right to choose from the recent effective packaging methods of their products packaging
Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:621-37-4
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Cas:621-37-4
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inquiry3-Hydroxyphenylacetic acid Basic information Product Name: 3-Hydroxyphenylacetic acid Synonyms: M-HYDROXYPHENYLACETIC ACID;3-hydroxy-benzeneaceticaci;META HYDROXY PHENYL ACETIC ACID;3-HYDROXYPHENYLACETIC ACID;3-HYDROXYPH
Cas:621-37-4
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inquiryProduct name: 3-Hydroxyphenylacetic Acid CAS No.:621-37-4 Molecule Formula:C8H8O3 Molecule Weight:152.14 Purity: 99% Package: 25kg/drum Description:White crystalline powder Manufacture Standards:Enterprise Standard TESTING ITEMS
Cas:621-37-4
Min.Order:1 Kilogram
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inquiryCAS:621-37-4 EINECS:210-684-4 MW:152.15 MF:C8H8O3 Melting point:129-133 °C(lit.) Appearance:White crystalline powder Package:Aluminum bag Transportation:by sea/air Port:Shanghai
High quality, competitive price, fast delivery and first-class service we possesses have won the trust and praise of customers. Standard: BP/USP/EP The purity is equal or greater than 99%. As a supplier, we can provide high-quality products. Cle
Cas:621-37-4
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inquiryProduct Name: 3-Hydroxyphenylacetic acid CAS: 621-37-4 MF: C8H8O3 MW: 152.15 EINECS: 210-684-4 Mol File: 621-37-4.mol 3-Hydroxyphenylacetic acid Structure 3-Hydroxyphenylacetic acid Chemical Properties Melting point 129-133 &d
Cas:621-37-4
Min.Order:1 Gram
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inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
Cas:621-37-4
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inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
Cas:621-37-4
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inquiry1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
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inquiry<3-(allyloxy)phenyl>acetic acid
3-hydroxyphenylacetic acid
Conditions | Yield |
---|---|
With sodium tetrahydroborate; tetrakis(triphenylphosphine) palladium(0) In tetrahydrofuran for 1h; | 98% |
3-hydroxyphenylacetic acid
Conditions | Yield |
---|---|
With water; lithium hydroxide In tetrahydrofuran; methanol at 20℃; for 12h; | 85% |
Conditions | Yield |
---|---|
With copper(I) oxide; 1D-1-O-Methyl-muco-inostol; sodium hydroxide In water at 100℃; for 6h; | 71% |
With copper(I) oxide; 1-D-O-Methyl-chiro-inositol; sodium hydroxide In water at 100℃; for 6h; | 71% |
Conditions | Yield |
---|---|
With caesium carbonate In methanol for 1h; UV-irradiation; Inert atmosphere; | A 53% B 45% |
methanol
3-chlorophenylacetic acid
A
benzyl methyl ether
B
3-hydroxyphenylacetic acid
C
benzyl alcohol
Conditions | Yield |
---|---|
With caesium carbonate In aq. buffer for 1h; UV-irradiation; Inert atmosphere; | A 8% B 47% C 34% |
3-hydroxyphenylacetic acid
Conditions | Yield |
---|---|
With indium; deuterated ammonium chloride In tetrahydrofuran-d8; water-d2 at 20℃; for 24h; Reflux; chemoselective reaction; | 32% |
Conditions | Yield |
---|---|
With sodium hydroxide; aluminum nickel |
Conditions | Yield |
---|---|
With diammonium sulfide; sulfur; isopropyl alcohol at 160℃; Erhitzen des von Ammoniak, Schwefelwasserstoff und Isopropylalkohol befreiten Reaktionsgemisches mit wss. Natronlauge; | |
Yield given. Multistep reaction; |
Conditions | Yield |
---|---|
With hydrogen iodide | |
With hydrogen iodide |
3-Hydroxyphenylacetonitrile
3-hydroxyphenylacetic acid
Conditions | Yield |
---|---|
With hydrogenchloride |
3-amino phenylacetic acid
3-hydroxyphenylacetic acid
Conditions | Yield |
---|---|
With sodium nitrite |
α,3-dihydroxybenzeneacetonitrile
3-hydroxyphenylacetic acid
Conditions | Yield |
---|---|
With phosphorus; hydrogen iodide |
phenylacetic acid
A
4-hydroxyphenylacetate
B
3-hydroxyphenylacetic acid
C
2-Hydroxyphenylacetic acid
Conditions | Yield |
---|---|
With iron(III) sulfate; dihydrogen peroxide; 3,4-dioxo-3,4-dihydronaphthalene-1-sulfonate In water Yield given. Yields of byproduct given; | |
With Fe2(SO4); dihydrogen peroxide; 3,4-dioxo-3,4-dihydronaphthalene-1-sulfonate In water Product distribution; | |
With dihydrogen peroxide; iron(III); benzene-1,2-diol In water Product distribution; Ambient temperature; further redox-systems and aromatic compounds investigated; |
phenylacetic acid
A
4-hydroxyphenylacetate
B
3-hydroxyphenylacetic acid
C
homogentisic acid
D
2-(2,6-dihydroxyphenyl)acetic acid
E
2-Hydroxyphenylacetic acid
Conditions | Yield |
---|---|
In various solvent(s) at 30℃; for 170h; Product distribution; Mechanism; biosynthesis by Trichosporum cutaneum strains, pH = 6, other incubation times; |
Conditions | Yield |
---|---|
With n-butyllithium; potassium tert-butylate 1.) hexane, reflux, 3 h, 2.) THF; Yield given. Multistep reaction; |
3-hydroxy-4-isopropylphenylacetic acid
3-hydroxyphenylacetic acid
Conditions | Yield |
---|---|
(i) CH2N2, Et2O, (ii) AlCl3, PhCl; Multistep reaction; |
Conditions | Yield |
---|---|
man behandelt mit KCN und kocht das entstandene rohe 3-Methoxy-mandelsaeurenitril mit Jodwasserstoffsaeure; |
3-hydroxyphenylacetic acid
Conditions | Yield |
---|---|
With sodium hydroxide |
Conditions | Yield |
---|---|
at 160℃; und Erhitzen des von NH3, H2S und Isopropylalkohol befreiten Reaktionsgemisches mit wss.NaOH auf Siedetemperatur; |
Conditions | Yield |
---|---|
man kocht das Reaktionsprodukt mit Jodwasserstoffsaeure; |
3-hydroxyphenylacetic acid
Conditions | Yield |
---|---|
With hydrogenchloride at 200℃; im geschlossenen Rohr; |
Conditions | Yield |
---|---|
at 200℃; im geschlossenen Rohr; |
2-(3-hydroxyphenyl)ethanol
3-hydroxyphenylacetic acid
Conditions | Yield |
---|---|
With Serratia marcescens In water at 30℃; |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: tin; hydrochloric acid 2: diluted hydrochloric acid; NaNO2 3: concentrated hydrochloric acid View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: diluted hydrochloric acid; NaNO2 2: concentrated hydrochloric acid View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: bei der Nitrierung 2: tin; hydrochloric acid 3: diluted hydrochloric acid; NaNO2 4: concentrated hydrochloric acid View Scheme |
6-isopropyl 6-acetoxy cyclohexa-2,4-dienone
3-hydroxyphenylacetic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: (i), (ii) (alkaline hydrolysis) 2: (i) CH2N2, Et2O, (ii) AlCl3, PhCl View Scheme |
phenylacetic acid
A
3-hydroxyphenylacetic acid
B
3,4-dihydroxyphenylacetate
C
homogentisic acid
Conditions | Yield |
---|---|
With sulfuric acid; water at 30℃; for 34h; Electrolysis; |
3-hydroxyphenylacetic acid
2-(3-hydroxyphenyl)ethanol
Conditions | Yield |
---|---|
With borane-THF In tetrahydrofuran at 0℃; for 1h; | 100% |
Stage #1: m-hydroxyphenylacetic acid With lithium aluminium tetrahydride In tetrahydrofuran at 0 - 60℃; for 2h; Stage #2: With hydrogenchloride; water In tetrahydrofuran | 88% |
Stage #1: m-hydroxyphenylacetic acid With sodium tetrahydroborate; boron trifluoride diethyl etherate In tetrahydrofuran for 3h; Heating / reflux; Stage #2: With water In tetrahydrofuran | 85% |
Conditions | Yield |
---|---|
thionyl chloride at 20℃; for 6h; | 100% |
thionyl chloride at 20℃; for 6h; | 100% |
With sulfuric acid Reflux; | 100% |
3-hydroxyphenylacetic acid
recorcinol
1-(2,4-dihydroxyphenyl)-2-(3-hydroxyphenyl)ethanone
Conditions | Yield |
---|---|
With boron trifluoride diethyl etherate for 1.5h; Reflux; | 100% |
With boron trifluoride diethyl etherate at 60 - 70℃; for 1h; | 93% |
With boron trifluoride diethyl etherate In toluene at 90℃; for 2h; | 57% |
With boron trifluoride diethyl etherate at 110℃; for 2h; Inert atmosphere; | |
With boron trifluoride diethyl etherate In N,N-dimethyl-formamide at 90℃; for 2h; |
methanol
3-hydroxyphenylacetic acid
3-hydroxy-benzeneacetic acid, methyl ester
Conditions | Yield |
---|---|
With sulfuric acid for 8h; Heating; | 100% |
With sulfuric acid for 18h; Heating / reflux; | 100% |
With sulfuric acid for 18h; Heating / reflux; | 100% |
3-hydroxyphenylacetic acid
trimethyl orthoformate
3-hydroxy-benzeneacetic acid, methyl ester
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In methanol for 4h; Heating; | 100% |
With toluene-4-sulfonic acid In methanol for 5h; Reflux; | |
With toluene-4-sulfonic acid In methanol for 5h; Reflux; |
3-hydroxyphenylacetic acid
3-hydroxy-benzeneacetic acid, methyl ester
Conditions | Yield |
---|---|
With sulfuric acid In methanol for 18h; Heating / reflux; | 100% |
With thionyl chloride In methanol; hexane; ethyl acetate | 94% |
27.8 g (100%) | |
With sodium bicarbonate In methanol |
3-hydroxyphenylacetic acid
3-hydroxy-benzeneacetic acid, methyl ester
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In methanol | 100% |
3-hydroxyphenylacetic acid
N,O-dimethylhydroxylamine*hydrochloride
2-(3-hydroxyphenyl)-N-methoxy-N-methylacetamide
Conditions | Yield |
---|---|
With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In acetonitrile at 20℃; for 2h; Inert atmosphere; | 100% |
3-hydroxyphenylacetic acid
2-(3-hydroxycyclohexyl)acetic acid
Conditions | Yield |
---|---|
With hydrogen; Rh on carbon In sodium hydroxide at 60℃; under 760 Torr; for 3h; | 99% |
With rhodium contaminated with carbon; hydrogen; sodium hydroxide In water at 80℃; under 7500.75 Torr; for 12h; | 600 mg |
3-hydroxyphenylacetic acid
benzyl bromide
phenylmethyl 2-[3-(phenylmethoxy)phenyl]acetate
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide | 99% |
With potassium carbonate In N,N-dimethyl-formamide | 99% |
With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 72h; | 92% |
With potassium carbonate In N,N-dimethyl-formamide at 80℃; for 72h; Etherification; | 83% |
With potassium carbonate In N-methyl-acetamide |
3-hydroxyphenylacetic acid
diazomethyl-trimethyl-silane
3-hydroxy-benzeneacetic acid, methyl ester
Conditions | Yield |
---|---|
In methanol; hexane; toluene | 99% |
3-hydroxyphenylacetic acid
allyl bromide
<3-(allyloxy)phenyl>acetic acid
Conditions | Yield |
---|---|
With sodium hydride In tetrahydrofuran for 15h; Heating; | 98% |
With n-Bu4POH In tetrahydrofuran; water at 0 - 20℃; | 83% |
Stage #1: m-hydroxyphenylacetic acid; allyl bromide With potassium carbonate In ethanol for 5h; Reflux; Stage #2: With potassium hydroxide In ethanol at 20℃; for 12h; | 71.2% |
Stage #1: m-hydroxyphenylacetic acid; allyl bromide With potassium carbonate In ethanol at 70℃; for 5h; Stage #2: With potassium hydroxide In ethanol at 20℃; for 12h; | 71.2% |
Conditions | Yield |
---|---|
In ethanol; water | 97% |
11.66 g (98%) |
3-hydroxyphenylacetic acid
L-alanine benzyl ester hydrochloride
Conditions | Yield |
---|---|
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In dichloromethane at 20℃; Inert atmosphere; | 95% |
3-hydroxyphenylacetic acid
2-bromomethylnaphthyl bromide
3-(naphth-2-ylmethoxy)phenylacetic acid
Conditions | Yield |
---|---|
With sodium hydroxide; concentrated aqueous hydrochloric acid; potassium carbonate In ethanol; acetone | 94% |
Conditions | Yield |
---|---|
With sulfuric acid-d2 at 60℃; for 1h; Sealed tube; | 94% |
Conditions | Yield |
---|---|
With potassium hydroxide; sodium iodide In ethanol for 16h; Heating; | 93% |
With potassium iodide; potassium hydroxide In tetrahydrofuran for 18h; Reflux; | 91% |
Stage #1: m-hydroxyphenylacetic acid With thionyl chloride In methanol at 0℃; for 4h; Heating / reflux; Stage #2: benzyl bromide With potassium carbonate In acetone at 20℃; Stage #3: With hydrogenchloride; sodium hydroxide more than 3 stages; | 91% |
3-hydroxyphenylacetic acid
3-acetoxyphenylacetic acid
Conditions | Yield |
---|---|
With pyridine In P2O5; water; acetic anhydride | 90% |
With pyridine In P2O5; water; acetic anhydride |
3-hydroxyphenylacetic acid
2-(3,4-dimethoxyphenyl)-ethylamine
N-[2-(3,4-Dimethoxy-phenyl)-ethyl]-2-(3-hydroxy-phenyl)-acetamide
Conditions | Yield |
---|---|
89% | |
With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃; Inert atmosphere; |
3-hydroxyphenylacetic acid
(3S)-3-(4-fluoro-3-nitrophenyl)-2-<(2R)-2-(4-hydroxy-phenyl)-2-<2-(3-hydroxyphenyl)-acetylamino>acetylamino>-propionic acid methyl ester
Conditions | Yield |
---|---|
With benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine In dichloromethane | 89% |
3-hydroxyphenylacetic acid
4-fluoroaniline
N-(4-fluorophenyl)-2-(3-hydroxyphenyl)acetamide
Conditions | Yield |
---|---|
89% |
3-hydroxyphenylacetic acid
4-{[2-(chloromethyl)phenoxy]methyl}-5-methyl-2-phenyl-1,3-oxazole
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 1 - 30℃; | 89% |
3-hydroxyphenylacetic acid
benzyl bromide
benzyl (3-hydroxyphenyl)acetate
Conditions | Yield |
---|---|
Stage #1: m-hydroxyphenylacetic acid With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 0.166667h; Stage #2: benzyl bromide In N,N-dimethyl-formamide at 20℃; for 48h; | 89% |
With 1,8-diazabicyclo[5.4.0]undec-7-ene In acetonitrile at 70℃; | 87% |
3-hydroxyphenylacetic acid
1,1,1,3,3,3-hexamethyl-disilazane
2-[3-(trimethylsilyloxy)phenyl]acetic acid
Conditions | Yield |
---|---|
With cross-linked poly((30percent)4-vinylpyridine/(70percent)styrene) copolymer-supported bismuth(III) triflate In dichloromethane at 20℃; for 0.333333h; | 88% |
Conditions | Yield |
---|---|
With triethylamine at 100 - 170℃; Microwave irradiation; | 87% |
3-hydroxyphenylacetic acid
phenethylamine
2-(3-hydroxyphenyl)-N-phenethylacetamide
Conditions | Yield |
---|---|
With 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 20℃; Inert atmosphere; | 85% |
2-hydroxy-5-methylbenzaldehyde
3-hydroxyphenylacetic acid
acetic anhydride
Conditions | Yield |
---|---|
With triethylamine at 120℃; for 8h; | 85% |
Conditions | Yield |
---|---|
With triethylamine at 100 - 170℃; Microwave irradiation; | 85% |
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