As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
Cas:5162-03-8
Min.Order:1 Kilogram
FOB Price: $3.0
Type:Lab/Research institutions
inquiryhigh quality Appearance:white powder Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea Port:shanghai
Cas:5162-03-8
Min.Order:1 Kilogram
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Cas:5162-03-8
Min.Order:5 Kiloliter
FOB Price: $1.2 / 5.0
Type:Manufacturers
inquiryOur advantage:Our company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scient
Cas:5162-03-8
Min.Order:1 Kilogram
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inquiryProduct Description Product website: http://www.finerchem.com Product Name 2-Chlorobenzophenone CAS No. 5162-03-8
Cas:5162-03-8
Min.Order:1 Gram
FOB Price: $12.0
Type:Lab/Research institutions
inquiryOur advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva
Cas:5162-03-8
Min.Order:1 Kilogram
FOB Price: $9.0 / 99.0
Type:Trading Company
inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:5162-03-8
Min.Order:1 Kilogram
FOB Price: $139.0 / 210.0
Type:Trading Company
inquiryOur Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
Cas:5162-03-8
Min.Order:10 Kilogram
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Type:Trading Company
inquiryName: 2-Chlorobenzophenone Synonyms: (2-Chlorophenyl)phenyl-methanone CAS:5162-03-8 MF: C13H9ClO Appearance:White powder Storage:Store in cool and dry place, away from sun light. Package:25kg/drum Application:Organic synthesis Transportation:By s
1.In No Less 10 years exporting experience. you can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specializ
Cas:5162-03-8
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:5162-03-8
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiry1. Timely and efficient service to ensure communication with customers 2. Produce products of different specifications and sizes according to your requirements. 3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures s
Cas:5162-03-8
Min.Order:1 Kilogram
FOB Price: $80.0 / 100.0
Type:Lab/Research institutions
inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
We are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov
Cas:5162-03-8
Min.Order:100 Gram
FOB Price: $100.0 / 2000.0
Type:Lab/Research institutions
inquiryGMP standard, high purity, competitive price, in stock 1. Quick Response: within 6 hours after receiving your email. 2. Quality Guarantee: All products are strictly tested by our QC, confirmed by QA, and approved by a third-party lab in China, USA,
Cas:5162-03-8
Min.Order:1 Milligram
Negotiable
Type:Trading Company
inquiryProduct Name: (2-Chlorophenyl)phenyl-methanone Synonyms: O-CHLOROBENZOPHENONE;RARECHEM AM UC 0602;LABOTEST-BB LT00159660;(2-chlorophenyl)phenyl-methanone;2-CHLOROBENZOPHENONE;(2-chlorophenyl)phenyl-methanon;2-Chlorobenzophenone/o-Chlorobenzophe
Cas:5162-03-8
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
Cas:5162-03-8
Min.Order:1 Kilogram
FOB Price: $18.0 / 20.0
Type:Trading Company
inquiryProduct name: 2-Chlorobenzophenone CAS No.:5162-03-8 Molecule Formula:C13H9ClO Molecule Weight:216.67 Purity: 99.0% Package: 25kg/drum Description:White to yellow crystalline powder Manufacture Standards:Enterprise Standard
Cas:5162-03-8
Min.Order:1 Kilogram
Negotiable
Type:Trading Company
inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
Cas:5162-03-8
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiry1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
Cas:5162-03-8
Min.Order:1 Metric Ton
FOB Price: $1.5
Type:Trading Company
inquiryAppearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea
Stock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai
Cas:5162-03-8
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryWe are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp
Cas:5162-03-8
Min.Order:1 Metric Ton
FOB Price: $1.0
Type:Trading Company
inquiryLower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe
Cas:5162-03-8
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryJinhua huayi chemical co., ltd. is dedicated to the development, production and marketing of chemicals. On the basis of equality and mutual benefit, and under the principle of customer first, credit first, quality first, we are ready to join hands
Cas:5162-03-8
Min.Order:100 Gram
Negotiable
Type:Lab/Research institutions
inquirygood quality and cheap price Package:25kg/200kg Application:as intermediates Transportation:by courier/sea/air
Our clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS
Conditions | Yield |
---|---|
With aluminium trichloride for 19.5h; Heating; | 100% |
Friedel-Crafts reaction; | 90% |
iron(III) chloride at 109℃; for 0.458333h; Product distribution / selectivity; Irradiation; | 83% |
(2-chlorophenyl)phenylmethanone oxime
(2-chlorophenyl)(phenyl)methanone
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid at 20℃; for 0.0166667h; neat (no solvent); | 98% |
With periodic acid at 20℃; for 0.3h; | 86% |
Conditions | Yield |
---|---|
With C4F9SO3H at 130℃; for 0.333333h; Product distribution; var. of time, conc. of reagent; | 96% |
With aluminum (III) chloride for 6h; Friedel-Crafts Acylation; Reflux; |
sodium tetraphenyl borate
o-chlorobenzoyl chloride
(2-chlorophenyl)(phenyl)methanone
Conditions | Yield |
---|---|
With potassium fluoride; bis-triphenylphosphine-palladium(II) chloride In acetone for 0.15h; microwave irradiation (525 W); | 94% |
With aluminum oxide; bis-triphenylphosphine-palladium(II) chloride; potassium fluoride In acetone for 0.0833333h; MW-irradiation; | 90% |
With silica-supported diphenylphosphine palladium(0) In tetrahydrofuran at 40℃; for 48h; | 74% |
(2-chlorophenyl)(phenyl)methanol
(2-chlorophenyl)(phenyl)methanone
Conditions | Yield |
---|---|
With cobalt(III) acetate; sodium bromide In acetic acid at 60℃; for 1h; | 93% |
With peracetic acid; 4-acetylamino-2,2,6,6-tetramethyl-1-piperidinoxy In acetonitrile at 20℃; for 9h; | 93% |
With 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione at 80℃; for 0.5h; Reagent/catalyst; | 92% |
(o-benzyl)chlorobenzene
(2-chlorophenyl)(phenyl)methanone
Conditions | Yield |
---|---|
With pyridine; tert.-butylhydroperoxide; iodine In water at 80℃; chemoselective reaction; | 93% |
With N-Bromosuccinimide; water In chloroform for 3h; Reflux; | 92% |
With lithium perchlorate In water; acetonitrile at 20℃; for 5h; Electrolysis; | 67% |
2-Chlorobenzeneboronic acid
benzoyl chloride
(2-chlorophenyl)(phenyl)methanone
Conditions | Yield |
---|---|
With 2C60H80NaO12(2+)*Cl6Pd2(2-); potassium carbonate; triphenylphosphine In toluene at 70℃; for 12h; Suzuki Coupling; | 93% |
With [Pd(η(5)-C5H5)Fe(η(5)-C5H3-C(CH3)=N-C6H4-4-CH3)Cl(P(C6H5)3)]; potassium carbonate In toluene at 60℃; for 12h; Inert atmosphere; | 90% |
1-(o-chlorophenyl)-1-phenylethylene
(2-chlorophenyl)(phenyl)methanone
Conditions | Yield |
---|---|
With oxygen at 110℃; for 8h; Schlenk technique; Green chemistry; | 91% |
With oxygen at 110℃; for 8h; Sealed tube; | 90.9% |
With cerium(III) chloride; 1,1,1-trichloroethanol In acetonitrile at 25℃; for 40h; Irradiation; | 78% |
Conditions | Yield |
---|---|
With sodium periodate; tetraethylammonium iodide In water; acetonitrile at 105℃; for 12h; Sealed tube; | 89% |
Conditions | Yield |
---|---|
With dichloro bis(acetonitrile) palladium(II); cesium fluoride In 1-methyl-pyrrolidin-2-one at 80℃; under 760.051 Torr; for 6h; Hiyama Coupling; | 88% |
2-Chlorobenzeneboronic acid
Benzoylformic acid
(2-chlorophenyl)(phenyl)methanone
Conditions | Yield |
---|---|
With silver carbonate In acetonitrile at 60℃; for 1h; | 87% |
carbon monoxide
Phenyl triflate
2-Chlorobenzeneboronic acid
(2-chlorophenyl)(phenyl)methanone
Conditions | Yield |
---|---|
With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium(II) trifluoroacetate In tert-butyl methyl ether at 80℃; under 760.051 Torr; for 6h; Suzuki-Miyaura Coupling; | 87% |
Conditions | Yield |
---|---|
With copper(l) iodide; palladium(II) iodide at 120℃; for 3h; | 85% |
ortho-chlorobenzoic acid
phenylboronic acid
(2-chlorophenyl)(phenyl)methanone
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); water; N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline In N,N-dimethyl-formamide at 60℃; for 15h; Inert atmosphere; | 84% |
2-Chlorobenzeneboronic acid
benzaldehyde
(2-chlorophenyl)(phenyl)methanone
Conditions | Yield |
---|---|
With [Pd(2-((1-naphthalenyl)methylene)-N-phenylhydrazinecarbothioamide)Cl(PPh3)]; caesium carbonate In toluene at 110℃; for 12h; | 84% |
With potassium phosphate; 3,3-dimethyl-butan-2-one; C14H10Cl2N2O2Ru; tri tert-butylphosphoniumtetrafluoroborate In water; toluene at 100℃; for 24h; | 65% |
Conditions | Yield |
---|---|
With dipotassium peroxodisulfate; N-chloro-succinimide; trifluorormethanesulfonic acid; palladium diacetate In 1,2-dichloro-ethane at 80℃; for 10h; Reagent/catalyst; | 83% |
carbon monoxide
2-iodochlorobenzene
triethoxyphenylsilane
(2-chlorophenyl)(phenyl)methanone
Conditions | Yield |
---|---|
With dichloro bis(acetonitrile) palladium(II); cesium fluoride In 1-methyl-pyrrolidin-2-one at 80℃; under 760.051 Torr; for 6h; Hiyama Coupling; | 83% |
carbon monoxide
toluene-4-sulfonic acid phenyl ester
2-Chlorobenzeneboronic acid
(2-chlorophenyl)(phenyl)methanone
Conditions | Yield |
---|---|
With palladium(II) trifluoroacetate; 1,2-bis-(diphenylphosphino)ethane In N,N-dimethyl acetamide at 80℃; under 760.051 Torr; for 6h; Suzuki-Miyaura Coupling; | 83% |
2-chloro-benzaldehyde
phenylboronic acid
(2-chlorophenyl)(phenyl)methanone
Conditions | Yield |
---|---|
With [Pd(2-((1-naphthalenyl)methylene)-N-phenylhydrazinecarbothioamide)Cl(PPh3)]; caesium carbonate In toluene at 110℃; for 12h; | 83% |
With C36H28NO2PPd; caesium carbonate In toluene for 18h; Reagent/catalyst; Reflux; | 79% |
o-chlorobenzoyl chloride
phenylboronic acid
(2-chlorophenyl)(phenyl)methanone
Conditions | Yield |
---|---|
With potassium carbonate; (t-Bu2POH)2PdCl2 In 1,4-dioxane; toluene at 80℃; for 1h; Suzuki cross-coupling reaction; | 82% |
With water; sodium carbonate; 3-butyl-1-methyl-1H-imidazol-3-ium hexafluorophosphate; palladium diacetate at 60℃; for 3h; Suzuki reaction; | 80% |
With C28H40Br4N4Pd2; potassium carbonate In ethanol; water at 50℃; for 5h; Suzuki Coupling; | 78% |
With sodium dodecyl-sulfate; potassium carbonate; palladium dichloride In water at 60℃; for 6h; | 40% |
2-chlorobenzoic anhydride
phenylboronic acid
(2-chlorophenyl)(phenyl)methanone
Conditions | Yield |
---|---|
With PEG200; sodium carbonate; palladium diacetate at 60℃; for 3h; Suzuki reaction; | 82% |
With sodium carbonate; palladium dichloride In water; acetone at 20℃; for 1.5h; Suzuki type reaction; Inert atmosphere; | 78% |
With sodium dodecyl-sulfate; potassium carbonate; palladium dichloride In water at 60℃; for 6h; | 68% |
N-amino-o-chlorobenzenesulfonamide
benzonitrile
(2-chlorophenyl)(phenyl)methanone
Conditions | Yield |
---|---|
With 2,2'-biquinoline; water; palladium diacetate In dimethyl sulfoxide at 80℃; under 760.051 Torr; for 6h; | 82% |
Conditions | Yield |
---|---|
With dichloro bis(acetonitrile) palladium(II); cesium fluoride In 1-methyl-pyrrolidin-2-one at 100℃; under 760.051 Torr; for 6h; Hiyama Coupling; | 81% |
o-(α,α-dichlorobenzyl)phenyl phosphochloridate
(2-chlorophenyl)(phenyl)methanone
Conditions | Yield |
---|---|
With trichlorophosphate at 220℃; under 1 Torr; | 80% |
phenylglyoxylic acid potassium salt
(2-chlorophenyl)(phenyl)methanone
Conditions | Yield |
---|---|
With dipotassium peroxodisulfate; silver nitrate In water at 25℃; for 1h; Green chemistry; | 79% |
carbon monoxide
2-iodochlorobenzene
benzene
(2-chlorophenyl)(phenyl)methanone
Conditions | Yield |
---|---|
With bis(η3-allyl-μ-chloropalladium(II)); silver trifluoromethanesulfonate In 1,2-dichloro-ethane at 100℃; under 3040.2 Torr; for 24h; Inert atmosphere; Sealed tube; Glovebox; Schlenk technique; Green chemistry; chemoselective reaction; | 79% |
(2-Chloro-phenyl)-phenyl-methanethione
(2-chlorophenyl)(phenyl)methanone
Conditions | Yield |
---|---|
With clay supported ferric nitrate; Clayfen In dichloromethane for 8h; Ambient temperature; | 78% |
2-bromo-1-chlorobenzene
carbon monoxide
triethoxyphenylsilane
(2-chlorophenyl)(phenyl)methanone
Conditions | Yield |
---|---|
With dichloro bis(acetonitrile) palladium(II); cesium fluoride In 1-methyl-pyrrolidin-2-one at 100℃; under 760.051 Torr; for 6h; Hiyama Coupling; | 78% |
Conditions | Yield |
---|---|
With phosphorus pentachloride at 215 - 220℃; | 77.2% |
(2-chlorophenyl)(phenyl)methanone
(2-chlorophenyl)(phenyl)methanol
Conditions | Yield |
---|---|
With N-methylpyrrolidine zinc borohydride In tetrahydrofuran for 0.5h; Heating; | 100% |
With [(OC-6-13)-RuCl2[P(p-CH3C6H5)3]2(en)]; potassium tert-butylate; hydrogen In isopropyl alcohol; tert-butyl alcohol at 28℃; under 6080.41 Torr; for 12h; Catalytic hydrogenation; | 95% |
With sodium tetrahydroborate In ethanol at 20℃; for 3h; | 94.1% |
(2-chlorophenyl)(phenyl)methanone
(S)-2-chlorobenzhydrol
Conditions | Yield |
---|---|
Stage #1: (2-chlorophenyl)(phenyl)methanone With (R)-((4,4’-bi-1,3-benzodioxole)-5,5’-diyl)bis(bis(3,5-di-t-butyl-4-methoxyphenyl))phosphine; polymethylhydrosiloxane; copper(l) chloride; sodium t-butanolate In toluene at -30℃; for 13h; Inert atmosphere; Stage #2: With sodium hydroxide; water In ethyl acetate; toluene for 1h; Inert atmosphere; optical yield given as %ee; enantioselective reaction; | 99% |
With formic acid; ((R,R)-Ts-DENEB)RuCl; triethylamine at 40℃; for 17h; Reagent/catalyst; Inert atmosphere; enantioselective reaction; | 99% |
With C32H39BrMnN2O2P; potassium tert-butylate; hydrogen In methanol at 20℃; under 22502.3 Torr; for 16h; Glovebox; Autoclave; enantioselective reaction; | 99% |
(2-chlorophenyl)(phenyl)methanone
p-tolylzinc(II) chloride
(4′-methylbiphenyl-2-yl)(phenyl)methanone
Conditions | Yield |
---|---|
With C26H24ClN2NiP*0.1C7H8 In tetrahydrofuran; 1-methyl-pyrrolidin-2-one at 80℃; for 24h; Negishi Coupling; Schlenk technique; Inert atmosphere; | 99% |
With Ni(Cl){2-(Ph2P(O))C6H4NCH(Ph)PPh2} In tetrahydrofuran; 1-methyl-pyrrolidin-2-one at 25℃; for 24h; Negishi coupling reaction; Inert atmosphere; | 98% |
With C27H22Cl2N3NiP In tetrahydrofuran; 1-methyl-pyrrolidin-2-one for 24h; Inert atmosphere; Schlenk technique; Heating; | 91% |
(2-chlorophenyl)(phenyl)methanone
Conditions | Yield |
---|---|
With bis(1,5-cyclooctadiene)diiridium(I) dichloride; C43H53FeN2O2PS; hydrogen; lithium tert-butoxide In isopropyl alcohol at 25 - 30℃; under 22801.5 Torr; for 12h; Autoclave; enantioselective reaction; | 98% |
With potassium tert-butylate; hydrogen; triphenylphosphine In toluene; tert-butyl alcohol at 25℃; under 15201 Torr; for 24h; Product distribution / selectivity; | 95% |
With hydrogen; C34H63ClIrNP2; lithium tert-butoxide In hexane; toluene at 20℃; under 38002.6 Torr; for 24h; Autoclave; enantioselective reaction; | 95% |
(2-chlorophenyl)(phenyl)methanone
4-methoxyphenyl magnesium bromide
(4′-methoxylbiphenyl-2-yl)(phenyl)methanone
Conditions | Yield |
---|---|
Stage #1: 4-methoxyphenyl magnesium bromide In tetrahydrofuran at -20℃; for 0.166667h; Stage #2: (2-chlorophenyl)(phenyl)methanone With para-fluorostyrene; tetra-(n-butyl)ammonium iodide; cobalt acetylacetonate In tetrahydrofuran; 1,2-dimethoxyethane at 25℃; for 1h; | 98% |
Stage #1: 4-methoxyphenyl magnesium bromide In tetrahydrofuran at -20℃; for 0.166667h; Stage #2: (2-chlorophenyl)(phenyl)methanone With 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; para-fluorostyrene; tetra-(n-butyl)ammonium iodide; cobalt acetylacetonate In tetrahydrofuran; 1,2-dimethoxyethane at 25℃; for 1h; Further stages.; | 98% |
(2-chlorophenyl)(phenyl)methanone
para-bromotoluene
(4′-methylbiphenyl-2-yl)(phenyl)methanone
Conditions | Yield |
---|---|
Stage #1: para-bromotoluene With lithium Stage #2: With zinc(II) chloride Stage #3: (2-chlorophenyl)(phenyl)methanone; nickel amido phosphine pincer complex In tetrahydrofuran; 1-methyl-pyrrolidin-2-one at 100℃; for 24h; Negishi cross-coupling; Further stages.; | 98% |
(2-chlorophenyl)(phenyl)methanone
(4-(trifluoromethyl)phenyl)zinc(II) chloride
Conditions | Yield |
---|---|
With C26H24ClN2NiP*0.1C7H8 In tetrahydrofuran; 1-methyl-pyrrolidin-2-one at 80℃; for 24h; Negishi Coupling; Schlenk technique; Inert atmosphere; | 98% |
(2-chlorophenyl)(phenyl)methanone
Conditions | Yield |
---|---|
With Li2CoCl4; sodium formate In tetrahydrofuran at 25℃; Negishi Coupling; Inert atmosphere; Schlenk technique; | 98% |
trifluoromethan
(2-chlorophenyl)(phenyl)methanone
2,2,2-trifluoro-1-(2-chlorophenyl)-1-phenylethanol
Conditions | Yield |
---|---|
Stage #1: trifluoromethan; (2-chlorophenyl)(phenyl)methanone With tris(trimethylsilyl)amine; phosphazene base-P4-tert-butyl In tetrahydrofuran at 20℃; for 10h; Schlenk technique; Stage #2: With tetrabutyl ammonium fluoride In tetrahydrofuran at 20℃; for 1h; Schlenk technique; | 98% |
With potassium tert-butylate In N,N-dimethyl-formamide at 20℃; under 750.075 Torr; for 0.000138889h; Flow reactor; | 74% |
Conditions | Yield |
---|---|
Stage #1: 3-cyanobromobenzene With TurboGrignard In tetrahydrofuran at 0℃; for 3h; Stage #2: In tetrahydrofuran at -20℃; for 0.166667h; Stage #3: (2-chlorophenyl)(phenyl)methanone With para-fluorostyrene; tetra-(n-butyl)ammonium iodide; cobalt acetylacetonate In tetrahydrofuran; 1,2-dimethoxyethane at 25℃; for 1.5h; | 96% |
Conditions | Yield |
---|---|
Stage #1: phenylmagnesium bromide In tetrahydrofuran at -20℃; for 0.166667h; Stage #2: (2-chlorophenyl)(phenyl)methanone With para-fluorostyrene; tetra-(n-butyl)ammonium iodide; cobalt acetylacetonate In tetrahydrofuran; 1,2-dimethoxyethane at 25℃; for 0.25h; | 95% |
Conditions | Yield |
---|---|
With 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; para-fluorostyrene; tetra-(n-butyl)ammonium iodide; cobalt acetylacetonate In tetrahydrofuran; 1,2-dimethoxyethane at 25℃; for 0.25h; | 95% |
Conditions | Yield |
---|---|
With potassium hexamethylsilazane In toluene at 20℃; for 0.25h; Inert atmosphere; | 95% |
(2-chlorophenyl)(phenyl)methanone
butyl magnesium bromide
(2-butyl-phenyl)-phenyl-methanone
Conditions | Yield |
---|---|
Stage #1: butyl magnesium bromide With lithium chloride; manganese(ll) chloride In tetrahydrofuran at -10℃; Stage #2: (2-chlorophenyl)(phenyl)methanone In tetrahydrofuran at -5℃; for 0.75h; | 94% |
(2-chlorophenyl)(phenyl)methanone
Conditions | Yield |
---|---|
With N-Methyldicyclohexylamine; [iridium(2-(4-fluorophenyl)pyridinato)2(2,2'-bipyridine)]hexafluorophosphate; water-d2; lithium carbonate In acetonitrile Irradiation; | 94% |
(2-chlorophenyl)(phenyl)methanone
Conditions | Yield |
---|---|
With chromium dichloride In tetrahydrofuran at 25℃; for 0.25h; Inert atmosphere; | 93% |
(2-chlorophenyl)(phenyl)methanone
Conditions | Yield |
---|---|
With Li2CoCl4; N,N,N,N,-tetramethylethylenediamine In tetrahydrofuran; 1,4-dioxane at 20℃; for 8h; Catalytic behavior; Reagent/catalyst; Solvent; Inert atmosphere; Schlenk technique; | 93% |
(2-chlorophenyl)(phenyl)methanone
para-methylphenylmagnesium bromide
A
(4,4'-dimethyl-1,1'-biphenyl)
B
(4′-methylbiphenyl-2-yl)(phenyl)methanone
Conditions | Yield |
---|---|
With C80H88Cl2N6NiP2; water; lithium chloride; zinc(II) chloride In tetrahydrofuran; 1-methyl-pyrrolidin-2-one at 55℃; Kumada coupling reaction; Inert atmosphere; | A n/a B 92% |
(2-chlorophenyl)(phenyl)methanone
phenylmagnesium bromide
2-phenylbenzophenone
Conditions | Yield |
---|---|
Stage #1: phenylmagnesium bromide With titanium(IV) tetraethanolate In tetrahydrofuran at 20℃; for 0.5h; Inert atmosphere; Stage #2: (2-chlorophenyl)(phenyl)methanone With tributylphosphine; cobalt(II) chloride In tetrahydrofuran at 20℃; Inert atmosphere; chemoselective reaction; | 92% |
Stage #1: (2-chlorophenyl)(phenyl)methanone With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate In tetrahydrofuran; toluene Kumada Cross-Coupling; Inert atmosphere; Sealed tube; Stage #2: phenylmagnesium bromide In tetrahydrofuran; toluene at 20℃; for 2h; Kumada Cross-Coupling; Inert atmosphere; Sealed tube; chemoselective reaction; | 82% |
Conditions | Yield |
---|---|
With W-7 Raney-Nickel In ethanol for 6h; Heating; | 91% |
(2-chlorophenyl)(phenyl)methanone
(3-dimethylaminopropyl)-triphenylphosphoniumbromide
Conditions | Yield |
---|---|
Stage #1: (3-dimethylaminopropyl)-triphenylphosphoniumbromide With n-butyllithium In tetrahydrofuran; hexane at 0℃; Wittig reaction; Stage #2: (2-chlorophenyl)(phenyl)methanone In tetrahydrofuran; hexane at 0 - 20℃; Further stages.; | 91% |
Conditions | Yield |
---|---|
Stage #1: phenyllithium With titanium(IV) tetraethanolate In tetrahydrofuran at 20℃; for 0.5h; Inert atmosphere; Stage #2: (2-chlorophenyl)(phenyl)methanone With tributylphosphine; cobalt(II) chloride In tetrahydrofuran at 20℃; Inert atmosphere; chemoselective reaction; | 91% |
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