As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
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inquiryTIANFUCHEM--2581-34-2--High purity 3-Methyl-4-nitrophenol factory price Our company was built in 2009 with an ISO certificate.In the past 10 years, we have grown up as a famous fine chemicals supplier in China And we had established stable
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inquiryProduct Name 4-Methyl-3-nitrophenol Synonyms 4-Methyl-3-nitrophenol;3-Nitro-p-cresol CAS: 2042-14-0 MF: - MW: - EINECS:
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquiry2581-34-2 C7H7NO3 3-Methyl-4-nitrophenolAppearance:white powder Storage:Normal temperature Package:according to customers' requirements Application:Aromatic Phenols;Phenoles and thiophenoles Transportation:By air(EMS or EUB
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inquirySuperior quality moderate price & quick delivery Appearance:YELLOWISH TO BEIGE CRYSTALLINE POWDER Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:1kg/bag, 1kg/drum or 25kg/drum or as per your request. Applic
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inquiryHangzhou Huarong Pharm Co., Ltd.established since 2006 , has been actively developing specialty products for Finished Dosages, APIs, Intermediates, and Fine chemicals markets in North America, Europe, Korea, Japan, Mid-East and all over the World. Hu
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We are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp
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inquiryhigh purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
R & D enterprises have their own stock in stockAppearance:To be subject to the object Package:Customized Application:pharmaceutical intermediates Transportation:Air Port:Shanghai;Guangzhou
high purity,in stock Package:25kg/drum,or as per customers'demand Application:API,Pharmaceutical intermediates Transportation:air,sea,courier
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Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
TIANFUCHEM--2581-34-2--High purity 3-Methyl-4-nitrophenol factory price Application:TIANFUCHEM--2581-34-2--High purity 3-Methyl-4-nitrophenol factory price
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inquiryConditions | Yield |
---|---|
With Vilsmeier reagent; potassium nitrate In neat (no solvent) at 100℃; under 1500.15 Torr; Reagent/catalyst; Temperature; Microwave irradiation; | 92% |
With potassium hydrogensulfate; potassium metaperiodate; sodium nitrite In water; acetonitrile at 30 - 35℃; for 15h; Reagent/catalyst; Solvent; | 78% |
With ferric nitrate; 1,3-di-n-butyl-imidazolium tetrafluoroborate at 30℃; for 1.5h; | 76% |
Conditions | Yield |
---|---|
With silica supported Al(NO3)3*9H2O In acetone at 20℃; for 0.416667h; regioselective reaction; | A 87% B 5% |
With tert.-butylnitrite In acetonitrile at 29.84℃; Kinetics; Solvent; Temperature; | A n/a B 80% |
With 3-(ethoxycarbonyl)-1-(5-methyl-5-(nitrosooxy)hexyl)pyridin-1-ium bis(trifluoromethanesulfonyl)imide at 20℃; for 2h; Ionic liquid; | A 34% B 63% |
danishefsky's diene
((Z)-1-Nitro-prop-1-ene-2-sulfinyl)-benzene
3-methyl-4-nitrophenol
Conditions | Yield |
---|---|
In benzene at 25℃; for 24h; | 73% |
Conditions | Yield |
---|---|
With sodium hydroxide; dihydrogen peroxide In water at 25 - 40℃; for 3h; | 58% |
With nitric acid at 40℃; |
3-methyl-phenol
A
2-nitro-5-methylphenol
B
3-methyl-4-nitrophenol
C
3-methyl-2-nitrophenol
Conditions | Yield |
---|---|
With Eu-Mo-modified montmorillonite HKSF; nitric acid In tetrahydrofuran at 20℃; for 12h; | A 25% B 53% C 9% |
With Yb-Mo-modified montmorillonite HKSF; nitric acid In tetrahydrofuran at 20℃; for 12h; | A 26% B 52% C 13% |
With nitro acetate; silica gel In chloroform at -20 - 20℃; Nitration; | A 50% B 20% C 30% |
3-methyl-1,4-benzoquinone 4-oxime
3-methyl-4-nitrophenol
Conditions | Yield |
---|---|
With sodium hydroxide; dihydrogen peroxide |
Conditions | Yield |
---|---|
With sulfuric acid Diazotization.Kochen der Diazoniumsalz-Loesung nach erneutem Zusatz von H2SO4; |
2-methyl-4-methoxynitrosobenzene
3-methyl-4-nitrophenol
Conditions | Yield |
---|---|
With nitric acid at 40℃; |
Conditions | Yield |
---|---|
With sulfuric acid; nitric acid at 12 - 15℃; zuletzt Behandeln bei 5grad, und Kochen des Reaktionsprodukts mit 10 prozentig. wss. Na2CO3-Loesung; |
3-hydroxy-6-nitro-toluene-4-sulfonic acid
3-methyl-4-nitrophenol
Conditions | Yield |
---|---|
With hydrogenchloride at 170℃; im Rohr; |
nitro acetate
acetic anhydride
3-methyl-phenol
A
2-nitro-5-methylphenol
B
3-methyl-4-nitrophenol
Conditions | Yield |
---|---|
at -5℃; |
nitro acetate
3-methyl-phenol
A
2-nitro-5-methylphenol
B
3-methyl-4-nitrophenol
Conditions | Yield |
---|---|
With acetic anhydride at -5℃; |
Conditions | Yield |
---|---|
With acetic anhydride at -5℃; |
diethyl ether
3-methyl-phenol
isopentyl nitrite
3-methyl-4-nitrophenol
Conditions | Yield |
---|---|
With diethyl ether |
Conditions | Yield |
---|---|
With nitrosylsulfuric acid; acetic acid at 0℃; | |
Multi-step reaction with 2 steps 1: glacial acetic acid; nitrosylsulfuric acid / -15 - -10 °C 2: diluted aqueous HNO3 / 40 °C View Scheme |
Conditions | Yield |
---|---|
With sodium hydroxide; tert-butyl alcohol In water Quantum yield; Irradiation; |
3-methyl-phenol
A
2-nitro-5-methylphenol
B
3-methyl-4-nitrophenol
C
3-methyl-2-nitrophenol
D
2-Methyl-1,4-benzoquinone
Conditions | Yield |
---|---|
With hydrogenchloride; sodium nitrate; sulfuric acid; sodium nitrite In diethyl ether for 0.133333h; Title compound not separated from byproducts; | A 27.9 % Chromat. B 41.0 % Chromat. C 22.5 % Chromat. D 7.3 % Chromat. |
With hydrogenchloride; sodium nitrate; sulfuric acid; sodium nitrite In diethyl ether for 0.133333h; Product distribution; two phase nitration of 3-substituted phenols with or without NaNO2 and urea; | A 27.9 % Chromat. B 41.0 % Chromat. C 22.5 % Chromat. D 7.3 % Chromat. |
With sulfuric acid; nitric acid; sodium nitrite In diethyl ether Mechanism; Product distribution; 2-phase nitration; further 3-alkylphenoles; | |
With hydrogenchloride; sodium nitrate; sulfuric acid; sodium nitrite In diethyl ether for 0.133333h; Title compound not separated from byproducts; | A 27.9 % Chromat. B 41.0 % Chromat. C 22.5 % Chromat. D 7.3 % Chromat. |
(4-nitrophenyl)ethanone
3-Methyl-4-nitro-phenol
A
3-methyl-4-nitrophenol
B
p-nitroacetophenone anion radical
Conditions | Yield |
---|---|
In water; isopropyl alcohol Rate constant; Thermodynamic data; Irradiation; electron transfer reaction ΔE exc.; |
Conditions | Yield |
---|---|
In benzonitrile at 25℃; Equilibrium constant; ionic strength 0.1 M (var.); |
Conditions | Yield |
---|---|
With sulfuric acid; nitric acid |
2,6-difluorophenol
A
3-methyl-4-nitrophenol
Conditions | Yield |
---|---|
With 2,6-dimethylpyridine In water at 25℃; Rate constant; |
Conditions | Yield |
---|---|
With sodium hydroxide; β‐cyclodextrin at 25℃; Kinetics; Further Variations:; Reagents; Hydrolysis; | |
With water; mercury dichloride In methanol at 25℃; pH=5.5; Kinetics; Further Variations:; pH-values; Hydrolysis; | |
With ethanol; sodium methylate; zinc trifluoromethanesulfonate at 25℃; Kinetics; |
Conditions | Yield |
---|---|
at 0 - 20℃; |
chloroform
nitric acid
3-methyl-phenol
A
2-nitro-5-methylphenol
B
3-methyl-4-nitrophenol
Conditions | Yield |
---|---|
at 35℃; |
nitric acid
acetic acid
3-methyl-phenol
A
2-nitro-5-methylphenol
B
3-methyl-4-nitrophenol
3-methyl-phenol
benzene
A
3-methyl-4-nitrophenol
B
3-methyl-2-nitrophenol
water
nitric acid
3-methyl-phenol
A
2-nitro-5-methylphenol
B
3-methyl-4-nitrophenol
C
3-methyl-2-nitrophenol
Conditions | Yield |
---|---|
at 25℃; |
nitric acid
acetic acid
3-methyl-phenol
A
2-nitro-5-methylphenol
B
3-methyl-4-nitrophenol
C
3-methyl-2-nitrophenol
3-methyl-phenol
benzene
A
2-nitro-5-methylphenol
B
3-methyl-4-nitrophenol
C
3-methyl-2-nitrophenol
3-methyl-4-nitrophenol
acetic anhydride
3-methyl-4-nitrophenyl acetate
Conditions | Yield |
---|---|
With magnesium(II) perchlorate at 80℃; for 0.5h; | 100% |
allyl iodid
3-methyl-4-nitrophenol
4-(allyloxy)-2-methyl-1-nitrobenzene
Conditions | Yield |
---|---|
With caesium carbonate In acetone for 24h; Ambient temperature; | 99% |
Conditions | Yield |
---|---|
With caesium carbonate In N,N-dimethyl-formamide at 20℃; for 16h; | 99% |
With potassium carbonate In acetone for 5h; Heating; | 99% |
With potassium carbonate In N,N-dimethyl-formamide at 90℃; for 2h; | 91% |
3-methyl-4-nitrophenol
9-(3-iodopropyl)anthracene
9-[3-(3-methyl-4-nitrophenoxy)propyl]anthracene
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 90℃; for 2h; | 99% |
3-methyl-4-nitrophenol
propyl bromide
2-methyl-4-propoxy-1-nitrobenzene
Conditions | Yield |
---|---|
Stage #1: 3-methyl-4-nitrophenol With potassium carbonate In butanone for 0.0833333h; Inert atmosphere; Reflux; Stage #2: propyl bromide In butanone for 18h; Inert atmosphere; | 99% |
Conditions | Yield |
---|---|
Stage #1: 3-methyl-4-nitrophenol With potassium carbonate In butanone for 0.0833333h; Inert atmosphere; Reflux; Stage #2: 1-bromo-butane In butanone for 18h; Inert atmosphere; | 99% |
3-methyl-4-nitrophenol
2,6-dibromo-3-methyl-4-nitro-phenol
Conditions | Yield |
---|---|
With benzyltrimethylammonium tribromide; calcium carbonate In methanol; dichloromethane | 98% |
With benzyltrimethylammonium tribromide; calcium carbonate In methanol; dichloromethane at 0 - 20℃; for 0.5 - 0.666667h; | 93% |
durch Bromieren; | |
With bromine; acetic acid at 15 - 20℃; |
3-methyl-4-nitrophenol
isopropyl bromide
4-isopropoxy-2-methyl-1-nitrobenzene
Conditions | Yield |
---|---|
Stage #1: 3-methyl-4-nitrophenol With potassium carbonate In butanone for 0.0833333h; Inert atmosphere; Reflux; Stage #2: isopropyl bromide In butanone for 18h; Inert atmosphere; | 98% |
With potassium carbonate In N,N-dimethyl-formamide at 50℃; for 22h; Inert atmosphere; | 96% |
With potassium carbonate In acetone | 58.5% |
With potassium carbonate In acetone for 5h; Heating; |
3-methyl-4-nitrophenol
N,N-Dimethylthiocarbamoyl chloride
O-(3-methyl-4-nitrophenyl)dimethylcarbamothioate
Conditions | Yield |
---|---|
Stage #1: 3-methyl-4-nitrophenol With 1,4-diaza-bicyclo[2.2.2]octane In 1-methyl-pyrrolidin-2-one at 50℃; Stage #2: N,N-Dimethylthiocarbamoyl chloride In 1-methyl-pyrrolidin-2-one at 50℃; for 2.5h; | 98% |
diethyl sulfate
3-methyl-4-nitrophenol
4-ethoxy-2-methyl-1-nitrobenzene
Conditions | Yield |
---|---|
With potassium carbonate In butanone at 70℃; for 2h; Inert atmosphere; | 97% |
With alkaline solution | |
With potassium carbonate In butanone at 110℃; for 2h; Williamson Ether Synthesis; Inert atmosphere; |
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 100℃; for 1h; | 97% |
With potassium carbonate In N,N-dimethyl-formamide at 120℃; for 2h; | 93% |
With ethanol; sodium ethanolate | |
With sodium hydroxide | |
With sodium hydroxide In ethanol; water |
3-methyl-4-nitrophenol
2,6-diiodo-3-methyl-4-nitrophenol
Conditions | Yield |
---|---|
With sodium hydrogencarbonate; N,N,N-trimethylbenzenemethanaminium dichloroiodate In methanol; dichloromethane for 6h; Ambient temperature; | 95% |
3-methyl-4-nitrophenol
allyl bromide
4-(allyloxy)-2-methyl-1-nitrobenzene
Conditions | Yield |
---|---|
With potassium carbonate In acetone for 6h; Heating; | 93% |
With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 12h; Inert atmosphere; |
Conditions | Yield |
---|---|
93% | |
(methylation); |
3-methyl-4-nitrophenol
potassium carbonate
ethyl iodide
4-ethoxy-2-methyl-1-nitrobenzene
Conditions | Yield |
---|---|
In ethyl acetate; butanone | 93% |
4,6-dichloropyrimidine
3-methyl-4-nitrophenol
4-chloro-6-(3-methyl-4-nitrophenoxy)pyrimidine
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 2h; | 93% |
Stage #1: 3-methyl-4-nitrophenol With potassium carbonate In acetonitrile at 20℃; for 0.166667h; Stage #2: 4,6-dichloropyrimidine In acetonitrile Reflux; | 62% |
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 80℃; for 23h; | 92.9% |
3-methyl-4-nitrophenol
N,N-diethylcarbamyl chloride
Diethyl-carbamic acid 3-methyl-4-nitro-phenyl ester
Conditions | Yield |
---|---|
With sodium hydride In N,N-dimethyl-formamide | 92% |
3-methyl-4-nitrophenol
(2s)-(+)-glycidyl 3-nitrobenzenesulfonate
(S)-glycidyl 3-methyl-4-nitrophenyl ether
Conditions | Yield |
---|---|
Stage #1: 3-methyl-4-nitrophenol With cesium fluoride In N,N-dimethyl-formamide at 20℃; for 1h; Stage #2: (2s)-(+)-glycidyl 3-nitrobenzenesulfonate In N,N-dimethyl-formamide at 20℃; for 24h; | 92% |
3-methyl-4-nitrophenol
3,4-Dichlorophenylmethyl chloride
1,2-dichloro-4-[(3-methyl-4-nitrophenoxy)methyl]benzene
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 50 - 100℃; | 91% |
3-methyl-4-nitrophenol
2-fluoroethyl tosylate
4-(2-fluoroethoxy)-2-methyl-1-nitrobenzene
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 80℃; for 3h; | 91% |
3-methyl-4-nitrophenol
2,6-dichloro-3-methyl-4-nitrophenol
Conditions | Yield |
---|---|
With sulfuryl dichloride In acetic acid at 90℃; for 3h; | 90% |
With benzyltrimethylazanium tetrachloro-λ3-iodanuide In acetic acid at 70℃; for 18h; | 70% |
With benzyltrimethylazanium tetrachloro-λ3-iodanuide; acetic acid at 70℃; for 18h; | 64% |
With hydrogenchloride; potassium chlorate | |
With chlorine; acetic acid |
formaldehyd
3-methyl-4-nitrophenol
diethylamine
2,6-bis(diethylaminomethyl)-3-methyl-4-nitrophenol
Conditions | Yield |
---|---|
In ethanol at 90 - 95℃; for 65h; | 90% |
3-methyl-4-nitrophenol
chlorophosphoric acid diphenyl ester
Phosphoric acid 3-methyl-4-nitro-phenyl ester diphenyl ester
Conditions | Yield |
---|---|
With triethylamine In diethyl ether at 25℃; for 4h; | 90% |
3-methyl-4-nitrophenol
4,5-dichloro-2-chloromethyl-pyridazin-3(2H)-one
4-chloro-5-(3-methyl-4-nitrophenoxy)-2-[(3-methyl-4-nitrophenoxy)methyl]pyridazin-3(2H)-ome
Conditions | Yield |
---|---|
With potassium carbonate In methanol for 0.333333h; Reflux; | 90% |
3-methyl-4-nitrophenol
Conditions | Yield |
---|---|
With caesium carbonate In N,N-dimethyl-formamide at 40℃; for 0.5h; Schlenk technique; Inert atmosphere; | 90% |
3-methyl-4-nitrophenol
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 100℃; for 3h; | 90% |
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 90℃; for 14h; Inert atmosphere; | 89% |
3-methyl-4-nitrophenol
t-butyl 4-hydroxy piperidine-1-carboxylate
1-tert-butyloxycarbonyl-4-(4-nitro-3-methylphenyloxy)piperidine
Conditions | Yield |
---|---|
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran at 0℃; for 1h; | 88% |
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