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Dayang Chem (Hangzhou) Co.,Ltd.

DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe

2-Methyl-5-nitrophenol Manufacturer/High quality/Best price/In stock

Cas:5428-54-6

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

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Wuhan Fortuna Chemical Co.,Ltd

Best price 2-Methyl-5-nitrophenol CAS 5428-54-6 with high purity Company profile Wuhan Fortuna Chemical Co.,Ltd established in 2006, is a big integrative chemical enterprise being engaged in Pharmaceutical & its intermediates, Food/Feed addi

Best price 2-Methyl-5-nitrophenol CAS 5428-54-6 with high purity

Cas:5428-54-6

Min.Order:10 Kilogram

FOB Price: $10.0

Type:Trading Company

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Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

5-Nitro-o-cresol (OH=1)

Cas:5428-54-6

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

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Hebei Nengqian Chemical Import and Export Co., LTD

Our advantages: 1, High quality with competitive price: 1) Standard:BP/USP/EP/Enterprise standard 2) All Purity≥99% 3) We are manufacturer and can provide high quality products with factory price. 2, Fast and safe delivery 1) Parcel can

2-Methyl-5-nitrophenol CAS:5428-54-6

Cas:5428-54-6

Min.Order:1 Metric Ton

FOB Price: $520.0 / 888.0

Type:Trading Company

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Henan Tianfu Chemical Co., Ltd.

Henan Tianfu Chemical Co., Ltd. is located in Zhengzhou High-tech Development Zone with import and export license. We passed ISO 9001:2008 in 2009, and won "High-tech Enterprise" by provincial government in 2013.The objective of the com

TIANFU-CHEM - 2-Methyl-5-nitrophenol

Cas:5428-54-6

Min.Order:1 Gram

FOB Price: $1000.0

Type:Lab/Research institutions

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Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

New production CAS 5428-54-6 with best quality

Cas:5428-54-6

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

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Henan Sinotech Import&Export Corporation

Chemical Name: 2-Methyl-5-nitrophenol CAS No.:5428-54-6 Molecular Formula:C7H7NO3 Molecular weight: 153.14 Appearance: Light yellow powder Appearance:Light yellow powder Storage:Store in cool and dry place, away from sun light. Package:25kg

2-Methyl-5-nitrophenol CAS: 5428-54-6

Cas:5428-54-6

Min.Order:5 Metric Ton

FOB Price: $1.0 / 2.0

Type:Other

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Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

2-Methyl-5-nitrophenol 5428-54-6

Cas:5428-54-6

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Qingdao Beluga Import and Export Co., LTD

2-Methyl-5-nitrophenol CAS:5428-54-6 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic in

2-Methyl-5-nitrophenol CAS:5428-54-6

Cas:5428-54-6

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

2-Methyl-5-nitrophenol

Cas:5428-54-6

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Hebei Quanhe Biotechnology Co. LTD

1. Timely and efficient service to ensure communication with customers 2. Produce products of different specifications and sizes according to your requirements. 3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures

2-Methyl-5-nitrophenol

Cas:5428-54-6

Min.Order:1 Kilogram

FOB Price: $1.0 / 3.0

Type:Lab/Research institutions

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Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

2-Methyl-5-nitrophenol

Cas:5428-54-6

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Xiamen Hisunny Chemical Co.,Ltd

Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia

5-Nitro-O-Cresol

Cas:5428-54-6

Min.Order:0

Negotiable

Type:Manufacturers

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Hubei Jiutian Bio-medical Technology Co., Ltd

1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists of highly qualifie

CAS 5428-54-6 2-Methyl-5-nitrophenol

Cas:5428-54-6

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

2-Methyl-5-nitrophenol

Cas:5428-54-6

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply 2-Methyl-5-nitrophenol

Cas:5428-54-6

Min.Order:0 Metric Ton

Negotiable

Type:Other

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Shanghai Massive Chemical Technology Co., Ltd.

Massive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and

2-Methyl-5-nitrophenol

Cas:5428-54-6

Min.Order:1 Gram

FOB Price: $1.0

Type:Lab/Research institutions

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Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

2-Methyl-5-nitrophenol

Cas:5428-54-6

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

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HANGZHOU YUNUO CHEMICAL CO.,LTD

superior quality moderate price & quick delivery Appearance:Brown solid Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:1kg/bag, 1kg/drum or 25kg/drum or as per your request. Application:Used to make other c

2-Methyl-5-nitrophenol

Cas:5428-54-6

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

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Siwei Development Group Ltd.

Product name: 5-Nitro-O-Cresol(2-Methyl-5-Nitrophenol) CAS No.:5428-54-6 Molecule Formula:C18H19Cl2NO4 Molecule Weight:384.25 Purity: 99.0% Package: 25kg/bag Description:Yellow crystalline powder Manufacture Standards:Enterprise Stand

Best Quality 5-Nitro-O-Cresol(2-Methyl-5-Nitrophenol)

Cas:5428-54-6

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

inquiry

Xiamen Jenny Chemical Technology Co., Ltd.

GMP standard, high purity, competitive price, in stock 1. Quick Response: within 6 hours after receiving your email. 2. Quality Guarantee: All products are strictly tested by our QC, confirmed by QA, and approved by a third-party lab in China, USA,

2-Methyl-5-nitrophenol

Cas:5428-54-6

Min.Order:1 Milligram

Negotiable

Type:Trading Company

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Shanghai Minstar Chemical Co., Ltd

2-Methyl-5-nitrophenol Chemical Properties Melting point 111-115 °C(lit.) Boiling point 180 °C / 15mmHg density 1.320±0.06 g/cm3(Predicted) pka 8.68±0.19(Predicted) CAS DataBase Reference 5428-54-6(CAS DataBase

2-Methyl-5-nitrophenol

Cas:5428-54-6

Min.Order:1 Gram

FOB Price: $66.0

Type:Lab/Research institutions

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Hunan chemfish Pharmaceutical co.,Ltd

Appearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea

2-Methyl-5-nitrophenol

Cas:5428-54-6

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Suzhou Health Chemicals Co., Ltd.

High quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use

2-Methyl-5-nitrophenol

Cas:5428-54-6

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Win-Win chemical Co.Ltd

Stock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai

2-methyl-5-nitrophenol cas no. 5428-54-6 98%

Cas:5428-54-6

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Kono Chem Co.,Ltd

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou

2-Methyl-5-nitrophenol

Cas:5428-54-6

Min.Order:0

Negotiable

Type:Other

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Hangzhou Dingyan Chem Co., Ltd

R & D enterprises have their own stock in stockAppearance:To be subject to the object Package:Customized Application:pharmaceutical intermediates Transportation:Air Port:Shanghai;Guangzhou

2-Methyl-5-nitrophenol

Cas:5428-54-6

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

GIHI CHEMICALS CO.,LIMITED

high purity,in stock Package:25kg/drum,or as per customers'demand Application:API,or Intermediates,fine chemicals Transportation:air,sea,courier

5-Nitro-o-cresol

Cas:5428-54-6

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Shanghai Acmec Biochemical Technology Co., Ltd.

Acmec is a leading manufacturer and supplier of biochemical reagents and life science products. We have over 40,000 items in stock (real-time inventory) and offer discounted prices to registered members of the online store ( www.acmec.com.cn ) Appea

Acmec 2-Methyl-5-nitrophenol 500g

Cas:5428-54-6

Min.Order:1 bottle

Negotiable

Type:Lab/Research institutions

inquiry

Henan Allgreen Chemical Co.,Ltd

high quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea

2-Methyl-5-nitrophenol

Cas:5428-54-6

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Synthetic route

2-methyl-5-nitroaniline
99-55-8

2-methyl-5-nitroaniline

2-methyl-5-nitrophenol
5428-54-6

2-methyl-5-nitrophenol

Conditions
ConditionsYield
With sulfuric acid; sodium nitrite In water for 0.333333h; Heating;93%
With sulfuric acid; sodium nitrite In water Heating;87%
Diazotization.Reaktion ueber mehrere Stufen;
5-Nitroso-o-kresol
21565-00-4

5-Nitroso-o-kresol

2-methyl-5-nitrophenol
5428-54-6

2-methyl-5-nitrophenol

Conditions
ConditionsYield
With sodium hydroxide; water; dihydrogen peroxide; sodium tungstate for 3h;61%
2-methyl-5-nitroaniline
99-55-8

2-methyl-5-nitroaniline

A

2-methyl-5-nitrophenol
5428-54-6

2-methyl-5-nitrophenol

B

6-nitroindazole
7597-18-4

6-nitroindazole

Conditions
ConditionsYield
With sulfuric acid; water; sodium nitrite Diazotization;
sulfuric acid
7664-93-9

sulfuric acid

2-methyl-5-nitroaniline
99-55-8

2-methyl-5-nitroaniline

sodium nitrite

sodium nitrite

A

2-methyl-5-nitrophenol
5428-54-6

2-methyl-5-nitrophenol

B

6-nitroindazole
7597-18-4

6-nitroindazole

Conditions
ConditionsYield
Diazotization;
sulfuric acid
7664-93-9

sulfuric acid

di-o-tolyl carbonate
617-09-4

di-o-tolyl carbonate

nitric acid
7697-37-2

nitric acid

A

2-methyl-4-nitrophenol
99-53-6

2-methyl-4-nitrophenol

B

2-methyl-5-nitrophenol
5428-54-6

2-methyl-5-nitrophenol

C

2-methyl-6-nitrophenol
13073-29-5

2-methyl-6-nitrophenol

Conditions
ConditionsYield
at -15 - 0℃; Kochen des Reaktionsprodukts mit wss. K2CO3-Loesung;
N-(2-methyl-5-nitro-phenyl)-N'-p-tolyl-triazene

N-(2-methyl-5-nitro-phenyl)-N'-p-tolyl-triazene

acid

acid

A

2-methyl-5-nitrophenol
5428-54-6

2-methyl-5-nitrophenol

B

p-toluidine
106-49-0

p-toluidine

C

nitrogen

nitrogen

hydrogenchloride
7647-01-0

hydrogenchloride

N-(2-methyl-5-nitro-phenyl)-N'-o-tolyl-triazene
861519-76-8

N-(2-methyl-5-nitro-phenyl)-N'-o-tolyl-triazene

A

2-methyl-5-nitrophenol
5428-54-6

2-methyl-5-nitrophenol

B

o-toluidine
95-53-4

o-toluidine

C

nitrogen

nitrogen

sulfuric acid
7664-93-9

sulfuric acid

N-(2-methyl-5-nitro-phenyl)-N'-o-tolyl-triazene
861519-76-8

N-(2-methyl-5-nitro-phenyl)-N'-o-tolyl-triazene

A

2-methyl-5-nitrophenol
5428-54-6

2-methyl-5-nitrophenol

B

o-toluidine
95-53-4

o-toluidine

C

nitrogen

nitrogen

N-(2-methyl-5-nitro-phenyl)-N'-o-tolyl-triazene
861519-76-8

N-(2-methyl-5-nitro-phenyl)-N'-o-tolyl-triazene

acetic acid
64-19-7

acetic acid

A

2-methyl-5-nitrophenol
5428-54-6

2-methyl-5-nitrophenol

B

o-toluidine
95-53-4

o-toluidine

C

nitrogen

nitrogen

hydrogenchloride
7647-01-0

hydrogenchloride

N-(2-methyl-5-nitro-phenyl)-N'-o-tolyl-triazene
861519-76-8

N-(2-methyl-5-nitro-phenyl)-N'-o-tolyl-triazene

β-naphthol
135-19-3

β-naphthol

A

2-methyl-5-nitrophenol
5428-54-6

2-methyl-5-nitrophenol

B

o-toluidine
95-53-4

o-toluidine

C

pigment orange 3
6410-15-7

pigment orange 3

D

nitrogen

nitrogen

o-toluidine
95-53-4

o-toluidine

ester of glycine

ester of glycine

2-methyl-5-nitrophenol
5428-54-6

2-methyl-5-nitrophenol

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 36 percent / conc. HNO3, conc. H2SO4 / 2 - 5 °C
2: 1.) H2SO4, NaNO2 / 1.) 2-5 deg C, 2.) heating
View Scheme
N-(2-methylphenyl)acetamide
120-66-1

N-(2-methylphenyl)acetamide

2-methyl-5-nitrophenol
5428-54-6

2-methyl-5-nitrophenol

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: sulfuric acid; HNO3+H2SO4 / Verseifung der Acetylverbindung
2: concentrated sulfuric acid; water; NaNO2 / Diazotization
View Scheme
o-toluidine
95-53-4

o-toluidine

2-methyl-5-nitrophenol
5428-54-6

2-methyl-5-nitrophenol

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: sulfuric acid; nitric acid
2: concentrated sulfuric acid; water; NaNO2 / Diazotization
View Scheme
2,4-dinitrotoluene
121-14-2

2,4-dinitrotoluene

A

2-methyl-5-nitrophenol
5428-54-6

2-methyl-5-nitrophenol

B

4-Methyl-3-nitroanilin
119-32-4

4-Methyl-3-nitroanilin

C

2-methyl-5-nitroaniline
99-55-8

2-methyl-5-nitroaniline

Conditions
ConditionsYield
With hydrogen In methanol at 36℃; under 760.051 Torr; for 0.25h;
2-methyl-5-nitrophenol
5428-54-6

2-methyl-5-nitrophenol

acetic anhydride
108-24-7

acetic anhydride

2-acetoxy-4-nitrotoluene
54362-24-2

2-acetoxy-4-nitrotoluene

Conditions
ConditionsYield
With sodium hydroxide In water at 20℃; for 0.666667h;100%
With dmap; triethylamine In dichloromethane at 20℃; for 2h; Inert atmosphere;99%
With pyridine at 20℃; for 6h;91%
With pyridine at 0 - 20℃; for 6h;91%
With pyridine at 20℃; for 24h;86%
1-iodohexadecane
544-77-4

1-iodohexadecane

2-methyl-5-nitrophenol
5428-54-6

2-methyl-5-nitrophenol

2-hexadecyloxy-4-nitrotoluene
915711-10-3

2-hexadecyloxy-4-nitrotoluene

Conditions
ConditionsYield
With 18-crown-6 ether; potassium carbonate In tetrahydrofuran Reflux;100%
With 18-crown-6 ether; potassium carbonate In tetrahydrofuran at 80℃;95%
2-methyl-5-nitrophenol
5428-54-6

2-methyl-5-nitrophenol

2-acetoxy-4-nitrotoluene
54362-24-2

2-acetoxy-4-nitrotoluene

Conditions
ConditionsYield
With acetic anhydride; sodium hydroxide In water at 20℃; for 0.666667h;100%
2-methyl-5-nitrophenol
5428-54-6

2-methyl-5-nitrophenol

A

3-acetoxy-4-methylaniline
61995-11-7

3-acetoxy-4-methylaniline

B

2-acetoxy-4-nitrotoluene
54362-24-2

2-acetoxy-4-nitrotoluene

Conditions
ConditionsYield
With sodium hydroxide; acetic anhydride; palladium In ethyl acetateA 94%
B 100%
With sodium hydroxide; acetic anhydrideA 94%
B 100%
2-methyl-5-nitrophenol
5428-54-6

2-methyl-5-nitrophenol

tert-butylchlorodiphenylsilane
58479-61-1

tert-butylchlorodiphenylsilane

3-tert-butyldiphenylsilyloxy-4-methylnitrobenzene

3-tert-butyldiphenylsilyloxy-4-methylnitrobenzene

Conditions
ConditionsYield
Stage #1: 2-methyl-5-nitrophenol With 1H-imidazole In N,N-dimethyl-formamide at 20℃; for 0.166667h;
Stage #2: tert-butylchlorodiphenylsilane In N,N-dimethyl-formamide at 20℃; for 4h;
100%
With 1H-imidazole In dichloromethane at 20℃; for 5h;88%
With 1H-imidazole In N,N-dimethyl-formamide at 20℃; under 3750.38 Torr; for 4h;
With 1H-imidazole In dichloromethane
2-methyl-5-nitrophenol
5428-54-6

2-methyl-5-nitrophenol

ethyl iodide
75-03-6

ethyl iodide

2-ethoxy-1-methyl-4-nitrobenzene
2486-63-7

2-ethoxy-1-methyl-4-nitrobenzene

Conditions
ConditionsYield
With potassium carbonate In N,N-dimethyl-formamide at 40℃; Inert atmosphere;100%
With potassium carbonate In acetone for 48h; Reflux;
2-methyl-5-nitrophenol
5428-54-6

2-methyl-5-nitrophenol

benzyl bromide
100-39-0

benzyl bromide

2-(benzyloxy)-1-methyl-4-nitrobenzene
219492-11-2

2-(benzyloxy)-1-methyl-4-nitrobenzene

Conditions
ConditionsYield
With potassium carbonate In acetone for 2h; Inert atmosphere; Reflux;99%
With potassium carbonate In acetonitrile at 80℃; for 2h;97%
With potassium carbonate In N,N-dimethyl-formamide at 60℃; Inert atmosphere;90%
With sodium carbonate In acetone1.06 g (33%)
2-methyl-5-nitrophenol
5428-54-6

2-methyl-5-nitrophenol

5-fluoro-2-nitrobenzoic acid
320-98-9

5-fluoro-2-nitrobenzoic acid

5-(2-methyl-5-nitrophenoxy)-2-nitrobenzoic acid
878743-92-1

5-(2-methyl-5-nitrophenoxy)-2-nitrobenzoic acid

Conditions
ConditionsYield
Stage #1: 2-methyl-5-nitrophenol; 5-fluoro-2-nitrobenzoic acid With potassium carbonate In N,N-dimethyl-formamide at 100℃; for 48h;
Stage #2: With hydrogenchloride In water; N,N-dimethyl-formamide
99%
2-methyl-5-nitrophenol
5428-54-6

2-methyl-5-nitrophenol

chloroacetone
78-95-5

chloroacetone

4-Methyl-1-nitro-3-(2'-oxopropyloxy)benzene
107188-56-7

4-Methyl-1-nitro-3-(2'-oxopropyloxy)benzene

Conditions
ConditionsYield
With potassium carbonate In acetone Heating;98%
2-methyl-5-nitrophenol
5428-54-6

2-methyl-5-nitrophenol

3-chloro-2-butanone
4091-39-8

3-chloro-2-butanone

1-methyl-2-(1-methyl-2-oxoprop-1-yloxy)-4-nitrobenzene
203940-76-5

1-methyl-2-(1-methyl-2-oxoprop-1-yloxy)-4-nitrobenzene

Conditions
ConditionsYield
With potassium carbonate In acetone for 10h; Heating;98%
2-methyl-5-nitrophenol
5428-54-6

2-methyl-5-nitrophenol

2-chloro-6-methyl-3-nitro-phenol
39183-20-5

2-chloro-6-methyl-3-nitro-phenol

Conditions
ConditionsYield
With chlorine In chloroform for 0.5h; Heating;96%
With chloroform; chlorine
2-methyl-5-nitrophenol
5428-54-6

2-methyl-5-nitrophenol

methyl iodide
74-88-4

methyl iodide

2-methyl-5-nitroanisole
13120-77-9

2-methyl-5-nitroanisole

Conditions
ConditionsYield
With tetra(n-butyl)ammonium hydrogensulfate; potassium hydroxide In water; toluene at 20℃;96%
With potassium carbonate In N,N-dimethyl-formamide at 40℃; Inert atmosphere;96%
With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 9h;74%
With potassium carbonate In acetone for 5h; Heating / reflux;72%
2-methyl-5-nitrophenol
5428-54-6

2-methyl-5-nitrophenol

1-iodo-propane
107-08-4

1-iodo-propane

1-methyl-4-nitro-2-n-propoxybenzene
854256-33-0

1-methyl-4-nitro-2-n-propoxybenzene

Conditions
ConditionsYield
With potassium carbonate In N,N-dimethyl-formamide at 40℃; Inert atmosphere;96%
2-methyl-5-nitrophenol
5428-54-6

2-methyl-5-nitrophenol

phenoxyethyl bromide
589-10-6

phenoxyethyl bromide

1-methyl-4-nitro-2-(2-phenoxyethoxy)benzene

1-methyl-4-nitro-2-(2-phenoxyethoxy)benzene

Conditions
ConditionsYield
With caesium carbonate In N,N-dimethyl-formamide at 40℃;96%
2-methyl-5-nitrophenol
5428-54-6

2-methyl-5-nitrophenol

2-propynyl chloride
624-65-7

2-propynyl chloride

4-methyl-1-nitro-3-propargyloxybenzene
136187-53-6

4-methyl-1-nitro-3-propargyloxybenzene

Conditions
ConditionsYield
With potassium carbonate In acetone Heating;95%
2-methyl-5-nitrophenol
5428-54-6

2-methyl-5-nitrophenol

1,1-dimethyl-2-propynyl trifluoroacetate
61570-79-4

1,1-dimethyl-2-propynyl trifluoroacetate

1-methyl-2-[(2-methylbut-3-yn-2-yl)oxy]-4-nitrobenzene
184896-34-2

1-methyl-2-[(2-methylbut-3-yn-2-yl)oxy]-4-nitrobenzene

Conditions
ConditionsYield
With copper(II) choride dihydrate; 1,8-diazabicyclo[5.4.0]undec-7-ene In acetonitrile at -10 - 20℃; Inert atmosphere;95%
With copper(II) chloride dihydrate; 1,8-diazabicyclo[5.4.0]undec-7-ene In acetonitrile at 0℃; for 7h;
1-iodo-butane
542-69-8

1-iodo-butane

2-methyl-5-nitrophenol
5428-54-6

2-methyl-5-nitrophenol

2-butoxy-1-methyl-4-nitrobenzene
57264-52-5

2-butoxy-1-methyl-4-nitrobenzene

Conditions
ConditionsYield
With potassium carbonate In N,N-dimethyl-formamide at 40℃; Inert atmosphere;93%
2-methyl-5-nitrophenol
5428-54-6

2-methyl-5-nitrophenol

isopropyl bromide
75-26-3

isopropyl bromide

2-isopropyloxy-1-methyl-4-nitrobenzene
136187-51-4

2-isopropyloxy-1-methyl-4-nitrobenzene

Conditions
ConditionsYield
With sodium hydroxide In N,N-dimethyl-formamide at 90℃; for 2.5h;92%
2-methyl-5-nitrophenol
5428-54-6

2-methyl-5-nitrophenol

2-methyl-but-3-yn-2-ol
115-19-5

2-methyl-but-3-yn-2-ol

1-methyl-2-[(2-methylbut-3-yn-2-yl)oxy]-4-nitrobenzene
184896-34-2

1-methyl-2-[(2-methylbut-3-yn-2-yl)oxy]-4-nitrobenzene

Conditions
ConditionsYield
Stage #1: 2-methyl-but-3-yn-2-ol With 1,8-diazabicyclo[5.4.0]undec-7-ene; trifluoroacetic anhydride In acetonitrile at -10℃; Inert atmosphere;
Stage #2: 2-methyl-5-nitrophenol With copper(II) choride dihydrate at -10 - 20℃; Inert atmosphere;
92%
2-methyl-5-nitrophenol
5428-54-6

2-methyl-5-nitrophenol

tert-butyldimethylsilyl chloride
18162-48-6

tert-butyldimethylsilyl chloride

tert-butyldimethyl(2-methyl-5-nitrophenoxy)silane
1226973-96-1

tert-butyldimethyl(2-methyl-5-nitrophenoxy)silane

Conditions
ConditionsYield
With triethylamine In N,N-dimethyl-formamide at 20℃; for 16h;91%
triisopropylsilyl chloride
13154-24-0

triisopropylsilyl chloride

2-methyl-5-nitrophenol
5428-54-6

2-methyl-5-nitrophenol

4-methyl-3-(triisopropylsilyloxy)aniline
582322-76-7

4-methyl-3-(triisopropylsilyloxy)aniline

Conditions
ConditionsYield
Stage #1: triisopropylsilyl chloride; 2-methyl-5-nitrophenol With 1H-imidazole In N,N-dimethyl-formamide at 20℃; for 21h; Inert atmosphere;
Stage #2: With iron; acetic acid at 40℃; for 4h;
90%
2-methyl-5-nitrophenol
5428-54-6

2-methyl-5-nitrophenol

1-(tert-butoxycarbonyl)piperidin-4-yl methanesulfonate
141699-59-4

1-(tert-butoxycarbonyl)piperidin-4-yl methanesulfonate

4-(2-methyl-5-nitrophenoxy)piperidine-1-carboxylic acid tert-butyl ester

4-(2-methyl-5-nitrophenoxy)piperidine-1-carboxylic acid tert-butyl ester

Conditions
ConditionsYield
With potassium carbonate In N,N-dimethyl-formamide at 80 - 85℃;89%
With potassium carbonate In N,N-dimethyl-formamide at 80℃;89%
With potassium carbonate In N,N-dimethyl-formamide at 80℃;89%
With potassium carbonate In N,N-dimethyl-formamide at 90℃;
2-methyl-5-nitrophenol
5428-54-6

2-methyl-5-nitrophenol

benzyl 4-(2-hydroxyethyl)-1-piperazinecarboxylate
14000-67-0

benzyl 4-(2-hydroxyethyl)-1-piperazinecarboxylate

benzyl 4-[2-(2-methyl-5-nitrophenoxy)ethyl]piperazine-1-carboxylate
1257423-70-3

benzyl 4-[2-(2-methyl-5-nitrophenoxy)ethyl]piperazine-1-carboxylate

Conditions
ConditionsYield
Stage #1: 2-methyl-5-nitrophenol; benzyl 4-(2-hydroxyethyl)-1-piperazinecarboxylate With triphenylphosphine In tetrahydrofuran at 0℃; for 0.166667h; Mitsunobu reaction; Inert atmosphere;
Stage #2: With diethylazodicarboxylate In tetrahydrofuran; toluene at 0 - 20℃; for 2h; Mitsunobu reaction; Inert atmosphere;
86%
2-methyl-5-nitrophenol
5428-54-6

2-methyl-5-nitrophenol

dimethyl sulfate
77-78-1

dimethyl sulfate

2-methyl-5-nitroanisole
13120-77-9

2-methyl-5-nitroanisole

Conditions
ConditionsYield
With sodium hydroxide In water at 70 - 75℃; for 2h;86%
1-bromo-butane
109-65-9

1-bromo-butane

2-methyl-5-nitrophenol
5428-54-6

2-methyl-5-nitrophenol

2-butoxy-1-methyl-4-nitrobenzene
57264-52-5

2-butoxy-1-methyl-4-nitrobenzene

Conditions
ConditionsYield
With potassium carbonate In N,N-dimethyl-formamide for 4h; Heating;81%
With sodium ethanolate
3-chloro-3-methylbut-1-yne
1111-97-3

3-chloro-3-methylbut-1-yne

2-methyl-5-nitrophenol
5428-54-6

2-methyl-5-nitrophenol

1-methyl-2-[(2-methylbut-3-yn-2-yl)oxy]-4-nitrobenzene
184896-34-2

1-methyl-2-[(2-methylbut-3-yn-2-yl)oxy]-4-nitrobenzene

Conditions
ConditionsYield
With potassium carbonate; potassium iodide In acetonitrile at 82℃; for 48h;81%
With tetrabutylammomium bromide; potassium carbonate In acetonitrile at 70℃;80%
2-methyl-5-nitrophenol
5428-54-6

2-methyl-5-nitrophenol

Bromoacetaldehyde diethyl acetal
2032-35-1

Bromoacetaldehyde diethyl acetal

3-(2,2-Diethoxyethoxy)-4-methylnitrobenzene
185684-93-9

3-(2,2-Diethoxyethoxy)-4-methylnitrobenzene

Conditions
ConditionsYield
With potassium carbonate In N,N-dimethyl-formamide at 153℃; for 3.5h;81%
With potassium carbonate In N,N-dimethyl-formamide at 153℃;81%
With potassium carbonate In N,N-dimethyl-formamide for 3.5h; Reflux;81%
2-methyl-5-nitrophenol
5428-54-6

2-methyl-5-nitrophenol

sodium chlorodifluoroacetate
1895-39-2

sodium chlorodifluoroacetate

2-(difluoromethoxy)-1-methyl-4-nitrobenzene

2-(difluoromethoxy)-1-methyl-4-nitrobenzene

Conditions
ConditionsYield
With caesium carbonate In N,N-dimethyl-formamide at 100℃; for 2h;81%
1-bromo-2,2-dimethoxyethane
7252-83-7

1-bromo-2,2-dimethoxyethane

2-methyl-5-nitrophenol
5428-54-6

2-methyl-5-nitrophenol

2-(2,2-dimethoxyethoxy)-1-methyl-4-nitrobenzene
603305-53-9

2-(2,2-dimethoxyethoxy)-1-methyl-4-nitrobenzene

Conditions
ConditionsYield
With potassium carbonate In DMF (N,N-dimethyl-formamide) for 2.5h; Heating / reflux;77%
With potassium carbonate In DMF (N,N-dimethyl-formamide) for 2.5h; Heating / reflux;77%

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