Product name: 3-(3'-Trifluoromethylphenyl)propanol Cas No:78573-45-2 Assay: 98%min Hangzhou Verychem Science And Technology Co. Ltd. was set up in year 2004, it’s a young but fast growing company. In the tw
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inquiryDayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities
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inquiryUnique advantages Guaranteed purity High quality & competitive price Quality control Fast feedback Prompt shipment Appearance:Colorless to light yellow liquid Storage:cool dry place Package:1kg/foil bag;25kg/drum Application:pharmaceutical
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inquiry3-(3'-Trifluoromethylphenyl)propanol CAS No.:78573-45-2 Name: 3-(3'-Trifluoromethylphenyl)propanol Synonyms: 3-(Trifluoromethyl)b
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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inquiryCangzhou Enke Pharma Tech Co.,ltd. is located in Cangzhou City, Hebei province ,where is a famous petroleum chemical industry city in China. Enke Pharma a high-tech enterprise ,and we are dedicated to developing and manufacturing new api, intermedi
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inquiryHebei Yanxi Chemical Co., Ltd. is a professional research, development and production of lead acetate benzene acetamide enterprise backbone members by local well-known entrepreneurs and professional senior engineers in the party's "low car
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inquiryProduct Description Product website: http://www.finerchem.com/pro01en/id/1177.html Product Name 3-(3'-Trifluoromethylphenyl)propanol CAS No.
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inquiryTIANFUCHEM--78573-45-2--3-(3'-TRIFLUOROMETHYL PHENYL) PROPANOL factory price Our company was built in 2009 with an ISO certificate.In the past 10 years, we have grown up as a famous fine chemicals supplier in China And we had establish
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inquiryAdvantage : LIDE PHARMACEUTICALS LTD. is a mid-small manufacturing-type enterprise, engaged in pharmaceutical intermediates of R&D, custom-made and production, and also involving trading chemicals for export. We have established the R&
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inquiryProducts: 3-(3-(trifluoromethyl)phenyl)propan-1-ol Cas No.: 78573-45-2 Molecular Formula: C10H11F3O Molecular Weight: 204.19 Assay: 98% HPLC Molecular Structure: App
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inquiryWe are leading fine chemicals supplier in China with ISO certificate, Our main business covers the fields below: 1.Noble Metal Catalysts (Pt.Pd...) 2.Organic Phosphine Ligands (Tert-butyl-phosphine.Cyclohexyl-phosphine...) 3.OLED
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inquiry3-(3'-TRIFLUOROMETHYL PHENYL) PROPANOL CAS: 78573-45-2 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in hi
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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Cas:78573-45-2
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inquiryProduct Name: 3-(3'-TRIFLUOROMETHYL PHENYL) PROPANOL Synonyms: 3-(3'-TRIFLUOROMETHYL PHENYL) PROPANOL;3-(3-TRIFLUOROMETHYL-PHENYL)-PROPAN-1-OL;3-(Trifluoromethyl)benzenepropanol;Cinacalcet Intermediate 1;Cinacalcet I;Cinacalcet InterMedia
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inquiryBest quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
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inquiryAppearance:Colorless liquid Storage:Store in a cool,dry place and keep away from direct strong light Package:As customer request Application:Used for research and industrial manufacture. Transportation:By Sea/Air/Courier Port:QI
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inquiryOur Services 1. New Molecules R&D 2. Own test center HPLC NMR GC LC-MS 3. API and Intermediates from China reputed manufacturers 4. Documents support COA MOA MSDS DMF open part Our advantages 1. Government awarded company. Top 100 enter
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inquiryWhy Choose Us: 1. Factory direct sales, so we can provide the competitive price and high quality product base on 8 years of production and R&D experience. 2. It is available in stock for quick shipment.Products could be packaged according to cu
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inquiryOur Advantages Production: Advanced chemical equipment with years of experience.Staffs for producing various extract products. Quality Control:A complete set of Testing Professional and Analysis Equipment ensures the Quality Requirements and Speci
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inquiry3-<3-(trifluoromethyl)phenyl>prop-2-en-1-ol
3-[3-(trifluoromethyl)phenyl]propan-1-ol
Conditions | Yield |
---|---|
With hydrogen In ethanol at 60℃; under 15001.5 Torr; for 6h; Pressure; Temperature; Solvent; Autoclave; | 99.4% |
With hydrogen; palladium on activated charcoal In ethanol at 20℃; under 750.06 Torr; for 26h; | 57% |
With 5%-palladium/activated carbon In 2-methyltetrahydrofuran at 30 - 40℃; under 1500.15 - 2250.23 Torr; Temperature; |
methyl 3-(3-(trifluoromethyl)phenyl)propanoate
3-[3-(trifluoromethyl)phenyl]propan-1-ol
Conditions | Yield |
---|---|
With hydrogen In methanol at 160℃; under 150015 Torr; Product distribution / selectivity; | 98% |
With lithium aluminium tetrahydride In diethyl ether at 0℃; | 97% |
With dimethylsulfide borane complex In 2-methyltetrahydrofuran at 90℃; under 7500.75 Torr; for 0.333333h; Inert atmosphere; Flow reactor; | 97% |
Stage #1: methyl 3-(3-(trifluoromethyl)phenyl)propanoate With sodium tetrahydroborate In tetrahydrofuran Inert atmosphere; Reflux; Stage #2: With methanol In tetrahydrofuran at 60 - 65℃; for 9h; Inert atmosphere; | 95% |
3-(3-trifluoromethylphenyl)propanoic acid
3-[3-(trifluoromethyl)phenyl]propan-1-ol
Conditions | Yield |
---|---|
Stage #1: 3-(3-trifluoromethylphenyl)propanoic acid With borane-THF In tetrahydrofuran at 0 - 20℃; for 25h; Stage #2: With water In tetrahydrofuran; methanol | 94% |
With borane In tetrahydrofuran at 0 - 20℃; for 25h; Inert atmosphere; | 94% |
Stage #1: 3-(3-trifluoromethylphenyl)propanoic acid With 4-methyl-morpholine; chloroformic acid ethyl ester In 2-methyltetrahydrofuran at -10 - -5℃; for 0.00166667h; Stage #2: With sodium tetrahydroborate In 2-methyltetrahydrofuran; water at 0 - 5℃; for 0.5h; Solvent; Reagent/catalyst; | 92.2% |
3-(3-(trifluoromethyl)phenyl)prop-2-yn-1-ol
3-[3-(trifluoromethyl)phenyl]propan-1-ol
Conditions | Yield |
---|---|
With palladium 10% on activated carbon; hydrogen In ethanol at 20℃; for 6h; | 82% |
With hydrogen; palladium 10% on activated carbon In isopropyl alcohol at 42 - 45℃; under 3750.38 Torr; for 5h; | 72.1% |
With hydrogen; 5% Pd(II)/C(eggshell) In methanol at 20℃; under 760.051 Torr; for 72h; | |
With hydrogen; 5% Pd(II)/C(eggshell) In methanol; water at 20℃; under 760.051 Torr; for 72h; |
(R)-1-(meta-trifluoromethylphenyl) 3-tosyloxy 2-propanol
A
meta-trifluoromethylphenyl-propane
B
3-[3-(trifluoromethyl)phenyl]propan-1-ol
C
(S)-1-[(3′-trifluoromethyl)phenyl]-2-propanol
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride In diethyl ether at 21℃; for 3h; | A 3% B 8% C 69% |
3-[3-(trifluoromethyl)phenyl]propan-1-ol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: aq. HClO4 / tetrahydrofuran 2: Pb(OAc)4 / CH2Cl2 3: LiAlH4 / diethyl ether View Scheme |
ethyl 3-(3-trifluoromethylphenyl)-propionate
3-[3-(trifluoromethyl)phenyl]propanal
3-[3-(trifluoromethyl)phenyl]propan-1-ol
Conditions | Yield |
---|---|
Stage #1: ethyl 3-(3-trifluoromethylphenyl)-propionate; 3-[3-(trifluoromethyl)phenyl]propanal With sodium tetrahydroborate In ethanol at 20℃; for 24h; Stage #2: With ethanol; water In ethyl acetate Product distribution / selectivity; |
ethyl 3-(3-trifluoromethylphenyl)-propionate
3-[3-(trifluoromethyl)phenyl]propan-1-ol
Conditions | Yield |
---|---|
Stage #1: ethyl 3-(3-trifluoromethylphenyl)-propionate With sodium tetrahydroborate In ethanol at 20℃; for 24h; Stage #2: With ethanol; water In ethyl acetate Product distribution / selectivity; |
ethyl 3-(3-trifluoromethylphenyl)-propionate
(E)-3-(3-(trifluoromethyl)phenyl)acrylaldehyde
A
3-[3-(trifluoromethyl)phenyl]propan-1-ol
B
(E)-3-(3-trifluoromethylphenyl)prop-2-en-1-ol
Conditions | Yield |
---|---|
Stage #1: ethyl 3-(3-trifluoromethylphenyl)-propionate; (E)-3-(3-(trifluoromethyl)phenyl)acrylaldehyde With sodium tetrahydroborate In ethanol at 20℃; for 24h; Stage #2: With ethanol; water In ethyl acetate Product distribution / selectivity; | |
Stage #1: ethyl 3-(3-trifluoromethylphenyl)-propionate; (E)-3-(3-(trifluoromethyl)phenyl)acrylaldehyde With lithium aluminium tetrahydride In tetrahydrofuran at -5℃; for 0.666667h; Stage #2: With sodium hydroxide; water In tetrahydrofuran; acetone Product distribution / selectivity; | |
Stage #1: ethyl 3-(3-trifluoromethylphenyl)-propionate; (E)-3-(3-(trifluoromethyl)phenyl)acrylaldehyde With lithium aluminium tetrahydride In tetrahydrofuran at -5℃; for 0.666667h; Stage #2: With sulfuric acid; water In tetrahydrofuran; acetone Product distribution / selectivity; |
3-Trifluoromethylbenzaldehyde
3-[3-(trifluoromethyl)phenyl]propan-1-ol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: piperidine / pyridine / 50 - 75 °C / Inert atmosphere 1.2: 0 °C / Cooling with ice 2.1: hydrogen / palladium 10% on activated carbon / methanol / 2.5 h / 750.08 Torr 3.1: borane / tetrahydrofuran / 25 h / 0 - 20 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 4 steps 1.1: pyridine; piperidine / 4.25 h / 20 - 120 °C / Inert atmosphere 1.2: pH 2 2.1: sodium hydroxide / water / 20 °C 2.2: 7 h / 25 - 30 °C / 750.08 Torr 2.3: pH 2 3.1: thionyl chloride / 4 h / Inert atmosphere; Reflux 4.1: sodium tetrahydroborate / tetrahydrofuran / Inert atmosphere; Reflux 4.2: 9 h / 60 - 65 °C / Inert atmosphere View Scheme |
3-(trifluoromethyl)cinnamic acid
3-[3-(trifluoromethyl)phenyl]propan-1-ol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: hydrogen / palladium 10% on activated carbon / methanol / 2.5 h / 750.08 Torr 2: borane / tetrahydrofuran / 25 h / 0 - 20 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 2 steps 1: palladium 10% on activated carbon; hydrogen / ethanol / 16 h / 20 °C / 760.05 Torr 2: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / 20 °C View Scheme | |
Multi-step reaction with 3 steps 1.1: sodium hydroxide / water / 20 °C 1.2: 7 h / 25 - 30 °C / 750.08 Torr 1.3: pH 2 2.1: thionyl chloride / 4 h / Inert atmosphere; Reflux 3.1: sodium tetrahydroborate / tetrahydrofuran / Inert atmosphere; Reflux 3.2: 9 h / 60 - 65 °C / Inert atmosphere View Scheme |
3-trifluoromethylbenzoic acid methyl ester
3-[3-(trifluoromethyl)phenyl]propan-1-ol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: potassium methanolate / iso-xylene / 12 h / 80 °C / 760.05 Torr / Industry scale 2: hydrogen / 5% Pd(II)/C(eggshell) / methanol / 48 h / 60 °C / 7500.75 Torr / Autoclave 3: hydrogen / / methanol / 160 °C / 150015 Torr View Scheme |
3-bromo-1-trifluoromethylbenzene
3-[3-(trifluoromethyl)phenyl]propan-1-ol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: triethylamine / triphenylphosphine; copper(l) iodide; palladium dichloride / N,N-dimethyl acetamide / 50 - 70 °C / Inert atmosphere 2: hydrogen / 5% Pd(II)/C(eggshell) / methanol / 72 h / 20 °C / 760.05 Torr View Scheme | |
Multi-step reaction with 2 steps 1: triethylamine / triphenylphosphine; copper(l) iodide; palladium dichloride / ISOPROPYLAMIDE / 17 h / 50 - 70 °C 2: hydrogen / 5% Pd(II)/C(eggshell) / water; methanol / 72 h / 20 °C / 760.05 Torr View Scheme | |
Multi-step reaction with 2 steps 1: copper(l) iodide; 1,8-diazabicyclo[5.4.0]undec-7-ene; tetrakis(triphenylphosphine) palladium(0) / tetrahydrofuran / 22 h / 0 - 55 °C / Inert atmosphere; Sealed tube 2: palladium 10% on activated carbon; hydrogen / ethanol / 6 h / 20 °C View Scheme |
3-[3-(trifluoromethyl)phenyl]propan-1-ol
methanesulfonyl chloride
methylsulfonyl-3-(3-trifluoromethylphenyl)propyl ester
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 20℃; | 100% |
With triethylamine In dichloromethane at -5℃; for 1.5h; Temperature; | 97.9% |
With triethylamine In toluene at 20 - 25℃; for 2h; | 93% |
3-[3-(trifluoromethyl)phenyl]propan-1-ol
3-[3-(trifluoromethyl)phenyl]propanal
Conditions | Yield |
---|---|
Stage #1: 3-[3-(trifluoromethyl)phenyl]propan-1-ol With phosphorus pentoxide; dimethyl sulfoxide In dichloromethane at 20℃; Swern Oxidation; Cooling with ice; Stage #2: With triethylamine In dichloromethane at 20℃; Cooling with ice; | 100% |
Stage #1: 3-[3-(trifluoromethyl)phenyl]propan-1-ol With phosphorus pentoxide; dimethyl sulfoxide In dichloromethane for 0.5h; Cooling; Stage #2: With triethylamine In dichloromethane for 1h; Cooling; | 100% |
With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; trichloroisocyanuric acid at 0 - 20℃; for 0.5h; | 100% |
3-[3-(trifluoromethyl)phenyl]propan-1-ol
p-toluenesulfonyl chloride
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 20℃; Autoclave; Large scale; | 100% |
With pyridine In chloroform | |
With triethylamine; dmap In dichloromethane at -5 - 10℃; Product distribution / selectivity; | |
With triethylamine; dmap In dichloromethane at 25 - 40℃; for 15h; Product distribution / selectivity; |
3-[3-(trifluoromethyl)phenyl]propan-1-ol
Conditions | Yield |
---|---|
With triphenylphosphine; diethylazodicarboxylate In toluene at 50℃; for 1h; | 100% |
(R)-1-(1-Naphthyl)ethylamine
3-[3-(trifluoromethyl)phenyl]propan-1-ol
cinacalcet
Conditions | Yield |
---|---|
With bis[dichloro(pentamethylcyclopentadienyl)iridium(III)]; D-sorbitol; choline chloride at 60℃; for 12h; | 98% |
Stage #1: 3-[3-(trifluoromethyl)phenyl]propan-1-ol With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene In dichloromethane at 20℃; for 2h; Stage #2: (R)-1-(1-Naphthyl)ethylamine With sodium tris(acetoxy)borohydride In dichloromethane optical yield given as %ee; | 84% |
With bis[dichloro(pentamethylcyclopentadienyl)iridium(III)]; sodium hydrogencarbonate In toluene at 110℃; for 17h; Inert atmosphere; Sealed tube; | 75% |
With C19H22MnN3O3P(1+); potassium hydride In 1,2-dimethoxyethane at 100℃; for 48h; Glovebox; Sealed tube; Inert atmosphere; | 50% |
3-[3-(trifluoromethyl)phenyl]propan-1-ol
1-(3-bromopropyl)-3- (trifluoromethyl)benzene
Conditions | Yield |
---|---|
With sulfuric acid; hydrogen bromide; tetra(n-butyl)ammonium hydrogensulfate In water at 82℃; for 25h; Temperature; Concentration; Reagent/catalyst; | 90.97% |
With hydrogen bromide In water at 85 - 90℃; for 15h; | 82% |
With 1H-imidazole; bromine; triphenylphosphine In dichloromethane at 0 - 25℃; | 81% |
3-[3-(trifluoromethyl)phenyl]propan-1-ol
1-(3-iodopropyl)-3-(trifluoromethyl)benzene
Conditions | Yield |
---|---|
With 1H-imidazole; iodine; triphenylphosphine In dichloromethane at 20 - 35℃; for 2h; | 85% |
With trimethylsilyl iodide In dichloromethane at 20℃; |
(R)-1-(1-Naphthyl)ethylamine
3-[3-(trifluoromethyl)phenyl]propan-1-ol
cinacalcet hydrochloride
Conditions | Yield |
---|---|
Stage #1: (R)-1-(1-Naphthyl)ethylamine; 3-[3-(trifluoromethyl)phenyl]propan-1-ol With bis[dichloro(pentamethylcyclopentadienyl)iridium(III)] In toluene at 110℃; for 6h; Inert atmosphere; Stage #2: With hydrogenchloride In diethyl ether; hexane; ethyl acetate; toluene Reagent/catalyst; Time; | 83% |
3-[3-(trifluoromethyl)phenyl]propan-1-ol
B
1-(3-bromopropyl)-3- (trifluoromethyl)benzene
Conditions | Yield |
---|---|
With sulfuric acid; hydrogen bromide In water at 25 - 55℃; | A n/a B 76.45% |
3-[3-(trifluoromethyl)phenyl]propan-1-ol
Conditions | Yield |
---|---|
With di-isopropyl azodicarboxylate; triphenylphosphine In toluene at 20℃; for 12h; Sealed tube; | 67% |
3-[3-(trifluoromethyl)phenyl]propan-1-ol
(R)-(1-naphthalen-1-ylethyl)carbamic acid 3-(3-trifluoromethylphenyl)propyl ester
Conditions | Yield |
---|---|
With pyridine In dichloromethane at -2 - 22℃; for 16.5h; Temperature; Inert atmosphere; | 48.17% |
3-[3-(trifluoromethyl)phenyl]propan-1-ol
methyl (S)-2-tert-butoxycarbonyl-7-hydroxy-1,2,3,4-tetrahydroisoquinoline-3-carboxylate
Conditions | Yield |
---|---|
With triphenylphosphine; diethylazodicarboxylate In tetrahydrofuran; toluene at 20℃; for 2h; Mitsunobu Displacement; | 40% |
3-[3-(trifluoromethyl)phenyl]propan-1-ol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 65 percent / (COCl)2/DMSO; Et3N View Scheme |
3-[3-(trifluoromethyl)phenyl]propan-1-ol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 65 percent / (COCl)2/DMSO; Et3N View Scheme |
3-[3-(trifluoromethyl)phenyl]propan-1-ol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: Py 2: (i) Na, KI, EtOH, (ii) /BRN= 2987616/ View Scheme |
3-[3-(trifluoromethyl)phenyl]propan-1-ol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: Py 2: (i) Na, KI, EtOH, (ii) /BRN= 2987616/ 3: aq. HCl View Scheme |
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