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Dayang Chem (Hangzhou) Co.,Ltd.

Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities

2'-Hydroxy-5'-methoxyacetophenone

Cas:705-15-7

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

inquiry

Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

2'-Hydroxy-5'-methoxyacetophenone

Cas:705-15-7

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

inquiry

Hebei Nengqian Chemical Import and Export Co., LTD

Our Advantage Rich Experience Our products are sold all over Europe,North&South America, Sino-East, Asia and pacific area as well as Africa,we establish long term. Quality service Company cooperates with research institutes. We strictly con

2'-Hydroxy-5'-methoxyacetophenone 705-15-7

Cas:705-15-7

Min.Order:1 Kilogram

FOB Price: $15.0 / 50.0

Type:Trading Company

inquiry

Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Manufacturer supply CAS 705-15-7 with best quality

Cas:705-15-7

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

inquiry

Leader Biochemical Group

About Product Details

China Biggest factory Supply High Quality 2'-Hydroxy-5'-methoxyacetophenone CAS 705-15-7

Cas:705-15-7

Min.Order:1 Kilogram

FOB Price: $1.0 / 5.0

Type:Lab/Research institutions

inquiry

Henan Sinotech Import&Export Corporation

Product Name: 2'-Hydroxy-5'-methoxyacetophenone CAS No.: 705-15-7 Molecular formula: C9H10O3 Molecular weight: 166 Appearance: Light yellow or light yellow-green crystals or powder

2'-Hydroxy-5'-methoxyacetophenone

Cas:705-15-7

Min.Order:1 Kilogram

FOB Price: $1.0

Type:Other

inquiry

Shanghai Upbio Tech Co.,Ltd

1.In No Less 10 years exporting experience. you can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specializ

Ethanone,1-(2-hydroxy-5-methoxyphenyl)-

Cas:705-15-7

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Qingdao Beluga Import and Export Co., LTD

2'-Hydroxy-5'-methoxyacetophenone CAS:705-15-7 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high q

2'-Hydroxy-5'-methoxyacetophenone CAS:705-15-7

Cas:705-15-7

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

Ethanone,1-(2-hydroxy-5-methoxyphenyl)-

Cas:705-15-7

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

CAS NO.:705-15-7

Cas:705-15-7

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hebei Quanhe Biotechnology Co. LTD

1. Timely and efficient service to ensure communication with customers 2. Produce products of different specifications and sizes according to your requirements. 3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures s

2'-Hydroxy-5'-methoxyacetophenone

Cas:705-15-7

Min.Order:1 Kilogram

FOB Price: $40.0 / 50.0

Type:Lab/Research institutions

inquiry

Wuhan Han Sheng New Material Technology Co.,Ltd

Our Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We

TIANFUCHEM--High purity 2'-Hydroxy-5'-methoxyacetophenone factory price

Cas:705-15-7

Min.Order:10 Kilogram

Negotiable

Type:Trading Company

inquiry

Baoji Guokang Healthchem co.,ltd

Our company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At present

2"-Hydroxy-5"-Methoxyacetophenone

Cas:705-15-7

Min.Order:1 Gram

FOB Price: $30.0

Type:Trading Company

inquiry

Triumph International Development Limilted

Appearance:white or light yellow crystalline powder Storage:Store in a cool,dry place and keep away from direct strong light Package:As customer request Application:Used for research and industrial manufacture. Transportation:By

1-(2-hydroxy-5-methoxyphenyl)ethan-1-one

Cas:705-15-7

Min.Order:100 Gram

Negotiable

Type:Lab/Research institutions

inquiry

HANGZHOU YUNUO CHEMICAL CO.,LTD

superior quality moderate price & quick delivery Appearance:yellow crystalline powder Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:1kg/bag, 1kg/drum or 25kg/drum or as per your request. Application:U

Ethanone,1-(2-hydroxy-5-methoxyphenyl)-

Cas:705-15-7

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

2'-Hydroxy-5'-methoxyacetophenone

Cas:705-15-7

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply 1-(2-hydroxy-5-methoxyphenyl)ethan-1-one

Cas:705-15-7

Min.Order:0 Metric Ton

Negotiable

Type:Other

inquiry

Shanghai Hope Chem Co., Ltd

1. Product advantages: exquisite appearance and unique functions. 2. Product Advantages: Our products are the best,fast speed ,in large stock 3. High-quality products and thoughtful service are your greatest satisfaction. 4. The product

1-(2-hydroxy-5-methoxyphenyl)ethanone

Cas:705-15-7

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

2'-Hydroxy-5'-methoxyacetophenone

Cas:705-15-7

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

inquiry

Henan Tianfu Chemical Co., Ltd.

CAS Number: 705-15-7 Molecular formula: C9H10O3 Molecular Weight: 166.17 EINECS number: 211-882-3 Related Categories: Aromatic Acetophenones & Derivatives (substituted);C9;Carbonyl Compounds;Ketones;B

TIANFUCHEM--High purity 2'-Hydroxy-5'-methoxyacetophenone factory price

Cas:705-15-7

Min.Order:1 Metric Ton

FOB Price: $20.0

Type:Lab/Research institutions

inquiry

Zibo Dorne chemical technology co. LTD

Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,

2'-Hydroxy-5'-methoxyacetophenone

Cas:705-15-7

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

EAST CHEMSOURCES LIMITED

factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B

TIANFUCHEM--High purity 2'-Hydroxy-5'-methoxyacetophenone factory price

Cas:705-15-7

Min.Order:1 Kilogram

FOB Price: $18.0 / 20.0

Type:Trading Company

inquiry

Shandong Mopai Biotechnology Co., LTD

Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W

TIANFUCHEM--High purity 2'-Hydroxy-5'-methoxyacetophenone factory price

Cas:705-15-7

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

KAISA GROUP INC

1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer

TIANFUCHEM--High purity 2'-Hydroxy-5'-methoxyacetophenone factory price

Cas:705-15-7

Min.Order:1 Metric Ton

FOB Price: $1.5

Type:Trading Company

inquiry

Hunan chemfish Pharmaceutical co.,Ltd

Appearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea

2'-Hydroxy-5'-methoxyacetylphenone

Cas:705-15-7

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Suzhou Health Chemicals Co., Ltd.

High quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use

2'-Hydroxy-5'-methoxyacetophenone

Cas:705-15-7

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

SAGECHEM LIMITED

SAGECHEM is a chemical R&D, manufacturing and distribution company in China since 2009, including pharmaceutical intermediates, agrochemical, dyestuff intermediates, organosilicone, API and etc. We also offer a full range of services in custom synthe

1-(2-hydroxy-5-methoxyphenyl)ethanone

Cas:705-15-7

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou Hysen Pharma co.,Ltd.

we are professional Pharmaceutical company. We are specialized in manufacturing and R&D of API & Intermediates, Contract Manufacturing, Contract Research, and International Trading business as well. *We own a R&D center in Hangzhou. I

2'-Hydroxy-5'-methoxyacetophenone

Cas:705-15-7

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Bluecrystal chem-union

We are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp

TIANFUCHEM--High purity 2'-Hydroxy-5'-methoxyacetophenone factory price

Cas:705-15-7

Min.Order:1 Metric Ton

FOB Price: $1.0

Type:Trading Company

inquiry

Win-Win chemical Co.Ltd

Stock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai

2-Hydroxy-5-methoxyacetophenone cas no. 705-15-7 98%

Cas:705-15-7

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Synthetic route

2',5'-dimethoxyacetophenone
1201-38-3

2',5'-dimethoxyacetophenone

1-(2-hydroxy-5-methoxyphenyl)ethan-1-one
705-15-7

1-(2-hydroxy-5-methoxyphenyl)ethan-1-one

Conditions
ConditionsYield
With aluminum (III) chloride In dichloromethane at -5 - 25℃;95%
With aluminium(III) iodide; N,N-dimethyl-formamide dimethyl acetal In acetonitrile at 80℃; for 18h;85%
With aluminium(III) iodide; N,N-dimethyl-formamide dimethyl acetal In acetonitrile at 80℃; for 18h;85%
With aluminium trichloride In acetonitrile for 6h; Thermodynamic data; Heating; ΔG(excit.), ΔH(excit.), ΔS(excit.); conversion vs. reaction time;
Dimethyl ether
115-10-6

Dimethyl ether

benzene-1,4-diyl diacetate
1205-91-0

benzene-1,4-diyl diacetate

1-(2-hydroxy-5-methoxyphenyl)ethan-1-one
705-15-7

1-(2-hydroxy-5-methoxyphenyl)ethan-1-one

Conditions
ConditionsYield
With boron trifluoride for 1h; Fries rearrangement; Heating;90%
4-methoxyphenyl acetate
1200-06-2

4-methoxyphenyl acetate

1-(2-hydroxy-5-methoxyphenyl)ethan-1-one
705-15-7

1-(2-hydroxy-5-methoxyphenyl)ethan-1-one

Conditions
ConditionsYield
With potassium carbonate In hexane at 25℃; for 12h; Irradiation;89%
With aluminum (III) chloride at 150℃; for 3.5h;75%
for 0.116667h; Rearrangement; microwave irradiation;62%
4-methoxy-phenol
150-76-5

4-methoxy-phenol

acetyl chloride
75-36-5

acetyl chloride

1-(2-hydroxy-5-methoxyphenyl)ethan-1-one
705-15-7

1-(2-hydroxy-5-methoxyphenyl)ethan-1-one

Conditions
ConditionsYield
With 1-carboxymethyl-3-methylimidazolium tetrachloroferrate In neat (no solvent) at 100℃; for 1.5h; Friedel-Crafts Acylation; Green chemistry; regioselective reaction;87%
2,5-Dihydroxyacetophenone
490-78-8

2,5-Dihydroxyacetophenone

methyl iodide
74-88-4

methyl iodide

1-(2-hydroxy-5-methoxyphenyl)ethan-1-one
705-15-7

1-(2-hydroxy-5-methoxyphenyl)ethan-1-one

Conditions
ConditionsYield
In acetone83%
With potassium carbonate In acetone for 6h; Heating;64%
With potassium carbonate; acetone
chloro-trimethyl-silane
75-77-4

chloro-trimethyl-silane

N,N-diethyl-2-hydroxy-5-methoxybenzamide
85630-32-6

N,N-diethyl-2-hydroxy-5-methoxybenzamide

1-(2-hydroxy-5-methoxyphenyl)ethan-1-one
705-15-7

1-(2-hydroxy-5-methoxyphenyl)ethan-1-one

Conditions
ConditionsYield
With lithium diisopropyl amide In tetrahydrofuran at 0 - 20℃; for 0.5h; Inert atmosphere;81%
acetic acid
64-19-7

acetic acid

1,4-dimethoxybezene
150-78-7

1,4-dimethoxybezene

1-(2-hydroxy-5-methoxyphenyl)ethan-1-one
705-15-7

1-(2-hydroxy-5-methoxyphenyl)ethan-1-one

Conditions
ConditionsYield
With boron trifluoride
acetic acid
64-19-7

acetic acid

1,4-dimethoxybezene
150-78-7

1,4-dimethoxybezene

A

1-(2-hydroxy-5-methoxyphenyl)ethan-1-one
705-15-7

1-(2-hydroxy-5-methoxyphenyl)ethan-1-one

B

2',5'-dimethoxyacetophenone
1201-38-3

2',5'-dimethoxyacetophenone

Conditions
ConditionsYield
With boron trifluoride
acetyl chloride
75-36-5

acetyl chloride

1,4-dimethoxybezene
150-78-7

1,4-dimethoxybezene

1-(2-hydroxy-5-methoxyphenyl)ethan-1-one
705-15-7

1-(2-hydroxy-5-methoxyphenyl)ethan-1-one

Conditions
ConditionsYield
With aluminium trichloride; diethyl ether
With carbon disulfide; aluminium trichloride Erwaermen des Reaktionsprodukts mit AlCl3 in Aether;
With aluminium trichloride In dichloromethane
aluminium trichloride
7446-70-0

aluminium trichloride

diethyl ether
60-29-7

diethyl ether

acetyl chloride
75-36-5

acetyl chloride

1,4-dimethoxybezene
150-78-7

1,4-dimethoxybezene

A

1-(2-hydroxy-5-methoxyphenyl)ethan-1-one
705-15-7

1-(2-hydroxy-5-methoxyphenyl)ethan-1-one

B

2',5'-dimethoxyacetophenone
1201-38-3

2',5'-dimethoxyacetophenone

acetyl chloride
75-36-5

acetyl chloride

1,4-dimethoxybezene
150-78-7

1,4-dimethoxybezene

A

1-(2-hydroxy-5-methoxyphenyl)ethan-1-one
705-15-7

1-(2-hydroxy-5-methoxyphenyl)ethan-1-one

B

quinoacetophenonedimethyl ether

quinoacetophenonedimethyl ether

Conditions
ConditionsYield
With carbon disulfide; aluminium trichloride
dimethyl sulfate
77-78-1

dimethyl sulfate

quinoacetophenone

quinoacetophenone

A

1-(2-hydroxy-5-methoxyphenyl)ethan-1-one
705-15-7

1-(2-hydroxy-5-methoxyphenyl)ethan-1-one

B

quinoacetophenonedimethyl ether

quinoacetophenonedimethyl ether

Conditions
ConditionsYield
With sodium hydroxide
aluminium trichloride
7446-70-0

aluminium trichloride

4-methoxyphenyl acetate
1200-06-2

4-methoxyphenyl acetate

A

1-(2-hydroxy-5-methoxyphenyl)ethan-1-one
705-15-7

1-(2-hydroxy-5-methoxyphenyl)ethan-1-one

B

2,5-Dihydroxyacetophenone
490-78-8

2,5-Dihydroxyacetophenone

Conditions
ConditionsYield
at 65℃;
acetic anhydride
108-24-7

acetic anhydride

hydroquinone
123-31-9

hydroquinone

dimethyl sulfate
77-78-1

dimethyl sulfate

1-(2-hydroxy-5-methoxyphenyl)ethan-1-one
705-15-7

1-(2-hydroxy-5-methoxyphenyl)ethan-1-one

Conditions
ConditionsYield
Stage #1: acetic anhydride; hydroquinone With sulfuric acid
Stage #2: With aluminium trichloride at 160℃;
Stage #3: dimethyl sulfate With potassium carbonate
2,5-Dihydroxyacetophenone
490-78-8

2,5-Dihydroxyacetophenone

MeX

MeX

1-(2-hydroxy-5-methoxyphenyl)ethan-1-one
705-15-7

1-(2-hydroxy-5-methoxyphenyl)ethan-1-one

Conditions
ConditionsYield
With potassium carbonate; sodium iodide In N,N-dimethyl-formamide at 60℃; for 24h;
1-(3-Methoxyphenyl)ethanone
586-37-8

1-(3-Methoxyphenyl)ethanone

A

1-(2-hydroxy-5-methoxyphenyl)ethan-1-one
705-15-7

1-(2-hydroxy-5-methoxyphenyl)ethan-1-one

B

acetic acid 3-methoxyphenyl ester
5451-83-2

acetic acid 3-methoxyphenyl ester

C

1-(2-hydroxy-3-methoxyphenyl)ethanone
703-98-0

1-(2-hydroxy-3-methoxyphenyl)ethanone

Conditions
ConditionsYield
With toluene-4-sulfonic acid; 3-chloro-benzenecarboperoxoic acid In acetonitrile at 80℃; for 2h; Baeyer-Villiger oxidation;A 2 % Chromat.
B 9 % Chromat.
C 4 % Chromat.
hydroquinone
123-31-9

hydroquinone

1-(2-hydroxy-5-methoxyphenyl)ethan-1-one
705-15-7

1-(2-hydroxy-5-methoxyphenyl)ethan-1-one

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: ZnCl2
2: aq. NaOH solution
View Scheme
4-methoxy-phenol
150-76-5

4-methoxy-phenol

1-(2-hydroxy-5-methoxyphenyl)ethan-1-one
705-15-7

1-(2-hydroxy-5-methoxyphenyl)ethan-1-one

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: pyridine / 3.5 h / 100 °C
2: aluminum (III) chloride / 3.5 h / 150 °C
View Scheme
Multi-step reaction with 3 steps
1: potassium carbonate / acetonitrile / 12 h / 20 °C / Inert atmosphere; Reflux
2: lithium diisopropyl amide / tetrahydrofuran / -78 - 20 °C / Inert atmosphere
3: lithium diisopropyl amide / tetrahydrofuran / 0.5 h / 0 - 20 °C / Inert atmosphere
View Scheme
Multi-step reaction with 2 steps
1: sulfuric acid
2: aluminum (III) chloride / 120 - 130 °C
View Scheme
Multi-step reaction with 2 steps
1: 90 °C
2: aluminum (III) chloride / 5 h / 120 °C
View Scheme
N,N-diethyl-O-(4-methoxyphenyl)carbamate
85630-18-8

N,N-diethyl-O-(4-methoxyphenyl)carbamate

1-(2-hydroxy-5-methoxyphenyl)ethan-1-one
705-15-7

1-(2-hydroxy-5-methoxyphenyl)ethan-1-one

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: lithium diisopropyl amide / tetrahydrofuran / -78 - 20 °C / Inert atmosphere
2: lithium diisopropyl amide / tetrahydrofuran / 0.5 h / 0 - 20 °C / Inert atmosphere
View Scheme
2,5-Dihydroxyacetophenone
490-78-8

2,5-Dihydroxyacetophenone

1-(2-hydroxy-5-methoxyphenyl)ethan-1-one
705-15-7

1-(2-hydroxy-5-methoxyphenyl)ethan-1-one

Conditions
ConditionsYield
With methyl iodide In acetone at 20℃; for 12h;
1-(2-hydroxy-5-methoxyphenyl)ethan-1-one
705-15-7

1-(2-hydroxy-5-methoxyphenyl)ethan-1-one

methylmagnesium bromide
75-16-1

methylmagnesium bromide

2-(1-hydroxy-1-methyl-ethyl)-4-methoxy-phenol
15000-00-7

2-(1-hydroxy-1-methyl-ethyl)-4-methoxy-phenol

Conditions
ConditionsYield
Stage #1: 1-(2-hydroxy-5-methoxyphenyl)ethan-1-one; methylmagnesium bromide In tetrahydrofuran at 0 - 20℃; for 16.5h;
Stage #2: With ammonium chloride In tetrahydrofuran; water
100%
In tetrahydrofuran at 0 - 20℃; for 16.5h;100%
In tetrahydrofuran at 0 - 20℃; for 16.5h;100%
In tetrahydrofuran at 0 - 20℃; for 16.5h;100%
1-(2-hydroxy-5-methoxyphenyl)ethan-1-one
705-15-7

1-(2-hydroxy-5-methoxyphenyl)ethan-1-one

2-(1-iminoethyl)-4-methoxyphenol
1247949-38-7

2-(1-iminoethyl)-4-methoxyphenol

Conditions
ConditionsYield
With ammonia In methanol at 20℃; Cooling with ice;100%
1-(2-hydroxy-5-methoxyphenyl)ethan-1-one
705-15-7

1-(2-hydroxy-5-methoxyphenyl)ethan-1-one

2,6-dimethoxybenzaldehyde
3392-97-0

2,6-dimethoxybenzaldehyde

(2E)-3-(2,6-dimethoxyphenyl)-1-(2-hydroxy-5-methoxyphenyl)prop-2-en-1-one

(2E)-3-(2,6-dimethoxyphenyl)-1-(2-hydroxy-5-methoxyphenyl)prop-2-en-1-one

Conditions
ConditionsYield
With sodium hydroxide In ethanol; water at 20℃; Aldol Condensation;100%
1-(2-hydroxy-5-methoxyphenyl)ethan-1-one
705-15-7

1-(2-hydroxy-5-methoxyphenyl)ethan-1-one

acetic anhydride
108-24-7

acetic anhydride

2'-acetoxy-5'-methoxyacetophenone
72229-47-1

2'-acetoxy-5'-methoxyacetophenone

Conditions
ConditionsYield
In pyridine for 0.5h; Heating;99%
1-(2-hydroxy-5-methoxyphenyl)ethan-1-one
705-15-7

1-(2-hydroxy-5-methoxyphenyl)ethan-1-one

benzyl bromide
100-39-0

benzyl bromide

2'-benzyloxy-5'-methoxyacetophenone
65547-82-2

2'-benzyloxy-5'-methoxyacetophenone

Conditions
ConditionsYield
With potassium carbonate In acetone for 72h; Heating;99%
1-(2-hydroxy-5-methoxyphenyl)ethan-1-one
705-15-7

1-(2-hydroxy-5-methoxyphenyl)ethan-1-one

2-methyl-but-2-ene
513-35-9

2-methyl-but-2-ene

1-(5-methoxy-2,2,3-trimethyl-2,3-dihydrobenzo[2,3-b]furan-7-yl)ethan-1-one

1-(5-methoxy-2,2,3-trimethyl-2,3-dihydrobenzo[2,3-b]furan-7-yl)ethan-1-one

Conditions
ConditionsYield
With lithium perchlorate; acetic acid In nitromethane Cycloaddition; Electrochemical reaction;99%
With lithium perchlorate; acetic acid In nitromethane; cyclohexane at 25 - 60℃; Electrochemical reaction;93%
With lithium perchlorate; acetic acid In nitromethane Electrolysis;90 %Spectr.
With acetic acid In nitromethane at 20℃; Reagent/catalyst; Electrolysis;
1-(2-hydroxy-5-methoxyphenyl)ethan-1-one
705-15-7

1-(2-hydroxy-5-methoxyphenyl)ethan-1-one

oxalic acid diethyl ester
95-92-1

oxalic acid diethyl ester

ethyl 6-methoxy-4-oxo-4H-chromene-2-carboxylate
52866-24-7

ethyl 6-methoxy-4-oxo-4H-chromene-2-carboxylate

Conditions
ConditionsYield
With sodium ethanolate In ethanol for 1h; Heating;98%
With sodium ethanolate In ethanol for 1h; Heating / reflux;98%
With ethanol; sodium ethanolate Behandeln des Reaktionsgemisches mit wss.-aethanol. Salzsaeure;
1-(2-hydroxy-5-methoxyphenyl)ethan-1-one
705-15-7

1-(2-hydroxy-5-methoxyphenyl)ethan-1-one

(E)-2-hydroxy-5-methoxyacetophenone oxime
23997-97-9

(E)-2-hydroxy-5-methoxyacetophenone oxime

Conditions
ConditionsYield
With pyridine; hydroxylamine hydrochloride In ethanol at 20℃;98%
1-(2-hydroxy-5-methoxyphenyl)ethan-1-one
705-15-7

1-(2-hydroxy-5-methoxyphenyl)ethan-1-one

1-(3-bromo-2-hydroxy-5-methoxyphenyl)ethan-1-one
37113-61-4

1-(3-bromo-2-hydroxy-5-methoxyphenyl)ethan-1-one

Conditions
ConditionsYield
With bromine; sodium acetate; acetic acid97%
With bromine; sodium acetate; acetic acid at 20℃; for 48h;87%
With bromine; sodium acetate In acetic acid at 15 - 25℃; for 16h;210 g
1-(2-hydroxy-5-methoxyphenyl)ethan-1-one
705-15-7

1-(2-hydroxy-5-methoxyphenyl)ethan-1-one

1-Amino-1-deoxy-D-glucitol
488-43-7

1-Amino-1-deoxy-D-glucitol

1-deoxy-1-(2-hydroxy-α-methyl-5-methoxybenzylidene)amino-D-glucitol

1-deoxy-1-(2-hydroxy-α-methyl-5-methoxybenzylidene)amino-D-glucitol

Conditions
ConditionsYield
In methanol; water at 90℃; for 0.333333h;97%
1-(2-hydroxy-5-methoxyphenyl)ethan-1-one
705-15-7

1-(2-hydroxy-5-methoxyphenyl)ethan-1-one

3-chloro-1-benzofuran-2-carbaldehyde
40620-00-6

3-chloro-1-benzofuran-2-carbaldehyde

(E)-3-(3-Chloro-benzofuran-2-yl)-1-(2-hydroxy-5-methoxy-phenyl)-propenone
87487-52-3

(E)-3-(3-Chloro-benzofuran-2-yl)-1-(2-hydroxy-5-methoxy-phenyl)-propenone

Conditions
ConditionsYield
With potassium hydroxide In ethanol; water Ambient temperature;96%
1-(2-hydroxy-5-methoxyphenyl)ethan-1-one
705-15-7

1-(2-hydroxy-5-methoxyphenyl)ethan-1-one

methanesulfonyl chloride
124-63-0

methanesulfonyl chloride

2-acetyl-4-methoxyphenyl methanesulfonate
72229-67-5

2-acetyl-4-methoxyphenyl methanesulfonate

Conditions
ConditionsYield
With triethylamine In dichloromethane at 0 - 20℃; for 4h;96%
1-(2-hydroxy-5-methoxyphenyl)ethan-1-one
705-15-7

1-(2-hydroxy-5-methoxyphenyl)ethan-1-one

acetone
67-64-1

acetone

6-methoxy-2,2-dimethylchroman-4-one
13229-59-9

6-methoxy-2,2-dimethylchroman-4-one

Conditions
ConditionsYield
Stage #1: acetone With pyrrolidine; butyric acid In dimethyl sulfoxide for 0.25h; Kabe Chromanone Synthesis;
Stage #2: 1-(2-hydroxy-5-methoxyphenyl)ethan-1-one In dimethyl sulfoxide at 20℃; for 1.5h; Kabe Chromanone Synthesis;
95%
With Amberlite IRA 400 basic resin for 0.0833333h; Microwave irradiation; Neat (no solvent);91%
With pyrrolidine In ethanol for 12h; Inert atmosphere; Reflux;84.6%
With pyrrolidine In toluene Ambient temperature; a) RT, 3 h, b) reflux, 18 h;53%
With pyrrolidine In ethanol at 75℃; for 4h; Inert atmosphere; Schlenk technique;
chloro-trimethyl-silane
75-77-4

chloro-trimethyl-silane

1-(2-hydroxy-5-methoxyphenyl)ethan-1-one
705-15-7

1-(2-hydroxy-5-methoxyphenyl)ethan-1-one

1-<2'-<(trimethylsilyl)oxy>-5'-methoxyphenyl>-1-<(trimethylsilyl)oxy>ethylene
158531-80-7

1-<2'-<(trimethylsilyl)oxy>-5'-methoxyphenyl>-1-<(trimethylsilyl)oxy>ethylene

Conditions
ConditionsYield
With triethylamine; sodium iodide In acetonitrile for 2h; Ambient temperature;95%
1-(2-hydroxy-5-methoxyphenyl)ethan-1-one
705-15-7

1-(2-hydroxy-5-methoxyphenyl)ethan-1-one

trifluoromethylsulfonic anhydride
358-23-6

trifluoromethylsulfonic anhydride

2-acetyl-4-methoxylphenyl triflate
1051384-12-3

2-acetyl-4-methoxylphenyl triflate

Conditions
ConditionsYield
With pyridine at 0 - 20℃; for 12h;95%
With triethylamine In dichloromethane at 0 - 20℃; Inert atmosphere;
1-(2-hydroxy-5-methoxyphenyl)ethan-1-one
705-15-7

1-(2-hydroxy-5-methoxyphenyl)ethan-1-one

oxalyl dichloride
79-37-8

oxalyl dichloride

N,N-dimethyl-formamide
68-12-2, 33513-42-7

N,N-dimethyl-formamide

6-methoxy-4-oxo-4H-chromene-3-carbaldehyde
42059-79-0

6-methoxy-4-oxo-4H-chromene-3-carbaldehyde

Conditions
ConditionsYield
Stage #1: 1-(2-hydroxy-5-methoxyphenyl)ethan-1-one; N,N-dimethyl-formamide In tetrahydrofuran at 0℃; Inert atmosphere;
Stage #2: oxalyl dichloride In tetrahydrofuran at 0 - 20℃; for 12h; Inert atmosphere;
95%
1-(2-hydroxy-5-methoxyphenyl)ethan-1-one
705-15-7

1-(2-hydroxy-5-methoxyphenyl)ethan-1-one

trimethylsilyl cyanide
7677-24-9

trimethylsilyl cyanide

ethylamine
75-04-7

ethylamine

1-(2-hydroxy-5-methoxyphenyl)-1-(ethylamino)ethylcyanide

1-(2-hydroxy-5-methoxyphenyl)-1-(ethylamino)ethylcyanide

Conditions
ConditionsYield
Stage #1: 1-(2-hydroxy-5-methoxyphenyl)ethan-1-one; ethylamine With zinc(II) oxide In neat (no solvent) at 20℃; for 0.166667h; Green chemistry;
Stage #2: trimethylsilyl cyanide In neat (no solvent) at 20℃; Green chemistry;
95%
isoquinoline
119-65-3

isoquinoline

1-(2-hydroxy-5-methoxyphenyl)ethan-1-one
705-15-7

1-(2-hydroxy-5-methoxyphenyl)ethan-1-one

4-(bromoacetyl)toluene
619-41-0

4-(bromoacetyl)toluene

[2-(3-methoxyphenyl)pyrrolo[2,1-a]isoquinolin-3-yl](4-methylphenyl)methanone

[2-(3-methoxyphenyl)pyrrolo[2,1-a]isoquinolin-3-yl](4-methylphenyl)methanone

Conditions
ConditionsYield
Stage #1: isoquinoline; 4-(bromoacetyl)toluene In water at 80℃; for 0.5h; Green chemistry;
Stage #2: 1-(2-hydroxy-5-methoxyphenyl)ethan-1-one With carbonic acid dimethyl ester In water at 80℃; for 3h; Green chemistry;
95%
isoquinoline
119-65-3

isoquinoline

1-(2-hydroxy-5-methoxyphenyl)ethan-1-one
705-15-7

1-(2-hydroxy-5-methoxyphenyl)ethan-1-one

2-Bromo-4'-methoxyacetophenone
2632-13-5

2-Bromo-4'-methoxyacetophenone

(4-methoxyphenyl)[2-(3-methoxyphenyl)pyrrolo[2,1-a]isoquinolin-3-yl]methanone

(4-methoxyphenyl)[2-(3-methoxyphenyl)pyrrolo[2,1-a]isoquinolin-3-yl]methanone

Conditions
ConditionsYield
Stage #1: isoquinoline; 2-Bromo-4'-methoxyacetophenone In water at 80℃; for 0.5h; Green chemistry;
Stage #2: 1-(2-hydroxy-5-methoxyphenyl)ethan-1-one With carbonic acid dimethyl ester In water at 80℃; for 3h; Green chemistry;
95%
1-(2-hydroxy-5-methoxyphenyl)ethan-1-one
705-15-7

1-(2-hydroxy-5-methoxyphenyl)ethan-1-one

4-methoxy-benzaldehyde
123-11-5

4-methoxy-benzaldehyde

4-Methoxyphenyl isothiocyanate
2284-20-0

4-Methoxyphenyl isothiocyanate

carbonic acid dimethyl ester
616-38-6

carbonic acid dimethyl ester

malononitrile
109-77-3

malononitrile

C29H23N3O6S

C29H23N3O6S

Conditions
ConditionsYield
Stage #1: 1-(2-hydroxy-5-methoxyphenyl)ethan-1-one; carbonic acid dimethyl ester With magnetic Fe3O4 nanoparticles and ZnO nanoparticles on multiwalled carbon nanotubes at 20℃; for 0.333333h;
Stage #2: 4-methoxy-benzaldehyde; malononitrile With magnetic Fe3O4 nanoparticles and ZnO nanoparticles on multiwalled carbon nanotubes at 20℃; for 1h;
Stage #3: 4-Methoxyphenyl isothiocyanate at 20℃; for 2h;
95%
1-(2-hydroxy-5-methoxyphenyl)ethan-1-one
705-15-7

1-(2-hydroxy-5-methoxyphenyl)ethan-1-one

4-fluorobenzoyl chloride
403-43-0

4-fluorobenzoyl chloride

1-(4-fluorophenyl)-3-(2-hydroxy-5-methoxyphenyl)propane-1,3-dione
312607-68-4

1-(4-fluorophenyl)-3-(2-hydroxy-5-methoxyphenyl)propane-1,3-dione

Conditions
ConditionsYield
Stage #1: 1-(2-hydroxy-5-methoxyphenyl)ethan-1-one With lithium hexamethyldisilazane In tetrahydrofuran; hexane at -78 - 20℃; Inert atmosphere;
Stage #2: 4-fluorobenzoyl chloride In tetrahydrofuran; hexane at -78 - 20℃; Inert atmosphere;
94.9%
1-(2-hydroxy-5-methoxyphenyl)ethan-1-one
705-15-7

1-(2-hydroxy-5-methoxyphenyl)ethan-1-one

Diethyl carbonate
105-58-8

Diethyl carbonate

4-hydroxy-6-methoxycoumarin
13252-84-1

4-hydroxy-6-methoxycoumarin

Conditions
ConditionsYield
With sodium hydride In mineral oil at 0 - 100℃;94%
With sodium hydride In toluene at 0℃; for 4.5h; Reflux;90%
Stage #1: 1-(2-hydroxy-5-methoxyphenyl)ethan-1-one With sodium hydride In toluene for 0.25h; Inert atmosphere; Cooling with ice;
Stage #2: Diethyl carbonate In toluene at 20℃; for 5.5h; Inert atmosphere; Reflux;
82%
1-(2-hydroxy-5-methoxyphenyl)ethan-1-one
705-15-7

1-(2-hydroxy-5-methoxyphenyl)ethan-1-one

phenylacetylene
536-74-3

phenylacetylene

2-(4-Phenyl-2-hydroxy-3-butyne-2-yl)-4-methoxyphenol

2-(4-Phenyl-2-hydroxy-3-butyne-2-yl)-4-methoxyphenol

Conditions
ConditionsYield
94%
1-(2-hydroxy-5-methoxyphenyl)ethan-1-one
705-15-7

1-(2-hydroxy-5-methoxyphenyl)ethan-1-one

N,N-Dimethylthiocarbamoyl chloride
16420-13-6

N,N-Dimethylthiocarbamoyl chloride

O-2-acetyl-4-methoxyphenyl N,N-dimethylcarbamothioate
1239890-31-3

O-2-acetyl-4-methoxyphenyl N,N-dimethylcarbamothioate

Conditions
ConditionsYield
With 1,4-diaza-bicyclo[2.2.2]octane In N,N-dimethyl-formamide at 50℃; for 5h; Inert atmosphere;94%
1-(2-hydroxy-5-methoxyphenyl)ethan-1-one
705-15-7

1-(2-hydroxy-5-methoxyphenyl)ethan-1-one

diphenyl-phosphinic acid
1707-03-5

diphenyl-phosphinic acid

O-2-acetyl-4-methoxyphenyl diphenylphosphinate

O-2-acetyl-4-methoxyphenyl diphenylphosphinate

Conditions
ConditionsYield
With N,N-dimethyl-aniline; 1,1'-carbonyldiimidazole In acetonitrile at 20℃; for 12h; Inert atmosphere;93%
1-(2-hydroxy-5-methoxyphenyl)ethan-1-one
705-15-7

1-(2-hydroxy-5-methoxyphenyl)ethan-1-one

ethyl bromoacetate
105-36-2

ethyl bromoacetate

ethyl 2-(2-acetyl-4-methoxyphenoxy)acetate
33038-04-9

ethyl 2-(2-acetyl-4-methoxyphenoxy)acetate

Conditions
ConditionsYield
With potassium carbonate In acetone92%
With potassium carbonate In butanone for 10h; Heating / reflux;40%
With potassium carbonate; acetone

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