CAS No.7789-61-9,Antimony tribromide Suppliers,MSDS download

Dayang Chem (Hangzhou) Co.,Ltd.

As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch

Antimony tribromide

Cas:7789-61-9

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

inquiry

Henan Tianfu Chemical Co., Ltd.

Our company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung, LG, Merck, Thermo Fisher Scientific and so o

7789-61-9 Antimony tribromide

Cas:7789-61-9

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Antimex Chemical Limied

Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali

ANTIMONY TRIBROMIDE

Cas:7789-61-9

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Zhuozhou Wenxi import and Export Co., Ltd

Product Description Description & Specification Category Pharmaceutical Raw Materials, Fine Chemicals, Bulk drug Standard Medical standard

GMP manufacturer CAS 7789-61-9 with reasonable price

Cas:7789-61-9

Min.Order:1 Kilogram

FOB Price: $112.0

Type:Trading Company

inquiry

Hangzhou Ocean Chemical Co., Ltd.

Ocean inorganic department is a professional supplier and exporter engaging in inorganic chemical materials and metal organic compounds. Over the past years, our company is committed to improving the product quality and developing new products, in or

Antimony (III) Bromide

Cas:7789-61-9

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hubei Langyou International Trading Co., Ltd

Antimony tribromide；Antimony bromide /High quality/Best price/In stock Application:Antimony tribromide；Antimony bromide /High quality/Best price/In stock

Antimony tribromide；Antimony bromide /High quality/Best price/In stock

Cas:7789-61-9

Min.Order:0

Negotiable

Type:Other

inquiry

Changchun Artel lmport and Export trade company

Supply top quality products with a reasonable price Application:api

7789-61-9

Cas:7789-61-9

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Hunan Russell Chemicals Technology Co.,Ltd

low price and high purityAppearance:solid or liquid Storage:in sealed air resistant place Package:As customer require Application:Pharma;Industry;Agricultural Transportation:by sea or by airplane Port:any port in China

Antimony(III) bromide, 99% 7789-61-9

Cas:7789-61-9

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Hunan Longxianng Runhui Trading Co.,Ltd

Antimony tribromide；Antimony bromide /High quality/Best price/In stockAppearance:Liquid Storage:Keep in a cool & dry place Package:Neutral Application:intermediate Transportation:By express (Door to door) such as FEDEX, DHL, EMS for small amount. By

Antimony tribromide；Antimony bromide /High quality/Best price/In stock

Cas:7789-61-9

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Beantown Chemical

in stock Application:7789-61-9

Antimony(III) bromide, 99%

Cas:7789-61-9

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Cerametek Materials（ShenZhen）Co., Ltd.

sub/micron to mesh powders (near/spheres, whiskers, flake, fiber, porous) and grain/ball, thin/ thick metal / alloys pieces / parts, thin and thick (particle) film materials /target, and custom-made crystals, substrates/parts. In the industries and a

Antimony bromide

Cas:7789-61-9

Min.Order:0

Negotiable

Type:Other

inquiry

Hangzhou Share Chemical Co., Ltd

At Share Chemical Company, we scrupulously abide by our policy of “Excellent Quality at a Reasonable Price”. We strive to satisfy all of our customers by providing the finest quality products supported by the finest in customer servi

AntiMony(III) broMide, ultra dry, 99.999% (Metals b

Cas:7789-61-9

Min.Order:1 Gram

Negotiable

Type:Other

inquiry

Strem Chemicals, Inc.

1.High Quality Specialty Chemicals2.Expertise and Experience in Manufacturing High Purity, High Quality Chemicals3.Long Term Focus in Inorganics, Organometallics and Metals4.ISO 9001 CertifiedAppearance:off-white pwdr.

Antimony(III) bromide, 99%

Cas:7789-61-9

Min.Order:0

Negotiable

Type:Other

inquiry

Nanjing Raymon Biotech Co., Ltd.

Antimony(III) bromide, 99% 7789-61-9Appearance:solid or liquid Storage:keep in dry and cool condition Package:25kg or according to cutomer's demand Application:Chemical research/pharma intermediate Transportation:By Sea,by Air,By courier like DHL or

Antimony(III) bromide, 99% 7789-61-9

Cas:7789-61-9

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Hebei Minshang Biotechnology Co., Ltd

Antimony tribromide；Antimony bromide /High quality/Best price/In stock Application:intermediate

7789-61-9

Cas:7789-61-9

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Skyrun Industrial Co.,Ltd

Adequate stocks available,prompt shipment,Strictly control on quality,Timely after-sales

AntiMony(III) broMide, ultra dry, 99.999% (Metals basis)

Cas:7789-61-9

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou Fenjun Chemical Co Ltd.

Antimony tribromide；Antimony bromide /High quality/Best price/In stock Application:Antimony tribromide；Antimony bromide /High quality/Best price/In stock

Antimony tribromide；Antimony bromide /High quality/Best price/In stock

Cas:7789-61-9

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Synthetic route

: 7440-36-0
antimony

: 74-83-9
methyl bromide

A: 54553-06-9
dibromo(methyl)stibine

B: 149442-29-5
dimethyltribromostibine

C: 7789-61-9
antimony(III) bromide

Conditions

Conditions	Yield
With copper passing CH3Br over powdered Sb and copper (ratio 10:1) at 350°C; fractionation; boiling range from 120 to 130°C at 14 Torr;	A 40% B 38% C 22%
With copper passing CH3Br over powdered Sb and copper (ratio 10:1) at 350°C; fractionation; boiling range from 120 to 130°C at 14 Torr;	A 40% B 38% C 22%

...Expand

: 7440-36-0
antimony

: 74-83-9
methyl bromide

A: 54553-06-9
dibromo(methyl)stibine

B: 7789-61-9
antimony(III) bromide

C: 53234-94-9
dimethylantimony bromide

Conditions

Conditions	Yield
With hydrogen heating of Sb and Cu powder on asbestos for 3 h at 350°C in H2, then introduction of CH3Br over 32 h;	A n/a B n/a C 30%
With Cu powder/asbestos; H2 heating of Sb and Cu powder on asbestos for 3 h at 350°C in H2, then introduction of CH3Br over 32 h;	A n/a B n/a C 30%

...Expand

: 7440-36-0
antimony

: 7726-95-6
bromine

: 7439-98-7
molybdenum

A: molybdenum(IV) oxide

B: 7789-61-9
antimony(III) bromide

Conditions

Conditions	Yield
With water In neat (no solvent) vac.; chemical transport; heating (500-1000°C);

...Expand

: 7440-36-0
antimony

: 7726-95-6
bromine

: 7789-61-9
antimony(III) bromide

Conditions

Conditions	Yield
In tetrachloromethane
In neat (no solvent) ratio bromine:Sb 3:1, heating (500°C);
Sb putting into one branch of right-angle quartz ampoule, stoich. Br2 putting in second branch, Br2 solidifying (brine), evac. (ca. 1E-5 mm Hg),Br2 liquefying, Sb portions addn. to Br2, then heating to 140-150.degre e.C, cooling after reaction ceased; SbBr3 sublimation at 140-150°C in cooled part of reactor; elem. anal.;
In tetrachloromethane for 5h; Inert atmosphere; Reflux;

: antimony(III) sulfide

: 7726-95-6
bromine

A: SbSBr

B: 13172-31-1
disulphur dibromide

C: 7789-61-9
antimony(III) bromide

Conditions

Conditions	Yield
reaction at room temperature;;
normal temp.;;
normal temp.;;
reaction at room temperature;;

...Expand

: silver(I) bromide

: SbBr2AlBr4

A: AgAlBr4

B: 7789-61-9
antimony(III) bromide

Conditions

Conditions	Yield
With aluminum tri-bromide

...Expand

: 10025-91-9
antimony(III) chloride

: 7558-02-3
potassium bromide

: 7789-61-9
antimony(III) bromide

Conditions

Conditions	Yield
byproducts: KCl;

: antimony(III) sulfate

: 7647-15-6
sodium bromide

: 7789-61-9
antimony(III) bromide

Conditions

Conditions	Yield
byproducts: Na2SO4;

: 7440-36-0
antimony

: 7789-61-9
antimony(III) bromide

Conditions

Conditions	Yield
With hydrogen sulfide byproducts: H2; above 360°C;
With bromine at 230°C with the mixt. of Br2 and CO2;
With bromine In carbon disulfide excess of powdered Sb; shaking; at the beginning cooling with H2O; at the end 40-45 °C; filtering, crystn.;

: 7783-56-4
antimony(III) fluoride

: 7789-61-9
antimony(III) bromide

Conditions

Conditions	Yield
With bromine
With Br2

: 10025-91-9
antimony(III) chloride

: 10294-33-4
boron tribromide

A: 10294-34-5
boron trichloride

B: 7789-61-9
antimony(III) bromide

...Expand

: 7647-18-9
antimonypentachloride

: 10294-33-4
boron tribromide

A: 10294-34-5
boron trichloride

B: 7789-61-9
antimony(III) bromide

Conditions

Conditions	Yield
byproducts: Br;

...Expand

: 10025-91-9
antimony(III) chloride

: 7789-61-9
antimony(III) bromide

Conditions

Conditions	Yield
With potassium bromide by heating in sealed tube; SbCl3 vapor reacted with KBr;
With KBr by heating in sealed tube; SbCl3 vapor reacted with KBr;

: 603-36-1
triphenylantimony

A: 10025-91-9
antimony(III) chloride

B: 7789-61-9
antimony(III) bromide

C: 594-31-0, 34716-91-1, 20265-29-6
triphenylantimony dichloride

Conditions

Conditions	Yield
With aluminium trichloride In chloroform reflux for 6 h;
With aluminium trichloride In carbon disulfide at room temp. for 12 h;
With AlCl3 In carbon disulfide at room temp. for 12 h;
With AlCl3 In chloroform reflux for 6 h;

...Expand

: antimony(III) sulfide

: arsenic trisulfide

A: diboron trisulfide

B: 7789-61-9
antimony(III) bromide

Conditions

Conditions	Yield
heating several h at 120-130°C;	A >99 B n/a
heating several h at 120-130°C;	A >99 B n/a

...Expand

: 7726-95-6
bromine

: 2714-61-6
Tetrakis(trifluormethyl)distiban

A: 75-63-8
Bromotrifluoromethane

B: 7789-61-9
antimony(III) bromide

Conditions

Conditions	Yield
20°C (24 h);	A >99 B >99

...Expand

: 432-05-3
tris(trifluoromethyl)stibane

: 7726-95-6
bromine

A: 75-63-8
Bromotrifluoromethane

B: 754-14-3
Trifluormethyl-dibromstiban

C: 758-46-3
Bis(trifluormethyl)-bromstiban

D: 7789-61-9
antimony(III) bromide

Conditions

Conditions	Yield
mixing at -30°C, then warming to 20°C for 17 h;
warming up from -30°C to 20°C within 17 h; isolation of (CF3)2SbBr and CF3SbBr2;
mixing at -30°C, then warming to 20°C for 17 h;

...Expand

: 77329-74-9
antimony pentapropine

: 10035-10-6, 12258-64-9
hydrogen bromide

: 7789-61-9
antimony(III) bromide

Conditions

Conditions	Yield
byproducts: Br2;

: 754-14-3
Trifluormethyl-dibromstiban

A: 758-46-3
Bis(trifluormethyl)-bromstiban

B: 7789-61-9
antimony(III) bromide

Conditions

Conditions	Yield
at storage;

: HgSbBr

A: 7440-36-0
antimony

B: mercury(I) bromide

C: Hg2SbBr2

D: 7789-61-9
antimony(III) bromide

E: mercury

Conditions

Conditions	Yield
decompn. above 180 °C and condensation at 170 or below 150 °C; dependence of product ratio on temp.;

...Expand

: 68781-05-5
ethyldiiodostibine

: 7789-61-9
antimony(III) bromide

Conditions

Conditions	Yield
With bromine In chloroform
With Br2 In chloroform

: 7790-44-5
antimony triiodide

A: 7789-33-5
iodine(I) bromide

B: 7789-61-9
antimony(III) bromide

Conditions

Conditions	Yield
With bromine

: antimony(III) sulfide

: 7789-51-7
selenyl bromide

A: 7789-61-9
antimony(III) bromide

B: 1015938-55-2, 7789-52-8
diselenium dibromide

Conditions

Conditions	Yield
In not given
In not given

...Expand

: antimony(III) sulfide

: 7789-69-7
phosphorus pentabromide

A: 3931-89-3
thiophosphoryl(V) bromide

B: 7789-61-9
antimony(III) bromide

Conditions

Conditions	Yield
In not given react. at ambient temp.;; removal of formed SbBr3 by distn. difficult;;
In not given react. at ambient temp.;; removal of formed SbBr3 by distn. difficult;;

...Expand

: diethyl ether ; compound with antimony pentabromide

: 7789-61-9
antimony(III) bromide

Conditions

Conditions	Yield
in desiccator standing over H2SO4;
standing in desiccator over H2SO4 (some days);
standing in desiccator over H2SO4 (some days);

: antimony(III) sulfate

: 7789-61-9
antimony(III) bromide

Conditions

Conditions	Yield
With KBr byproducts: K2SO4; heating dry mixt.;

: 7803-52-3
stibane

: 7789-61-9
antimony(III) bromide

Conditions

Conditions	Yield
With bromine

: antimony(III) sulfide

: 7789-69-7
phosphorus(V) bromide

A: 3931-89-3
thiophosphoryl(V) bromide

B: 7789-61-9
antimony(III) bromide

Conditions

Conditions	Yield
In neat (no solvent)
In neat (no solvent)

...Expand

: antimony(III) trioxide

: 7789-61-9
antimony(III) bromide

Conditions

Conditions	Yield
With potassium bromide In acetic acid with anhydrous acetic acid; in dry conditions;
In acetic acid

: MgBr2*SbBr3*8H2O

A: 7789-61-9
antimony(III) bromide

B: magnesium bromide

Conditions

Conditions	Yield
In neat (no solvent) byproducts: H2O; decomposition in a desiccator in vacuum over H2SO4;;
In neat (no solvent) byproducts: H2O; decomposition in a desiccator in vacuum over H2SO4;;

: 7789-61-9
antimony(III) bromide

: 1135-32-6
trans-1,2-bis(4-pyridyl)ethylene

: C12H10N2*Sb(3+)*3Br(1-)

Conditions

Conditions	Yield
In neat (no solvent) for 48h; Inert atmosphere; Sealed tube;	100%

: 553-26-4
4,4'-bipyridine

: 7789-61-9
antimony(III) bromide

: C10H8N2*Sb(3+)*3Br(1-)

Conditions

Conditions	Yield
In neat (no solvent) for 72h; Inert atmosphere; Sealed tube;	100%

: 1,3-bis(2’,6’-diisopropylphenyl)imidazol-2-ylidene

: 7789-61-9
antimony(III) bromide

: C54H72Br2N4Sb(1+)*Br(1-)

Conditions

Conditions	Yield
In tetrahydrofuran at 80℃; Sealed tube;	96%

: 7789-61-9
antimony(III) bromide

: 79-19-6
thiosemicarbazide

: 97252-78-3
Sb(CH5N3S)Br3*C4H8O2

Conditions

Conditions	Yield
With 1,4-dioxane In 1,4-dioxane soln. of salt in dioxane was heated, soln. of ligand was added, mixt. was kept at 50°C for 1 h then left at room temp.; crystd. for 48 h, ppt. was filtered off, washed with dioxane, air-driedthen dried over P2O5 under vac.; elem. anal.;	95%

: 917-23-7
5,10,15,20-tetraphenyl-21H,23H-porphine

: 7789-61-9
antimony(III) bromide

: 177417-17-3
Sb(C20H8N4(C6H5)4)Br

Conditions

Conditions	Yield
With 2,6-lutidine In dichloromethane Ar-atmosphere; excess SbBr3, refluxing in CH2Cl2/2,6-lutidine=12:1 v/v for 1 d; addn. of water, hexane and CH2Cl2, filtration (Celite), extn. of aq. layer (CH2Cl2), drying combined org. layers (MgSO4), evapn.;	95%
In pyridine refluxing;	14%

: 904689-15-2
N,N-bis(2-bromobenzyl)-N-(2-methylpropyl)amine

: 7789-61-9
antimony(III) bromide

: 904689-26-5
12-bromo-N-(2-methylpropyl)-5,6,7,12-tetrahydrodibenz[c,f][1,5]azastibocine

Conditions

Conditions	Yield
With n-BuLi In diethyl ether; hexane under Ar; ligand disolved in Et2O; cooled in methanol-ice bath (-15 to -20 degree.C); n-BuLi in hexane added; stirred for 1 h; etherial soln. ofSbBr3 added; stirred at room temp. for 12 h; quenched with H2O; diluted with CHCl3; org. layer sepd.; washed with satd. aq. NaHCO3 and brine; dried (anhyd. MgSO4); removed in vac.; purifiedby column chromy. (silica gel, CH2Cl2-ethyl acetate 4:1); recrystd. fro m CHCl3-EtOH; elem. anal.;	95%

Yield

With n-BuLi In diethyl ether; hexane under Ar; ligand disolved in Et2O; cooled in methanol-ice bath (-15 to -20 degree.C); n-BuLi in hexane added; stirred for 1 h; etherial soln. ofSbBr3 added; stirred at room temp. for 12 h; quenched with H2O; diluted with CHCl3; org. layer sepd.; washed with satd. aq. NaHCO3 and brine; dried (anhyd. MgSO4); removed in vac.; purifiedby column chromy. (silica gel, CH2Cl2-ethyl acetate 4:1); recrystd. fro m CHCl3-EtOH; elem. anal.;

95%

: 7726-95-6
bromine

: 14527-51-6
5,10,15,20-tetra(p-tolyl)porphyrin

: 7789-61-9
antimony(III) bromide

: dibromo[tetra(p-tolyl)phenylporphyrinato]antimony(V) bromide

Conditions

Conditions	Yield
Stage #1: 5,10,15,20-tetra(p-tolyl)porphyrin; antimony(III) bromide With 2,6-dimethylpyridine In dichloromethane at 40℃; for 1h; Inert atmosphere; Stage #2: bromine In dichloromethane for 0.666667h; Inert atmosphere;	95%

...Expand

: 7789-61-9
antimony(III) bromide

: 2751-90-8
tetraphenylphosphonium bromide

: tetraphenylphosphonium octabromodiantimonate

Conditions

Conditions	Yield
In further solvent(s) exclusion of moisture; SbBr3 in CH2Br2 was dropwise added to soln. of PPh4Br in CH2Br2; CCl4 was added; ppt. was crystd. within few days at 5°C, filtered and dried in vac.; elem. anal.;	94%

: trimethyl antimonite

: 7789-61-9
antimony(III) bromide

: 111838-72-3
bromodimethoxostibane

Conditions

Conditions	Yield
In dichloromethane without moisture, stirred for 24 h at room temp. (stoich. amts.); filtered, dried in vac., elem. anal.;	93%

: 87-85-4
Hexamethylbenzene

: 7789-61-9
antimony(III) bromide

: 110296-09-8
((hexamethylbenzene)bis[tribromoantimony(III)])n

Conditions

Conditions	Yield
In benzene under dry N2, soln. of SbBr3 and C6Me6 in benzene is heated until boiling; slowly cooling; elem. anal.;	92%

: 904689-16-3
N,N-bis(2-bromobenzyl)-N-cyclohexylamine

: 7789-61-9
antimony(III) bromide

: 904689-28-7
12-bromo-N-cyclohexyl-5,6,7,12-tetrahydrodibenz[c,f][1,5]azastibocine

Conditions

Conditions	Yield
With n-BuLi In diethyl ether; hexane under Ar; ligand disolved in Et2O; cooled in methanol-ice bath (-15 to -20 degree.C); n-BuLi in hexane added; stirred for 1 h; etherial soln. ofSbBr3 added; stirred at room temp. for 12 h; quenched with H2O; diluted with CHCl3; org. layer sepd.; washed with satd. aq. NaHCO3 and brine; dried (anhyd. MgSO4); removed in vac.; purifiedby column chromy. (silica gel, CH2Cl2-ethyl acetate 4:1); recrystd. fro m CHCl3-EtOH; elem. anal.;	92%

Yield

92%

: 904689-24-3
N,N-bis(2-bromobenzyl)-N-phenylamine

: 7789-61-9
antimony(III) bromide

: 12-bromo-6-phenyl-5,6,7,12-tetrahydrodibenzo[c,f][1,5]azastibocine

Conditions

Conditions	Yield
Stage #1: N,N-bis(2-bromobenzyl)-N-phenylamine With n-butyllithium In diethyl ether; hexane at -78 - 20℃; Inert atmosphere; Stage #2: antimony(III) bromide In diethyl ether at -78 - 20℃; for 14h; Inert atmosphere;	92%

: 7789-61-9
antimony(III) bromide

: 53234-94-9
dimethylantimony bromide

A: 54553-06-9
dibromo(methyl)stibine

B: 5835-64-3, 24606-08-4, 91002-43-6
trimethylantimony(V) dibromide

Conditions

Conditions	Yield
In neat (no solvent) react. under dry Ar, stirring at room temp. (2 h); addn. of petroleum ether, crystn. at -18°C;	A 90% B 8%

...Expand

: (C5H5)2(ZrSC3H2(CH3)2)

: 7789-61-9
antimony(III) bromide

: 122115-78-0
Br(SbSC3H2(CH3)2)

Conditions

Conditions	Yield
In benzene byproducts: zirconocene dibromide; room temp., according to Buchwald, S. L.; Fisher, R. A.; Davis, W. M. Organometallics 1989, 8, 2082;	90%

: 194285-51-3
N,N -bis(2-bromobenzyl)-2-methylpropan-2-amine

: 7789-61-9
antimony(III) bromide

: 904689-29-8
12-bromo-N-t-butyl-5,6,7,12-tetrahydrodibenz[c,f][1,5]azastibocine

Conditions

Conditions	Yield
With n-BuLi In diethyl ether; hexane under Ar; ligand disolved in Et2O; cooled in methanol-ice bath (-15 to -20 degree.C); n-BuLi in hexane added; stirred for 1 h; etherial soln. ofSbBr3 added; stirred at room temp. for 12 h; quenched with H2O; diluted with CHCl3; org. layer sepd.; washed with satd. aq. NaHCO3 and brine; dried (anhyd. MgSO4); removed in vac.; purifiedby column chromy. (silica gel, CH2Cl2-ethyl acetate 4:1); recrystd. fro m CHCl3-EtOH; elem. anal.;	90%

Yield

90%

: 111-49-9
hexamethylene imine

: 7732-18-5
water

: 10035-10-6, 12258-64-9
hydrogen bromide

: 7789-61-9
antimony(III) bromide

: 2C6H13N*2H(1+)*Sb(3+)*5Br(1-)

Conditions

Conditions	Yield
In methanol	90%

...Expand

: 700-12-9
pentamethylbenzene,

: 7789-61-9
antimony(III) bromide

: 110296-11-2
((pentamethylbenzene)bis[tribromoantimony(III)])n

Conditions

Conditions	Yield
In toluene heating of SbBr3 and pentamethylbenzene in toluene at reflux temp. under dry pure N2, cooling, crystn.; washing (toluene), drying (vac.); elem. anal.;	89%
In toluene under dry N2, soln. of SbBr3 and C6HMe5 in toluene is heated until boiling; elem. anal.;	89%

: 103-83-3
N,N'-dimethylbenzylamine

: 7789-61-9
antimony(III) bromide

: 654070-31-2
[2-(dimethylaminomethyl)phenyl]antimony(III) dibromide

Conditions

Conditions	Yield
With BuLi In toluene under Ar; BuLi in hexane added dropwise at room temp. to stirred soln. of ligand in hexane; stirred for 5 h; ppt. washed with hexane; suspended in toluene; added dropwise under stirring to cooled (-78°C) soln.of SbBr3 (1 equiv.) in toluene; stirred (-78°C, 1 h); warmed to room temp. with stirring overnight; filtered; solvent removed under vac.; recrystd. from CHCl3;	88%

: 7789-61-9
antimony(III) bromide

: 7375-70-4
N(1),N(2)-bis(2-bromobenzyl)-N(1),N(2)-dimethylpropane-1,3-diamine

: 904689-17-4
12-bromo-N-methyl-5,6,7,12-tetrahydrodibenz[c,f][1,5]azastibocine

Conditions

Conditions	Yield
With n-BuLi In diethyl ether; hexane under Ar; ligand disolved in Et2O; cooled in methanol-ice bath (-15 to -20 degree.C); n-BuLi in hexane added; stirred for 1 h; etherial soln. ofSbBr3 added; stirred at room temp. for 12 h; quenched with H2O; diluted with CHCl3; org. layer sepd.; washed with satd. aq. NaHCO3 and brine; dried (anhyd. MgSO4); removed in vac.; recrystd. from CHCl3-EtOH; elem. anal.;	88%

Yield

88%

: 7789-61-9
antimony(III) bromide

: 108-67-8
1,3,5-trimethyl-benzene

: 35075-49-1
(1,3,5-trimethylbenzene)tribromoantimony(III)

Conditions

Conditions	Yield
In 1,3,5-trimethyl-benzene under dry N2, SbBr3 is dissolved in boiling mesitylene; soln. is cooled to -25°C, after some hours mother liquor is decanted off, crystals are dried in vac.; elem. anal.;	87%

: 7789-61-9
antimony(III) bromide

: 19629-22-2
di-n-propylantimonbromide

: 118399-66-9
n-propylantimondibromide

Conditions

Conditions	Yield
In neat (no solvent) react. under dry Ar, stirring (5 h); distilling the oily product, addn. of petroleum ether, crystn. at -15°C, elem. anal.;	85%

: 5711-05-7
sodium (4-N-ethyl)piperazine-1-carbodithioate

: 7789-61-9
antimony(III) bromide

: 1017266-23-7
(C2H5NC4H8NCS2)2SbBr

Conditions

Conditions	Yield
In acetone 2 equiv. of organic ligand added to stirring soln. of SbBr3 in acetone; stirred for 5 h at room temp.; filtered; solvent gradually removed by evapn. under vacuum; recrystallized from CHCl3; elem. anal.;	85%

: 7789-61-9
antimony(III) bromide

: 128-04-1
sodium dimethyldithiocarbamate

: 903499-43-4, 145120-00-9
(CH3CH3NCS2)2SbBr

Conditions

Conditions	Yield
In acetone 2 equiv. of organic ligand added to stirring soln. of SbBr3 in acetone; stirred for 5 h at room temp.; filtered; solvent gradually removed by evapn. under vacuum; recrystallized from EtOH; elem. anal.;	85%

: 7789-61-9
antimony(III) bromide

: 5712-49-2
sodium 4-methyl-1-piperazinecarbodithioate

: 1017266-24-8
(CH3NC4H8NCS2)2SbBr

Conditions

Conditions	Yield
In acetone 2 equiv. of organic ligand added to stirring soln. of SbBr3 in acetone; stirred for 5 h at room temp.; filtered; solvent gradually removed by evapn. under vacuum; recrystallized from EtOH; elem. anal.;	85%

: 66-71-7
1,10-Phenanthroline

: 7789-61-9
antimony(III) bromide

: [Sb2(1,10-phenanthroline)4Br8]

Conditions

Conditions	Yield
In acetone mixt. was stirred for 12 h at room temp.; mixt. was filtered, filtrate was gradually removed by evapn. under vac.,ppt. was recrystd. from EtOH; elem.anal.;	85%

: 7789-61-9
antimony(III) bromide

: 534-13-4
N,N-dimethylthiourea

: mer-SbBr3(N,N-dimethylthiourea)3

Conditions

Conditions	Yield
In dichloromethane; acetonitrile for 0.5h;	83.5%

: 617-85-6
triethylantimony

: 7789-61-9
antimony(III) bromide

: 4669-91-4
diethylantimony bromide

Conditions

Conditions	Yield
In further solvent(s) equimolar amts. of educts used, in a sealed tube at 100°C for one day;	83%
In N,N-dimethyl-formamide in sealed tube, one day, 100°C, molar ratio of SbBr3 and stibine = 1 : 2;	83%

Related products

7789-64-2

Iridium bromide (IrBr4)

7789-66-4

Silane, tetrabromo-

7789-67-5

Stannane, tetrabromo-

7789-68-6

Titanium bromide(TiBr4), (T-4)- (9CI)

7789-69-7

Phosphorane,pentabromo-

778-97-2

5-Pyrimidinecarboxylicacid, 4-amino-2-(ethylthio)-, ethyl ester

77897-21-3

Morpholine,3-(1-methylethyl)-, (3S)-

77897-22-4

Morpholine,3-(2-methylpropyl)-, (3S)-

77897-23-5

Morpholine,3-(phenylmethyl)-, (3S)-

7789-75-5

Calciumfluoride (CaF2)

Hot Products

7790-21-8

Potassium periodate

7790-38-7

PALLADIUM(II) IODIDE

7790-53-6

Potassium metaphosphate

77907-28-9

Disperse Red 311

77907-32-5

Reactive Navy Blue Ker

7790-75-2

Calcium tungstate

7790-78-5

Cadmium chloride hydrate

77934-47-5

N,N-di(1-Methyl heptyl) acetamide

104987-11-3

Tacrolimus

141-53-7

Sodium formate

8001-54-5

Quaternary ammonium compounds, alkylbenzyldimethyl, chlorides

9003-39-8

Povidone

10161-34-9

Trenbolone acetate

402957-28-2

Telaprevir

68-19-9

Cyanocobalamin

Products

Refine

Country

Business Type

Certificate

Display

Dayang Chem (Hangzhou) Co.,Ltd.

Henan Tianfu Chemical Co., Ltd.

Antimex Chemical Limied

Zhuozhou Wenxi import and Export Co., Ltd

Hangzhou Ocean Chemical Co., Ltd.

Hubei Langyou International Trading Co., Ltd

Changchun Artel lmport and Export trade company

Hunan Russell Chemicals Technology Co.,Ltd

Hunan Longxianng Runhui Trading Co.,Ltd

Beantown Chemical

Cerametek Materials（ShenZhen）Co., Ltd.

Hangzhou Share Chemical Co., Ltd

Strem Chemicals, Inc.

Nanjing Raymon Biotech Co., Ltd.

Hebei Minshang Biotechnology Co., Ltd

Skyrun Industrial Co.,Ltd

Hangzhou Fenjun Chemical Co Ltd.

Synthetic route

Related products

Hot Products