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Dayang Chem (Hangzhou) Co.,Ltd.

Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities

2,6-Diiodo-4-nitrophenol

Cas:305-85-1

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

inquiry

Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

2,6-Diiodo-4-nitrophenol

Cas:305-85-1

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

inquiry

Henan Tianfu Chemical Co., Ltd.

Our company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so

305-85-1 C6H3I2NO3 2,6-Diiodo-4-nitrophenol

Cas:305-85-1

Min.Order:1 Metric Ton

Negotiable

Type:Lab/Research institutions

inquiry

Shanghai Upbio Tech Co.,Ltd

1.In No Less 10 years exporting experience. you can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specializ

Phenol,2,6-diiodo-4-nitro-

Cas:305-85-1

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Hebei Quanhe Biotechnology Co. LTD

1. Timely and efficient service to ensure communication with customers 2. Produce products of different specifications and sizes according to your requirements. 3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures s

2,6-Diiodo-4-nitrophenol

Cas:305-85-1

Min.Order:1 Kilogram

FOB Price: $40.0 / 50.0

Type:Lab/Research institutions

inquiry

Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

Phenol,2,6-diiodo-4-nitro-

Cas:305-85-1

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou Keyingchem Co.,Ltd

Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det

2,6-Diiodo-4-nitrophenol

Cas:305-85-1

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

inquiry

Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply 2,6-Diiodo-4-nitrophenol

Cas:305-85-1

Min.Order:0 Metric Ton

Negotiable

Type:Other

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

Phenol,2,6-diiodo-4-nitro-

Cas:305-85-1

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Xiamen Jenny Chemical Technology Co., Ltd.

GMP standard, high purity, competitive price, in stock 1. Quick Response: within 6 hours after receiving your email. 2. Quality Guarantee: All products are strictly tested by our QC, confirmed by QA, and approved by a third-party lab in China, USA,

2,6-Diiodo-4-nitrophenol

Cas:305-85-1

Min.Order:1 Milligram

Negotiable

Type:Trading Company

inquiry

Shandong Mopai Biotechnology Co., LTD

Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W

Phenol,2,6-diiodo-4-nitro-

Cas:305-85-1

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Win-Win chemical Co.Ltd

Stock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai

2,6-Diiodo-4-nitrophenol cas no. 305-85-1 98%

Cas:305-85-1

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Henan Allgreen Chemical Co.,Ltd

high quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea

2,6-Diiodo-4-nitrophenol, 97%

Cas:305-85-1

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Henan Sinotech Import&Export Corporation

Appearance:White powder Storage:Store in cool and dry place, away from sun light. Package:drum Application:Anthelmintic Transportation:By sea or by air Port:Qingdao Port

2,6-Diiodo-4-nitrophenol

Cas:305-85-1

Min.Order:1 Kilogram

FOB Price: $1.0

Type:Other

inquiry

Nanjing HuaNuo Bio-Pharmacuetical Co.,Ltd

Independent research and development of impurities, familiar with the market and impurity characteristics; We can ship out on the same day if the products are in stock; Focus on impurity development of new products in the market; Expert in customizi

Disophenol

Cas:305-85-1

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou Ocean Chemical Co., Ltd.

★.Best quality according to requirement ★.Competitive price in China market ★.Mature Technical support ★.Professional logistic support

2,6-Diiodo-4-nitrophenol

Cas:305-85-1

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Antimex Chemical Limied

factory?direct?sale Application:Fine chemical intermediates, used as the main raw material for the synthesis of various pesticides, medicines, surfactants, polymer monomers, and antifungal agents

Phenol,2,6-diiodo-4-nitro-

Cas:305-85-1

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Guangdong Juda Chemical Industrial Co.,Limited

Appearance:solid or liquid Storage:sealed in cool and dry place Package:As customer's requested Application:Pharma Intermediate Transportation:by courier/air/sea Port:Any port in China

2,6-Diiodo-4-nitrophenol CAS No.305-85-1

Cas:305-85-1

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Hangzhou Fandachem Co.,Ltd

2,6-Diiodo-4-nitrophenol cas 305-85-1Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express

2,6-Diiodo-4-nitrophenol cas 305-85-1

Cas:305-85-1

Min.Order:0

Negotiable

Type:Other

inquiry

Asure Biochem CO.,LTD.

*stable and better quality products*efficient and meticulous servicesAppearance:Powder Storage:Store in dry, cool and ventilated place Package:10G/bottle 1kg/tin 5kg/tin 25kg/carton Application:1. Chemical raw materials 2. Used as an analytical reage

2,6-Diiodo-4-nitrophenol

Cas:305-85-1

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Shanghai Yuanye Bio-Technology Co., Ltd.

good quality, competitive price, thoughtful after sale serviceAppearance:white powder Storage:Keep it in dry,shady and cool place Package:100mg Application:Pharma;Industry;Agricultural;chemical reaserch Transportation:by express or by sea Port:Any po

2,6-Diiodo-4-Nitrophenol

Cas:305-85-1

Min.Order:0

Negotiable

Type:Trading Company

inquiry

ZHEJIANG JIUZHOU CHEM CO.,LTD

factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin

2,6-Diiodo-4-nitrophenol

Cas:305-85-1

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Amadis Chemical Co., Ltd.

1.Professional synthesis laboratory and production base. 2.Strong synthesis team and service team. 3.Professional data management system. 4.We provide the professional test date and product information ,ex. HNMR ,CNMR,FNMR, HPLC/G

2,6-diiodo-4-nitrophenolate

Cas:305-85-1

Min.Order:10 Milligram

Negotiable

Type:Lab/Research institutions

inquiry

HENAN SUNLAKE ENTERPRISE CORPORATION

2,6-Diiodo-4-nitrophenol

Cas:305-85-1

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

inquiry

Hubei Jusheng Technology Co., Ltd.,

1, High quality with competitive price: We are manufacturer and can provide high quality products with factory price. 2, Fast and safe delivery 1) Parcels can be sent out within 24 hours after payment. Tracking number is available. 2)

high quality Disophenol in stock with best price

Cas:305-85-1

Min.Order:10 Gram

Negotiable

Type:Trading Company

inquiry

Capot Chemical Co., Ltd.

At Capot,We can synthesize and purify your complex molecules from 100 gram to 10 tons.Appearance:Clear colorless to light yellow liquid Storage:Dry,Seal and Cool place Package:1G,5G,10G,25G,100G,250G,500G,1KG,5KG,10KG,25KG,50KG,100KG,150KG,200KG. App

2,6-Diiodo-4-nitrophenol

Cas:305-85-1

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Finetech Industry Limited

FINETECH INDUSTRY LIMITED is a LONDON based CRO company providing drug discovery & development services to worldwide clients. FINETECH INDUSTRY LIMITED supplies the 2,6-Diiodo-4-nitrophenol, CAS:305-85-1 with the most competitive price and the best q

2,6-Diiodo-4-nitrophenol

Cas:305-85-1

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Wuxi Morality Chemical Co., Ltd

Do best quality products, erect the morality model Application:please email us, thanks

2,6-Diiodo-4-nitrophenol

Cas:305-85-1

Min.Order:0

Negotiable

Type:Other

inquiry

ZHENFEI INDUSTRY CO.,LTD

better purity and qualityAppearance:white crystalline powder Package:25KG/drum Application:pharm?and?intermediates Transportation:By courier/sir/sea

2,6-Diiodo-4-nitrophenol

Cas:305-85-1

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Debye Scientific

Debyesci is here who supplied several kinds of chemical products to global pharmaceutical, drug discovery, agrochemical and biotechnology industries for four yearsOur key scientific leadership team has gained experience in top research and developmen

2,6-Diiodo-4-nitrophenol

Cas:305-85-1

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Synthetic route

4-nitro-phenol
100-02-7

4-nitro-phenol

2,6-diiodo-4-nitrophenol
305-85-1

2,6-diiodo-4-nitrophenol

Conditions
ConditionsYield
With hydrogenchloride; potassium iodate; potassium iodide In methanol; water at 20℃;99%
With sodium periodate; sulfuric acid; iodine; potassium iodide; sodium sulfite In water; acetic acid at 25℃; for 4h;98%
With N-iodo-S-methyl-S-phenyl sulfoximine; acetic acid at 22℃; for 3h; Sealed tube;98%
4-nitro-phenol
100-02-7

4-nitro-phenol

A

2,6-diiodo-4-nitrophenol
305-85-1

2,6-diiodo-4-nitrophenol

B

2-iodo-4-nitrophenol
89487-91-2

2-iodo-4-nitrophenol

Conditions
ConditionsYield
With iodine; silver sulfate In ethanol at 20℃; for 0.5h;A 22%
B 50%
With sulfuric acid; dihydrogen peroxide; potassium iodide In methanol at 60℃; for 2h;A 18%
B 42%
With iodine; silver nitrate In acetonitrile for 2h; Ambient temperature;A 5%
B 12%
p-nitrobenzene iodide
636-98-6

p-nitrobenzene iodide

A

para-dinitrobenzene
100-25-4

para-dinitrobenzene

B

2,6-diiodo-4-nitrophenol
305-85-1

2,6-diiodo-4-nitrophenol

Conditions
ConditionsYield
With sodium nitrite
2,4,6-Triiodophenol
609-23-4

2,4,6-Triiodophenol

A

2,6-diiodo-4-nitrophenol
305-85-1

2,6-diiodo-4-nitrophenol

B

diiodo-4,6 nitro-2 phenol
20294-48-8

diiodo-4,6 nitro-2 phenol

Conditions
ConditionsYield
With acetic acid; sodium nitrite; benzene Trennung durch fraktionierte Krystallisation der Kaliumsalze;
With acetic acid; sodium nitrite; benzene
2-hydroxyl-5-nitrobenzenesulfonic acid
616-59-1

2-hydroxyl-5-nitrobenzenesulfonic acid

A

2,6-diiodo-4-nitrophenol
305-85-1

2,6-diiodo-4-nitrophenol

B

2-hydroxy-3-iodo-5-nitro-benzenesulfonic acid

2-hydroxy-3-iodo-5-nitro-benzenesulfonic acid

Conditions
ConditionsYield
With ethanol; iodine; mercury(II) oxide
5-nitrosalicylic acid
96-97-9

5-nitrosalicylic acid

2,6-diiodo-4-nitrophenol
305-85-1

2,6-diiodo-4-nitrophenol

Conditions
ConditionsYield
With iodine; mercury(II) oxide
5-nitrosalicylic acid
96-97-9

5-nitrosalicylic acid

A

2,6-diiodo-4-nitrophenol
305-85-1

2,6-diiodo-4-nitrophenol

B

2-hydroxy-3-iodo-5-nitro-benzoic acid
861565-06-2

2-hydroxy-3-iodo-5-nitro-benzoic acid

Conditions
ConditionsYield
With ethanol; iodine; mercury(II) oxide
2,6-diiodo-phenol
28177-54-0

2,6-diiodo-phenol

2,6-diiodo-4-nitrophenol
305-85-1

2,6-diiodo-4-nitrophenol

Conditions
ConditionsYield
durch Nitrierung;
2,6-diiodo-phenol
28177-54-0

2,6-diiodo-phenol

A

2,6-diiodo-4-nitrophenol
305-85-1

2,6-diiodo-4-nitrophenol

B

2-iodo-6-nitro-phenol
13073-26-2

2-iodo-6-nitro-phenol

Conditions
ConditionsYield
With nitric acid
1-iodyl-4-nitrobenzene
16825-79-9

1-iodyl-4-nitrobenzene

2,6-diiodo-4-nitrophenol
305-85-1

2,6-diiodo-4-nitrophenol

Conditions
ConditionsYield
With sodium nitrite
With sodium azide
4-nitro-phenol
100-02-7

4-nitro-phenol

iodine
7553-56-2

iodine

iodic acid
7782-68-5

iodic acid

alkali

alkali

2,6-diiodo-4-nitrophenol
305-85-1

2,6-diiodo-4-nitrophenol

4-nitro-phenol
100-02-7

4-nitro-phenol

ammonia
7664-41-7

ammonia

iodine-potassium iodide solution

iodine-potassium iodide solution

2,6-diiodo-4-nitrophenol
305-85-1

2,6-diiodo-4-nitrophenol

4-nitro-phenol
100-02-7

4-nitro-phenol

mercury oxide

mercury oxide

2,6-diiodo-4-nitrophenol
305-85-1

2,6-diiodo-4-nitrophenol

Conditions
ConditionsYield
durch Jodierung;
2-hydroxy-3-iodo-5-nitro-benzoic acid
861565-06-2

2-hydroxy-3-iodo-5-nitro-benzoic acid

alkali

alkali

2,6-diiodo-4-nitrophenol
305-85-1

2,6-diiodo-4-nitrophenol

Conditions
ConditionsYield
bei der Jodierung;
ethanol
64-17-5

ethanol

5-nitrosalicylic acid
96-97-9

5-nitrosalicylic acid

iodine
7553-56-2

iodine

mercury oxide

mercury oxide

A

2,6-diiodo-4-nitrophenol
305-85-1

2,6-diiodo-4-nitrophenol

B

2-hydroxy-3-iodo-5-nitro-benzoic acid
861565-06-2

2-hydroxy-3-iodo-5-nitro-benzoic acid

2,4,6-Triiodophenol
609-23-4

2,4,6-Triiodophenol

acetic acid
64-19-7

acetic acid

benzene
71-43-2

benzene

NaNO2

NaNO2

A

2,6-diiodo-4-nitrophenol
305-85-1

2,6-diiodo-4-nitrophenol

B

diiodo-4,6 nitro-2 phenol
20294-48-8

diiodo-4,6 nitro-2 phenol

Conditions
ConditionsYield
at 12 - 15℃;
2-hydroxyl-5-nitrobenzenesulfonic acid
616-59-1

2-hydroxyl-5-nitrobenzenesulfonic acid

A

2,6-diiodo-4-nitrophenol
305-85-1

2,6-diiodo-4-nitrophenol

B

6-iodo-4-nitro-phenol-sulfonic acid-(2)

6-iodo-4-nitro-phenol-sulfonic acid-(2)

Conditions
ConditionsYield
With ethanol; iodine; mercury
2-hydroxyl-5-nitrobenzenesulfonic acid
616-59-1

2-hydroxyl-5-nitrobenzenesulfonic acid

iodine
7553-56-2

iodine

mercury oxide

mercury oxide

A

2,6-diiodo-4-nitrophenol
305-85-1

2,6-diiodo-4-nitrophenol

B

6-iodo-4-nitro-phenol-sulfonic acid-(2)

6-iodo-4-nitro-phenol-sulfonic acid-(2)

5-nitrosalicylic acid
96-97-9

5-nitrosalicylic acid

A

2,6-diiodo-4-nitrophenol
305-85-1

2,6-diiodo-4-nitrophenol

B

x-iodo-5-nitro-2-oxy-benzoic acid

x-iodo-5-nitro-2-oxy-benzoic acid

Conditions
ConditionsYield
With iodine; mercury(II) oxide
1-iodyl-4-nitrobenzene
16825-79-9

1-iodyl-4-nitrobenzene

sodium nitrite

sodium nitrite

A

para-dinitrobenzene
100-25-4

para-dinitrobenzene

B

2,6-diiodo-4-nitrophenol
305-85-1

2,6-diiodo-4-nitrophenol

1-iodyl-4-nitrobenzene
16825-79-9

1-iodyl-4-nitrobenzene

aqueous NaNO2-solution

aqueous NaNO2-solution

A

p-nitrobenzene iodide
636-98-6

p-nitrobenzene iodide

B

para-dinitrobenzene
100-25-4

para-dinitrobenzene

C

2,6-diiodo-4-nitrophenol
305-85-1

2,6-diiodo-4-nitrophenol

1-iodyl-4-nitrobenzene
16825-79-9

1-iodyl-4-nitrobenzene

aqueous NaN3-solution

aqueous NaN3-solution

A

4-nitrophenyl azide
1516-60-5

4-nitrophenyl azide

B

2,6-diiodo-4-nitrophenol
305-85-1

2,6-diiodo-4-nitrophenol

2,6-diiodo-phenol
28177-54-0

2,6-diiodo-phenol

nitric acid
7697-37-2

nitric acid

acetic acid
64-19-7

acetic acid

A

2,6-diiodo-4-nitrophenol
305-85-1

2,6-diiodo-4-nitrophenol

B

2-iodo-6-nitro-phenol
13073-26-2

2-iodo-6-nitro-phenol

Conditions
ConditionsYield
at -5℃;
phenol
108-95-2

phenol

phosphorous oxychloride

phosphorous oxychloride

2,6-diiodo-4-nitrophenol
305-85-1

2,6-diiodo-4-nitrophenol

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 25 percent / AgNO3, Br2 / acetonitrile / 2 h / Ambient temperature
2: 5 percent / AgNO3, I2 / acetonitrile / 2 h / Ambient temperature
View Scheme
Multi-step reaction with 2 steps
1: 29 percent / AgNO3, I2 / acetonitrile / 2 h / Ambient temperature
2: 5 percent / AgNO3, I2 / acetonitrile / 2 h / Ambient temperature
View Scheme
sodium phenoxide
139-02-6

sodium phenoxide

2,6-diiodo-4-nitrophenol
305-85-1

2,6-diiodo-4-nitrophenol

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: CS2; iodine
2: durch Nitrierung
View Scheme
Multi-step reaction with 2 steps
1: CS2; iodine
2: nitric acid
View Scheme
2,6-diiodo-4-nitrophenol
305-85-1

2,6-diiodo-4-nitrophenol

ethyl iodide
75-03-6

ethyl iodide

3,5-diiodo-4-ethoxy-nitrobenzene
31199-98-1

3,5-diiodo-4-ethoxy-nitrobenzene

Conditions
ConditionsYield
With potassium carbonate In acetone at 60℃;95%
2,6-diiodo-4-nitrophenol
305-85-1

2,6-diiodo-4-nitrophenol

dimethyl sulfate
77-78-1

dimethyl sulfate

1-methoxy-2,6-diiodido-4-nitrobenzene
31106-75-9

1-methoxy-2,6-diiodido-4-nitrobenzene

Conditions
ConditionsYield
With potassium carbonate In acetone at 0℃; for 18h; Reflux; Schlenk technique;92%
With potassium carbonate In acetone at 65℃; for 18h; Inert atmosphere;87%
With potassium carbonate In acetone at 0 - 65℃; for 18h; Inert atmosphere;87%
With alkali
2,6-diiodo-4-nitrophenol
305-85-1

2,6-diiodo-4-nitrophenol

p-toluenesulfonyl chloride
98-59-9

p-toluenesulfonyl chloride

2,6-diiodo-4-nitrophenyl 4-methylbenzenesulfonate
851077-63-9

2,6-diiodo-4-nitrophenyl 4-methylbenzenesulfonate

Conditions
ConditionsYield
With pyridine at 0 - 20℃;90%
2,6-diiodo-4-nitrophenol
305-85-1

2,6-diiodo-4-nitrophenol

1-(bromomethyl)-4-(1,1-dimethylethyl)benzene
18880-00-7

1-(bromomethyl)-4-(1,1-dimethylethyl)benzene

4-(t-butyl)benzyl 2,6-diiodo-4-nitrophenyl ether
1423135-83-4

4-(t-butyl)benzyl 2,6-diiodo-4-nitrophenyl ether

Conditions
ConditionsYield
With potassium carbonate In acetonitrile for 24h; Reflux;80%
Cyclopropylacetylene
6746-94-7

Cyclopropylacetylene

2,6-diiodo-4-nitrophenol
305-85-1

2,6-diiodo-4-nitrophenol

2-cyclopropyl-7-iodo-5-nitro-1-benzofuran

2-cyclopropyl-7-iodo-5-nitro-1-benzofuran

Conditions
ConditionsYield
With pyridine; copper(I) oxide for 2h; Reflux;78%
With pyridine; copper(I) oxide for 2h; Reflux;78%
pent-1-yn-3-ol
4187-86-4

pent-1-yn-3-ol

2,6-diiodo-4-nitrophenol
305-85-1

2,6-diiodo-4-nitrophenol

1-[2-(1-hydroxy-propyl)-5-nitro-benzofuran-7-yl]-pent-1-yn-3-ol

1-[2-(1-hydroxy-propyl)-5-nitro-benzofuran-7-yl]-pent-1-yn-3-ol

Conditions
ConditionsYield
Stage #1: 2,6-diiodo-4-nitrophenol With copper(l) iodide; triphenylphosphine; (S)-1-Pyrrolidin-2-yl-methanol; palladium on activated charcoal In water at 25℃; for 1h; Sonogashira coupling;
Stage #2: pent-1-yn-3-ol In water at 80℃; for 3h;
75%
2,6-diiodo-4-nitrophenol
305-85-1

2,6-diiodo-4-nitrophenol

2-methyl-but-3-yn-2-ol
115-19-5

2-methyl-but-3-yn-2-ol

4-[2-(1-hydroxy-1-methyl-ethyl)-5-nitro-benzofuran-7-yl]-2-methyl-but-3-yn-2-ol

4-[2-(1-hydroxy-1-methyl-ethyl)-5-nitro-benzofuran-7-yl]-2-methyl-but-3-yn-2-ol

Conditions
ConditionsYield
Stage #1: 2,6-diiodo-4-nitrophenol With copper(l) iodide; triphenylphosphine; (S)-1-Pyrrolidin-2-yl-methanol; palladium on activated charcoal In water at 25℃; for 1h; Sonogashira coupling;
Stage #2: 2-methyl-but-3-yn-2-ol In water at 80℃; for 3h;
75%
2,6-diiodo-4-nitrophenol
305-85-1

2,6-diiodo-4-nitrophenol

(R)-(4-(2,5-dimethyl-1H-pyrrol-1-yl)cyclopent-1-en-1-yl)methanol

(R)-(4-(2,5-dimethyl-1H-pyrrol-1-yl)cyclopent-1-en-1-yl)methanol

(R)-1-(3-((2,6-diiodo-4-nitrophenoxy)methyl)cyclopent-3-en-1-yl)-2,5-dimethyl-1H-pyrrole

(R)-1-(3-((2,6-diiodo-4-nitrophenoxy)methyl)cyclopent-3-en-1-yl)-2,5-dimethyl-1H-pyrrole

Conditions
ConditionsYield
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran at 20℃; for 16h;71%
2,6-diiodo-4-nitrophenol
305-85-1

2,6-diiodo-4-nitrophenol

epichlorohydrin
106-89-8

epichlorohydrin

1-<2',6'-diiodo-4'-nitrophenoxy->-2,3-epoxy propane
95646-27-8

1-<2',6'-diiodo-4'-nitrophenoxy->-2,3-epoxy propane

Conditions
ConditionsYield
With pyridine at 90 - 95℃; for 1h;70%
2,6-diiodo-4-nitrophenol
305-85-1

2,6-diiodo-4-nitrophenol

but-3-yn-2-ol
2028-63-9

but-3-yn-2-ol

4-[2-(1-hydroxy-ethyl)-5-nitro-benzofuran-7-yl]-but-3-yn-2-ol

4-[2-(1-hydroxy-ethyl)-5-nitro-benzofuran-7-yl]-but-3-yn-2-ol

Conditions
ConditionsYield
Stage #1: 2,6-diiodo-4-nitrophenol With copper(l) iodide; triphenylphosphine; (S)-1-Pyrrolidin-2-yl-methanol; palladium on activated charcoal In water at 25℃; for 1h; Sonogashira coupling;
Stage #2: but-3-yn-2-ol In water at 80℃; for 3h;
70%
2,6-diiodo-4-nitrophenol
305-85-1

2,6-diiodo-4-nitrophenol

2-(trimethylsilyl)phenyl trifluoromethanesulfonate
88284-48-4

2-(trimethylsilyl)phenyl trifluoromethanesulfonate

1,3-diiodo-5-nitro-2-phenoxybenzene

1,3-diiodo-5-nitro-2-phenoxybenzene

Conditions
ConditionsYield
With cesium fluoride In acetonitrile at 20℃; for 24h;65%
2,6-diiodo-4-nitrophenol
305-85-1

2,6-diiodo-4-nitrophenol

phenylacetylene
536-74-3

phenylacetylene

7-iodo-5-nitro-2-phenyl-1-benzofuran

7-iodo-5-nitro-2-phenyl-1-benzofuran

Conditions
ConditionsYield
With pyridine; copper(I) oxide Inert atmosphere; Reflux;63%
1,7-dibromoheptane
4549-31-9

1,7-dibromoheptane

2,6-diiodo-4-nitrophenol
305-85-1

2,6-diiodo-4-nitrophenol

1,3-dibromo-2-(7-bromoheptyloxy)-5-nitrobenzene
1374327-23-7

1,3-dibromo-2-(7-bromoheptyloxy)-5-nitrobenzene

Conditions
ConditionsYield
With potassium carbonate In acetonitrile52%
2,6-diiodo-4-nitrophenol
305-85-1

2,6-diiodo-4-nitrophenol

allyl bromide
106-95-6

allyl bromide

2,6-diiodo-4-nitro-(2-allyl)-oxybenzene
95646-25-6

2,6-diiodo-4-nitro-(2-allyl)-oxybenzene

Conditions
ConditionsYield
With sodium carbonate In N,N-dimethyl-formamide at 80℃; for 6h;50%
2,6-diiodo-4-nitrophenol
305-85-1

2,6-diiodo-4-nitrophenol

methyl iodide
74-88-4

methyl iodide

1-methoxy-2,6-diiodido-4-nitrobenzene
31106-75-9

1-methoxy-2,6-diiodido-4-nitrobenzene

Conditions
ConditionsYield
With potassium carbonate In N,N-dimethyl-formamide at 70℃; for 60h;42%
With potassium carbonate In acetone for 6h; Heating;
2,6-diiodo-4-nitrophenol
305-85-1

2,6-diiodo-4-nitrophenol

trimethylsilylacetylene
1066-54-2

trimethylsilylacetylene

4-nitro-2,6-bis-trimethylsilanylethynyl-phenol

4-nitro-2,6-bis-trimethylsilanylethynyl-phenol

Conditions
ConditionsYield
With bis-triphenylphosphine-palladium(II) chloride; copper diacetate; diisopropylamine at 20℃; for 1h;40%
2,6-diiodo-4-nitrophenol
305-85-1

2,6-diiodo-4-nitrophenol

4-amino-2-iodophenol
89640-51-7

4-amino-2-iodophenol

Conditions
ConditionsYield
With sodium hydroxide; sodium dithionite at 75℃;30%
2,6-diiodo-4-nitrophenol
305-85-1

2,6-diiodo-4-nitrophenol

2-(3,4,5-trimethoxyphenyl)-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyrrole

2-(3,4,5-trimethoxyphenyl)-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyrrole

2,6-bis[5-(3,4,5-trimethoxyphenyl)pyrrol-2-yl]-4-nitrophenol

2,6-bis[5-(3,4,5-trimethoxyphenyl)pyrrol-2-yl]-4-nitrophenol

Conditions
ConditionsYield
With palladium diacetate; sodium carbonate; XPhos In 1,2-dimethoxyethane; water Suzuki Coupling; Inert atmosphere; Reflux;24%
2,6-diiodo-4-nitrophenol
305-85-1

2,6-diiodo-4-nitrophenol

2-(3,4,5-trihexadecyloxyphenyl)-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyrrole

2-(3,4,5-trihexadecyloxyphenyl)-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyrrole

2,6-bis(5-(3,4,5-trihexadecyloxyphenyl)pyrrol-2-yl)-4-nitrophenol

2,6-bis(5-(3,4,5-trihexadecyloxyphenyl)pyrrol-2-yl)-4-nitrophenol

Conditions
ConditionsYield
With tri-tert-butyl phosphine; palladium diacetate; sodium carbonate In 1,2-dimethoxyethane; water for 5h; Suzuki Coupling; Inert atmosphere; Reflux;22%
2,6-diiodo-4-nitrophenol
305-85-1

2,6-diiodo-4-nitrophenol

p-chlorobenzylisocyanide
39546-47-9

p-chlorobenzylisocyanide

1-amino-2-propene
107-11-9

1-amino-2-propene

isovaleraldehyde
590-86-3

isovaleraldehyde

C22H24ClI2N3O3
1007383-12-1

C22H24ClI2N3O3

Conditions
ConditionsYield
With ammonium chloride In water; toluene at 100℃; for 20h; Ugi-Smiles reaction; Inert atmosphere;18%
2,6-diiodo-4-nitrophenol
305-85-1

2,6-diiodo-4-nitrophenol

5-ethoxycarbonyl-3,4-dimethyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxoborolan-2-yl)pyrrole

5-ethoxycarbonyl-3,4-dimethyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxoborolan-2-yl)pyrrole

2,6-bis(5-ethoxycarbonyl-3,4-dimethylpyrrol-2-yl)-4-nitrophenol

2,6-bis(5-ethoxycarbonyl-3,4-dimethylpyrrol-2-yl)-4-nitrophenol

Conditions
ConditionsYield
With tri-tert-butyl phosphine; palladium diacetate; sodium carbonate In 1,2-dimethoxyethane; water at 90℃; for 14h; Suzuki Coupling; Inert atmosphere;18%
2,6-diiodo-4-nitrophenol
305-85-1

2,6-diiodo-4-nitrophenol

5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-2-phenylpyrrole

5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-2-phenylpyrrole

4-nitro-2,6-di(5-phenylpyrrol-2-yl)phenol

4-nitro-2,6-di(5-phenylpyrrol-2-yl)phenol

Conditions
ConditionsYield
With tri-tert-butyl phosphine; palladium diacetate; sodium carbonate In 1,2-dimethoxyethane; water Suzuki Coupling; Inert atmosphere; Reflux;8.7%
2,6-diiodo-4-nitrophenol
305-85-1

2,6-diiodo-4-nitrophenol

2-(3,4,5-tridodecyloxyphenyl)-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyrrole

2-(3,4,5-tridodecyloxyphenyl)-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyrrole

2,6-bis(5-(3,4,5-tridodecyloxyphenyl)pyrrol-2-yl)-4-nitrophenol

2,6-bis(5-(3,4,5-tridodecyloxyphenyl)pyrrol-2-yl)-4-nitrophenol

Conditions
ConditionsYield
With tri-tert-butyl phosphine; palladium diacetate; sodium carbonate In 1,2-dimethoxyethane; water for 7h; Suzuki Coupling; Inert atmosphere; Reflux;5.5%
2,6-diiodo-4-nitrophenol
305-85-1

2,6-diiodo-4-nitrophenol

5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-2-(3,4,5-trioctyloxyphenyl)pyrrole

5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-2-(3,4,5-trioctyloxyphenyl)pyrrole

4-nitro-2,6-bis(5-(3,4,5-trioctyloxyphenyl)pyrrol-2-yl)phenol

4-nitro-2,6-bis(5-(3,4,5-trioctyloxyphenyl)pyrrol-2-yl)phenol

Conditions
ConditionsYield
With tri-tert-butyl phosphine; palladium diacetate; sodium carbonate In 1,2-dimethoxyethane; water Suzuki Coupling; Inert atmosphere; Reflux;1.6%
2,6-diiodo-4-nitrophenol
305-85-1

2,6-diiodo-4-nitrophenol

2,6-diiodo-p-benzoquinone
20389-01-9

2,6-diiodo-p-benzoquinone

Conditions
ConditionsYield
With tin; acetic acid anschliessendes Behandeln mit CrO3 in wss. H2SO4;
Multi-step reaction with 3 steps
1: sodium dithionite; aqueous sodium carbonate
2: ethanolic H2SO4 / Diazotization.anschliessendes Kochen
3: aqueous KOH; CrO3; water
View Scheme
2,6-diiodo-4-nitrophenol
305-85-1

2,6-diiodo-4-nitrophenol

2,6-diiodo-4-aminophenol
2297-82-7

2,6-diiodo-4-aminophenol

Conditions
ConditionsYield
With hydrogenchloride; tin(ll) chloride
With sodium dithionite; sodium carbonate
With tin; acetic acid
With hydrochloride of tin dichloride
With tin(II) chloride dihdyrate In ethanol at 78℃; for 5h;4 g

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