1,8-Dinitroanthraquinone supplier

Name
1,8-Dinitroanthraquinone
EINECS 204-943-0
CAS No. 129-39-5
Article Data15
CAS DataBase
Density 1.631 g/cm³
Solubility
Melting Point 318-322
Formula C₁₄H₆N₂O₆
Boiling Point 563.4 ºC at 760 mmHg
Molecular Weight 298.211
Flash Point 294 ºC
Transport Information
Appearance
Safety
Risk Codes
Molecular Structure
Hazard Symbols
Synonyms Anthraquinone,1,8-dinitro- (6CI,7CI,8CI);1,8-Dinitro-9,10-anthraquinone;1,8-Dinitroanthraquinone;Alizarine Violet R Base;NSC 37108;Waxoline VioletBA;
PSA 125.78000
LogP 3.32480

Synthetic route

: 82-35-9
1.5-dinitroanthraquinone

: 129-39-5
1,8-dinitroanthraquinone

Conditions

Conditions	Yield
In 5,5-dimethyl-1,3-cyclohexadiene	77%

: 59471-77-1
1-amino-8-nitro-anthraquinone

: 129-39-5
1,8-dinitroanthraquinone

Conditions

Conditions	Yield
With peracetic acid

: 3-nitro-2-(2-nitro-benzoyl)-benzoic acid

: 129-39-5
1,8-dinitroanthraquinone

Conditions

Conditions	Yield
With sulfuric acid; boric acid at 150℃;

: 84-65-1
9,10-phenanthrenequinone

A: 82-34-8
1-nitroanthraquinone

B: 82-35-9
1.5-dinitroanthraquinone

C: 129-39-5
1,8-dinitroanthraquinone

Conditions

Conditions	Yield
With phosphoric acid; sulfuric acid; nitric acid In tetrachloromethane at 55℃; for 0.5h; var. mole ratio of acids, var. temp. and time;

...Expand

: 84-65-1
9,10-phenanthrenequinone

A: 82-35-9
1.5-dinitroanthraquinone

B: 129-39-5
1,8-dinitroanthraquinone

Conditions

Conditions	Yield
With sulfuric acid; nitric acid multistep reaction; potentiometric studies of optimum reaction conditions;
With sulfuric acid; nitric acid Yield given. Yields of byproduct given;
With sulfuric acid; nitric acid 20 to 25 deg C; 3 h; Yield given. Yields of byproduct given;

: 84-65-1
9,10-phenanthrenequinone

HNO3+H2SO4: HNO3+H2SO4

A: 82-35-9
1.5-dinitroanthraquinone

B: 1604-43-9
1,7-dinitro-anthraquinone

C: 129-39-5
1,8-dinitroanthraquinone

D: 1604-40-6
2,6-dinitro-anthraquinone

Conditions

Conditions	Yield
Product distribution;

...Expand

: 7664-93-9
sulfuric acid

: 7697-37-2
nitric acid

: 84-65-1
9,10-phenanthrenequinone

A: 82-35-9
1.5-dinitroanthraquinone

B: 1604-43-9
1,7-dinitro-anthraquinone

C: 129-39-5
1,8-dinitroanthraquinone

D: 1604-42-8
1,6-dinitro-anthraquinone

Conditions

Conditions	Yield
at 80℃;

...Expand

: 84-65-1
9,10-phenanthrenequinone

HNO3+H2SO4: HNO3+H2SO4

A: 82-35-9
1.5-dinitroanthraquinone

B: 1604-43-9
1,7-dinitro-anthraquinone

C: 129-39-5
1,8-dinitroanthraquinone

D: 1604-42-8
1,6-dinitro-anthraquinone

Conditions

Conditions	Yield
Product distribution;

...Expand

: 84-65-1
9,10-phenanthrenequinone

HNO3+H2SO4: HNO3+H2SO4

A: 1604-43-9
1,7-dinitro-anthraquinone

B: 129-39-5
1,8-dinitroanthraquinone

C: 1604-40-6
2,6-dinitro-anthraquinone

D: 1604-42-8
1,6-dinitro-anthraquinone

...Expand

: 82-34-8
1-nitroanthraquinone

: 7664-93-9
sulfuric acid

: 7697-37-2
nitric acid

A: 82-35-9
1.5-dinitroanthraquinone

B: 1604-43-9
1,7-dinitro-anthraquinone

C: 129-39-5
1,8-dinitroanthraquinone

D: 1604-42-8
1,6-dinitro-anthraquinone

Conditions

Conditions	Yield
at 80℃;

...Expand

: 84-65-1
9,10-phenanthrenequinone

A: 129-39-5
1,8-dinitroanthraquinone

B 1.5-, 1.6-, 1.7-, 2.6-and 2.7-dinitro-anthraquinone: 1.5-, 1.6-, 1.7-, 2.6-and 2.7-dinitro-anthraquinone

Conditions

Conditions	Yield
With sulfuric acid; nitric acid

: 82-34-8
1-nitroanthraquinone

A: 129-39-5
1,8-dinitroanthraquinone

B 1.5-dinitro-anthraquinone, 1.6-dinitro-anthraquinone, 1.7-dinitro-anthraquinone: 1.5-dinitro-anthraquinone, 1.6-dinitro-anthraquinone, 1.7-dinitro-anthraquinone

Conditions

Conditions	Yield
With sulfuric acid; nitric acid at 80℃;

: 7664-93-9
sulfuric acid

: 3-nitro-2-(2-nitro-benzoyl)-benzoic acid

: 13460-50-9
metaboric acid

: 129-39-5
1,8-dinitroanthraquinone

Conditions

Conditions	Yield
at 150℃;

...Expand

: 612-35-1
2-Benzylbenzoic acid

: 129-39-5
1,8-dinitroanthraquinone

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1: nitric acid 2: chromic acid; acetic acid 3: fuming sulfuric acid; boric acid / 150 °C View Scheme

: 3-nitro-2-(2-nitro-benzyl)-benzoic acid

: 129-39-5
1,8-dinitroanthraquinone

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: chromic acid; acetic acid 2: fuming sulfuric acid; boric acid / 150 °C View Scheme

: 84-65-1
9,10-phenanthrenequinone

: 129-39-5
1,8-dinitroanthraquinone

: 57875-61-3
dinitro-anthraquinone

: 129-39-5
1,8-dinitroanthraquinone

Conditions

Conditions	Yield
In water; nitric acid

: 129-39-5
1,8-dinitroanthraquinone

: 129-42-0
1,8-diamino-anthraquinone

Conditions

Conditions	Yield
With sodium sulfide In ethanol; water for 12h; Heating;	98%
With sodium sulfide In ethanol; water for 64.5h; Reflux;	98%
With sodium sulfide; sodium hydroxide In ethanol; water for 6h; Reflux;	98%

α,α-dinitroanthraquinone: α,α-dinitroanthraquinone

: 129-39-5
1,8-dinitroanthraquinone

A HNO3 -moist 1,5-dinitroanthraquinone: HNO3 -moist 1,5-dinitroanthraquinone

B: 82-35-9
1.5-dinitroanthraquinone

Conditions

Conditions	Yield
	A n/a B 97.1%

...Expand

: 123-39-7
N-Methylformamide

: 129-39-5
1,8-dinitroanthraquinone

: 60316-43-0
1,8-bis-methylaminoanthraquinone

Conditions

Conditions	Yield
In methanol	94.3%

: 129-39-5
1,8-dinitroanthraquinone

: 139312-39-3
anthracene-1,8-diamine

Conditions

Conditions	Yield
With sodium tetrahydroborate In isopropyl alcohol for 36h; Inert atmosphere; Reflux;	93%
With sodium tetrahydroborate In isopropyl alcohol	30%
Multi-step reaction with 2 steps 1: 98 percent / Na2S*9H2O / H2O; ethanol / 12 h / Heating 2: 83 percent / NaBH4; NaOH / propan-2-ol / 8 h / Heating View Scheme

: sulfonamide

: 129-39-5
1,8-dinitroanthraquinone

: 6407-55-2
1,8-dimethoxy-9,10-anthracenedione

Conditions

Conditions	Yield
With potassium hydroxide In methanol	90%

: 129-39-5
1,8-dinitroanthraquinone

: 108-90-7
chlorobenzene

: 13676-91-0
1,8-bis(phenylthio)anthracene-9,10-dione

Conditions

Conditions	Yield
Stage #1: chlorobenzene With potassium hydrosulfide; 18-crown-6 ether In dimethyl sulfoxide at 110 - 120℃; for 16h; Large scale; Stage #2: 1,8-dinitroanthraquinone In dimethyl sulfoxide at 40 - 50℃; Solvent; Reagent/catalyst; Large scale;	87.3%

: 129-39-5
1,8-dinitroanthraquinone

: 93102-05-7
N-benzyl-N-(methoxymethyl)-N-[(trimethylsilyl)methyl]amine

: 15,22-dinitro-6,7,13,14-dibenzo-3,11-dibenzyl-1,9-dioxa-3,11-diazadispiro[4.2.4.2]tetradecane

Conditions

Conditions	Yield
With trifluoroacetic acid In dichloromethane at 0 - 20℃; for 5h; Inert atmosphere;	66%

: 129-39-5
1,8-dinitroanthraquinone

: 114645-02-2
9,10-dihydro-1,8-diaminoanthracene

Conditions

Conditions	Yield
With sodium tetrahydroborate In isopropyl alcohol for 43h; Inert atmosphere; Reflux;	31%
Multi-step reaction with 2 steps 1: sodium sulfide / ethanol; water / 64.5 h / Reflux 2: sodium hydroxide; sodium tetrahydroborate / isopropyl alcohol / 15.5 h / Inert atmosphere; Reflux View Scheme

: 110-89-4
piperidine

: 129-39-5
1,8-dinitroanthraquinone

: 1-nitro-8-piperidino-anthraquinone

Conditions

Conditions	Yield
With pyridine at 60 - 70℃;

: 67-56-1
methanol

: 129-39-5
1,8-dinitroanthraquinone

: 6407-55-2
1,8-dimethoxy-9,10-anthracenedione

Conditions

Conditions	Yield
With sodium hydroxide
With sodium hydroxide

: 635-46-1
1,2,3,4-tetrahydroisoquinoline

: 129-39-5
1,8-dinitroanthraquinone

: 64-19-7
acetic acid

: 59471-77-1
1-amino-8-nitro-anthraquinone

...Expand

: 699-09-2
4-ethoxy-benzenethiol

: 129-39-5
1,8-dinitroanthraquinone

: 1,8-bis-(4-ethoxy-phenylsulfanyl)-anthraquinone

Conditions

Conditions	Yield
With alkali

: 129-39-5
1,8-dinitroanthraquinone

: 100-67-4
potassium phenolate

: 82-17-7
1,8-diphenoxyanthracene-9,10-dione

: 129-39-5
1,8-dinitroanthraquinone

: 117-10-2
1,8-dihydroxy-9,10-anthracenedione

Conditions

Conditions	Yield
With potassium acetate; acetic acid at 170℃;
Multi-step reaction with 2 steps 1: water; alkali sulfite 2: quicklime; water / 180 - 200 °C View Scheme
With pyridine
With quicklime; water at 190 - 200℃;

: 129-39-5
1,8-dinitroanthraquinone

: 82-48-4
1,8-anthraquinonedisulphonic acid

Conditions

Conditions	Yield
With alkali sulfite; water
With alkali sulfite; water

: 129-39-5
1,8-dinitroanthraquinone

: 59471-77-1
1-amino-8-nitro-anthraquinone

Conditions

Conditions	Yield
With 1,2,3,4-tetrahydroisoquinoline; acetic acid

: 129-39-5
1,8-dinitroanthraquinone

: 60080-33-3
1,8-bis-hydroxyamino-anthraquinone

Conditions

Conditions	Yield
With tin oxide; sodium carbonate

: 129-39-5
1,8-dinitroanthraquinone

: 3224-33-7
1,8-diamino-2,4,5,7-tetrabromo-anthraquinone

Conditions

Conditions	Yield
With bromine; acetic acid at 150℃; im geschlossenen Rohr;

: 129-39-5
1,8-dinitroanthraquinone

: 3,6-dihydroxy-4,5-diimino-1,8,9,10-tetraoxo-1,4,5,8,9,10-hexahydro-anthracene-2,7-disulfonic acid

Conditions

Conditions	Yield
With sulfuric acid; sulfur trioxide; sulfur at 120 - 130℃; eventuell unter Zusatz von Borsaeure, bis zur Wasserloeslichkeit und Eingiessen der abgekuehlten Schmelze in eine auf -10grad gekuehlte 20prozentige NaCl- oder KCl-Loesung;

: 129-39-5
1,8-dinitroanthraquinone

: 106-49-0
p-toluidine

A: 82-16-6
1,8-bis(p-tolylamino)anthraquinone

B: 1-nitro-8-p-toluidino-anthraquinone

Conditions

Conditions	Yield
With pyridine

...Expand

: 129-39-5
1,8-dinitroanthraquinone

: 75-04-7
ethylamine

: 1-ethylamino-8-nitro-anthraquinone

Conditions

Conditions	Yield
With pyridine at 50℃;

: 129-39-5
1,8-dinitroanthraquinone

: 127-08-2
potassium acetate

: 64-19-7
acetic acid

: 81-64-1
1,4-dihydroxy-9,10-anthracenedione

Conditions

Conditions	Yield
at 170℃;

...Expand

: 129-39-5
1,8-dinitroanthraquinone

: 95-48-7
ortho-cresol

: 1-nitro-8-o-tolyloxy-anthraquinone

Conditions

Conditions	Yield
With potassium hydroxide

: 129-39-5
1,8-dinitroanthraquinone

: 121-69-7
N,N-dimethyl-aniline

: 59471-77-1
1-amino-8-nitro-anthraquinone

: 129-39-5
1,8-dinitroanthraquinone

: 124-40-3
dimethyl amine

: 1-dimethylamino-8-nitro-anthraquinone

: 129-39-5
1,8-dinitroanthraquinone

: 107-15-3
ethylenediamine

: 94068-88-9
1,8-di(2-aminoethylamino)anthracene-9,10-dione

: 129-39-5
1,8-dinitroanthraquinone

: 109-89-7
diethylamine

: 1-diethylamino-8-nitro-anthraquinone

Conditions

Conditions	Yield
With pyridine at 50 - 70℃;

1,8-Dinitroanthraquinone Specification

1,8-DINITROANTHRAQUINONE , with the CAS register number 129-39-5, has the systematic name of 1,8-dinitroanthracene-9,10-dione. And it has other names such as 1,8-dinitro-10-anthracenedione ,1,8-Dinitro-9,10-anthracenedione ,10-Anthracenedione,1,8-dinitro-9;1,8-DINITROANTHRAQUINONE ,1,8-dinitroanthracene-9,10-dione ,1,8-DINITRO ANTHRAQUINONE 97% MIN , and 1,8-Dinitro-9,10-anthraquinone .

The characteristics of this chemical are as below: (1)ACD/LogP: 3.04 ; (2)ACD/LogD (pH 5.5): 3.04 ; (3)ACD/LogD (pH 7.4): 3.04 ; (4)ACD/BCF (pH 5.5): 121.26 ; (5)ACD/BCF (pH 7.4): 121.26 ; (6)ACD/KOC (pH 5.5): 1079.26 ; (7)ACD/KOC (pH 7.4): 1079.26 ; (8)#H bond acceptors: 8 ; (9)#Freely Rotating Bonds: 2 ; (10)Polar Surface Area: 125.78; (11)Index of Refraction: 1.714 ; (12)Molar Refractivity: 71.75 cm³ ; (13)Molar Volume: 182.7 cm³ ; (14)Polarizability: 28.44 ×10-24cm³ ; (15)Surface Tension: 81.4 dyne/cm ; (16)Density: 1.631 g/cm³ ; (17)Flash Point: 294 °C ; (18)Enthalpy of Vaporization: 84.67 kJ/mol ; (19)Boiling Point: 563.4 °C at 760 mmHg ; (20)Vapour Pressure: 1.02E-12 mmHg at 25°C .

1,8-DINITROANTHRAQUINONE belongs to the product categories of Intermediates of Dyes and Pigments ,C13 to C14 ,Carbonyl Compounds , and Ketones . When it comes to raw materials, we need to list the following: SULFURIC ACID ,Sodium sulfite , Anthraquinone , and 1 5-DINITROANTHRAQUINONE 97 . And its preparation products is Disperse Blue 56 . Besides, if you need the safety information, you could refer to WGK Germany 3.

Additionally, you could convert the following data information into the molecular structure:
SMILES:
[O-][N+](=O)c3cccc2C(=O)c1cccc(c1C(=O)c23)[N+]([O-])=O
InChI:
InChI=1/C14H6N2O6/c17-13-7-3-1-5-9(15(19)20)11(7)14(18)12-8(13)4-2-6-10(12)16(21)22/h1-6H
InChIKey:
MBIJFIUDKPXMAV-UHFFFAOYAM

As to the market condition of 1,8-DINITROANTHRAQUINONE , it has many suppliers in China, such as Sunwell Chemicals Co., Ltd.

Product Name

1,8-Dinitroanthraquinone

Synthetic route

1,8-Dinitroanthraquinone Specification

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