Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities
Cas:30433-91-1
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inquiryhigh quality Appearance:White or off-white Solid Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea Port:shanghai
Thiophene-2-Ethylamine CAS NO.: 30433-91-1 Formula: C6H9NS Molecular Weight: 127.21 Characteristic: It is clear colorless to light brown liquid. Usage: It is mainly used for synthetic thiophene pyridine and clopidogrel intermediate.
Cas:30433-91-1
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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Cas:30433-91-1
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Cas:30433-91-1
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Cas:30433-91-1
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inquiryProduct Name Thiophene-2-ethylamine Synonyms THIOPHENE ETHYLAMINE;THIOPHENE-2-ETHYLAMINE;THIOPHENE-2-ETHYLAMINE HCL SALT;RARECHEM AL BW 0099;2-(2-AMINOETHYL)THIOPHENE;2-(2'-THIENYL)ETHYL AMINE;2-(2-THI
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Cas:30433-91-1
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Cas:30433-91-1
Min.Order:1 Gram
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Type:Trading Company
inquiryThiophene-2-ethylamine CAS:30433-91-1 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic in
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Cas:30433-91-1
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inquiryProduct Detail Minimum Order Qty. 10 Gram
Cas:30433-91-1
Min.Order:10 Gram
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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Cas:30433-91-1
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
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inquiryCompany Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments
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Min.Order:1 Gram
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inquiry1. Timely and efficient service to ensure communication with customers 2. Produce products of different specifications and sizes according to your requirements. 3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures
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Wuhan Xinweiye Chemical Co., Ltd. is mainly engaged in the process development and production of customized synthesis and pharmaceutical intermediates. We have professional researchers in organic synthesis, analytical chemistry and production process
Cas:30433-91-1
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:30433-91-1
Min.Order:10 Gram
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Type:Lab/Research institutions
inquiry30433-91-1 Thiophene-2-ethylamineAppearance:White powder Storage:Store in cool & dry place Package:according to customers' requirements Application:Pharmaceutical Intermediates Transportation:By air(EMS or EUB or FedEx or TNT ect...) or by sea(FOB or
Superior quality, moderate price & quick delivery Appearance:colorless to yellow liquid Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:25kg/drum;200kg/drum as per your request Application:Used as antithrombot
Product Name: Thiophene-2-ethylamine Synonyms: THIOPHENE ETHYLAMINE;THIOPHENE-2-ETHYLAMINE;THIOPHENE-2-ETHYLAMINE HCL SALT;RARECHEM AL BW 0099;2-(2-AMINOETHYL)TH
Cas:30433-91-1
Min.Order:1 Metric Ton
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inquiryProduct name: Thiophene-2-Ethylamine CAS No.: 30433-91-1 Molecule Formula:C6H10NS Molecule Weight:128.21 Purity: 98.0% Package: 25kg/drum Description:White to off-white powder Manufacture Standards:Enterprise Standard
Cas:30433-91-1
Min.Order:1 Kilogram
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Type:Trading Company
inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Cas:30433-91-1
Min.Order:1 Gram
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inquiry2-(2-nitroethenyl)thiophene
[2-(2-thyenyl)ethyl]amine
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride In tetrahydrofuran Cooling with ice; Reflux; | 92% |
With lithium aluminium tetrahydride In tetrahydrofuran Reflux; Cooling with ice; | 92% |
With lithium aluminium tetrahydride In tetrahydrofuran Cooling with ice; Reflux; | 92% |
2-(2-azidoethyl)thiophene
[2-(2-thyenyl)ethyl]amine
Conditions | Yield |
---|---|
With palladium on activated charcoal; hydrogen In methanol at 20℃; for 16h; | 100% |
With 1,2-bis(diphenylphosphino)ethane nickel(II) chloride; tri-n-butyl-tin hydride In tetrahydrofuran at 0℃; for 0.5h; Reduction; | 89% |
2-cyanomethylthiophene
[2-(2-thyenyl)ethyl]amine
Conditions | Yield |
---|---|
With indium(III) chloride; sodium tetrahydroborate In tetrahydrofuran at 25℃; for 4h; Inert atmosphere; | 98% |
With lithium aluminium tetrahydride In tetrahydrofuran | 71% |
With lithium aluminium tetrahydride; aluminium trichloride In diethyl ether for 1h; Ambient temperature; | 56% |
3-(thiophen-2-yl)-propionamide
[2-(2-thyenyl)ethyl]amine
Conditions | Yield |
---|---|
With sodium hydroxide; sodium hypochlorite Zusatz von Kaliumhydroxid; | |
With bromine at 70℃; for 1h; Hofmann Rearrangement; Large scale; | 1110g |
2-(thiophen-2-yl)acetamide
4,5,6,7-tetrahydrothieno[3,2-c]pyridine
[2-(2-thyenyl)ethyl]amine
Conditions | Yield |
---|---|
In hydrogenchloride; sodium hydroxide | 74.5% |
1-(2-thienyl)-2-nitroethene
[2-(2-thyenyl)ethyl]amine
Conditions | Yield |
---|---|
With diborane | |
With hydrogenchloride; sodium borohydrid; trifluoroborane diethyl ether In tetrahydrofuran; water; toluene |
acetylacetone
[2-(2-thyenyl)ethyl]amine
Conditions | Yield |
---|---|
With sodium carbonate In 2-methoxy-ethanol; water |
[2-(2-thyenyl)ethyl]amine
Conditions | Yield |
---|---|
With bromine at 60℃; for 1h; Hofmann Rearrangement; |
4-(thiophen-2-yl)butan-2-one
[2-(2-thyenyl)ethyl]amine
Conditions | Yield |
---|---|
With hydrogen azide at 60 - 120℃; |
2-(2-nitroethyl)thiophene
[2-(2-thyenyl)ethyl]amine
Conditions | Yield |
---|---|
With hydrogen at 120℃; for 12h; Autoclave; | 1009 g |
[2-(2-thyenyl)ethyl]amine
Conditions | Yield |
---|---|
With sulfuric acid; water at 20℃; |
2-thiophenethanol
[2-(2-thyenyl)ethyl]amine
Conditions | Yield |
---|---|
With dmap; trifluoromethylsulfonic anhydride; ammonia 1.) CH2Cl2, from -30 deg C to RT, 2.) THF, from -30 deg C to RT; Multistep reaction; | |
Multi-step reaction with 3 steps 1: Et3N / CH2Cl2 / 12 h / -5 °C 2: 85 percent / dimethylformamide / 6 h / 60 °C 3: 89 percent / TBTH; Ni(diphenylphosphinoethane)Cl2 / tetrahydrofuran / 0.5 h / 0 °C View Scheme | |
Multi-step reaction with 2 steps 1: chloroform; pyridine; phosphorus (III)-bromide 2: ammonia; ethanol View Scheme | |
Multi-step reaction with 3 steps 1: triethylamine / dichloromethane / 0.5 h / 20 °C 2: sodium azide / dimethyl sulfoxide / 1 h / 80 °C 3: palladium on activated charcoal; hydrogen / methanol / 16 h / 20 °C View Scheme |
1,3,5-tris-(2-(2-thienyl)ethyl)isocyanurate
[2-(2-thyenyl)ethyl]amine
Conditions | Yield |
---|---|
With sodium hydroxide In butan-1-ol for 72h; Heating; | 83% |
thiophene-2-carbaldehyde
[2-(2-thyenyl)ethyl]amine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: acetic acid; ammonium acetate / 10 h / Heating 2: lithium aluminium tetrahydride / tetrahydrofuran / Cooling with ice; Reflux View Scheme | |
Multi-step reaction with 2 steps 1: acetic acid; ammonium acetate / 10 h / 80 °C 2: lithium aluminium tetrahydride / tetrahydrofuran / Reflux; Cooling with ice View Scheme | |
Multi-step reaction with 2 steps 1: ammonium acetate / acetic acid / 10 h / 80 °C 2: lithium aluminium tetrahydride / tetrahydrofuran / Cooling with ice; Reflux View Scheme | |
Multi-step reaction with 2 steps 1: ammonium acetate / 2 h / Reflux 2: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / 0 - 20 °C View Scheme |
2-(2-Bromoethyl)thiophene
[2-(2-thyenyl)ethyl]amine
Conditions | Yield |
---|---|
With ethanol; ammonia |
2-(thiophen-2-yl)acetamide
[2-(2-thyenyl)ethyl]amine
N-(2-(thien-2-yl)ethyl)-phthalimide
[2-(2-thyenyl)ethyl]amine
Conditions | Yield |
---|---|
With hydrazine In ethanol; water for 14h; Reflux; |
N-<2-(2-Thienyl)ethyl>benzolsulfonamid
[2-(2-thyenyl)ethyl]amine
Conditions | Yield |
---|---|
With sodium bis(2-methoxyethoxy)aluminium dihydride In toluene for 72h; Heating; | 25% |
4-methyl-N-(2-(thiophen-2-yl)ethyl)benzenesulfonamide
[2-(2-thyenyl)ethyl]amine
Conditions | Yield |
---|---|
With sodium bis(2-methoxyethoxy)aluminium dihydride In toluene for 24h; Heating; | 6% |
diethyl N-[2-(thien-2-yl)-ethyl]-phosphoramidate
[2-(2-thyenyl)ethyl]amine
Conditions | Yield |
---|---|
With hydrogenchloride at 80 - 85℃; for 1.5h; Yield given; |
isopropyl N-[2-(thien-2-yl)-ethyl]-amino-phenylphosphinate
[2-(2-thyenyl)ethyl]amine
Conditions | Yield |
---|---|
With hydrogenchloride at 80 - 85℃; for 1.5h; Yield given; |
2-(thiophen-2-yl)ethyl methanesulfonate
[2-(2-thyenyl)ethyl]amine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 85 percent / dimethylformamide / 6 h / 60 °C 2: 89 percent / TBTH; Ni(diphenylphosphinoethane)Cl2 / tetrahydrofuran / 0.5 h / 0 °C View Scheme | |
Multi-step reaction with 2 steps 1: sodium azide / dimethyl sulfoxide / 1 h / 80 °C 2: palladium on activated charcoal; hydrogen / methanol / 16 h / 20 °C View Scheme |
Diethyl N-[β-(thien-2-yl)-vinyl]-phosphoramidate
[2-(2-thyenyl)ethyl]amine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: NaBH4 / ethanol / 1 h / 50 °C 2: aq. HCl / 1.5 h / 80 - 85 °C View Scheme |
Isopropyl N-[β-(thien-2-yl)-vinyl]-amino-phenylphosphinate
[2-(2-thyenyl)ethyl]amine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: NaBH4 / ethanol / 1 h / 50 °C 2: aq. HCl / 1.5 h / 80 - 85 °C View Scheme |
2-Chloromethylthiophene
[2-(2-thyenyl)ethyl]amine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: N-benzyl-N,N,N-triethylammonium chloride / water-d2 2: lithium aluminium tetrahydride / tetrahydrofuran View Scheme |
Thiophene-2-acetic acid
[2-(2-thyenyl)ethyl]amine
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: lithium aluminium tetrahydride / tetrahydrofuran / 0.33 h / 20 °C 2: triethylamine / dichloromethane / 0.5 h / 20 °C 3: sodium azide / dimethyl sulfoxide / 1 h / 80 °C 4: palladium on activated charcoal; hydrogen / methanol / 16 h / 20 °C View Scheme |
3-thiophen-2-yl-2-thioxo-propionic acid
[2-(2-thyenyl)ethyl]amine
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: ethanol; hydroxylamine 2: acetic acid anhydride 3: lithium alanate; diethyl ether View Scheme |
5-(2'-thiophenemethylene)rhodamine
[2-(2-thyenyl)ethyl]amine
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: aq. NaOH solution 2: ethanol; hydroxylamine 3: acetic acid anhydride 4: lithium alanate; diethyl ether View Scheme |
2-hydroxyimino-3-[2]thienyl-propionic acid
[2-(2-thyenyl)ethyl]amine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: acetic acid anhydride 2: lithium alanate; diethyl ether View Scheme |
3-(2-thienyl)propanoic acid
[2-(2-thyenyl)ethyl]amine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: chloroform; thionyl chloride / Behandeln des Reaktionsgemisches mit wss. Ammoniak und wss. Natronlauge 2: aqueous sodium hypochlorite solution; aq. NaOH solution / Zusatz von Kaliumhydroxid View Scheme |
[2-(2-thyenyl)ethyl]amine
chloroacetyl chloride
2-chloro-N-(2-(thiophen-2-yl)ethyl)acetamide
Conditions | Yield |
---|---|
With potassium carbonate In dichloromethane Ambient temperature; | 100% |
With triethylamine In dichloromethane at 0℃; | 82% |
In benzene at 0℃; Reflux; |
[2-(2-thyenyl)ethyl]amine
N-((tert-butyloxy)carbonyl)-N'-(2-(4-fluorophenyl)ethyl)iminodiacetic acid monoamide
N-((tert-butyloxy)carbonyl)-N'-(2-(4-fluorophenyl)ethyl)-N''-(2-(2'-thienyl)ethyl)iminodiacetic acid diamide
Conditions | Yield |
---|---|
With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 25℃; for 16h; Substitution; | 100% |
With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 25℃; Acylation; | 93% |
With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 25℃; for 16h; |
[2-(2-thyenyl)ethyl]amine
4-biphenyl-carboxylic acid chloride
Conditions | Yield |
---|---|
With sodium hydroxide In water at 0℃; | 100% |
With triethylamine In tetrahydrofuran for 0.5h; | 96% |
With sodium hydroxide In water for 12h; Cooling with ice; | 82% |
With triethylamine In tetrahydrofuran at 20℃; | 55% |
[2-(2-thyenyl)ethyl]amine
1,2,3-Benzotriazole
formaldehyd
benzotriazol-1-ylmethyl-(2-thiophen-2-yl-ethyl)-amine
Conditions | Yield |
---|---|
In diethyl ether; water at 20℃; | 100% |
[2-(2-thyenyl)ethyl]amine
2-[(4R)-2,2-dimethyl-5-oxo-1,3-dioxolan-4-yl]acetic acid
C13H17NO4S
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine; HATU In N,N-dimethyl-formamide | 100% |
[2-(2-thyenyl)ethyl]amine
1,4-Dihydroxynaphthalene
Conditions | Yield |
---|---|
With cerium(III) chloride heptahydrate; triethylamine In ethanol at 20℃; Further stages; | 100% |
[2-(2-thyenyl)ethyl]amine
phenyl isothiocyanate
1-phenyl-3-(2-(thiophen-2-yl)ethyl)thiourea
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 2h; Addition; | 99% |
[2-(2-thyenyl)ethyl]amine
Cyclohexanecarboxylic acid
cyclohexanecarboxylic acid (2-thiophen-2-ylethyl)amide
Conditions | Yield |
---|---|
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In N,N-dimethyl-formamide at 20℃; for 15h; Substitution; | 99% |
[2-(2-thyenyl)ethyl]amine
formaldehyd
6,7-dihydro-4H-thieno[3,2-c]pyridine hydrochloride
Conditions | Yield |
---|---|
Stage #1: [2-(2-thyenyl)ethyl]amine; formaldehyd In dichloromethane at 40 - 45℃; Stage #2: With hydrogenchloride In dichloromethane; water; N,N-dimethyl-formamide at 20 - 70℃; | 99% |
Stage #1: [2-(2-thyenyl)ethyl]amine; formaldehyd In toluene for 1.5h; Reflux; Inert atmosphere; Dean-Stark; Stage #2: With hydrogenchloride In 1,4-dioxane; toluene at 60℃; for 0.5h; Inert atmosphere; | 98% |
Stage #1: [2-(2-thyenyl)ethyl]amine; formaldehyd In 1,2-dichloro-ethane for 4h; Heating / reflux; Stage #2: With hydrogenchloride In 1,2-dichloro-ethane; N,N-dimethyl-formamide at 70℃; for 4h; | 90% |
[2-(2-thyenyl)ethyl]amine
Diethyl maleate
Conditions | Yield |
---|---|
In acetonitrile at 20℃; for 16h; | 99% |
In acetonitrile at 20℃; for 16h; | 99% |
Conditions | Yield |
---|---|
With sodium hydroxide In water for 12h; Cooling with ice; | 99% |
With sodium hydroxide In water at 0℃; | 98% |
With sodium hydroxide In water for 12h; | 80% |
[2-(2-thyenyl)ethyl]amine
di-tert-butyl dicarbonate
tert-butyl (2-(thiophen-2-yl)ethyl)carbamate
Conditions | Yield |
---|---|
With triethylamine In dichloromethane for 72h; Inert atmosphere; | 98% |
With triethylamine In dichloromethane at 20℃; Schlenk technique; Inert atmosphere; | 98% |
In chloroform for 6h; Heating; | |
In dichloromethane at 20℃; Inert atmosphere; |
[2-(2-thyenyl)ethyl]amine
5-methoxy-2-tetralone
5-methoxy-N-2'-(thien-2-yl)ethyltetralin-2-amine
Conditions | Yield |
---|---|
Stage #1: [2-(2-thyenyl)ethyl]amine; 5-methoxy-2-tetralone With sodium tris(acetoxy)borohydride In dichloromethane at 20℃; Inert atmosphere; Industry scale; Stage #2: With acetic acid In dichloromethane at 20℃; Stage #3: With sodium hydroxide In dichloromethane; water Product distribution / selectivity; cooling with ice-water; Alkaline conditions; | 98% |
With sodium tris(acetoxy)borohydride; acetic acid In dichloromethane at 20℃; Solvent; Reagent/catalyst; Temperature; Time; Inert atmosphere; | 98% |
Conditions | Yield |
---|---|
With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; | 98% |
[2-(2-thyenyl)ethyl]amine
m-Toluic acid
Conditions | Yield |
---|---|
With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃; | 98% |
[2-(2-thyenyl)ethyl]amine
carbon disulfide
1,3-di(2-(thiophen-2-yl)ethyl)thiourea
Conditions | Yield |
---|---|
In water at 20℃; for 0.166667h; Green chemistry; | 98% |
[2-(2-thyenyl)ethyl]amine
formaldehyd
N-(thiophen-2-ylethyl)methyleneamine
Conditions | Yield |
---|---|
In ethanol at 49 - 53℃; for 3h; Temperature; Solvent; Eschweiler-Clarke Methylation; | 97.69% |
In water Heating; | |
In water at 20 - 90℃; for 18h; | |
With titanium(IV) isopropylate at 80℃; for 2h; Inert atmosphere; |
[2-(2-thyenyl)ethyl]amine
benzoyl chloride
N-<2-(2-thienyl)ethyl>benzamide
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In dichloromethane at 0 - 20℃; for 0.25h; | 97% |
With sodium hydroxide In water for 12h; Cooling with ice; | 95% |
With sodium hydroxide In water for 12h; | 80% |
[2-(2-thyenyl)ethyl]amine
formic acid ethyl ester
N-(2-(thien-2-yl)ethyl)formamide
Conditions | Yield |
---|---|
With sodium hydrogencarbonate at 20℃; | 97% |
[2-(2-thyenyl)ethyl]amine
Glyoxilic acid
4,5,6,7-Tetrahydro-thieno[3,2-c]pyridine-4-carboxylic acid
Conditions | Yield |
---|---|
In water for 0.5h; Ambient temperature; | 97% |
Conditions | Yield |
---|---|
Shvo complex In tert-Amyl alcohol at 150℃; for 24h; | 97% |
[2-(2-thyenyl)ethyl]amine
4-chloro-2-(4-methanesulfonylphenyl)-6-trifluoromethylpyrimidine
C18H16F3N3O2S2
Conditions | Yield |
---|---|
With triethylamine | 97% |
[2-(2-thyenyl)ethyl]amine
3-fluoro-5-(trifluoromethyl)benzoic acid
C14H11F4NOS
Conditions | Yield |
---|---|
With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; triethylamine In dichloromethane; acetonitrile at 20℃; | 97% |
Conditions | Yield |
---|---|
Stage #1: [2-(2-thyenyl)ethyl]amine; trans-Crotonaldehyde With magnesium sulfate In dichloromethane at 20℃; for 1h; Inert atmosphere; Stage #2: With sodium tetrahydroborate In methanol at 0 - 20℃; for 16h; Inert atmosphere; | 97% |
[2-(2-thyenyl)ethyl]amine
9-chloro-2-methoxyacridine
2-methoxy-N-(2-(thiophen-2-yl)ethyl)acridin-9-amine
Conditions | Yield |
---|---|
In methanol for 14h; Reflux; | 96% |
[2-(2-thyenyl)ethyl]amine
5-bromo-3-chloro-1H-pyrrolo[2,3-b]pyridine
3-chloro-N-(2-(thiophen-2-yl)ethyl)-1H-pyrrolo[2,3-b]pyridin-5-amine
Conditions | Yield |
---|---|
With dicyclohexyl-(2′,4′,6′-triisopropyl-3,6-dimethoxy-[1,1′-biphenyl]-2-yl)phosphine; chloro[2-(dicyclohexylphosphino)-3,6-dimethoxy-2’,4’,6’-triisopropyl-1,1’-biphenyl] [2-(2-aminoethyl)phenyl]palladium(II); lithium hexamethyldisilazane In tetrahydrofuran at 65℃; for 4h; Inert atmosphere; Sealed vial; | 96% |
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