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inquiryBest quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
Reliable quality 6282-02-6 Competitive price N-(Hydroxymethyl)benzamide hot selling Molecular Formula C8H9NO2 Molar Mass 151.16 Density 1.2023 (rough estimate) Melting Point 95-100°C Bolin
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
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inquiryN-(Hydroxymethyl)benzamide Chemical Properties Melting point 95-100 °C Boiling point 273.17°C (rough estimate) density 1.2023 (rough estimate) refractive index 1.5810 (estimate) pka 13.25±0.46(Predicted) BRN 2045
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Conditions | Yield |
---|---|
With NaY zeolite In water at 100℃; for 1h; Reagent/catalyst; Time; | 96% |
With water at 100℃; for 1h; Reagent/catalyst; | 96% |
With aluminum oxide; water at 60 - 65℃; for 0.133333h; microwave irradiation; | 75% |
Conditions | Yield |
---|---|
With formaldehyd | 84% |
Conditions | Yield |
---|---|
With water at 100℃; for 10h; Reagent/catalyst; Sealed tube; | 62% |
formaldehyd
benzamide
A
N-(hydroxymethyl)benzamide
B
N,N'-methylenebisbenzamide
C
bis-N-benzamidomethyl ether
Conditions | Yield |
---|---|
With potassium carbonate In water Heating; | A 57% B n/a C n/a |
N-<(phenylsulfenyl)methyl>benzamide
A
1-Benzamido-1-methoxymethane
B
N-(hydroxymethyl)benzamide
C
N-<(phenylsulfonyl)methyl>benzamide
D
N-<(phenylsulfinyl)methyl>benzamide
Conditions | Yield |
---|---|
With sodium periodate In methanol for 60h; Ambient temperature; | A 8 % Spectr. B 4 % Spectr. C 40% D 8 % Spectr. |
formaldehyd
benzamide
A
N-(hydroxymethyl)benzamide
B
N,N'-methylenebisbenzamide
Conditions | Yield |
---|---|
With HY zeolite In water at 100℃; for 12h; Reagent/catalyst; | A 28% B 35% |
In 1,4-dioxane; water at 40 - 60℃; Thermodynamic data; Kinetics; Mechanism; activation energy, pH 3.5-4.0; |
formaldehyd
benzamide
m-xylene
A
N-(2,4-dimethylbenzyl)benzamide
B
N-(hydroxymethyl)benzamide
Conditions | Yield |
---|---|
With water at 100℃; for 10h; Sealed tube; | A 20% B 35% |
With water at 100℃; for 10h; Concentration; Reagent/catalyst; Sealed tube; | A n/a B 10% |
Conditions | Yield |
---|---|
With water In acetonitrile at 25℃; Rate constant; | |
With water; acetic acid In acetonitrile at 25℃; Rate constant; various buffer concentrations; | |
With sulfuric acid; water In acetonitrile at -258.2℃; Kinetics; Thermodynamic data; ΔS(excit.) ΔH(excit.), var. temp., var. acid concentrations; |
Conditions | Yield |
---|---|
at 25℃; Rate constant; sowie bei 50grad und 70grad; |
Conditions | Yield |
---|---|
at 15℃; Equilibrium constant; sowie bei 20grad, 25grad und 30grad; | |
at 25℃; |
N-(hydroxymethyl)benzamide
Benzeneselenol
N-<(phenylselenyl)methyl>benzamide
Conditions | Yield |
---|---|
With hydrogenchloride at 60 - 70℃; for 0.75h; | 95% |
Conditions | Yield |
---|---|
In water | 94.4% |
Conditions | Yield |
---|---|
With C54H43ClN3P2Ru(1+)*F6P(1-); caesium carbonate In toluene at 140℃; for 72h; Inert atmosphere; Glovebox; Green chemistry; | 92% |
With tris(2-diphenylphosphinoethyl)phosphine; potassium tert-butylate; water; caesium carbonate; cobalt(II) bromide In m-xylene at 140℃; for 30h; Green chemistry; |
GLUTATHIONE
N-(hydroxymethyl)benzamide
trifluoroacetic acid
S-benzamidomethylglutathione trifluoroacetate salt hydrate
Conditions | Yield |
---|---|
for 0.0833333h; | 90% |
N-(hydroxymethyl)benzamide
Conditions | Yield |
---|---|
With sulfuric acid In acetic acid for 14h; Heating; | 90% |
N-(hydroxymethyl)benzamide
β-naphthol
N-((2-hydroxynaphthalen-1-yl)methyl)benzamide
Conditions | Yield |
---|---|
With sulfuric acid In ethanol for 7h; Friedel-Crafts Acylation; Heating; Green chemistry; | 89% |
With sulfuric acid In ethanol at 50℃; for 7h; | 71% |
With hydrogenchloride; ethanol | |
With hydrogenchloride In ethanol for 4h; Heating; Yield given; | |
With hydrogenchloride; ethanol |
N-(hydroxymethyl)benzamide
tert-butyldichlorophosphine
aminomethyl-P-t-butyl-phosphinic acid
Conditions | Yield |
---|---|
With hydrogenchloride In acetic acid 1.) 60 min, 25 deg C then reflux, 60 min; 2.) reflux; | 89% |
With hydrogenchloride 1.) glacial acetic acid, reflux, 30 min, 2.) reflux, 6 h; Yield given. Multistep reaction; |
Conditions | Yield |
---|---|
With sulfuric acid In ethanol at 35℃; for 120h; Friedel-Crafts Alkylation; | 88.9% |
Conditions | Yield |
---|---|
With sulfuric acid In ethanol at 35℃; for 72h; Reagent/catalyst; Friedel-Crafts Acylation; | 87% |
Conditions | Yield |
---|---|
With sodium hydride In dichloromethane at 20℃; | 86.5% |
N-(hydroxymethyl)benzamide
thiophenol
N-<(phenylsulfenyl)methyl>benzamide
Conditions | Yield |
---|---|
With hydrogenchloride 1.) 60-70 deg C, 1h, 2.) RT, 2h; | 86% |
N-(hydroxymethyl)benzamide
N-(chloromethyl)benzamide
Conditions | Yield |
---|---|
With phosphorus pentachloride In diethyl ether at 5 - 20℃; for 2.5h; | 85% |
With thionyl chloride In dichloromethane | 77% |
With thionyl chloride In dichloromethane | 45% |
N-(hydroxymethyl)benzamide
p-Chlorothiophenol
N-(4-chlorophenylthiomethyl)benzamide
Conditions | Yield |
---|---|
With hydrogenchloride; ethanol Ambient temperature; | 85% |
N-(hydroxymethyl)benzamide
Conditions | Yield |
---|---|
With d(4)-methanol; C54H43ClN3P2Ru(1+)*F6P(1-); caesium carbonate In toluene at 140℃; for 72h; Inert atmosphere; Sealed tube; Green chemistry; | 85% |
Conditions | Yield |
---|---|
With sulfuric acid In ethanol at 35℃; for 120h; Friedel-Crafts Alkylation; | 83.3% |
N-(hydroxymethyl)benzamide
para-thiocresol
N-(4-methylphenylthiomethyl)benzamide
Conditions | Yield |
---|---|
With hydrogenchloride In ethanol | 83.2% |
N-(hydroxymethyl)benzamide
1-mercapto-2-hydroxybutane
1-<(benzamidomethyl)thio>-2-butanol
Conditions | Yield |
---|---|
With sulfuric acid In water for 48h; | 83% |
N-(hydroxymethyl)benzamide
6-Phenoxy-2-phenyl-imidazo[1,2-b]pyridazine
Conditions | Yield |
---|---|
With sulfuric acid In acetic acid for 14h; Heating; | 83% |
N-(hydroxymethyl)benzamide
2-(4'-t-butylphenyl)-6-chloroimidazo<1,2-b>pyridazine
Conditions | Yield |
---|---|
With sulfuric acid In acetic acid at 120℃; | 82% |
N-(hydroxymethyl)benzamide
Conditions | Yield |
---|---|
With sulfuric acid In acetic acid for 14h; Heating; | 82% |
2-acetylpropanoic acid ethyl ester
N-(hydroxymethyl)benzamide
2-(benzoylamino-methyl)-2-methyl-acetoacetic acid ethyl ester
Conditions | Yield |
---|---|
With boron trifluoride diethyl etherate at 0 - 20℃; for 2h; | 82% |
Conditions | Yield |
---|---|
With boron trifluoride diethyl etherate at 0 - 20℃; for 2h; | 81% |
N-(hydroxymethyl)benzamide
mercaptoacetic acid
Benzamidomethyl-thioessigsaeure
Conditions | Yield |
---|---|
With hydrogenchloride at 0℃; for 0.5h; | 80% |
N-(hydroxymethyl)benzamide
2-Naphthalen-2-yl-6-phenylsulfanyl-imidazo[1,2-b]pyridazine
Conditions | Yield |
---|---|
With sulfuric acid In acetic acid for 14h; Heating; | 79% |
N-(hydroxymethyl)benzamide
2-(4-tert-Butyl-phenyl)-6-iodo-imidazo[1,2-a]pyridine
Conditions | Yield |
---|---|
With sulfuric acid In acetic acid for 14h; Heating; | 79% |
Conditions | Yield |
---|---|
With sulfuric acid In ethanol at 35℃; for 120h; Friedel-Crafts Alkylation; | 76.5% |
N-(hydroxymethyl)benzamide
phosphorisocyanatidic acid dimethyl ester
dimethyl (N-benzamidomethyl)amidophosphate
Conditions | Yield |
---|---|
With triethylamine In benzene at 40 - 50℃; for 3h; | 75% |
N-(hydroxymethyl)benzamide
Conditions | Yield |
---|---|
With sulfuric acid In acetic acid at 120℃; | 74% |
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