1,2,4-Butanetriol CAS:3068-00-6 Specification Test Item Standard: USP Identification IR spectrum similar to that of RS HPLC retention time similar to that of RS Related substa
Cas:3068-00-6
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inquiryAs a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem’s R&D center offer custom synthesis according to the contract research and development services for
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inquiryItems Standard Result Appearance Light yellow to colourless Colourless Purity (%, GC) 98.0 m
Cas:3068-00-6
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inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Cangzhou Enke Pharma Tech Co.,ltd. is located in Cangzhou City, Hebei province ,where is a famous petroleum chemical industry city in China. Enke Pharma a high-tech enterprise ,and we are dedicated to developing and manufacturing new ap
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inquiryLIDE PHARMACEUTICALS LIMITED is a professional chemicals and APIs leading manufacturer in China. Our core business line covers APIs, Intermediates, Herb extract, etc. We are specialized in chemical synthesis, process development of pharmaceu
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inquiry1,2,4-Butanetriol Basic information Product Name: 1,2,4-Butanetriol Synonyms: 1,3,4-Butanetriol;2-Deoxyerythritol;Triol 124;triol124;butane-1,2,4-triol;1,2,4-TRIHYDROXYBUTANE;1,2,4-BUTAN
Our advantages: 1, High quality with competitive price: 1) Standard:BP/USP/EP/Enterprise standard 2) All Purity≥99% 3) We are manufacturer and can provide high quality products with factory price. 2, Fast and safe delivery 1) Parcel can be sent
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inquiryProduct name 1 2 4-Butanetriol Synonyms Butanetriol,97%;1 2 4-BUTANETRIOL 96%;trihydroxybutane;1,2,4-BUTANETRIOL 99.5%;1,2,4-BUTANETRIOL 98+%;1,2,4-Butanetriol,95%;(±)-1,2,4-Butanetriol (BT);(
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inquiryAbout Our Group Since 1996 when our factory was put into production to year of 2020, our group has successively invested in more than 52 factories with shares and subordinates.We focus on manufacture Pharm & c
Cas:3068-00-6
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inquiry1,2,4-Butanetriol CAS:3068-00-6 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermed
Cas:3068-00-6
Min.Order:1 Gram
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:3068-00-6
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
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inquiryCompany Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments
J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
Cas:3068-00-6
Min.Order:4 Kilogram
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inquiryEstablished in 2010, located in Hangzhou Qinglan science park, lingruichem is a technical company mainly focus on the Custom synthesis, manufacturing, sales of chemicals to various industries. In our R&D centre, we have a staff of skilled and experie
Massive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and
Cas:3068-00-6
Min.Order:1 Gram
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
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Min.Order:10 Gram
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inquirySuperior quality, moderate price & quick delivery. Appearance:Transparent colourless viscous liquid Storage:sealed in a cool dry place Package:200kg/drum or 1kg, 10kg, 20kg/PVC drum Application:1、Important intermediates of medicine preparation
Product name: 1,2,4-Butanetriol CAS No.: 3068-00-6 Molecule Formula:C4H10O3 Molecule Weight:106.12 Purity: 99.0% Package: 200kg/drum Description:Colorless transparent liquid Manufacture Standards:Enterprise Standard TESTING ITEMS
Cas:3068-00-6
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inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
Cas:3068-00-6
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Type:Trading Company
inquiryHangzhou Huarong Pharm Co., Ltd.established since 2006 , has been actively developing specialty products for Finished Dosages, APIs, Intermediates, and Fine chemicals markets in North America, Europe, Korea, Japan, Mid-East and all over the World. Hu
Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
Conditions | Yield |
---|---|
With hydrogen; 5% activated charcoal-supported ruthenium catalyst In ethanol at 120℃; under 120012 Torr; for 70 - 90h; Product distribution / selectivity; | 90% |
In water | 77% |
With hydrogen; 5% activated charcoal-supported ruthenium catalyst In water at 100 - 120℃; under 7500.75 - 90009 Torr; for 6 - 24h; Product distribution / selectivity; | 63% |
Conditions | Yield |
---|---|
With ruthenium on silica; hydrogen In tetrahydrofuran at 200℃; under 75007.5 Torr; for 12h; Temperature; Pressure; Time; | 87% |
malic acid dimethyl ester
D,L-1,2,4-butanetriol
Conditions | Yield |
---|---|
With hydrogen; CuO/ZnO/Al2O3 In tetrahydrofuran at 180℃; under 7500.75 - 75007.5 Torr; for 4h; Product distribution / selectivity; | 80% |
With potassium tert-butylate In 1,4-dioxane at 70℃; for 48h; Temperature; Time; | 62% |
With potassium borohydride In ethanol | |
With hydrogenchloride; sodium borohydrid In tetrahydrofuran; methanol; isopropyl alcohol; acetone | |
With hydrogen; [(MeC(CH2PPh2)3)Ru(acetonitrile)3](CF3SO3)2 In methanol at 100℃; under 30003 Torr; for 14h; Product distribution / selectivity; Inert atmosphere; Autoclave; | >= 99.9 %Chromat. |
malic acid
A
propylene glycol
B
Butane-1,4-diol
C
D,L-1,2,4-butanetriol
D
ethylene glycol
Conditions | Yield |
---|---|
With hydrogen; Ru-carbon In water at 135℃; under 258574 Torr; for 10h; Further byproducts given; | A 11% B 8% C 74% D 3% |
Conditions | Yield |
---|---|
Stage #1: homoalylic alcohol With formic acid; water; dihydrogen peroxide at 55 - 60℃; for 7h; Stage #2: With methanol; Marlon-AS3 at 55 - 85℃; for 3h; | 72% |
With sulfuric acid; water; dihydrogen peroxide | |
Stage #1: homoalylic alcohol With sodium periodate; acetic acid; lithium bromide at 95℃; for 18h; Prevost-Woodward reaction; Stage #2: With potassium carbonate In methanol at 25℃; for 24h; | |
With potassium permanganate |
rac-3,4-dihydroxybutyl bromide
A
D,L-1,2,4-butanetriol
Conditions | Yield |
---|---|
With 3-Hydroxytetrahydrofuran; trisodium arsenite; hydrogen bromide for 96h; Ambient temperature; | A 5% B 17% |
Conditions | Yield |
---|---|
With copper chromite; ethanol at 100 - 150℃; under 257428 Torr; Hydrogenation; | |
With ethanol; nickel at 100 - 150℃; under 257428 Torr; Hydrogenation; |
Conditions | Yield |
---|---|
With water; nickel at 60 - 100℃; under 147102 Torr; Hydrogenation; | |
With copper oxide-chromium oxide; water; silica gel at 80 - 100℃; under 147102 Torr; Hydrogenation; |
formaldehyd
A
D,L-1,2,4-butanetriol
B
1,2,3,4-butanetetrol
C
ethylene glycol
D
2-C-hydroxymethyltetritol
E
glycerol
Conditions | Yield |
---|---|
With calcium oxide Product distribution; Heating; reduction of formed monosacharides;; |
3-Benzoyloxytetrahydrofuran
D,L-1,2,4-butanetriol
Conditions | Yield |
---|---|
With titanium tetrachloride 1) CH2Cl2, 72h, reflux 2) saponification; Multistep reaction; |
4-Methoxy-benzoic acid tetrahydro-furan-3-yl ester
D,L-1,2,4-butanetriol
Conditions | Yield |
---|---|
With titanium tetrachloride; potassium carbonate 1) CH2Cl2, 72h, reflux 2) MeOH, 10h, r.t.; Yield given. Multistep reaction; |
2-6'-acetoxy-6'-formyloxy-4'-oxo-2'-hexenamido-3-hydroxy-2-cyclopenten-1-one
A
D,L-1,2,4-butanetriol
B
2-glycolamido-3-hydroxy-2-cyclopenten-1-one
Conditions | Yield |
---|---|
With sodium tetrahydroborate; ozone 1.) dichloromethane, cooled with dry ice-acetone, 40 min.; 2.) ethanol, water, 30 min, cooling; room temperature, 30 min; Yield given. Multistep reaction. Yields of byproduct given; | |
With sodium tetrahydroborate; ozone 1.) dichloromethane, cooled with dry ice-acetone, 40 min.; 2.) ethanol, water, 30 min. cooling; room temperature, 30 min; Yield given. Multistep reaction. Yields of byproduct given; |
D,L-1,2,4-butanetriol
Conditions | Yield |
---|---|
With 1-methyl-pyrrolidin-2-one; RhCl(PPh3)3 at 130℃; for 0.5h; | 90 % Chromat. |
Conditions | Yield |
---|---|
With titanium silicate; dihydrogen peroxide at 24.9℃; for 6h; Title compound not separated from byproducts; |
Adipic acid
A
butane-1,2,3-triol
B
D,L-1,2,4-butanetriol
C
meso-erythritol
D
ethylene glycol
Conditions | Yield |
---|---|
Das Natriumsalz bei der reduzierenden Verseifung mit Ba(SH)2 in Butandiol-(1.2); |
D,L-1,2,4-butanetriol
Conditions | Yield |
---|---|
With hydrogenchloride; methanol | |
With methanol; sulfuric acid |
D,L-1,2,4-butanetriol
Conditions | Yield |
---|---|
With sodium nitrate Electrolysis.an einer Platinanode und reduzierende Verseifung des Reaktionsgemisches mit Ba(SH)2; |
D,L-1,2,4-butanetriol
Conditions | Yield |
---|---|
With sodium nitrate Electrolysis.an einer Platinanode und reduzierende Verseifung des Reaktionsgemisches mit Ba(SH)2; |
D,L-1,2,4-butanetriol
Conditions | Yield |
---|---|
With sodium nitrate Electrolysis.an einer Platinanode und reduzierende Verseifung des Reaktionsgemisches mit Ba(SH)2; |
Conditions | Yield |
---|---|
at 60 - 100℃; under 147102 Torr; Hydrogenation; |
D,L-1,2,4-butanetriol
Conditions | Yield |
---|---|
With barytes |
1,2-dibromo-4-methoxy-butane
water
A
3-Hydroxytetrahydrofuran
B
D,L-1,2,4-butanetriol
C
4-methoxy-1,2-butanediol
dimethyl (S)-malate
A
D,L-1,2,4-butanetriol
B
(3S)-3-hydroxydihydrofuran-2(3H)-one
C
2-buten-4-olide
D
methyl 3,4-dihydroxybutanoate
Conditions | Yield |
---|---|
With hydrogen In Dimethyl ether at 56 - 110℃; under 120012 Torr; for 0.5 - 2h; Product distribution / selectivity; | A n/a B n/a C n/a D n/a |
Conditions | Yield |
---|---|
With hydrogen; Ni(30 wt%)/SiO2 In isopropyl alcohol at 90 - 120℃; under 68404.6 Torr; Product distribution / selectivity; | |
With hydrogen; nickel In isopropyl alcohol at 120℃; under 68404.6 Torr; for 6h; Product distribution / selectivity; | |
With hydrogen; 5%-palladium/activated carbon In isopropyl alcohol at 120℃; under 68404.6 Torr; for 5h; Product distribution / selectivity; |
(R)-dimethyl malate
D,L-1,2,4-butanetriol
Conditions | Yield |
---|---|
With sodium hydroxide In tetrahydrofuran; water | |
With sodium hydroxide In tetrahydrofuran; water |
Conditions | Yield |
---|---|
In tetrahydrofuran |
D-sorbitol
A
propylene glycol
B
ethanol
C
1.3-butanediol
D
D,L-1,2,4-butanetriol
E
XYLITOL
F
ethylene glycol
G
isopropyl alcohol
H
glycerol
I
2.3-butanediol
J
1,2-dihydroxybutane
Conditions | Yield |
---|---|
With potassium hydroxide; hydrogen; nickel-rhenium-on-carbon In water at 220℃; under 31029.7 - 62059.4 Torr; for 4h; Product distribution / selectivity; |
Conditions | Yield |
---|---|
100% |
D,L-1,2,4-butanetriol
benzoyl chloride
(+/-)-1,2,4-tris(benzoyloxy)butane
Conditions | Yield |
---|---|
With dmap; triethylamine In tetrahydrofuran at 25℃; | 100% |
D,L-1,2,4-butanetriol
2,2-diphenylacetaldehyde dimethyl acetal
Conditions | Yield |
---|---|
With chloro-trimethyl-silane; cobalt(II) chloride In acetonitrile at 20℃; for 17h; | 100% |
D,L-1,2,4-butanetriol
orthobenzoic acid trimethyl ester
3-Benzoyloxytetrahydrofuran
Conditions | Yield |
---|---|
With trimethylsilyl trifluoromethanesulfonate In dichloromethane at 0℃; for 2h; | 99% |
Conditions | Yield |
---|---|
sulfuric acid at 140℃; under 49.505 Torr; Product distribution / selectivity; Reactive distillation; Intramolecular dehydration; | 98% |
samarium(III) trifluoromethanesulfonate at 140℃; under 49.505 Torr; Product distribution / selectivity; Reactive distillation; Intramolecular dehydration; | 97% |
strong acid ion exchange resin (Amberlyst 15, H+ form) In 1,4-dioxane at 100℃; under 760.051 Torr; for 20h; Product distribution / selectivity; | 96% |
D,L-1,2,4-butanetriol
acetone
4-(2-hydroxyethyl)-2,2-dimethyl-1,3-dioxolane
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid at 20℃; for 4h; | 98% |
With toluene-4-sulfonic acid at 20℃; for 20h; | 97% |
With toluene-4-sulfonic acid | 86% |
D,L-1,2,4-butanetriol
cyclohexanone
2-(1,4-dioxa-spiro[4.5]dec-2-yl)-ethanol
Conditions | Yield |
---|---|
With boron trifluoride diethyl etherate In diethyl ether at 0 - 20℃; | 97% |
D,L-1,2,4-butanetriol
2,2-dimethoxy-propane
(2,2-Dimethyl-[1,3]dioxolan-4-yl)-ethanol
Conditions | Yield |
---|---|
In dichloromethane | 96.7% |
D,L-1,2,4-butanetriol
Conditions | Yield |
---|---|
With water-d2; phospho(enol)pyruvic acid mono potassium salt; adenosine 5'-triphosphate disodium salt; barium(II) chloride; magnesium chloride; glycerol kinase from S. cerevisiae or from E. coli and pyruvate kinase In various solvent(s) for 1h; | 95% |
D,L-1,2,4-butanetriol
tert-butyldimethylsilyl chloride
1,4-di(tert-butyldimethylsilanyloxy)butan-2-ol
Conditions | Yield |
---|---|
With dmap; triethylamine In dichloromethane at 20℃; | 95% |
With 1H-imidazole In dichloromethane Inert atmosphere; chemoselective reaction; | |
With 1H-imidazole In N,N-dimethyl-formamide at 20℃; Cooling; |
D,L-1,2,4-butanetriol
Conditions | Yield |
---|---|
With pyridinium p-toluenesulfonate In toluene Reflux; Inert atmosphere; Dean-Stark; | 95% |
D,L-1,2,4-butanetriol
(6Z,9Z,28Z,31Z)-heptatriaconta-6,9,28,31-tetraen-19-one
2,2-dilinoleyl-4-(2-hydroxyethyl)-[1,3]-dioxolane
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid for 3h; Reflux; Molecular sieve; | 90% |
With toluene-4-sulfonic acid In toluene Reflux; Dean-Stark; | 47% |
With pyridinium p-toluenesulfonate In toluene Reflux; Inert atmosphere; | |
With pyridinium p-toluenesulfonate In toluene | |
With pyridinium p-toluenesulfonate In toluene Inert atmosphere; Reflux; Dean-Stark tube; |
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In toluene for 3h; Reflux; Molecular sieve; | 90% |
With toluene-4-sulfonic acid In toluene for 3h; Reflux; Molecular sieve; | 90% |
D,L-1,2,4-butanetriol
(benzoyloxy)acetaldehyde diethyl acetal
Conditions | Yield |
---|---|
With chloro-trimethyl-silane; cobalt(II) chloride In acetonitrile at 20℃; for 0.1h; stereoselective reaction; | 90% |
D,L-1,2,4-butanetriol
1-amino-3-methylbenzene
1-m-tolyl-pyrrolidin-3-ol
Conditions | Yield |
---|---|
Stage #1: D,L-1,2,4-butanetriol With [ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2; caesium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene In toluene at 20℃; for 0.666667h; Molecular sieve; Inert atmosphere; Schlenk technique; Green chemistry; Stage #2: 1-amino-3-methylbenzene In toluene at 20℃; for 48.33h; Inert atmosphere; Schlenk technique; Sealed tube; Reflux; Green chemistry; | 90% |
D,L-1,2,4-butanetriol
hexaethylphosphoric triamide
2,7,8-trioxa-1-phosphabicyclo<3.2.1>octane
Conditions | Yield |
---|---|
at 100℃; | 89% |
3-chloro-1,1-diethoxy-propane
D,L-1,2,4-butanetriol
Conditions | Yield |
---|---|
With chloro-trimethyl-silane; cobalt(II) chloride In acetonitrile at 20℃; Inert atmosphere; stereoselective reaction; | 89% |
D,L-1,2,4-butanetriol
ethenyltrimethylsilane
1,2,4-Tris-trimethylsiloxy-butan
Conditions | Yield |
---|---|
Wilkinson's catalyst In toluene at 130℃; for 6h; | 88% |
D,L-1,2,4-butanetriol
benzaldehyde
(+/-)-cis-4-(hydroxymethyl)-2-phenyl-1,3-dioxane
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In toluene for 4.5h; Heating; | 87% |
With toluene-4-sulfonic acid In toluene for 1h; Reflux; | 53% |
With molecular sieve; toluene-4-sulfonic acid In toluene Heating; |
(1,3-bis(diphenylphosphino)propane)Pt(CO3)
D,L-1,2,4-butanetriol
[(1,3-bis(diphenylphosphino)propane)]platinum(II)(1,2,4-butanetriolate)
Conditions | Yield |
---|---|
In dichloromethane byproducts: CO2, H2O; under Ar; Pt-complex and 1.05 equiv of the triol dissolved in CH2Cl2, soln. stirred 2 h, soln. purged with Ar 4 times over a period of 3 h; evapn. (vac.), dried (vac., 1 h), dissolved in min. amt. CH2Cl2, layered with ether (crystn.), cryst. isolated, dried (vac.), elem. anal.; | 87% |
D,L-1,2,4-butanetriol
benzyl chloride
(+/-)-4-(2-benzyloxyethyl)-2,2-dimethyl-1,3-dioxolane
Conditions | Yield |
---|---|
With sodium hydride; sodium iodide In N,N-dimethyl-formamide for 12h; Ambient temperature; | 86% |
Conditions | Yield |
---|---|
With pyridinium p-toluenesulfonate In toluene Inert atmosphere; Reflux; | 86% |
D,L-1,2,4-butanetriol
m-Anisidine
1-(3-methoxy-phenyl)-pyrrolidin-3-ol
Conditions | Yield |
---|---|
Stage #1: D,L-1,2,4-butanetriol With [ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2; caesium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene In toluene at 20℃; for 0.666667h; Molecular sieve; Inert atmosphere; Schlenk technique; Green chemistry; Stage #2: m-Anisidine In toluene at 20℃; for 48.33h; Inert atmosphere; Schlenk technique; Sealed tube; Reflux; Green chemistry; | 86% |
Conditions | Yield |
---|---|
With C30H42N4O6Pd2(2+)*2CF3O3S(1-); p-benzoquinone In water; acetonitrile at 55℃; for 24h; Darkness; chemoselective reaction; | 85% |
With Candida boidinii KK912 In methanol; water at 30℃; for 48h; phosphate buffer (pH=7); other butanols; | 78.1% |
With phosphate buffer; Candida boidinii KK912 In methanol; water at 30℃; for 48h; | 78.1% |
With [(neocuproine)Pd(OAc)]2(OTf)2; oxygen In water; acetonitrile at 25℃; for 20h; Reagent/catalyst; Temperature; chemoselective reaction; | 71% |
With 2-Picolinic acid; manganese(II) perchlorate hexahydrate; butanedial; dihydrogen peroxide; sodium acetate In acetonitrile at 0 - 20℃; for 1h; Solvent; |
D,L-1,2,4-butanetriol
2,2-dimethoxy-propane
4-(2-hydroxyethyl)-2,2-dimethyl-1,3-dioxolane
Conditions | Yield |
---|---|
With camphor-10-sulfonic acid | 85% |
With camphor-10-sulfonic acid In acetonitrile at 20℃; | 80% |
Stage #1: D,L-1,2,4-butanetriol; 2,2-dimethoxy-propane With pyridinium p-toluenesulfonate In acetone at 20℃; for 4h; Reflux; Stage #2: In methanol at 0℃; for 12h; | 74% |
Conditions | Yield |
---|---|
With chloro-trimethyl-silane; cobalt(II) chloride In acetonitrile at 20℃; Inert atmosphere; stereoselective reaction; | 85% |
D,L-1,2,4-butanetriol
benzaldehyde dimethyl acetal
(+/-)-cis-4-(hydroxymethyl)-2-phenyl-1,3-dioxane
Conditions | Yield |
---|---|
With chloro-trimethyl-silane; cobalt(II) chloride In acetonitrile at 20℃; Inert atmosphere; stereoselective reaction; | 84% |
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