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inquiryAluminum acetate CAS:139-12-8 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermedia
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Tetradecyl dimethyl benzyl ammonium chlorideAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air
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inquiryConditions | Yield |
---|---|
With aluminium trichloride Abdestillieren des gebildeten Acetylchlorids und Erhitzen des Rueckstands auf 160-180grad; |
Conditions | Yield |
---|---|
With aluminium trichloride |
Conditions | Yield |
---|---|
at 90℃; |
Conditions | Yield |
---|---|
In neat (no solvent) symmetrization on heating;; |
Conditions | Yield |
---|---|
In water purification from Pb ions with H2S, from SO4 ions with barium acetate; | |
In water purification from Pb ions with H2S, from SO4 ions with barium acetate; |
Conditions | Yield |
---|---|
With diethylsulfide In benzene byproducts: (C2H5)2SO2; addn. of t-BuOOH to soln. of (t-BuO)3Al and Et2S in benzene for 1-2 min at 20°C; condencing of solvent and volatile components with liq. N2; addn. of H2SO4 to residue, treatment with acetic acid; filtration, removal of volatiles under reduced pressure; | |
With diisopropylsulfide In benzene byproducts: (isopropyl)2SO2; addn. of t-BuOOH to soln. of (t-BuO)3Al and i-Pr2S in benzene for 1-2 min at 20°C; condencing of solvent and volatile components with liq. N2; addn. of H2SO4 to residue, treatment with acetic acid; filtration, removal of volatiles under reduced pressure; | |
With dimethylsulfide In benzene byproducts: (CH3)2SO2; addn. of t-BuOOH to soln. of (t-BuO)3Al and Me2S in benzene for 1-2 min at 20°C; condencing of solvent and volatile components with liq. N2; addn. of H2SO4 to residue, treatment with acetic acid; filtration, removal of volatiles under reduced pressure; |
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide In benzene byproducts: (isopropyl)2SO2, (CH3)3COH; (Ar); addn. of (CH3)3COOH (2 equiv.) to soln. of ((CH3)3CO)3Al (1 equiv.) and (isopropyl)2S (1 equiv.) in benzene at 20°C; self-heating; treatment with AcOH; filtration; removal of volatiles under reduced pressure; | |
With tert.-butylhydroperoxide; diethyl sulphide In benzene byproducts: (C2H5)2SO2, (CH3)3COH; (Ar); addn. of (CH3)3COOH (2 equiv.) to soln. of ((CH3)3CO)3Al (1 equiv.) and (C2H5)2S (1 equiv.) in benzene at 20°C; self-heating; treatment with AcOH; filtration; removal of volatiles under reduced pressure; | |
With tert.-butylhydroperoxide; dimethylsulfide In benzene byproducts: (CH3)2SO2, (CH3)3COH; (Ar); addn. of (CH3)3COOH (2 equiv.) to soln. of ((CH3)3CO)3Al (1 equiv.) and (CH3)2S (1 equiv.) in benzene at 20°C; self-heating; treatment with AcOH; filtration; removal of volatiles under reduced pressure; |
Conditions | Yield |
---|---|
In water Electrochem. Process; electrolytical dissolution of Al in acetic acid; calcium acetate addition for increase of electric conductivity; | |
dissolving Al in water free acetic acid; | |
In water influence of concentration and temperature were examined; |
aluminium trichloride
acetic acid
A
hydrogenchloride
B
aluminum acetate
Conditions | Yield |
---|---|
water free AlCl3, water free acetic acid; driving away HCl; inpurity less then 1 % Cl; |
Conditions | Yield |
---|---|
With barium carbonate In water | |
With calcium carbonate In water | |
With BaCO3 In water | |
With CaCO3 In water |
Conditions | Yield |
---|---|
In water | |
In water | |
With acetic anhydride In acetic acid Al(OH)3 in 1:1-mixt. of glacial acetic acid and acetic anhydride refluxed for 24 h; suspn. filtered, solid washed with acetone; |
Conditions | Yield |
---|---|
With hydroxide In acetic acid Al(OH)3 pptd. from soln. of aluminum ammonium sulfate; Al(OH)3 filtered out; quickly dissolved in glacial CH3COOH; |
Conditions | Yield |
---|---|
In water equiv. amount of educts; | |
In water equiv. amount of educts; |
Conditions | Yield |
---|---|
In water | |
In water |
aluminium trichloride
acetic anhydride
A
aluminum acetate
B
acetyl chloride
Conditions | Yield |
---|---|
distn. the formed acetyl chloride and heating the residue at 160-180 °C; | |
distn. the formed acetyl chloride and heating the residue at 160-180 °C; |
Conditions | Yield |
---|---|
In water purification from Pb ions with H2S, from SO4 ions with barium acetate; | |
In water purification from Pb ions with H2S, from SO4 ions with barium acetate; |
Conditions | Yield |
---|---|
In water | |
In water |
aluminum ethoxide
acetic anhydride
A
aluminum acetate
B
ethyl acetate
Conditions | Yield |
---|---|
heating at 90 °C and distn. the formed ethyl acetate; | |
heating at 90 °C and distn. the formed ethyl acetate; |
Conditions | Yield |
---|---|
heating in sealed tube; | |
heating in sealed tube; |
Conditions | Yield |
---|---|
In neat (no solvent) symmetrization on heating;; |
Allyl acetate
phenylaluminium dichloride
A
allylbenzene
B
biphenyl
C
aluminum acetate
Conditions | Yield |
---|---|
tetrakis(triphenylphosphine) palladium(0) In diethyl ether Ar atmosphere; stirring (20°C, 5 mole-% catalyst, 20 h); | A 0% B <1 C n/a |
Conditions | Yield |
---|---|
Stage #1: acetic anhydride With acetic acid at 110℃; for 0.5h; Stage #2: aluminum (III) chloride at 20℃; |
Conditions | Yield |
---|---|
at 100℃; for 0.166667h; |
Conditions | Yield |
---|---|
In aq. acetate buffer at 50℃; for 1h; pH=5; pH-value; Temperature; | 94.38% |
aluminum acetate
Conditions | Yield |
---|---|
In pentan-1-ol mixt. of octakis(benzylthio)phthalocyaninato lithium and metal salt wererefluxed in n-pentanol for 1 h, cooled to room temp.; centrifuged, washed with hot EtOH, dried in desiccator; | 69% |
Conditions | Yield |
---|---|
at 320℃; |
Conditions | Yield |
---|---|
Stage #1: zinc diacetate; aluminum acetate With potassium hydroxide In water at 20℃; pH=14; Acidic conditions; Stage #2: With acetic acid In water pH=8; |
Conditions | Yield |
---|---|
With acetic anhydride In acetic acid |
Conditions | Yield |
---|---|
slow reaction, 90°C; | |
slow reaction, 90°C; |
aluminum acetate
Conditions | Yield |
---|---|
With ammonium fluoride; manganese(II) acetate In water to anodic aluminum hydroxyde added satd. solns. of ammonium fluoride, aluminum acetate, and manganese acetate; mixt. heated at 1000-1200°C for 0.5-5 h; elem. anal.; |
Conditions | Yield |
---|---|
Al salt introduced into SiO2 sol, hydrolyzed, pptd. by (CH2)6N4, heatedat 1200-1250°C for 1 h; not isolated, detected by XRD; |
Conditions | Yield |
---|---|
In water pptn. and washing with ethanol; |
Conditions | Yield |
---|---|
In neat (no solvent) mixt. heated at 950°C for 1 h, mixt. ground up in a mortar, fired at 900°C for 1 h in air; not isolated, mixt. of phases: NaAlO2 and γ-Al2O3; |
Conditions | Yield |
---|---|
In neat (no solvent) mixt. heated at 950°C for 10 h, mixt. ground up in a mortar, fired at 900°C for 1 h in air; not isolated, mixt. of phases: NaAlO2, β-Al2O3 and γ-Al2O3; |
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