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Conditions | Yield |
---|---|
In water reduction with Mg in neutral or acidic soln.; | 100% |
In water reduction with Mg in neutral or acidic soln.; | 100% |
In water reaction in neutral and acid solutions complete;; |
Conditions | Yield |
---|---|
In water room temp.; X-ray diffraction, gravimetric anal.; | 99% |
platinum 1,3-divinyl-1,1,3,3-tetramethyldisiloxane
platinum
Conditions | Yield |
---|---|
With 1-decene; 1,1,3,3-tetramethyldisiloxane In toluene mixt. of tetramethyldisiloxane, 1-decene in unhyd. toluene stirred at room temp., evacuated, refilled with N2 three times, Pt-complex added, stirred at 100°C for 5 d; centrifuged, decanted, washed by toluene, centrifuged twice, dried indervac.; detd. by XRD, TEM; | 96% |
platinum
Conditions | Yield |
---|---|
With hydrogen In water Reagent/catalyst; Temperature; | 96% |
Irradiation (UV/VIS); photodeposition on NaInS2; | |
With aluminium In water 65 % surfactant contg. Pt-compd. soln., heating to 85 °C, coolingto room temp., heating to 80 °C, thermal aging was repeated 3 ti mes, Pt was deposited onto an Au/Ti/Si substrate with plating with Al; Pt film was washed with EtOH; |
platinum
Conditions | Yield |
---|---|
In ethanol; water Kinetics; Irradiation (UV/VIS); photoreduction of K2(Pt(NO2)4) in a suspension of anatase in H2O with 4 vol.-% C2H5OH at various temp. (pH: 3.6);; deposition of Pt on the TiO2 surface;; | 90% |
With hydrogenchloride; zinc In water byproducts: KCl, ZnCl2; aq. K2(Pt(NO2)4) soln., at elevated temp. or in coldness;; | |
With HCl; Zn In water byproducts: KCl, ZnCl2; aq. K2(Pt(NO2)4) soln., at elevated temp. or in coldness;; |
Conditions | Yield |
---|---|
In acetonitrile byproducts: H2O; suspn. of Pt complex and ligand (molar ratio 1:2) in MeCN stirred at room temp. for a few min; stored at room temp. overnight; filtered; Et2O added to filtrate; filtered; solid washed with Et2O; dried under vac.; dissolved in MeCN; crystd. by slow condensation of Et2O vapors; elem. anal.; | A 81% B 1% |
bis(η3-allyl)(tetracyanoethylene)platinum
A
CH2CHCH2C(CN)2C(CN)2CH2CHCH2
B
platinum
Conditions | Yield |
---|---|
With triphenylphosphine In dichloromethane a soln. PPh3 in CH2Cl2 was added dropwise with stirring to a CH2Cl2 soln. of Pt-complex under N2, mixt. was stirred for 2 h at room temp.; Pt metal was removed by filtration through Florisil, filtrate concd. and subjected to HLPC; | A 73% B n/a |
With triphenylphosphine In dichloromethane-d2 a soln. PPh3 in CH2Cl2 was added dropwise with stirring to a CH2Cl2 soln. of Pt-complex under N2; followed by (1)H and (31)P NMR; |
Conditions | Yield |
---|---|
With cinchonine In water byproducts: HCl; heating (140+/-5°C); filtn. (G4 filter), washing (aq. NaHCO3; H2O), freeze drying; | A n/a B 71% |
B
platinum
Conditions | Yield |
---|---|
With sodium acetate trihydrate In dimethyl sulfoxide byproducts: NaBr, acetic acid; PtBr2, Na salt and ligand (molar ratio 1:2:1) dissolved in DMSO; heated to 80°C for 2 h and then to 100°C for 1 h; cooled to room temp.; filtered; solvent evapd. from filtrate; washed with CH2Cl2; extd. with small amt. of H2O; residue washed with THF; dried under high vac.; elem. anal.; | A 64.2% B n/a |
B
(E)-2,3-dimethoxybut-2-ene
C
(Z)-2,3-dimethoxybut-2-ene
D
platinum
Conditions | Yield |
---|---|
With cobaltocene In dichloromethane-d2 | A n/a B n/a C 64% D n/a |
Ru3Pt(μ-H)(μ4-η2-CC(t-Bu))(CO)9(cycloocta-1,5-diene)
A
Ru3(μ-H)(μ3-η2-CC(t-Bu))(CO)9
B
Pt{Ru3(μ-H)(μ4-η2-CC(t-Bu))(CO)9}2
C
platinum
Conditions | Yield |
---|---|
In toluene N2-atmosphere; ambient temp., 5 days (crystn.); washing (petroleum ether); elem. anal.; | A n/a B 50% C n/a |
In dichloromethane N2-atmosphere; ambient temp., 5 days (crystn.); washing (petroleum ether); elem. anal.; | A n/a B 50% C n/a |
A
dichlorobis(triethylphosphine)platinum
B
methane
C
ethane
D
ethene
E
platinum
Conditions | Yield |
---|---|
In decalin Kinetics; Pt complex was heated in decalin under Ar at 170 and 200°C; rateconst for decompn. at 200°C is given; Pt was filtered off, light petroleum was added to the concd. soln., crystals were collected, gas. products were detd. by GLS; | A 48% B n/a C 2% D <1 E 43% |
trans-{PtCH3(CN)(PEt3)2}
B
methane
C
ethane
D
ethene
E
platinum
Conditions | Yield |
---|---|
In decalin Kinetics; Pt complex was heated in decalin under Ar at 170 and 200°C; rateconst for decompn. at 200°C is given; Pt was filtered off, light petroleum was added to the concd. soln., crystals were collected, gas. products were detd. by GLS; | A 48% B n/a C 2% D <1 E 43% |
A
methane
B
ethane
C
ethene
D
Pt(PEt3)2I2
E
platinum
Conditions | Yield |
---|---|
In decalin Kinetics; Pt complex was heated in decalin under Ar at 170 and 200°C; rateconst for decompn. at 200°C is given; Pt was filtered off, light petroleum was added to the concd. soln., crystals were collected, gas. products were detd. by GLS; | A n/a B 2% C <1 D 48% E 43% |
Conditions | Yield |
---|---|
In water reduction with Mg in neutral or acidic soln.; | 100% |
In water reduction with Mg in neutral or acidic soln.; | 100% |
In water reaction in neutral and acid solutions complete;; |
Conditions | Yield |
---|---|
In water room temp.; X-ray diffraction, gravimetric anal.; | 99% |
platinum 1,3-divinyl-1,1,3,3-tetramethyldisiloxane
platinum
Conditions | Yield |
---|---|
With 1-decene; 1,1,3,3-tetramethyldisiloxane In toluene mixt. of tetramethyldisiloxane, 1-decene in unhyd. toluene stirred at room temp., evacuated, refilled with N2 three times, Pt-complex added, stirred at 100°C for 5 d; centrifuged, decanted, washed by toluene, centrifuged twice, dried indervac.; detd. by XRD, TEM; | 96% |
platinum
Conditions | Yield |
---|---|
With hydrogen In water Reagent/catalyst; Temperature; | 96% |
Irradiation (UV/VIS); photodeposition on NaInS2; | |
With aluminium In water 65 % surfactant contg. Pt-compd. soln., heating to 85 °C, coolingto room temp., heating to 80 °C, thermal aging was repeated 3 ti mes, Pt was deposited onto an Au/Ti/Si substrate with plating with Al; Pt film was washed with EtOH; |
platinum
Conditions | Yield |
---|---|
In ethanol; water Kinetics; Irradiation (UV/VIS); photoreduction of K2(Pt(NO2)4) in a suspension of anatase in H2O with 4 vol.-% C2H5OH at various temp. (pH: 3.6);; deposition of Pt on the TiO2 surface;; | 90% |
With hydrogenchloride; zinc In water byproducts: KCl, ZnCl2; aq. K2(Pt(NO2)4) soln., at elevated temp. or in coldness;; | |
With HCl; Zn In water byproducts: KCl, ZnCl2; aq. K2(Pt(NO2)4) soln., at elevated temp. or in coldness;; |
Conditions | Yield |
---|---|
In acetonitrile byproducts: H2O; suspn. of Pt complex and ligand (molar ratio 1:2) in MeCN stirred at room temp. for a few min; stored at room temp. overnight; filtered; Et2O added to filtrate; filtered; solid washed with Et2O; dried under vac.; dissolved in MeCN; crystd. by slow condensation of Et2O vapors; elem. anal.; | A 81% B 1% |
bis(η3-allyl)(tetracyanoethylene)platinum
A
CH2CHCH2C(CN)2C(CN)2CH2CHCH2
B
platinum
Conditions | Yield |
---|---|
With triphenylphosphine In dichloromethane a soln. PPh3 in CH2Cl2 was added dropwise with stirring to a CH2Cl2 soln. of Pt-complex under N2, mixt. was stirred for 2 h at room temp.; Pt metal was removed by filtration through Florisil, filtrate concd. and subjected to HLPC; | A 73% B n/a |
With triphenylphosphine In dichloromethane-d2 a soln. PPh3 in CH2Cl2 was added dropwise with stirring to a CH2Cl2 soln. of Pt-complex under N2; followed by (1)H and (31)P NMR; |
Conditions | Yield |
---|---|
With cinchonine In water byproducts: HCl; heating (140+/-5°C); filtn. (G4 filter), washing (aq. NaHCO3; H2O), freeze drying; | A n/a B 71% |
B
platinum
Conditions | Yield |
---|---|
With sodium acetate trihydrate In dimethyl sulfoxide byproducts: NaBr, acetic acid; PtBr2, Na salt and ligand (molar ratio 1:2:1) dissolved in DMSO; heated to 80°C for 2 h and then to 100°C for 1 h; cooled to room temp.; filtered; solvent evapd. from filtrate; washed with CH2Cl2; extd. with small amt. of H2O; residue washed with THF; dried under high vac.; elem. anal.; | A 64.2% B n/a |
B
(E)-2,3-dimethoxybut-2-ene
C
(Z)-2,3-dimethoxybut-2-ene
D
platinum
Conditions | Yield |
---|---|
With cobaltocene In dichloromethane-d2 | A n/a B n/a C 64% D n/a |
Ru3Pt(μ-H)(μ4-η2-CC(t-Bu))(CO)9(cycloocta-1,5-diene)
A
Ru3(μ-H)(μ3-η2-CC(t-Bu))(CO)9
B
Pt{Ru3(μ-H)(μ4-η2-CC(t-Bu))(CO)9}2
C
platinum
Conditions | Yield |
---|---|
In toluene N2-atmosphere; ambient temp., 5 days (crystn.); washing (petroleum ether); elem. anal.; | A n/a B 50% C n/a |
In dichloromethane N2-atmosphere; ambient temp., 5 days (crystn.); washing (petroleum ether); elem. anal.; | A n/a B 50% C n/a |
A
dichlorobis(triethylphosphine)platinum
B
methane
C
ethane
D
ethene
E
platinum
Conditions | Yield |
---|---|
In decalin Kinetics; Pt complex was heated in decalin under Ar at 170 and 200°C; rateconst for decompn. at 200°C is given; Pt was filtered off, light petroleum was added to the concd. soln., crystals were collected, gas. products were detd. by GLS; | A 48% B n/a C 2% D <1 E 43% |
trans-{PtCH3(CN)(PEt3)2}
B
methane
C
ethane
D
ethene
E
platinum
Conditions | Yield |
---|---|
In decalin Kinetics; Pt complex was heated in decalin under Ar at 170 and 200°C; rateconst for decompn. at 200°C is given; Pt was filtered off, light petroleum was added to the concd. soln., crystals were collected, gas. products were detd. by GLS; | A 48% B n/a C 2% D <1 E 43% |
A
methane
B
ethane
C
ethene
D
Pt(PEt3)2I2
E
platinum
Conditions | Yield |
---|---|
In decalin Kinetics; Pt complex was heated in decalin under Ar at 170 and 200°C; rateconst for decompn. at 200°C is given; Pt was filtered off, light petroleum was added to the concd. soln., crystals were collected, gas. products were detd. by GLS; | A n/a B 2% C <1 D 48% E 43% |
trans-(triethylphosphine)2PtMeBr
A
methane
B
ethane
C
ethene
D
[PtBr2(P(CH2CH3)3)2]
E
platinum
Conditions | Yield |
---|---|
In decalin Kinetics; Pt complex was heated in decalin under Ar at 170 and 200°C; rateconst for decompn. at 200°C is given; Pt was filtered off, light petroleum was added to the concd. soln., crystals were collected, gas. products were detd. by GLS; | A n/a B 2% C <1 D 48% E 43% |
platinum
Conditions | Yield |
---|---|
With 1-butanol; oleylamine; acetic acid In toluene High Pressure; mixt. of 10 mM Pt(acac)2 (2 ml), 80 mM CH3COOH (0.5 ml) and 0.1 M oleylamine (1 ml) in toluene, 1-butanol (1 ml) and DMF (2.5 ml) heated in autoclave (185°C, 16 h); cooled naturally to room temp.; centrifuged; ppt. washed with EtOH; | 45% |
With 1-butanol; oleylamine; acetic acid In N,N-dimethyl-formamide; toluene High Pressure; mixt. of 10 mM Pt(acac)2 (2 ml), 80 mM CH3COOH (0.5 ml) and 0.1 M oleylamine (1 ml) in toluene, 1-butanol (1 ml) and DMF (2.5 ml) heated in autoclave (185°C, 16 h); cooled naturally to room temp.; centrifuged; ppt. washed with EtOH; | 45% |
With 1-butanol; oleylamine; acetic acid In N,N-dimethyl-formamide; toluene High Pressure; mixt. of 10 mM Pt(acac)2 (2 ml), 80 mM CH3COOH (0.5 ml) and 0.1 M oleylamine (1 ml) in toluene, 1-butanol (1 ml) and DMF (2.5 ml) heated in autoclave (145°C); cooled naturally to room temp.; centrifuged; ppt. washed with EtOH; |
iodine
trans-diiodobis(triphenylphosphane)platinum(II)
B
platinum
C
dinitrogen monoxide
Conditions | Yield |
---|---|
With Et3N In dichloromethane byproducts: PPh3O; Pt-compd. and Et3N were dissolved in CH2Cl2, cooling to -78 °C, 2equiv. of I2 was added, warming to room temp. over 1 h; ppt. was filtered off; | A 45% B n/a C n/a |
trans-chlorohydridobis(triethylphosphine)platinum(II)
tetrabutylammonium perchlorate
A
1-butylene
trans-{PtH(CH2CN)(PEt3)2}
C
tributyl-amine
D
platinum
Conditions | Yield |
---|---|
In acetonitrile; benzene byproducts: H2; Electrolysis; electrochemically reducing trans-(PtH(Cl)(PEt3)2) at -2.1 V vs Ag/AgCl in CH3CN/C6H6 (5/2, v/v), terminating electrolysis at constancy of current; 36% of hydrido complex recovered; 31P NMR; | A n/a B 38% C n/a D n/a |
Conditions | Yield |
---|---|
With hydrogen In acetic acid under 760.051 Torr; for 1.5h; | |
With hydrogenchloride; hydrogen In hydrogenchloride bubbling of H2 through suspn. of PtO2 in aq. HCl for 20 min; | |
With hydrogen In water react. of PtO2 with H2 (50 psi) in water at room temp. for 30 min; |
platinum
Conditions | Yield |
---|---|
With poly(1-vinyl-2-pyrrolidone) In ethanol; water at 100℃; for 14.5h; Heating / reflux; | |
With J-0381V; L-10D; ethanol; sodium hydrogencarbonate In water at 70℃; | |
With ethanol; sodium hydrogencarbonate; polysorbate 80 In water at 70℃; |
platinum
Conditions | Yield |
---|---|
In 1-ethenyl-2-pyrrolidinone; ethanol; water at 100℃; for 2.66667h; Product distribution / selectivity; Heating / reflux; | |
In poly(sodium acrylate); ethanol; water at 100℃; for 2.66667h; Product distribution / selectivity; Heating / reflux; |
Conditions | Yield |
---|---|
With sodium carbonate In not given heating; | |
With Na2CO3 In not given heating; |
cisplatine
platinum
Conditions | Yield |
---|---|
In ammonia Electrochem. Process; solution of {Pt(NH3)2Cl2} in aq. NH3, 90°C;; | |
With NaB(C2H5)3H In tetrahydrofuran byproducts: NaCl, B(C2H5)3, H2; 23°C, 2 h; Washing with H2O to separate alkali halogenide from metal powder.; | |
In ammonia Electrochem. Process; no pptn. of Pt out of a satd. soln. of {Pt(NH3)2(CNS)2} in aq. NH3, evolution of H2 at the cathode;; | 0% |
In ammonia Electrochem. Process; solution of {Pt(NH3)2Cl2} in aq. NH3, 90°C;; |
Conditions | Yield |
---|---|
In neat (no solvent) under He; mixt. of Co-Pt complex and NH4Cl (1:10 wt/wt) heated to 500°C; detd. by X-ray powder diffraction; |
platinum tetrabromide
platinum
Conditions | Yield |
---|---|
In water Electrochem. Process; pptn. from a concd. aq. soln. of PtBr4 (bunsen cell);; | |
With alc. In not given heating; | |
With diethyl ether In not given heating; |
bismuth
sulfuric acid
pyrographite
2-butyl-5-hydroxymethyl-1H-imidazole
platinum
2-butyl-1H-imidazole-5-carboxaldehyde
Conditions | Yield |
---|---|
With sodium hydroxide In water | 100% |
With sodium hydroxide In water | 98.2% |
With sodium hydroxide In methanol; water | 94.5% |
Conditions | Yield |
---|---|
With hydrogen | 100% |
bis(diethoxyphosphoryl)disulphide
platinum
bis(O,O'-diethyldithiophosphato-S,S')platinum(II)
Conditions | Yield |
---|---|
In styrene at 20℃; for 0.333333h; Product distribution / selectivity; | 100% |
Conditions | Yield |
---|---|
In neat (no solvent) at 600 - 950℃; for 111h; Sealed tube; Schlenk technique; Inert atmosphere; Glovebox; | 100% |
Conditions | Yield |
---|---|
Stage #1: platinum With hydrogenchloride; dihydrogen peroxide In water Stage #2: hydrogenchloride In water Stage #3: CYANAMID With hydrogenchloride In water | 100% |
acetic acid-(5-chloro-2-hydroxy-3-nitro-anilide)
platinum
Conditions | Yield |
---|---|
With carbon disulfide; potassium hydroxide In ethanol; ethyl acetate | 99% |
rac.-N-[1-(5-chloro-1H-benzoimidazol-2-yl)-ethyl]-3-ethynyl-4-(pyrrolidine-1-carbonyl)-benzamide
platinum
Conditions | Yield |
---|---|
With hydrogen In 1,4-dioxane; water | 99% |
2,4-diamino-5-nitroso-6-hydroxypyrimidine
platinum
2-amino-1,9-dihydro-6H-purin-6-one
Conditions | Yield |
---|---|
98.9% |
Conditions | Yield |
---|---|
With trichlorosilane; [SG]-S-Pt In hexane | 98% |
Conditions | Yield |
---|---|
96.5% |
ethyl 2-methyl-4,4,4-trifluoroacetoacetate
platinum
ethyl 3-hydroxy-2-methyl-4,4,4-trifluorobutanoate
Conditions | Yield |
---|---|
With nitrogen; hydrogen; triethylamine; Pt/C | 96% |
platinum
Conditions | Yield |
---|---|
With nitrogen; hydrogen; triethylamine; Pt/C | 96% |
ethyl 4,4,4-trifluoroacetoacetate
platinum
ethyl 3-hydroxy-4,4,4-trifluorobutyrate
Conditions | Yield |
---|---|
With nitrogen; hydrogen; triethylamine; Pt/C | 96% |
With nitrogen; hydrogen; triethylamine; Pt/C | 96% |
With nitrogen; hydrogen; triethylamine; Pt/C | 96% |
With nitrogen; hydrogen; triethylamine | 96% |
With methanesulfonic acid; nitrogen; hydrogen; Pt/C | 50% |
2-(2-carbamoyloxyethyl)-5-(3,5-dichlorophenylthio)-4-isopropyl-1-(p-nitrobenzyl)-1H-imidazole
platinum
1-(4-Aminobenzyl)-5-(3,5-dichlorophenylthio)-2-(2-carbamoyloxyethyl)-4-isopropyl-1H-imidazole
Conditions | Yield |
---|---|
In ethyl acetate | 95% |
Conditions | Yield |
---|---|
In water; toluene | 95% |
hydrogenchloride
platinum
1,5-dicyclooctadiene
dichloro(1,5-cyclooctadiene)platinum(ll)
Conditions | Yield |
---|---|
With HNO3; SnCl2*2H2O In further solvent(s) byproducts: nitrogen oxides; N2-atmosphere; dissoln. of Pt in aqua regia by stirring overnight at 60°C, concn., addn. of concd. HCl, evapn., dissoln. in H2O/PrOH=4:3,addn. of excess COD and slight excess SnCl2, stirring (12°C, 7 d , pptn.); filtration, washing (H2O), drying (SiO2); elem. anal.; | 95% |
Conditions | Yield |
---|---|
In neat (no solvent) loading and unloading carried out in inert gas; RbH and Pt with a molar ratio of 2.1:1 mixed and filled in molybdenum boat; transferred into a low pressure autoclave; evacuated; filled with H2 up to 1 bar; heated at 620 K for 6 h; unloaded in the glove box; | 95% |
Conditions | Yield |
---|---|
In neat (no solvent) loading and unloading carried out in inert gas; RbH and Pt with a molar ratio of 3.1:1 mixed and filled in molybdenum boat; transferred into a low pressure autoclave; evacuated; filled with H2 up to 1 bar; heated at 620 K for 6 h; unloaded in the glove box; | 95% |
Conditions | Yield |
---|---|
With hydrogen In methanol | 93.7% |
sulfuryl dichloride
carbon monoxide
platinum
cis-dicarbonyldichloroplatinum(II)
Conditions | Yield |
---|---|
In thionyl chloride addn. of platinum black to soln. of SO2Cl2 in SOCl2 under CO; after 150h soln. evapd. and residue dissolved in toluene; detn. by IR; | 92% |
With platinum In thionyl chloride soln. of SO2Cl2 in SOCl2 under CO (1 atm) and platinum black sealed in tube; suspn. stirred 30 h at temp. 60°C; not isolated; detn. by IR; |
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