As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem’s R&D center offer custom synthesis according to the contract research and development services for t
Cas:4965-33-7
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inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
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inquiryThe company has a professional R & D team, mature technology, very competitive prices and stable high quality products for customers to order high quality and low price product efforts! Appearance:White or off-white Solid Storage:Sealed, dry, m
chengdu and import and export trade co., LTD., who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do res
Cas:4965-33-7
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inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Cas:4965-33-7
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inquiryAbout Product Details
Cas:4965-33-7
Min.Order:1 Kilogram
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inquiry7-Chloro-2-methylquinoline Basic information Product Name: 7-Chloro-2-methylquinoline Synonyms: 7ChloroQuinaldineMontelukast;7-CHLOROQUINALDINE 99%;7-Chloroquinaldine ,99%;7-Chloro-2-methylqui;7-Chloroquinaldine, 7-Chloro-2-methyl-1-azanaphthalene;
Our advantages: 1. High quality and competitive price: 1) Standard: BP/USP/EP/ enterprise standard 2) All purity ≥99% 3) We are manufacturers and can provide high quality products at factory prices. 2. Fast and safe delivery 1) The package c
Cas:4965-33-7
Min.Order:1 Kilogram
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inquiryTIANFUCHEM--4965-33-7--High purity 7-Chloro-2-methylquinoline factory price Our company was built in 2009 with an ISO certificate.In the past 10 years, we have grown up as a famous fine chemicals supplier in China And we had established st
Cas:4965-33-7
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:4965-33-7
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inquiryProduct Name 7-Chloro-2-methylquinoline Synonyms 7ChloroQuinaldineMontelukast;7-CHLOROQUINALDINE 99%;7-Chloroquinaldine ,99%;7-Chloro-2-methylqui;2-Methyl-7-chloroquinline;7-Chloroquinaldine, 7-Chloro-2-
Cas:4965-33-7
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inquiry1. Guaranteed purity; 2. Large quantity in stock; 3. Largest manufacturer; 4. Best service after shipment with email; 5. High quality & competitive price; Appearance:White Crystalline Powder Storage:Store in sealed containers
Cas:4965-33-7
Min.Order:100 Gram
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inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
Cas:4965-33-7
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inquiry★.Best quality according to requirement ★.Competitive price in China market ★.Mature Technical support ★.Professional logistic support
Cas:4965-33-7
Min.Order:1 Kilogram
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inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At prese
Cas:4965-33-7
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FOB Price: $68.0 / 72.0
Type:Trading Company
inquiry7-Chloro-2-methylquinoline CAS: 4965-33-7 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organi
Cas:4965-33-7
Min.Order:1 Gram
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:4965-33-7
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Cas:4965-33-7
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inquiryBest quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
Appearance:white powder/crystal Storage:Store in a cool,dry place and keep away from direct strong light Package:As customer request Application:Used for research and industrial manufacture. Transportation:Common products:Sea/Ai
Cas:4965-33-7
Min.Order:100 Metric Ton
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:4965-33-7
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inquiryCompany Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments
J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Cas:4965-33-7
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inquiry4965-33-7 7-Chloro-2-methylquinoline Appearance:white powder Storage:room temperature Package:according to customers' requirements Application:Pharma intermediates Transportation:By air(EMS or EUB or FedEx or TNT ect...) or by sea(FOB or CIF or CNF
Massive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and
Cas:4965-33-7
Min.Order:1 Gram
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:4965-33-7
Min.Order:10 Gram
FOB Price: $100.0
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inquirySuperior quality, moderate price & quick delivery. Appearance:white crystal powder Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:25kg/drum, or as per your request. Application:Used as Pharmaceutical Inte
Cas:4965-33-7
Min.Order:1 Kilogram
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Type:Trading Company
inquiryEstablished in May 2015, TaiChem Ltd. is initially invested by a British research and development company and started by PhDs back from aboard. The company is registered in China Medical City (CMC), Taizhou, Jiangsu Province, and the production site
Cas:4965-33-7
Min.Order:10 Gram
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Type:Lab/Research institutions
inquiryProduct name: 7-Chloro-2-Methylquinoline CAS No.:4965-33-7 Molecule Formula:C10H8ClN Molecule Weight:177.63 Purity: 99.0% Package: 25kg/drum Description:White crystalline powder Manufacture Standards:Enterprise Standard
Cas:4965-33-7
Min.Order:1 Kilogram
Negotiable
Type:Trading Company
inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Cas:4965-33-7
Min.Order:1 Gram
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Type:Lab/Research institutions
inquiry4-Hydroxy-4-methyl-2-pentanone
2-amino-4-chlorobenzaldehyde
2-methyl-7-chloroquinoline
Conditions | Yield |
---|---|
With chloro[1,3-bis(2,6-di-i-propylphenyl)imidazol-2-ylidene]copper(I); sodium t-butanolate In toluene at 70℃; Inert atmosphere; Schlenk technique; chemoselective reaction; | 90% |
Conditions | Yield |
---|---|
With phospho-tungstic acid; phosphotungstic acid; silica gel for 0.2h; Doebner-Miller reaction; microwave irradiation; | 86% |
With hydrogenchloride; chloranil In tetrahydrofuran; methanol; iso-butanol |
2-methyl-7-chloroquinoline
Conditions | Yield |
---|---|
With tetrasodium cobalt(II) 4,4',4'',4'''-tetrasulphophthalocyanine In water; ethyl acetate at 20℃; for 18h; Irradiation; Green chemistry; | 85% |
With rose bengal; oxygen In N,N-dimethyl acetamide at 20℃; for 24h; Irradiation; | 73% |
With rose bengal In N,N-dimethyl acetamide at 20℃; for 28h; Irradiation; | 73% |
With tris(bipyridine)ruthenium(II) dichloride hexahydrate; Co(dmgH)2(4-MeCO2Py)Cl In water at 28℃; for 12h; Schlenk technique; Inert atmosphere; Irradiation; | 73% |
With 1,10-Phenanthroline; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; potassium tert-butylate; oxygen; nickel dibromide In tert-Amyl alcohol at 95℃; for 48h; | 42% |
Conditions | Yield |
---|---|
With magnetite-palladium-graphene nanocomposite In acetonitrile at 80℃; for 12h; | 72% |
ethanol
3-chloro-aniline
A
2-methyl-7-chloroquinoline
B
2-methyl-5-chloroquinoline
Conditions | Yield |
---|---|
With iron(III) chloride hexahydrate In tetrachloromethane at 140℃; for 4h; Autoclave; Inert atmosphere; Sealed tube; | A 11% B 67% |
Conditions | Yield |
---|---|
Stage #1: 3-chloro-aniline; crotonaldehyde With hydrogenchloride In water; toluene at 110℃; for 1.5h; Stage #2: With zinc(II) chloride In tetrahydrofuran; water; acetone; toluene at 60℃; for 1h; Cooling with ice; | 30% |
With hydrogenchloride In water; toluene for 2h; Doebner-Miller Quinoline Synthesis; Reflux; | |
With hydrogenchloride; 1-methyl-2-nitrobenzene In water at 100℃; for 9h; Reagent/catalyst; Skraup Quinoline Synthesis; Reflux; |
1,1,3-trimethoxybutane
3-chloroaniline hydrochloride
2-methyl-7-chloroquinoline
Conditions | Yield |
---|---|
With ethanol; iron(III) chloride; zinc(II) chloride |
Conditions | Yield |
---|---|
With hydrogenchloride |
acetaldehyde
3-chloro-aniline
A
2-methyl-7-chloroquinoline
B
2-methyl-5-chloroquinoline
Conditions | Yield |
---|---|
With di-μ-chlorobis(norbornadiene)dirhodium(I); 3-Nitrochlorobenzene In ethanol at 180℃; for 4h; Yield given. Yields of byproduct given; |
β-(m-chloroanilino)crotonaldehyde
A
2-methyl-7-chloroquinoline
B
2-methyl-5-chloroquinoline
Conditions | Yield |
---|---|
With sulfuric acid at 25℃; Rate constant; |
formaldehyd
3-chloro-aniline
A
2-methyl-7-chloroquinoline
B
2-methyl-5-chloroquinoline
Conditions | Yield |
---|---|
With sulfuric acid; sodium 3-nitrobenzenesulfonate at 120 - 130℃; for 1.83333h; | A 8.64 g B 0.28 g |
With sulfuric acid; sodium 3-nitrobenzenesulfonate at 120 - 130℃; for 1.83333h; | A 8.64 g B 0.79 g |
trans-Crotonaldehyde
3-chloro-aniline
A
2-methyl-7-chloroquinoline
B
2-methyl-5-chloroquinoline
Conditions | Yield |
---|---|
With hydrogenchloride; chloranil In various solvent(s) for 0.333333h; Heating; |
Conditions | Yield |
---|---|
at 120 - 130℃; Behandeln mit Paraldehyd; Trennung der Isomeren ueber die Pikrate; |
trans-Crotonaldehyde
3-chloro-aniline
A
2-methyl-7-chloroquinoline
B
2-methyl-5-chloroquinoline
C
N-ethyl-3-chloroaniline
D
Butyl-(3-chloro-phenyl)-amine
Conditions | Yield |
---|---|
With hydrogenchloride; chloranil In ethanol; water Product distribution; Heating; other substituted anilines; var. solvents, var. oxidants and acids, var. temperatures; |
1-(m-chlorophenylamino)-3-(m-chlorophenylimino)-1-butene hydrochloride
2-methyl-7-chloroquinoline
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 0.29 g / NaOH / H2O; ethanol / 2 h / 80 °C 2: 8.64 g / sodium m-nitrobenzenesulfonate, 72.2 percent H2SO4 / 1.83 h / 120 - 130 °C View Scheme |
Conditions | Yield |
---|---|
zinc(II) chloride In hydrogenchloride; water |
ethyl vinyl ether
3-chloro-aniline
A
2-methyl-7-chloroquinoline
B
N-ethyl-3-chloroaniline
Conditions | Yield |
---|---|
With palladium on activated charcoal; palladium dichloride In acetonitrile at 80℃; for 24h; | A 68 %Chromat. B 23 %Chromat. |
(E)-1-Bromo-2-butene
3,3'-dichloroazobenzene
A
2-methyl-7-chloroquinoline
B
2-methyl-5-chloroquinoline
Conditions | Yield |
---|---|
With copper(l) iodide In 1,2-dichloro-ethane at 120℃; for 12h; Inert atmosphere; Sealed tube; Overall yield = 44 %; Overall yield = 15.6 mg; |
3-chloro-aniline
A
2-methyl-7-chloroquinoline
B
2-methyl-5-chloroquinoline
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: copper(I) bromide; pyridine / toluene / 20 h / 60 °C 2: copper(l) iodide / 1,2-dichloro-ethane / 12 h / 120 °C / Inert atmosphere; Sealed tube View Scheme |
ethylene glycol
3-chloro-aniline
A
2-methyl-7-chloroquinoline
B
2-methyl-5-chloroquinoline
Conditions | Yield |
---|---|
With tetrachloromethane; iron(III) chloride hexahydrate at 150℃; for 8h; Inert atmosphere; Sealed tube; Autoclave; Overall yield = 56 %; |
1.3-butanediol
3-chloro-aniline
A
2-methyl-7-chloroquinoline
B
2-methyl-5-chloroquinoline
C
7-chloro-4-methyl-quinoline
Conditions | Yield |
---|---|
With iron(III) chloride hexahydrate In tetrachloromethane at 150℃; for 8h; Inert atmosphere; Overall yield = 79 %; |
(2-amino-4-chlorophenyl)methanol
2-methyl-7-chloroquinoline
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: manganese(IV) oxide / dichloromethane / Inert atmosphere 2: chloro[1,3-bis(2,6-di-i-propylphenyl)imidazol-2-ylidene]copper(I); sodium t-butanolate / toluene / 70 °C / Inert atmosphere; Schlenk technique View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: lithium aluminium tetrahydride / tetrahydrofuran / Inert atmosphere 2: manganese(IV) oxide / dichloromethane / Inert atmosphere 3: chloro[1,3-bis(2,6-di-i-propylphenyl)imidazol-2-ylidene]copper(I); sodium t-butanolate / toluene / 70 °C / Inert atmosphere; Schlenk technique View Scheme |
A
2-methyl-7-chloroquinoline
Conditions | Yield |
---|---|
With monoamine oxidase from Pseudomonas monteilii ZMU-T01 In aq. buffer at 37℃; pH=7.5; Resolution of racemate; enantioselective reaction; | A n/a B n/a |
2-methyl-7-chloroquinoline
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: dichloromethane / 5 h / 40 °C / Acidic conditions 2: sulfuric acid / toluene; water / 100 °C 3: water / 70 °C View Scheme |
2-methyl-7-chloroquinoline
Conditions | Yield |
---|---|
In water at 70℃; Temperature; Reagent/catalyst; |
2-methyl-7-chloroquinoline
Conditions | Yield |
---|---|
With (R)-3,3'-bis(2,4,6-triisopropylphenyl)binol phosphoric acid; diethyl 2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylate at -10℃; Green chemistry; enantioselective reaction; | 99% |
Conditions | Yield |
---|---|
With {Au(dppm)}2Cl2; trifluoroacetic acid In methanol Inert atmosphere; UV-irradiation; | 99% |
2-methyl-7-chloroquinoline
Conditions | Yield |
---|---|
With hydrogen In toluene at 100℃; under 37503.8 Torr; for 24h; chemoselective reaction; | 99% |
With C46H49CoN3P4(2+)*2BF4(1-); hydrogen; potassium hydroxide In toluene; acetonitrile at 100℃; under 22801.5 Torr; for 48h; Autoclave; Glovebox; chemoselective reaction; | 87% |
With sodium tetrahydroborate; hydrogen; cobalt(II) chloride In water at 150℃; under 30003 Torr; for 17h; Green chemistry; chemoselective reaction; | 67% |
With sodium cyanoborohydride; acetic acid at 20℃; Sealed tube; |
2-methyl-7-chloroquinoline
(-)-7-chloro-2-methyl-1,2,3,4-tetrahydroquinoline
Conditions | Yield |
---|---|
With bromopentacarbonylmanganese(I); potassium tert-butylate; hydrogen; E-1-(1H-benzo[d]imidazol-2-yl)-N-((SC,RFC)-1-(2-diphenylphosphino)ferrocenyl)methanimine In 1,4-dioxane at 80℃; under 45004.5 Torr; for 16h; Autoclave; enantioselective reaction; | 98% |
With bis(1,5-cyclooctadiene)diiridium(I) dichloride; C73H100O2P2; hydrogen; iodine In toluene at 20℃; under 15201 Torr; for 24h; optical yield given as %ee; enantioselective reaction; |
Conditions | Yield |
---|---|
With potassium phosphate; copper(l) iodide; N1-benzyl-N2-(5-methyl-[1,1'-biphenyl]-2-yl)oxalamide In dimethyl sulfoxide at 120℃; for 24h; Inert atmosphere; | 98% |
Conditions | Yield |
---|---|
With C51H57ClNiO2P2; sodium t-butanolate at 25℃; | 98% |
2-methyl-7-chloroquinoline
Isophthalaldehyde
(E)-3-[2-(7-chloro-2-quinolinyl)ethenyl]benzaldehyde
Conditions | Yield |
---|---|
With lanthanum pentafluorobenzoate In toluene at 120℃; for 24h; | 97% |
With tert-butylammonium hexafluorophosphate(V); calcium(II) trifluoromethanesulfonate In neat (no solvent) at 130℃; Green chemistry; | 93% |
With acetic anhydride In toluene at 100 - 105℃; for 12 - 15h; | 75.15% |
2-methyl-7-chloroquinoline
N-Benzylaniline
(E)-7-chloro-2-styrylquinoline
Conditions | Yield |
---|---|
Stage #1: N-Benzylaniline With 2,3-dicyano-5,6-dichloro-p-benzoquinone In N,N-dimethyl-formamide at 20℃; for 0.0833333h; Inert atmosphere; Stage #2: 2-methyl-7-chloroquinoline In N,N-dimethyl-formamide at 70℃; for 24h; Inert atmosphere; diastereoselective reaction; | 97% |
Conditions | Yield |
---|---|
With lanthanum pentafluorobenzoate In toluene at 120℃; for 24h; | 97% |
With tert.-butylhydroperoxide; N-Bromosuccinimide In water; acetonitrile at 100℃; for 48h; Schlenk technique; Darkness; Green chemistry; | 95% |
With 1,10-phenanthroline-5,6-dione; trifluorormethanesulfonic acid; oxygen In chlorobenzene at 80℃; under 760.051 Torr; for 24h; | 86% |
With tert.-butylhydroperoxide; water; sodium chloride at 100℃; | 75% |
2-methyl-7-chloroquinoline
Conditions | Yield |
---|---|
With water-d2; benzoic acid at 80℃; for 4h; | 97% |
With water-d2; benzoic acid at 90℃; for 8h; Inert atmosphere; Schlenk technique; |
Conditions | Yield |
---|---|
With (PhPAd-DalPhos)NiCl(o-tol); sodium t-butanolate In toluene at 25℃; for 18h; Inert atmosphere; Glovebox; Sealed tube; | 97% |
Conditions | Yield |
---|---|
With 2-Picolinic acid; ferrous(II) sulfate heptahydrate; sodium bromate In water; dimethyl sulfoxide at 20℃; for 24h; Inert atmosphere; Irradiation; | 97% |
Conditions | Yield |
---|---|
With (4,4′-di-tert-butyl-2,2′-dipyridyl)Ni(o-tolyl)(Br); 1,8-diazabicyclo[5.4.0]undec-7-ene In toluene at 80℃; for 12h; Inert atmosphere; Sealed tube; UV-irradiation; | 97% |
Conditions | Yield |
---|---|
With C33H43ClNiO6P2; sodium t-butanolate In toluene at 25℃; for 18h; Inert atmosphere; Sealed tube; | 97% |
2-methyl-7-chloroquinoline
benzaldehyde
(E)-7-chloro-2-styrylquinoline
Conditions | Yield |
---|---|
With tert-butylammonium hexafluorophosphate(V); calcium(II) trifluoromethanesulfonate In neat (no solvent) at 130℃; Green chemistry; | 96% |
With cobalt(II) chloride In water at 120℃; for 24h; | 93% |
With 1,3-dimethylbarbituric acid; acetic acid In 1,4-dioxane; water at 60℃; for 24h; | 93% |
2-methyl-7-chloroquinoline
2-methylquinolin-7-amine
Conditions | Yield |
---|---|
With ammonium hydroxide; potassium phosphate; copper(l) iodide; N1,N2-bis(5-methyl-[1,1'-biphenyl]-2-yl)oxalamide In water; dimethyl sulfoxide at 110℃; for 24h; Inert atmosphere; | 96% |
With bis(1,5-cyclooctadiene)nickel (0); (R)-1-[(Sp)-2-(dicyclohexylphosphanyl)ferrocenyl]ethyldicyclohexylphosphane; ammonia; sodium t-butanolate In 1,4-dioxane; toluene at 105℃; under 5895.64 - 7757.43 Torr; for 18h; Sealed tube; | 92% |
Conditions | Yield |
---|---|
With tris-(dibenzylideneacetone)dipalladium(0); N,N,N,N,-tetramethylethylenediamine; C38H62P2 In tetrahydrofuran at 20℃; for 16h; Negishi Coupling; Inert atmosphere; | 96% |
Conditions | Yield |
---|---|
With potassium phosphate; ((2-dicyclohexylphosphino-2',4’,6’-triisopropyl-1,1‘-biphenyl)[2-(2‘-amino-1,1‘-biphenyl)]palladium(II) methanesulfonate) In tetrahydrofuran at 20℃; for 0.5h; Suzuki-Miyaura Coupling; | 95% |
With potassium phosphate; methanesulfonic acid(2-dicyclohexylphosphino-2′,4′,6′-triisopropyl-1,1′-biphenyl)[2-(2′-amino-1,1′-biphenyl)]palladium(II) In tetrahydrofuran at 20℃; for 0.5h; Inert atmosphere; | 95% |
Conditions | Yield |
---|---|
With tert-butylammonium hexafluorophosphate(V); calcium(II) trifluoromethanesulfonate In neat (no solvent) at 130℃; Green chemistry; | 95% |
Conditions | Yield |
---|---|
With diethyl amine hydrochloride; triethylamine In 1,4-dioxane at 100℃; for 0.5h; Reagent/catalyst; Solvent; Temperature; | 95% |
Conditions | Yield |
---|---|
With iodine; oxygen In dimethyl sulfoxide at 110℃; | 95% |
2-methyl-7-chloroquinoline
tetramethylammonium trifluoromethylselenate(0)
Conditions | Yield |
---|---|
With 1,1'-bis-(diphenylphosphino)ferrocene; bis(1,5-cyclooctadiene)nickel (0) In toluene at 50℃; for 12h; Inert atmosphere; | 95% |
Conditions | Yield |
---|---|
With tert-butylammonium hexafluorophosphate(V); calcium(II) trifluoromethanesulfonate In neat (no solvent) at 130℃; Green chemistry; | 94% |
Conditions | Yield |
---|---|
With η3-1-tert-butylindenyl palladium chloride dimer In toluene at 70℃; for 4h; Hiyama Coupling; Inert atmosphere; Glovebox; Sealed tube; | 94% |
methanol
2-methyl-7-chloroquinoline
7-chloro-4-(hydroxymethyl)-2-methylquinoline
Conditions | Yield |
---|---|
With silver nitrate; Selectfluor In water at 80℃; for 4h; Sealed tube; | 94% |
With sodium persulfate In water at 80℃; for 4h; Reagent/catalyst; Inert atmosphere; | 85% |
With ferrous(II) sulfate heptahydrate; sulfuric acid; hydroxylamine-O-sulfonic acid In water for 3h; | 78% |
2-methyl-7-chloroquinoline
Conditions | Yield |
---|---|
With bis(1,5-cyclooctadiene)diiridium(I) dichloride; hydrogen; iodine; (((1R,3S,3'S)-3,3'-diethyl-3H,3'H-1,1'-spirobi[isobenzofuran]-7,7'-diyl)bis(oxy))bis(diphenylphosphane) In tetrahydrofuran at 20℃; under 18100.7 Torr; for 10h; Inert atmosphere; enantioselective reaction; | 94% |
2-methyl-7-chloroquinoline
methyl 2-(3-(3-formylphenyl)-3-oxopropyl)benzoate
methyl 2-(3-(3-(2-(7-chloro-2-quinolinyl)ethenyl)phenyl)-3-oxopropyl)benzoate
Conditions | Yield |
---|---|
With acetic anhydride at 140℃; for 8h; | 93% |
Conditions | Yield |
---|---|
With tert-butylammonium hexafluorophosphate(V); calcium(II) trifluoromethanesulfonate In neat (no solvent) at 130℃; Green chemistry; | 93% |
Conditions | Yield |
---|---|
With benzophenone In acetone at 20℃; for 4h; Microwave irradiation; | 93% |
2-methyl-7-chloroquinoline
7-chloro-quinoline-2-carbaldehyde
Conditions | Yield |
---|---|
With selenium(IV) oxide In 1,4-dioxane at 60℃; Inert atmosphere; | 92% |
With selenium(IV) oxide In 1,4-dioxane for 2.5h; Oxidation; Heating; | 84% |
With selenium(IV) oxide; water In tetrahydrofuran at 25℃; for 6h; | 78% |
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