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Jinan Finer Chemical Co., Ltd

Product Description Product website: http://www.finerchem.com/pro01en/id/796.html Product Name Mecarbinate CAS No. 15574-49-9

Mecarbinate

Cas:15574-49-9

Min.Order:1 Gram

FOB Price: $52.0

Type:Lab/Research institutions

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Dayang Chem (Hangzhou) Co.,Ltd.

Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities

Mecarbinate Manufacturer/High quality/Best price/In stock

Cas:15574-49-9

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

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Simagchem Corporation

Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our

High quality Mecarbinate supplier in China

Cas:15574-49-9

Min.Order:1 Metric Ton

Negotiable

Type:Manufacturers

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Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply ethyl 5-hydroxy-1,2-dimethylindole-3-carboxylate

Cas:15574-49-9

Min.Order:1

Negotiable

Type:Other

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Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

1,2-Dimethyl-5-hydroxy-2-indolecarboxylic acid ethyl ester

Cas:15574-49-9

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

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Hebei Nengqian Chemical Import and Export Co., LTD

Our advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva

Mecarbinate

Cas:15574-49-9

Min.Order:1 Kilogram

FOB Price: $9.0 / 99.0

Type:Trading Company

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Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Standard CAS 15574-49-9 with fast shipping

Cas:15574-49-9

Min.Order:10 Gram

FOB Price: $146.0 / 176.0

Type:Trading Company

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Henan Sinotech Import&Export Corporation

Alias: 1,2-Dimethyl-5-hydroxyindole-3-Carboxylate Ethyl; Ethyl 1,2-dimethyl-5-hydroxyindole-2-carboxylate ; 1,3-dimethyl-5-Hydroxy-3-indolecarboxylicacidethylester;ethyl5-hydroxy-1,2-dimethyl-1H-indole-3-carboxylate;IFLAB-BBF1920-0014;Methyl1,2-d

Mecarbinate CAS:15574-49-9

Cas:15574-49-9

Min.Order:5 Metric Ton

FOB Price: $1.0 / 2.0

Type:Other

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Hubei Langyou International Trading Co., Ltd

1. Guaranteed purity; 2. Large quantity in stock; 3. Largest manufacturer; 4. Best service after shipment with email; 5. High quality & competitive price; Appearance:White to white crystalline powder Storage:Store in sealed co

Mecarbinate / CAS No 15574-49-9 / Arbidol hydrochloride intermediates

Cas:15574-49-9

Min.Order:100 Gram

Negotiable

Type:Other

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Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

1H-Indole-3-carboxylicacid, 5-hydroxy-1,2-dimethyl-, ethyl ester 15574-49-9

Cas:15574-49-9

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Qingdao Beluga Import and Export Co., LTD

Mecarbinate CAS: 15574-49-9 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermediat

Mecarbinate CAS: 15574-49-9

Cas:15574-49-9

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

1H-Indole-3-carboxylicacid, 5-hydroxy-1,2-dimethyl-, ethyl ester

Cas:15574-49-9

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

1H-Indole-3-carboxylicacid, 5-hydroxy-1,2-dimethyl-, ethyl ester

Cas:15574-49-9

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Changchun Artel lmport and Export trade company

Product Detail Minimum Order Qty. 10 Gram

High quality Mecarbinate supplier in China CAS NO.15574-49-9

Cas:15574-49-9

Min.Order:10 Gram

Negotiable

Type:Trading Company

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Xiamen Hisunny Chemical Co.,Ltd

Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia

Mecarbinate

Cas:15574-49-9

Min.Order:0

Negotiable

Type:Manufacturers

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Afine Chemicals Limited

Our Services 1. New Molecules R&D 2. Own test center HPLC NMR GC LC-MS 3. API and Intermediates from China reputed manufacturers 4. Documents support COA MOA MSDS DMF open part Our advantages 1. Government awarded company. Top 100 enter

Mecarbinate

Cas:15574-49-9

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Shanghai SE Pharm Co., Ltd

1. made in GMP like plant, commerially 2. Normal Stock: 500kgs 3. Audit accepted. Related documents are available to offer and audited by many clients, such as Lupin, MSN, Dr reddy etc 4. Chromatographic Purity (HPLC): not less than 99.0% Appearan

Ethyl1,2-dimethyl-5-hydroxyindole-3-carboxylate

Cas:15574-49-9

Min.Order:0 Metric Ton

Negotiable

Type:Manufacturers

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Hangzhou Keyingchem Co.,Ltd

Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det

Mecarbinate

Cas:15574-49-9

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

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Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

Mecarbinate

Cas:15574-49-9

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

High quality Mecarbinate

Cas:15574-49-9

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

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HANGZHOU YUNUO CHEMICAL CO.,LTD

Superior quality Appearance:Off-white solid Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:1kg/bag, 1kg/drum or 25kg/drum or as per your request. Application:Mecarbinate is a chemical intermediate of arbidol hydr

Mecarbinate

Cas:15574-49-9

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

inquiry

TaiChem Taizhou Limited

Established in May 2015, TaiChem Ltd. is initially invested by a British research and development company and started by PhDs back from aboard. The company is registered in China Medical City (CMC), Taizhou, Jiangsu Province, and the production site

Mecarbinate

Cas:15574-49-9

Min.Order:10 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Henan Tianfu Chemical Co., Ltd.

Our company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O

15574-49-9 Mecarbinate

Cas:15574-49-9

Min.Order:1 Metric Ton

Negotiable

Type:Lab/Research institutions

inquiry

Zibo Dorne chemical technology co. LTD

Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,

Ethyl 1,2-dimethyl-5-hydroxyindole-2-carboxylate

Cas:15574-49-9

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Xiamen Jenny Chemical Technology Co., Ltd.

GMP standard, high purity, competitive price, in stock 1. Quick Response: within 6 hours after receiving your email. 2. Quality Guarantee: All products are strictly tested by our QC, confirmed by QA, and approved by a third-party lab in China, USA,

Mecarbinate

Cas:15574-49-9

Min.Order:1 Milligram

Negotiable

Type:Trading Company

inquiry

Shandong Mopai Biotechnology Co., LTD

Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W

Mecarbinate

Cas:15574-49-9

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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KAISA GROUP INC

1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer

15574-49-9 CAS NO.15574-49-9

Cas:15574-49-9

Min.Order:1 Metric Ton

FOB Price: $7.0 / 8.0

Type:Trading Company

inquiry

Hangzhou Zhongqi chem Co.,Ltd.

Located in Hangzhou National Hi-Tech Industrial Development Zone, zhongqichem is a technical company mainly focus on the Custom synthesis, manufacturing, sales of chemicals to various industries. Benefiting from the outstanding customer service and h

1H-Indole-3-carboxylicacid, 5-hydroxy-1,2-dimethyl-, ethyl ester

Cas:15574-49-9

Min.Order:0

Negotiable

Type:Other

inquiry

Hunan chemfish Pharmaceutical co.,Ltd

Appearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea

Ethyl 1,2-dimethyl-5-hydroxyindole-3-carboxylate

Cas:15574-49-9

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Hangzhou Lingrui Chemical Co.,Ltd.

advantage: 1. The best price, satisfactory quality; 2. customers have the right to choose the delivery of parcels (EMS, DHL, FedEx, UPS); 3. customers have the right to choose from the recent effective packaging methods of their products packaging

Hot Sale High purity 15574-49-9 Mecarbinate Free samples

Cas:15574-49-9

Min.Order:1 Kilogram

Negotiable

Type:Other

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Synthetic route

ethyl N-methyl-β-aminocrotonate
21759-71-7

ethyl N-methyl-β-aminocrotonate

p-benzoquinone
106-51-4

p-benzoquinone

mecarbinate
15574-49-9

mecarbinate

Conditions
ConditionsYield
With zinc(II) iodide In dichloromethane at -30℃; for 15h; Product distribution; Further Variations:; Solvents; Reagents; Nenitzescu reaction;92%
ethyl (Z)-3-(methylamino)-2-butenoate
21759-70-6

ethyl (Z)-3-(methylamino)-2-butenoate

p-benzoquinone
106-51-4

p-benzoquinone

mecarbinate
15574-49-9

mecarbinate

Conditions
ConditionsYield
In acetone at 30℃; for 2h; Nenitzescu Synthesis;75.2%
In acetone at 30℃; for 2h;75.2%
In 1,2-dichloro-ethane at 20 - 60℃; Heating / reflux;
ethyl 3-methylaminocrotonate
870-85-9

ethyl 3-methylaminocrotonate

p-benzoquinone
106-51-4

p-benzoquinone

mecarbinate
15574-49-9

mecarbinate

Conditions
ConditionsYield
In 1,2-dichloro-ethane at 50℃; for 12h; Reflux;74.9%
In acetone at 30℃; for 2h;73.7%
In acetone at 30℃; for 2h;73.7%
ethyl N-methyl β-aminocrotonate
65578-36-1

ethyl N-methyl β-aminocrotonate

p-benzoquinone
106-51-4

p-benzoquinone

mecarbinate
15574-49-9

mecarbinate

Conditions
ConditionsYield
With zinc(II) chloride In dichloromethane at 10 - 20℃; for 4h; Reagent/catalyst;73.3%
In nitromethane for 24h;30.6%
ethyl N-methyl-β-aminocrotonate
21759-71-7

ethyl N-methyl-β-aminocrotonate

p-benzoquinone
106-51-4

p-benzoquinone

A

ethyl 5-hydroxy-2-methyl-benzofuran-3-carboxylate
7287-40-3

ethyl 5-hydroxy-2-methyl-benzofuran-3-carboxylate

B

mecarbinate
15574-49-9

mecarbinate

C

α-(Hydrochinonyl)-β-(methylamino)-crotonsaeureethylester
75785-33-0

α-(Hydrochinonyl)-β-(methylamino)-crotonsaeureethylester

Conditions
ConditionsYield
With trifluoroacetic acid In dichloromethane Nenitzescu reaction;A 14%
B n/a
C n/a
ethyl 3-methylaminocrotonate
870-85-9

ethyl 3-methylaminocrotonate

acetone
67-64-1

acetone

p-benzoquinone
106-51-4

p-benzoquinone

mecarbinate
15574-49-9

mecarbinate

ethyl acetoacetate
141-97-9

ethyl acetoacetate

methylamine
74-89-5

methylamine

p-benzoquinone
106-51-4

p-benzoquinone

mecarbinate
15574-49-9

mecarbinate

Conditions
ConditionsYield
Stage #1: ethyl acetoacetate; methylamine In methanol at 20℃;
Stage #2: p-benzoquinone With acetic acid at 20℃; Nenitzescu reaction; Further stages.;
ethyl acetoacetate
141-97-9

ethyl acetoacetate

mecarbinate
15574-49-9

mecarbinate

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: water / 3 h / 20 °C
2: acetone / 2 h / 30 °C
View Scheme
Multi-step reaction with 2 steps
1: water / 3 h / 20 °C
2: acetone / 2 h / 30 °C
View Scheme
Multi-step reaction with 2 steps
1: silica gel / water
2: nitromethane / 24 h
View Scheme
ethyl 3-methylaminocrotonate
870-85-9

ethyl 3-methylaminocrotonate

1,4-Cyclohexanedione
637-88-7

1,4-Cyclohexanedione

mecarbinate
15574-49-9

mecarbinate

Conditions
ConditionsYield
In 1,2-dichloro-ethane for 8h; Reflux;
C28H31NO3Si

C28H31NO3Si

mecarbinate
15574-49-9

mecarbinate

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 0 - 20 °C
2: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C
View Scheme
C29H33NO3Si

C29H33NO3Si

mecarbinate
15574-49-9

mecarbinate

Conditions
ConditionsYield
With tetrabutyl ammonium fluoride In tetrahydrofuran at 20℃; for 2h;
ethyl 5-hydroxy-2-methylindole-3-carboxylate
7598-91-6

ethyl 5-hydroxy-2-methylindole-3-carboxylate

mecarbinate
15574-49-9

mecarbinate

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 1H-imidazole / dichloromethane / 16 h / 20 °C
2: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 0 - 20 °C
3: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C
View Scheme
p-benzoquinone
106-51-4

p-benzoquinone

mecarbinate
15574-49-9

mecarbinate

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: acetic acid / 5 h / 20 - 45 °C
2: 1H-imidazole / dichloromethane / 16 h / 20 °C
3: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 0 - 20 °C
4: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C
View Scheme
ethyl aminocrotonate
626-34-6, 7318-00-5, 41867-20-3

ethyl aminocrotonate

mecarbinate
15574-49-9

mecarbinate

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: acetic acid / 5 h / 20 - 45 °C
2: 1H-imidazole / dichloromethane / 16 h / 20 °C
3: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 0 - 20 °C
4: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C
View Scheme
1-hydroxygermatrane monohydrate
101151-96-6

1-hydroxygermatrane monohydrate

mecarbinate
15574-49-9

mecarbinate

1,2-dimethyl-3-carboethoxy-5-germatranoxyindole
133517-08-5

1,2-dimethyl-3-carboethoxy-5-germatranoxyindole

Conditions
ConditionsYield
In m-xylene=m-xylol byproducts: H2O; mixt. of the germatrane with the hydroxy compd. in m-xylene refluxed with azeotropic distn. of H2O; residue filtered off, washed with n-pentane, recrystn. from CH3CN; elem. anal.;99%
mecarbinate
15574-49-9

mecarbinate

acetyl chloride
75-36-5

acetyl chloride

C14H15NO4

C14H15NO4

Conditions
ConditionsYield
With triethylamine In acetone at 20℃; for 6h;94.1%
mecarbinate
15574-49-9

mecarbinate

N-[2-(bromomethyl)-3-fluoro-allyl]carbamic acid tert-butyl ester

N-[2-(bromomethyl)-3-fluoro-allyl]carbamic acid tert-butyl ester

5-[(E)-2-[(tert-butoxycarbonylamino)methyl]-3-fluoroallyloxy]-1,2-dimethylindole-3-carboxylic acid ethyl ester

5-[(E)-2-[(tert-butoxycarbonylamino)methyl]-3-fluoroallyloxy]-1,2-dimethylindole-3-carboxylic acid ethyl ester

Conditions
ConditionsYield
With caesium carbonate In N,N-dimethyl-formamide at 40℃; for 4.5h;94%
mecarbinate
15574-49-9

mecarbinate

acetic anhydride
108-24-7

acetic anhydride

1,2-dimethyl-5-acetoxy-1H-indole-3-carboxylic acid ethyl ester
40945-79-7

1,2-dimethyl-5-acetoxy-1H-indole-3-carboxylic acid ethyl ester

Conditions
ConditionsYield
With sodium acetate In dichloromethane for 3h; Reagent/catalyst; Reflux;91.5%
for 4h; Reflux;65%
With pyridine
With triethylamine
mecarbinate
15574-49-9

mecarbinate

triethylmethoxystannane
1067-21-6

triethylmethoxystannane

1,2-dimethyl-3-carboethoxy-5-triethylstannoxyindole
133642-00-9

1,2-dimethyl-3-carboethoxy-5-triethylstannoxyindole

Conditions
ConditionsYield
In neat (no solvent) byproducts: MeOH; mixt. of the hydroxy deriv. and triethylmethoxystannane heated (formed MeOH removed continuously during react.); residue washed with n-pentane, dried in vac.; elem. anal.;91%
mecarbinate
15574-49-9

mecarbinate

p-toluenesulfonyl chloride
98-59-9

p-toluenesulfonyl chloride

1,2-Dimethyl-3-ethoxycarbonyl-5-tosyloxyindole
88461-72-7

1,2-Dimethyl-3-ethoxycarbonyl-5-tosyloxyindole

Conditions
ConditionsYield
With potassium carbonate In acetone for 5h; Heating;88.5%
mecarbinate
15574-49-9

mecarbinate

methyl iodide
74-88-4

methyl iodide

ethyl 5-methoxy-1,2-dimethyl-1H-indole-3-carboxylate
40963-98-2

ethyl 5-methoxy-1,2-dimethyl-1H-indole-3-carboxylate

Conditions
ConditionsYield
With potassium hydride In N,N-dimethyl-formamide at 0 - 20℃; for 4h;81%
With potassium carbonate In N,N-dimethyl-formamide at 20℃;81%
Stage #1: mecarbinate With potassium hydroxide In dimethyl sulfoxide at 20℃; for 0.5h;
Stage #2: methyl iodide
75.5%
mecarbinate
15574-49-9

mecarbinate

1,2-dimethyl-5-hydroxy-1H-indole-3-carboxylic acid
25888-01-1

1,2-dimethyl-5-hydroxy-1H-indole-3-carboxylic acid

Conditions
ConditionsYield
With water; sodium hydroxide In ethanol for 12h; Reflux;77%
With water; sodium hydroxide In ethanol for 12h; Reflux;77%
With water; sodium hydroxide In ethanol for 12h; Reflux;76.98%
With sodium hydroxide In ethanol; water for 12h; Reflux;76.98%
but-3-enoic acid
625-38-7

but-3-enoic acid

mecarbinate
15574-49-9

mecarbinate

C17H19NO4

C17H19NO4

Conditions
ConditionsYield
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 20℃;70%
mecarbinate
15574-49-9

mecarbinate

chloroacetic acid ethyl ester
105-39-5

chloroacetic acid ethyl ester

1-methyl-3-ethoxycarbonyl-5-ethoxycarbonylmethoxy-2-methylindole
64199-44-6

1-methyl-3-ethoxycarbonyl-5-ethoxycarbonylmethoxy-2-methylindole

Conditions
ConditionsYield
With potassium carbonate; potassium iodide In acetone for 30h; Alkylation; Heating;65%
[13C]methyl iodide
4227-95-6

[13C]methyl iodide

mecarbinate
15574-49-9

mecarbinate

C13(13)CH17NO3
1271786-83-4

C13(13)CH17NO3

Conditions
ConditionsYield
With sodium hydride64%
mecarbinate
15574-49-9

mecarbinate

propargyl bromide
106-96-7

propargyl bromide

ethyl 5-[(prop-2-yn-1-yl)oxy]-1,2-dimethyl-1H-indole-3-carboxylate

ethyl 5-[(prop-2-yn-1-yl)oxy]-1,2-dimethyl-1H-indole-3-carboxylate

Conditions
ConditionsYield
With sodium hydroxide In water for 0.0333333h; Heating;63%
formaldehyd
50-00-0

formaldehyd

6-methoxy-1,2,3,4-tetrahydro-isoquinoline
42923-77-3

6-methoxy-1,2,3,4-tetrahydro-isoquinoline

mecarbinate
15574-49-9

mecarbinate

ethyl 5-hydroxy-4-((6-methoxy-3,4-dihydroisoquinolin-2(1H)-yl)methyl)-1,2-dimethyl-1H-indole-3-carboxylate

ethyl 5-hydroxy-4-((6-methoxy-3,4-dihydroisoquinolin-2(1H)-yl)methyl)-1,2-dimethyl-1H-indole-3-carboxylate

Conditions
ConditionsYield
With acetic acid In water at 90℃; for 0.5h;63%
mecarbinate
15574-49-9

mecarbinate

C13H14FNO5S

C13H14FNO5S

Conditions
ConditionsYield
With fluorosulfonyl fluoride; triethylamine In 1,4-dioxane at 20℃; under 760.051 Torr; for 24h;57%
formaldehyd
50-00-0

formaldehyd

mecarbinate
15574-49-9

mecarbinate

ethyl 4-formyl-5-hydroxy-1,2-dimethyl-1H-indole-3-carboxylate

ethyl 4-formyl-5-hydroxy-1,2-dimethyl-1H-indole-3-carboxylate

Conditions
ConditionsYield
Stage #1: formaldehyd With triethylamine; magnesium chloride In tetrahydrofuran for 0.166667h;
Stage #2: mecarbinate In tetrahydrofuran at 75℃; for 24h;
50%
mecarbinate
15574-49-9

mecarbinate

acetic acid
64-19-7

acetic acid

ethyl 4-formyl-5-hydroxy-1,2-dimethyl-1H-indole-3-carboxylate

ethyl 4-formyl-5-hydroxy-1,2-dimethyl-1H-indole-3-carboxylate

Conditions
ConditionsYield
With hexamethylenetetramine at 90℃; for 6h;12%
formaldehyd
50-00-0

formaldehyd

mecarbinate
15574-49-9

mecarbinate

dimethyl amine
124-40-3

dimethyl amine

6-dimethylaminomethyl-5-hydroxy-1,2-dimethyl-indole-3-carboxylic acid ethyl ester

6-dimethylaminomethyl-5-hydroxy-1,2-dimethyl-indole-3-carboxylic acid ethyl ester

Conditions
ConditionsYield
With acetic acid
mecarbinate
15574-49-9

mecarbinate

chloroacetic acid
79-11-8

chloroacetic acid

5-carboxymethoxy-1,2-dimethyl-indole-3-carboxylic acid ethyl ester
64199-47-9

5-carboxymethoxy-1,2-dimethyl-indole-3-carboxylic acid ethyl ester

Conditions
ConditionsYield
With 1,4-dioxane; sodium hydroxide
mecarbinate
15574-49-9

mecarbinate

dimethyl sulfate
77-78-1

dimethyl sulfate

ethyl 5-methoxy-1,2-dimethyl-1H-indole-3-carboxylate
40963-98-2

ethyl 5-methoxy-1,2-dimethyl-1H-indole-3-carboxylate

Conditions
ConditionsYield
With 1,4-dioxane; sodium hydroxide
formaldehyd
50-00-0

formaldehyd

mecarbinate
15574-49-9

mecarbinate

methylamine hydrochloride
593-51-1

methylamine hydrochloride

2,7,8-trimethyl-1,2,3,7-tetrahydro-[1,3]oxazino[5,6-e]indole-9-carboxylic acid ethyl ester

2,7,8-trimethyl-1,2,3,7-tetrahydro-[1,3]oxazino[5,6-e]indole-9-carboxylic acid ethyl ester

Conditions
ConditionsYield
In 1,4-dioxane; water
formaldehyd
50-00-0

formaldehyd

mecarbinate
15574-49-9

mecarbinate

n-butylamine hydrochloride
3858-78-4

n-butylamine hydrochloride

2-butyl-7,8-dimethyl-1,2,3,7-tetrahydro-[1,3]oxazino[5,6-e]indole-9-carboxylic acid ethyl ester

2-butyl-7,8-dimethyl-1,2,3,7-tetrahydro-[1,3]oxazino[5,6-e]indole-9-carboxylic acid ethyl ester

Conditions
ConditionsYield
In 1,4-dioxane; water
bis-(dimethylamino)methane
51-80-9

bis-(dimethylamino)methane

mecarbinate
15574-49-9

mecarbinate

1,2-Dimethyl-3-ethoxycarbonyl-4,6-bis(dimethylaminomethyl)-5-hydroxyindole
88461-90-9

1,2-Dimethyl-3-ethoxycarbonyl-4,6-bis(dimethylaminomethyl)-5-hydroxyindole

Conditions
ConditionsYield
In acetic acid Heating; Yield given;
mecarbinate
15574-49-9

mecarbinate

p-toluidine
106-49-0

p-toluidine

5-Hydroxy-1,2-dimethyl-4-p-tolylazo-1H-indole-3-carboxylic acid ethyl ester
76921-18-1

5-Hydroxy-1,2-dimethyl-4-p-tolylazo-1H-indole-3-carboxylic acid ethyl ester

Conditions
ConditionsYield
With hydrogenchloride; sodium nitrite 1.)-5 to 0 deg C 2.)dioxane, 0 deg C, 3 h; Yield given. Multistep reaction;
mecarbinate
15574-49-9

mecarbinate

4-chloro-aniline
106-47-8

4-chloro-aniline

4-(4-Chloro-phenylazo)-5-hydroxy-1,2-dimethyl-1H-indole-3-carboxylic acid ethyl ester
76921-20-5

4-(4-Chloro-phenylazo)-5-hydroxy-1,2-dimethyl-1H-indole-3-carboxylic acid ethyl ester

Conditions
ConditionsYield
With hydrogenchloride; sodium nitrite 1.)-5 to 0 deg C 2.)dioxane, 0 deg C, 3 h; Yield given. Multistep reaction;

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