As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
Cas:5402-55-1
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inquiryhebei yanxi chemical co., LTD who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do research and developm
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inquiry2-(2-Thienyl)ethanol 【Chemical Name】 2-(2-HYDROXYETHYL)THIOPHENE; 2-THIENYLETHANOL; 2-THIOPHENEETHANOL; 2-THIOPHENETHANOL; THIOPHENE-2-ETHANOL; Ethanol, 2-(2-thienyl)-; Thiopheneethanol; B-(B-THIENYL)ETHANOL; THIOPHENE-2-ETHYANOL; 2-THIOPHEN-2-YL
Cas:5402-55-1
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
Cas:5402-55-1
Min.Order:1 Gram
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inquiryCangzhou Enke Pharma Tech Co.,ltd. is located in Cangzhou City, Hebei province ,where is a famous petroleum chemical industry city in China. Enke Pharma a high-tech enterprise ,and we are dedicated to developing and manufacturing new api, intermedi
Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Cas:5402-55-1
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Type:Manufacturers
inquiryProduct Description Product website: http://www.finerchem.com/pro01en/id/1416.html Product Name 2-Thiopheneethanol CAS No. 5271-38-5
Cas:5402-55-1
Min.Order:1 Gram
FOB Price: $22.0
Type:Lab/Research institutions
inquiry2-Thiopheneethanol Basic information Product Name: 2-Thiopheneethanol Synonyms: 2-(2-HYDROXYETHYL)THIOPHENE;2-(2-THIENYL)ETHANOL;2-THIENYLETHANOL;2-THIOPHENETHANOL;2-THIOPHENEETHANOL;THI
Cas:5402-55-1
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryOur advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva
Cas:5402-55-1
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:5402-55-1
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inquiryProduct Name: 2-Thiopheneethanol Synonyms: 2-(2-HYDROXYETHYL)THIOPHENE;2-(2-THIENYL)ETHANOL;2-THIENYLETHANOL;2-THIOPHENETHANOL;2-THIOPHENEETHANOL;THIOPHENE-2-ETHANOL;Ethanol, 2-(2-thienyl)-;Thiopheneethanol CAS: 5402-55-1 MF: C6H8OS MW: 128.1
Appearance:Colorless or light yellow clear liquid Storage:ln stock Package:25kg/Barrel Application:Intermediates Transportation:Express/Sea/Air Port:Any port of china
Cas:5402-55-1
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inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
Cas:5402-55-1
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inquiryPacking: According to customer requirements Delivery time: In stock or depands Port of shipment: Ningbo/Shanghai/Qingdao OEM/ODM:Welcome Sample:We can offer our existing samples at once Appearance:Clear colorless liquid Storage:Refer to COA / M
Cas:5402-55-1
Min.Order:1 Kilogram
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Type:Trading Company
inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At prese
Cas:5402-55-1
Min.Order:1 Kilogram
FOB Price: $32.0 / 36.0
Type:Trading Company
inquiry2-Thiopheneethanol CAS:5402-55-1 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic interme
Cas:5402-55-1
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:5402-55-1
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryISO9001 Exporting Japan, Korea regularly. ProductName:2-Thiopheneethanol Synonyms:2-(2-Thienyl)ethanol CASNo:5402-55-1 EINECS:226-452-0 MolecularFormula:C6H8OS Appearance:- Storage:Store in dry and cool place with good seal Packag
1. Timely and efficient service to ensure communication with customers 2. Produce products of different specifications and sizes according to your requirements. 3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures
Cas:5402-55-1
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Type:Lab/Research institutions
inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
1.Prompt Goods; 2.Flexible payment terms; 3.Documents & Certificate support. Name: 2-Thiopheneethanol Molecular Structure: Formula: C6H8OS Molecular Weight : 128.19 Synonyms: 2-(2-THIENYL)ETHANOL(THIOPHENE-2-ETHANOL);2-(2-Hydroxyethyl)th
Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
Lorcaserin(856681-05-5)is an orally administered agent and a selective 5-HT2C receptor agonist for the treatment of obesity. It had been approved for marketing in US by FDA on 27 June in 2012. In clinical studies, lorcaserin h
Cas:5402-55-1
Min.Order:0 Metric Ton
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inquiryOur advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We have s
Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:5402-55-1
Min.Order:0 Metric Ton
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inquiryFactory direct sales, accept customization. 2-Thiopheneethanol, is used as the antithrombotics thiophene chlorine match piperidine intermediates. It is also used as a ticlopidine Intermediate. Kind Pharma has its own laboratory, we can do analytica
Cas:5402-55-1
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryCompany Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments
J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
Cas:5402-55-1
Min.Order:4 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryethyl thiophen-2-ylacetate
2-thiophenethanol
Conditions | Yield |
---|---|
With phenylsilane; cobalt(II) diacetate tetrahydrate; sodium triethylborohydride In 1,2-dimethoxyethane; toluene at 25℃; for 15h; Reagent/catalyst; Solvent; Temperature; Inert atmosphere; Schlenk technique; | 100% |
Stage #1: ethyl thiophen-2-ylacetate With sodium tetrahydroborate In tetrahydrofuran at 70℃; for 0.25h; Stage #2: In tetrahydrofuran; methanol at 70℃; for 0.15h; | 94% |
With ethylmagnesium bromide; poly(methylhydrosiloxane); bis(cyclopentadienyl)titanium dichloride In tetrahydrofuran; diethyl ether for 17.5h; Ambient temperature; | 89% |
methyl 2-thiopheneacetate
2-thiophenethanol
Conditions | Yield |
---|---|
Stage #1: methyl 2-thiopheneacetate With diethylzinc; lithium chloride In tetrahydrofuran; hexane at 20℃; for 6h; Inert atmosphere; Stage #2: With sodium hydroxide In tetrahydrofuran; hexane; water at 20℃; for 8h; Inert atmosphere; chemoselective reaction; | 98% |
Stage #1: methyl 2-thiopheneacetate With sodium tetrahydroborate In tetrahydrofuran at 70℃; for 0.25h; Stage #2: In tetrahydrofuran; methanol at 70℃; for 0.15h; | 97% |
With strain of the zygomycete fungus S. racemosum MUT 770 In dimethyl sulfoxide for 72h; Enzymatic reaction; | 96% |
Conditions | Yield |
---|---|
With dimethylsulfide borane complex In tetrahydrofuran at 0 - 20℃; for 6h; | 97% |
With tricarbonyl(η(4)-cycloocta-1,5-diene)iron; phenylsilane In tetrahydrofuran at 20℃; for 24h; Inert atmosphere; UV-irradiation; chemoselective reaction; | 95% |
With indium(III) bromide; 1,1,3,3-Tetramethyldisiloxane In chloroform at 60℃; for 2h; Inert atmosphere; | 73% |
oxirane
2,5-dilithiothiophene
A
2-thiophenethanol
B
2,2′-(thiophene-2,5-diyl)diethanol
Conditions | Yield |
---|---|
In hexane 1) -10 deg C, 2 h, 2) r.t., 24 h; | A 95% B 5% |
2-[2-(tert-butyldimethylsilyloxy)ethyl]thiophene
2-thiophenethanol
Conditions | Yield |
---|---|
With Povidone-Iodine In methanol at 30℃; for 1h; Solvent; Temperature; | 91% |
2,2,2-trichloro-1-(thien-2-yl)-ethanol
2-thiophenethanol
Conditions | Yield |
---|---|
With lithium borohydride; sodium hydroxide In isopropyl alcohol Temperature; Jocic Reaction; Heating; Inert atmosphere; | 89% |
Conditions | Yield |
---|---|
Stage #1: thiophene With sodium; polyethylene; isoprene In tetrahydrofuran; toluene at -1 - 1℃; for 3.5h; Stage #2: oxirane In tetrahydrofuran; toluene at 19 - 21℃; for 2h; Stage #3: With water; ammonium chloride In tetrahydrofuran; toluene at 0 - 22℃; for 0.25h; Product distribution / selectivity; Cooling with ice-methanol bath; | 83% |
Stage #1: thiophene With cis-Octadecenoic acid; sodium; isopropenylbenzene In tetrahydrofuran; toluene at -1 - 1℃; for 3.5h; Stage #2: oxirane In tetrahydrofuran; toluene at 19 - 21℃; for 2h; Stage #3: With water In tetrahydrofuran; toluene at 0 - 20℃; for 0.166667 - 0.25h; Product distribution / selectivity; Cooling with ice-methanol bath; | 83% |
Stage #1: thiophene With cis-Octadecenoic acid; sodium; 2,3-dimethyl-buta-1,3-diene In tetrahydrofuran; toluene at -1 - 1℃; for 2h; Stage #2: oxirane In tetrahydrofuran; toluene at 20℃; for 0.333333h; Stage #3: With water In tetrahydrofuran; toluene at 0 - 13℃; for 0.5h; Product distribution / selectivity; | 83% |
With n-butyllithium In tetrahydrofuran; hexane at 0℃; | 68% |
With n-butyllithium; diethyl ether |
Conditions | Yield |
---|---|
Stage #1: thiophene With n-butyllithium In tetrahydrofuran; hexane at -78℃; Stage #2: ethyleneglycol sulfate In tetrahydrofuran; hexane at -78 - 20℃; Stage #3: With sulfuric acid In tetrahydrofuran; hexane for 3h; Heating; Further stages.; | 79% |
A
2-thiophenethanol
Conditions | Yield |
---|---|
With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride In benzene for 12h; Heating; | A 74% B 13% C 9% |
2-thiophenethanol
Conditions | Yield |
---|---|
Stage #1: thiophen-2-yl-acetic acid propyl ester With sodium tetrahydroborate In tetrahydrofuran at 70℃; for 0.25h; Stage #2: In tetrahydrofuran; methanol at 70℃; for 0.15h; | 68% |
Thiophene-2-acetic acid
1,1,3,3-Tetramethyldisiloxane
2-thiophenethanol
Conditions | Yield |
---|---|
Stage #1: Thiophene-2-acetic acid; 1,1,3,3-Tetramethyldisiloxane With C24H23ClCrIrNO3; sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate In dichloromethane at 40℃; for 15h; Schlenk technique; Glovebox; Inert atmosphere; Stage #2: With water In dichloromethane at 25℃; for 1h; | 68% |
Conditions | Yield |
---|---|
Stage #1: 2-Chloromethylthiophene With chloro-trimethyl-silane; ethylene dibromide; zinc In tetrahydrofuran at 70℃; for 2h; Schlenk technique; Inert atmosphere; Stage #2: formaldehyd In tetrahydrofuran at 70℃; for 6h; Schlenk technique; Inert atmosphere; | 45% |
oxirane
thiophene
A
2-thiophenethanol
B
2,2′-(thiophene-2,5-diyl)diethanol
Conditions | Yield |
---|---|
With n-butyllithium; diethyl ether |
Conditions | Yield |
---|---|
With sodium amalgam; benzene unter Stickstoff; |
Conditions | Yield |
---|---|
With diethyl ether |
Conditions | Yield |
---|---|
With diethyl ether |
methyl 2-thiopheneacetate
A
2-thiophenethanol
Conditions | Yield |
---|---|
With titanium(IV) isopropylate; sodium hydroxide; polymethylhydrosiloxane 1.) 65 deg C, 23 h, 2.) THF, 12 h; Yield given. Multistep reaction. Yields of byproduct given; |
D-Fructose
GLUTATHIONE
A
Thiophene-2-thiol
B
Tetrahydrothiophen-3-one
C
2-ethylthiophene
D
2-Methylpyrazine
E
5-Methylfurfural
F
2-thiophenethanol
G
1-(2-furyl)-1-ethanone
H
2-methylthiophene-3-thiol
I
2-Acetylpyrrole
J
2-methylfuran-3-thiol
Conditions | Yield |
---|---|
In water at 160℃; for 2h; pH=7.5; Maillard reaction; |
Conditions | Yield |
---|---|
With (2-methyl-4-phenyl-1-oxabuta-1,3-diene)tricarbonyliron(0); 1,1,3,3-tetramethyldisilazane In toluene at 50℃; for 24h; Inert atmosphere; chemoselective reaction; |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: Dess-Martin periodane / 0 °C / Inert atmosphere 1.2: 0 - 20 °C / Inert atmosphere 2.1: sodium hydroxide; lithium borohydride / isopropyl alcohol / Heating; Inert atmosphere View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: N,N-dimethyl-formamide / 20 °C / Inert atmosphere 2: sodium hydroxide; lithium borohydride / isopropyl alcohol / Heating; Inert atmosphere View Scheme |
Conditions | Yield |
---|---|
With 2-methyltetrahydrofuran; iodine; zinc for 1h; | 112 g |
2-thiophenethanol
methanesulfonyl chloride
2-(thiophen-2-yl)ethyl methanesulfonate
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0 - 10℃; for 1h; | 100% |
With triethylamine In dichloromethane at 0℃; for 0.5h; | 100% |
With triethylamine In dichloromethane at 25℃; for 2.25h; Cooling with ice; | 99% |
2-thiophenethanol
tert-butyldimethylsilyl chloride
2-[2-(tert-butyldimethylsilyloxy)ethyl]thiophene
Conditions | Yield |
---|---|
With 1H-imidazole In N,N-dimethyl-formamide at 20℃; | 100% |
With dmap; triethylamine In dichloromethane 1.) 0 deg C, 30 min, 2.) RT, 18 h; | 99% |
With dmap; triethylamine In dichloromethane | 98% |
2-thiophenethanol
acetic anhydride
acetic acid-(2-[2]thienyl-ethyl ester)
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine; dmap In dichloromethane at 0 - 20℃; for 3h; | 100% |
With sulfuric acid | |
With dmap; triethylamine In dichloromethane at 20℃; for 0.5h; |
2-thiophenethanol
1-iodo-2-(thien-2-yl)ethane
Conditions | Yield |
---|---|
With 1H-imidazole; iodine; triphenylphosphine In dichloromethane Cooling with ice; | 99% |
With 1H-imidazole; iodine; triphenylphosphine In dichloromethane at 0 - 20℃; for 1.16667h; Inert atmosphere; | 96% |
With 1H-imidazole; iodine; triphenylphosphine In diethyl ether; acetonitrile at 20℃; for 4h; Inert atmosphere; | 88% |
2-thiophenethanol
2-thienylacetaldehyde
Conditions | Yield |
---|---|
With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione In acetonitrile at 80℃; for 2h; | 99% |
With Dess-Martin periodane In dichloromethane at 0 - 20℃; for 2h; | 60% |
With sulfur trioxide pyridine complex; N-ethyl-N,N-diisopropylamine In dichloromethane; dimethyl sulfoxide at -15℃; for 0.5h; Parikh-Doering Oxidation; Inert atmosphere; | 11% |
Conditions | Yield |
---|---|
With iron(II) triflate In toluene at 70℃; for 6h; Pictet-Spengler Synthesis; Green chemistry; | 99% |
2-thiophenethanol
2-bromo-5-(2-hydroxyethyl)thiophene
Conditions | Yield |
---|---|
With N-Bromosuccinimide In toluene at -20.16℃; for 2h; Inert atmosphere; Darkness; | 98.5% |
With N-Bromosuccinimide In toluene at -20 - 20℃; | 90% |
With N-Bromosuccinimide In toluene at -20 - 25℃; for 12h; Inert atmosphere; | 90% |
2-thiophenethanol
p-toluenesulfonyl chloride
2-(2-thienyl)ethyl tosylate
Conditions | Yield |
---|---|
With triethylamine at 35℃; Cooling with ice; | 98% |
With triethylamine In toluene at 5 - 30℃; for 20.8333h; Product distribution / selectivity; | 96.37% |
With triethylamine In dichloromethane at -5 - 20℃; for 2h; | 96.5% |
2-thiophenethanol
chlorophosphoric acid diphenyl ester
diphenyl 2-(thiophen-2-yl)ethyl phosphate
Conditions | Yield |
---|---|
With tris(pentafluorophenyl)borate; triethylamine In dichloromethane at 20℃; for 0.5h; | 97% |
Conditions | Yield |
---|---|
With oxygen; triethylamine at 80℃; for 15h; Reagent/catalyst; Temperature; | 96.5% |
With Iron(III) nitrate nonahydrate; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; potassium chloride; oxygen In 1,2-dichloro-ethane at 25℃; for 12h; | 85% |
With sodium hypochlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical In aq. phosphate buffer; water; acetonitrile at 35℃; for 6h; Catalytic behavior; Reagent/catalyst; Temperature; Green chemistry; | 85% |
With iridium hexafluoride; sulphate-doped anatase; potassium oxide In dichloromethane at 85℃; Temperature; |
Conditions | Yield |
---|---|
With sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride In toluene at 20℃; for 4h; | 96% |
2-thiophenethanol
Dimethoxymethane
2-(2-methoxymethoxyethyl)thiophene
Conditions | Yield |
---|---|
With lithium chloride; toluene-4-sulfonic acid for 5h; Heating / reflux; | 96% |
2-thiophenethanol
6-chloroquinoline
6-(2-(thiophen-2-yl)ethoxy)quinoline
Conditions | Yield |
---|---|
With CH3O3S(1-)*C31H49OP*C12H9NPd(1+); caesium carbonate In toluene at 90℃; for 16h; Inert atmosphere; | 96% |
Conditions | Yield |
---|---|
With 1,10-Phenanthroline; iron(II) acetylacetonate; potassium carbonate In toluene at 130℃; for 24h; Schlenk technique; Inert atmosphere; Sealed tube; | 96% |
Conditions | Yield |
---|---|
With iron(II) triflate In toluene at 70℃; for 24h; Pictet-Spengler Synthesis; Green chemistry; | 95% |
2-thiophenethanol
2-(2-Bromoethyl)thiophene
Conditions | Yield |
---|---|
With carbon tetrabromide; triphenylphosphine In tetrahydrofuran at 0℃; Schlenk technique; Inert atmosphere; | 94% |
With bromine; triphenylphosphine In dichloromethane at 20℃; | 69% |
64% |
2-thiophenethanol
5-bromosalicylaldehyde dimethyl acetal
2-(2-(4-bromo-2-(dimethoxymethyl)phenoxy)ethyl)thiophene
Conditions | Yield |
---|---|
With diisopropyl (E)-azodicarboxylate; triphenylphosphine In benzene at 0 - 20℃; for 0.5h; | 93.4% |
With di-isopropyl azodicarboxylate; triphenylphosphine In benzene at 0 - 20℃; for 0.5h; | 93.4% |
Conditions | Yield |
---|---|
With sodium hydride In tetrahydrofuran; paraffin for 1h; Ambient temperature; | 93% |
With sodium hydride In tetrahydrofuran at 50℃; for 1h; | 87% |
With sodium amide In diethyl ether; ammonia at -60 - -50℃; for 0.5h; | 69% |
Stage #1: 2-thiophenethanol With sodium hydride In N,N-dimethyl-formamide at 20℃; for 0.5h; Stage #2: methyl iodide In DMF (N,N-dimethyl-formamide) at 20℃; for 0.5h; |
2-thiophenethanol
2-Methoxyethoxymethyl chloride
2-(2-((2-methoxyethoxy)methoxy)ethyl)thiophene
Conditions | Yield |
---|---|
With dmap; N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 12h; | 93% |
With diisopropylamine In dichloromethane at 0℃; for 4h; Heating / reflux; | 85% |
With N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 2.5h; Inert atmosphere; |
Conditions | Yield |
---|---|
Stage #1: 2-thiophenethanol With sodium hydride In tetrahydrofuran; mineral oil at 0℃; Inert atmosphere; Stage #2: Tetrafluorophthalonitrile In tetrahydrofuran; mineral oil at -50 - 20℃; Reagent/catalyst; Temperature; Inert atmosphere; | 93% |
2-thiophenethanol
(E)-2-(3-(thiophen-2-yl)prop-1-enyl)thiophene
Conditions | Yield |
---|---|
With (bis[(2-diisopropylphosphino)ethyl]amine)Mn(CO)2Br; sodium hydroxide In 5,5-dimethyl-1,3-cyclohexadiene at 145℃; for 16h; Schlenk technique; Inert atmosphere; | 93% |
With tris(triphenylphosphine)ruthenium(II) chloride; 1,3-bis-(diphenylphosphino)propane; sodium t-butanolate In toluene at 111℃; for 24h; Inert atmosphere; | 56% |
Conditions | Yield |
---|---|
Stage #1: 4-cyanophenylacetic acid With dmap; dicyclohexyl-carbodiimide In dichloromethane at 20℃; for 0.166667h; Stage #2: 2-thiophenethanol In dichloromethane at 20℃; | 93% |
Conditions | Yield |
---|---|
With C12H10N(1-)*Pd(2+)*CH3O3S(1-)*C31H49O2P; sodium t-butanolate In 1,4-dioxane at 20℃; for 12h; Sealed tube; Schlenk technique; Inert atmosphere; | 93% |
2-thiophenethanol
carbon monoxide
Conditions | Yield |
---|---|
With dipotassium hydrogenphosphate; palladium diacetate; (S)-(-)-(6,6’-dimethoxybiphenyl-2,2’-diyl)bis(diphenylphosphine) In chlorobenzene; acetone at 20 - 80℃; for 30h; Schlenk technique; enantioselective reaction; | 93% |
Conditions | Yield |
---|---|
With C10H10Zr(2+)*2CF3O3S(1-)*C4H8O at 80℃; for 24h; Sealed tube; | 91% |
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