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inquiryItems Standard Result Appearance White crystalline powder Complies ZrO2+HfO2 36%min
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inquiryAppearance:White filamentous or needle-like crystals Storage:Room temperature Package:25kg/drum Application:Intermediates of other zirconium products, also used as rubber additives, paint driers Transportation:Express/Sea/Air Port:Any port in china
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inquiryPacking: According to customer requirements Delivery time: In stock or depands Port of shipment: Ningbo/Shanghai/Qingdao OEM/ODM:Welcome Sample:We can offer our existing samples at once Appearance:white powder/ Refer to COA Storage:Refer to COA
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inquiryZirconyl chloride octahydrate CAS:13520-92-8 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality org
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inquiryZirconium oxychloride properties Melting point 400 ° C (dec.) The density is 1.91 Store at + 15 ° C to + 25 ° C. Solubility H2O: soluble
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inquiryroduct Name: Zirconyl chloride octahydrate CAS: 13520-92-8 MF: Cl2H16O9Zr MW: 322.25 EINECS: 603-909-6 Product Categories: Mol File: 13520-92-8.mol Zirconyl chloride octahydrate Structure Zirconyl chloride octahydrate Chemical
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inquiryroName: High purity Zirconium(IV) oxide chlori... CasNo: 13520-92-8 Molecular Formula: H16Cl2O9Zr Appearance: White crystalline powder Application: intermediate for organic synthesis DeliveryTime: Prompt PackAge: 25kg net/paper drum Port: Sh
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inquiryConditions | Yield |
---|---|
In hydrogenchloride byproducts: CO2; Zr(CO3)2 dissolved in concd. HCl, refluxed for 1 h; cooled, filtered, washed with cold concd. HCl, recrystd. from aq. HCl, air dried; |
ziconium(IV) oxychloride octahydrate
dimethyl methane phosphonate
Conditions | Yield |
---|---|
With aq. HCl In water reflux (24 h or 112 h); aq. HBr or H2O alone may also be used; filtration, washing (H2O; acetone), drying (40°C, 18 h, then 200°C, 24 h); elem. anal.; | 99% |
Conditions | Yield |
---|---|
In water | 95% |
Conditions | Yield |
---|---|
In water | 95% |
Conditions | Yield |
---|---|
In water | 95% |
Conditions | Yield |
---|---|
In water | 95% |
Conditions | Yield |
---|---|
In water | 95% |
ziconium(IV) oxychloride octahydrate
sodium tungstate (VI) dihydrate
Conditions | Yield |
---|---|
With hydrogenchloride In water at 160℃; Autoclave; | 95% |
ziconium(IV) oxychloride octahydrate
Acetylenedicarboxylic acid
Conditions | Yield |
---|---|
Stage #1: ziconium(IV) oxychloride octahydrate; Acetylenedicarboxylic acid With acetic acid In N,N-dimethyl-formamide Sonication; Stage #2: In N,N-dimethyl-formamide at 85℃; for 6h; Sealed tube; | 94% |
ziconium(IV) oxychloride octahydrate
Acetylenedicarboxylic acid
Conditions | Yield |
---|---|
Stage #1: ziconium(IV) oxychloride octahydrate; Acetylenedicarboxylic acid With acetic acid In water; N,N-dimethyl-formamide for 0.0333333h; Sonication; Stage #2: at 85℃; for 6h; Sealed tube; | 94% |
ziconium(IV) oxychloride octahydrate
ammonium fluoride
Conditions | Yield |
---|---|
Stage #1: ziconium(IV) oxychloride octahydrate; potassium oleate With Elaidic Acid; oleylamine at 20℃; for 2h; Stage #2: ammonium fluoride; potassium fluoride In water at 50 - 200℃; for 12.5h; Reagent/catalyst; Autoclave; | A 89.4% B n/a |
ziconium(IV) oxychloride octahydrate
ammonium fluoride
Conditions | Yield |
---|---|
Stage #1: ziconium(IV) oxychloride octahydrate; potassium oleate With Elaidic Acid; oleylamine at 20℃; for 2h; Stage #2: ammonium fluoride; potassium fluoride In water at 50 - 200℃; for 12.5h; Autoclave; | 89.4% |
ziconium(IV) oxychloride octahydrate
(2E)-but-2-enedioic acid
Conditions | Yield |
---|---|
With acetic acid In water at 85℃; Microwave irradiation; Flow reactor; Green chemistry; | 88% |
ziconium(IV) oxychloride octahydrate
water
Conditions | Yield |
---|---|
With hydrogen fluoride In methanol at 80℃; for 48h; | 86% |
ziconium(IV) oxychloride octahydrate
piperidinomethylphosphonic acid
hydrogen fluoride
Conditions | Yield |
---|---|
In propan-1-ol; water a soln. piperidine-compound in n-propanol-water was added to a soln. of Zr-compound and HF, maintained in closed plastic vessel at 80°C for 3 days; ppt. was centrifuged, washed with propanol-water, dried in an oven at 70°C; elem. anal.; | 85% |
ziconium(IV) oxychloride octahydrate
formic acid
benzene-1,3,5-tricarboxylic acid
N,N-dimethyl-formamide
Conditions | Yield |
---|---|
at 130℃; for 0.48h; | 85% |
ziconium(IV) oxychloride octahydrate
1,10-Phenanthroline
salicylaldehyde anthranilic acid
Conditions | Yield |
---|---|
In ethanol for 12h; Reflux; | 84% |
ziconium(IV) oxychloride octahydrate
ammonium fluoride
sodium oleate
Conditions | Yield |
---|---|
Stage #1: ziconium(IV) oxychloride octahydrate; sodium oleate With Elaidic Acid; oleylamine at 20℃; for 6h; Stage #2: ammonium fluoride; sodium fluoride In water at 25℃; for 12.5h; | 83.1% |
ziconium(IV) oxychloride octahydrate
water
Conditions | Yield |
---|---|
at 80℃; for 3h; | 82% |
ziconium(IV) oxychloride octahydrate
benzene-1,3,5-tricarboxylic acid
Conditions | Yield |
---|---|
With acetic acid In water at 95℃; for 5h; Microwave irradiation; Green chemistry; Large scale; | 81% |
ziconium(IV) oxychloride octahydrate
carbamazepin
Conditions | Yield |
---|---|
In ethanol for 3h; Reflux; | 79.8% |
Conditions | Yield |
---|---|
In methanol methanolic soln. of ZrOCl2*8H2O was added to moxifloxacin in methanol, stirred at room temp. for 22 h; slow evapn., ppt. was filtered off, washed with bidistilled water several times, dried over CaCl2 in desecrator, ppt. was filtered off, dried invac. over CaCl2; elem. anal.; | 78.34% |
ziconium(IV) oxychloride octahydrate
Conditions | Yield |
---|---|
In ethanol at 70℃; for 3h; | 74% |
ziconium(IV) oxychloride octahydrate
(3E)-2-(hydroxyimino)-N-p-tolyl-3-(p-tolylimino)butanamide
Conditions | Yield |
---|---|
In ethanol; N,N-dimethyl acetamide Reflux; | 73% |
ziconium(IV) oxychloride octahydrate
water
Conditions | Yield |
---|---|
With sodium hydroxide for 72h; pH=3.5; Reflux; | 72% |
With sodium hydroxide for 72h; pH=3.5; Reflux; | 72% |
ziconium(IV) oxychloride octahydrate
formic acid
N,N-dimethyl-formamide
Conditions | Yield |
---|---|
at 120℃; for 48h; Autoclave; | 72% |
ziconium(IV) oxychloride octahydrate
N-phosphonoethyl-4-carboxypyridinium chloride
hydrogen fluoride
C8H9F3NO5PZr
Conditions | Yield |
---|---|
at 80℃; for 72h; | 71% |
ziconium(IV) oxychloride octahydrate
Thiophene-2,5-dicarboxylic acid
Conditions | Yield |
---|---|
With acetic acid In water at 95℃; for 1h; Microwave irradiation; Green chemistry; Large scale; | 70% |
ziconium(IV) oxychloride octahydrate
formic acid
benzene-1,3,5-tricarboxylic acid
water
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 100℃; for 48h; Inert atmosphere; Schlenk technique; | 70% |
ziconium(IV) oxychloride octahydrate
diethyl amine hydrochloride
Conditions | Yield |
---|---|
With Na2CO3; HCl In water to a soln. of polyoxotungstate in water was added Na2CO3, stirred for 20min., ZrCl2O*8H2O was added, stirred for 5 min, 1 M aq. HCl was added f or 1 min, stirred for 15 min, a soln. of Hf-compound in aq. HCl was added, stirred for 30 min; passed through a folded filter paper, evapd. at 40°C, stirred for1 min in a water bath at more than 90°C, (C2H5)2NH2Cl was added, stirred for 5 min, cooled to roomtemp., filtered, washed with C2H5OH, d ried in vac. for 2 h; elem. anal.; | 69.7% |
ziconium(IV) oxychloride octahydrate
N-(phosphonemethyl)glycine
hydrogen fluoride
Conditions | Yield |
---|---|
at 80℃; for 48h; pH=2.17; | 68% |
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