Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities
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inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
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inquiryOur Advantage Rich Experience Our products are sold all over Europe,North&South America, Sino-East, Asia and pacific area as well as Africa,we establish long term. Quality service Company cooperates with research institutes. We strictly con
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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inquiryAbout Product Details
Cas:705-15-7
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inquiryProduct Name: 2'-Hydroxy-5'-methoxyacetophenone CAS No.: 705-15-7 Molecular formula: C9H10O3 Molecular weight: 166 Appearance: Light yellow or light yellow-green crystals or powder
Cas:705-15-7
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inquiry1.In No Less 10 years exporting experience. you can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specializ
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inquiry2'-Hydroxy-5'-methoxyacetophenone CAS:705-15-7 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high q
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
1. Timely and efficient service to ensure communication with customers 2. Produce products of different specifications and sizes according to your requirements. 3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures s
Cas:705-15-7
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FOB Price: $40.0 / 50.0
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inquiryOur Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
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inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At present
Cas:705-15-7
Min.Order:1 Gram
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inquiryAppearance:white or light yellow crystalline powder Storage:Store in a cool,dry place and keep away from direct strong light Package:As customer request Application:Used for research and industrial manufacture. Transportation:By
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Min.Order:100 Gram
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inquirysuperior quality moderate price & quick delivery Appearance:yellow crystalline powder Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:1kg/bag, 1kg/drum or 25kg/drum or as per your request. Application:U
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Cas:705-15-7
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Cas:705-15-7
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inquiry1. Product advantages: exquisite appearance and unique functions. 2. Product Advantages: Our products are the best,fast speed ,in large stock 3. High-quality products and thoughtful service are your greatest satisfaction. 4. The product
Cas:705-15-7
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:705-15-7
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inquiryCAS Number: 705-15-7 Molecular formula: C9H10O3 Molecular Weight: 166.17 EINECS number: 211-882-3 Related Categories: Aromatic Acetophenones & Derivatives (substituted);C9;Carbonyl Compounds;Ketones;B
Cas:705-15-7
Min.Order:1 Metric Ton
FOB Price: $20.0
Type:Lab/Research institutions
inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Cas:705-15-7
Min.Order:1 Kilogram
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inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
Cas:705-15-7
Min.Order:1 Kilogram
FOB Price: $18.0 / 20.0
Type:Trading Company
inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
Cas:705-15-7
Min.Order:1 Gram
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Type:Lab/Research institutions
inquiry1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
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Min.Order:1 Metric Ton
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Type:Trading Company
inquiryAppearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea
High quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use
Cas:705-15-7
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inquirySAGECHEM is a chemical R&D, manufacturing and distribution company in China since 2009, including pharmaceutical intermediates, agrochemical, dyestuff intermediates, organosilicone, API and etc. We also offer a full range of services in custom synthe
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inquirywe are professional Pharmaceutical company. We are specialized in manufacturing and R&D of API & Intermediates, Contract Manufacturing, Contract Research, and International Trading business as well. *We own a R&D center in Hangzhou. I
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Min.Order:1 Gram
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Type:Lab/Research institutions
inquiryWe are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp
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inquiryStock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai
Cas:705-15-7
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Negotiable
Type:Lab/Research institutions
inquiryConditions | Yield |
---|---|
With aluminum (III) chloride In dichloromethane at -5 - 25℃; | 95% |
With aluminium(III) iodide; N,N-dimethyl-formamide dimethyl acetal In acetonitrile at 80℃; for 18h; | 85% |
With aluminium(III) iodide; N,N-dimethyl-formamide dimethyl acetal In acetonitrile at 80℃; for 18h; | 85% |
With aluminium trichloride In acetonitrile for 6h; Thermodynamic data; Heating; ΔG(excit.), ΔH(excit.), ΔS(excit.); conversion vs. reaction time; |
Dimethyl ether
benzene-1,4-diyl diacetate
1-(2-hydroxy-5-methoxyphenyl)ethan-1-one
Conditions | Yield |
---|---|
With boron trifluoride for 1h; Fries rearrangement; Heating; | 90% |
Conditions | Yield |
---|---|
With potassium carbonate In hexane at 25℃; for 12h; Irradiation; | 89% |
With aluminum (III) chloride at 150℃; for 3.5h; | 75% |
for 0.116667h; Rearrangement; microwave irradiation; | 62% |
Conditions | Yield |
---|---|
With 1-carboxymethyl-3-methylimidazolium tetrachloroferrate In neat (no solvent) at 100℃; for 1.5h; Friedel-Crafts Acylation; Green chemistry; regioselective reaction; | 87% |
2,5-Dihydroxyacetophenone
methyl iodide
1-(2-hydroxy-5-methoxyphenyl)ethan-1-one
Conditions | Yield |
---|---|
In acetone | 83% |
With potassium carbonate In acetone for 6h; Heating; | 64% |
With potassium carbonate; acetone |
chloro-trimethyl-silane
N,N-diethyl-2-hydroxy-5-methoxybenzamide
1-(2-hydroxy-5-methoxyphenyl)ethan-1-one
Conditions | Yield |
---|---|
With lithium diisopropyl amide In tetrahydrofuran at 0 - 20℃; for 0.5h; Inert atmosphere; | 81% |
Conditions | Yield |
---|---|
With boron trifluoride |
acetic acid
1,4-dimethoxybezene
A
1-(2-hydroxy-5-methoxyphenyl)ethan-1-one
B
2',5'-dimethoxyacetophenone
Conditions | Yield |
---|---|
With boron trifluoride |
acetyl chloride
1,4-dimethoxybezene
1-(2-hydroxy-5-methoxyphenyl)ethan-1-one
Conditions | Yield |
---|---|
With aluminium trichloride; diethyl ether | |
With carbon disulfide; aluminium trichloride Erwaermen des Reaktionsprodukts mit AlCl3 in Aether; | |
With aluminium trichloride In dichloromethane |
aluminium trichloride
diethyl ether
acetyl chloride
1,4-dimethoxybezene
A
1-(2-hydroxy-5-methoxyphenyl)ethan-1-one
B
2',5'-dimethoxyacetophenone
acetyl chloride
1,4-dimethoxybezene
A
1-(2-hydroxy-5-methoxyphenyl)ethan-1-one
Conditions | Yield |
---|---|
With carbon disulfide; aluminium trichloride |
Conditions | Yield |
---|---|
With sodium hydroxide |
aluminium trichloride
4-methoxyphenyl acetate
A
1-(2-hydroxy-5-methoxyphenyl)ethan-1-one
B
2,5-Dihydroxyacetophenone
Conditions | Yield |
---|---|
at 65℃; |
acetic anhydride
hydroquinone
dimethyl sulfate
1-(2-hydroxy-5-methoxyphenyl)ethan-1-one
Conditions | Yield |
---|---|
Stage #1: acetic anhydride; hydroquinone With sulfuric acid Stage #2: With aluminium trichloride at 160℃; Stage #3: dimethyl sulfate With potassium carbonate |
Conditions | Yield |
---|---|
With potassium carbonate; sodium iodide In N,N-dimethyl-formamide at 60℃; for 24h; |
1-(3-Methoxyphenyl)ethanone
A
1-(2-hydroxy-5-methoxyphenyl)ethan-1-one
B
acetic acid 3-methoxyphenyl ester
C
1-(2-hydroxy-3-methoxyphenyl)ethanone
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid; 3-chloro-benzenecarboperoxoic acid In acetonitrile at 80℃; for 2h; Baeyer-Villiger oxidation; | A 2 % Chromat. B 9 % Chromat. C 4 % Chromat. |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: ZnCl2 2: aq. NaOH solution View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: pyridine / 3.5 h / 100 °C 2: aluminum (III) chloride / 3.5 h / 150 °C View Scheme | |
Multi-step reaction with 3 steps 1: potassium carbonate / acetonitrile / 12 h / 20 °C / Inert atmosphere; Reflux 2: lithium diisopropyl amide / tetrahydrofuran / -78 - 20 °C / Inert atmosphere 3: lithium diisopropyl amide / tetrahydrofuran / 0.5 h / 0 - 20 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 2 steps 1: sulfuric acid 2: aluminum (III) chloride / 120 - 130 °C View Scheme | |
Multi-step reaction with 2 steps 1: 90 °C 2: aluminum (III) chloride / 5 h / 120 °C View Scheme |
N,N-diethyl-O-(4-methoxyphenyl)carbamate
1-(2-hydroxy-5-methoxyphenyl)ethan-1-one
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: lithium diisopropyl amide / tetrahydrofuran / -78 - 20 °C / Inert atmosphere 2: lithium diisopropyl amide / tetrahydrofuran / 0.5 h / 0 - 20 °C / Inert atmosphere View Scheme |
Conditions | Yield |
---|---|
With methyl iodide In acetone at 20℃; for 12h; |
1-(2-hydroxy-5-methoxyphenyl)ethan-1-one
methylmagnesium bromide
2-(1-hydroxy-1-methyl-ethyl)-4-methoxy-phenol
Conditions | Yield |
---|---|
Stage #1: 1-(2-hydroxy-5-methoxyphenyl)ethan-1-one; methylmagnesium bromide In tetrahydrofuran at 0 - 20℃; for 16.5h; Stage #2: With ammonium chloride In tetrahydrofuran; water | 100% |
In tetrahydrofuran at 0 - 20℃; for 16.5h; | 100% |
In tetrahydrofuran at 0 - 20℃; for 16.5h; | 100% |
In tetrahydrofuran at 0 - 20℃; for 16.5h; | 100% |
1-(2-hydroxy-5-methoxyphenyl)ethan-1-one
2-(1-iminoethyl)-4-methoxyphenol
Conditions | Yield |
---|---|
With ammonia In methanol at 20℃; Cooling with ice; | 100% |
Conditions | Yield |
---|---|
With sodium hydroxide In ethanol; water at 20℃; Aldol Condensation; | 100% |
1-(2-hydroxy-5-methoxyphenyl)ethan-1-one
acetic anhydride
2'-acetoxy-5'-methoxyacetophenone
Conditions | Yield |
---|---|
In pyridine for 0.5h; Heating; | 99% |
1-(2-hydroxy-5-methoxyphenyl)ethan-1-one
benzyl bromide
2'-benzyloxy-5'-methoxyacetophenone
Conditions | Yield |
---|---|
With potassium carbonate In acetone for 72h; Heating; | 99% |
Conditions | Yield |
---|---|
With lithium perchlorate; acetic acid In nitromethane Cycloaddition; Electrochemical reaction; | 99% |
With lithium perchlorate; acetic acid In nitromethane; cyclohexane at 25 - 60℃; Electrochemical reaction; | 93% |
With lithium perchlorate; acetic acid In nitromethane Electrolysis; | 90 %Spectr. |
With acetic acid In nitromethane at 20℃; Reagent/catalyst; Electrolysis; |
1-(2-hydroxy-5-methoxyphenyl)ethan-1-one
oxalic acid diethyl ester
ethyl 6-methoxy-4-oxo-4H-chromene-2-carboxylate
Conditions | Yield |
---|---|
With sodium ethanolate In ethanol for 1h; Heating; | 98% |
With sodium ethanolate In ethanol for 1h; Heating / reflux; | 98% |
With ethanol; sodium ethanolate Behandeln des Reaktionsgemisches mit wss.-aethanol. Salzsaeure; |
1-(2-hydroxy-5-methoxyphenyl)ethan-1-one
(E)-2-hydroxy-5-methoxyacetophenone oxime
Conditions | Yield |
---|---|
With pyridine; hydroxylamine hydrochloride In ethanol at 20℃; | 98% |
1-(2-hydroxy-5-methoxyphenyl)ethan-1-one
1-(3-bromo-2-hydroxy-5-methoxyphenyl)ethan-1-one
Conditions | Yield |
---|---|
With bromine; sodium acetate; acetic acid | 97% |
With bromine; sodium acetate; acetic acid at 20℃; for 48h; | 87% |
With bromine; sodium acetate In acetic acid at 15 - 25℃; for 16h; | 210 g |
Conditions | Yield |
---|---|
In methanol; water at 90℃; for 0.333333h; | 97% |
1-(2-hydroxy-5-methoxyphenyl)ethan-1-one
3-chloro-1-benzofuran-2-carbaldehyde
(E)-3-(3-Chloro-benzofuran-2-yl)-1-(2-hydroxy-5-methoxy-phenyl)-propenone
Conditions | Yield |
---|---|
With potassium hydroxide In ethanol; water Ambient temperature; | 96% |
1-(2-hydroxy-5-methoxyphenyl)ethan-1-one
methanesulfonyl chloride
2-acetyl-4-methoxyphenyl methanesulfonate
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0 - 20℃; for 4h; | 96% |
1-(2-hydroxy-5-methoxyphenyl)ethan-1-one
acetone
6-methoxy-2,2-dimethylchroman-4-one
Conditions | Yield |
---|---|
Stage #1: acetone With pyrrolidine; butyric acid In dimethyl sulfoxide for 0.25h; Kabe Chromanone Synthesis; Stage #2: 1-(2-hydroxy-5-methoxyphenyl)ethan-1-one In dimethyl sulfoxide at 20℃; for 1.5h; Kabe Chromanone Synthesis; | 95% |
With Amberlite IRA 400 basic resin for 0.0833333h; Microwave irradiation; Neat (no solvent); | 91% |
With pyrrolidine In ethanol for 12h; Inert atmosphere; Reflux; | 84.6% |
With pyrrolidine In toluene Ambient temperature; a) RT, 3 h, b) reflux, 18 h; | 53% |
With pyrrolidine In ethanol at 75℃; for 4h; Inert atmosphere; Schlenk technique; |
chloro-trimethyl-silane
1-(2-hydroxy-5-methoxyphenyl)ethan-1-one
1-<2'-<(trimethylsilyl)oxy>-5'-methoxyphenyl>-1-<(trimethylsilyl)oxy>ethylene
Conditions | Yield |
---|---|
With triethylamine; sodium iodide In acetonitrile for 2h; Ambient temperature; | 95% |
1-(2-hydroxy-5-methoxyphenyl)ethan-1-one
trifluoromethylsulfonic anhydride
2-acetyl-4-methoxylphenyl triflate
Conditions | Yield |
---|---|
With pyridine at 0 - 20℃; for 12h; | 95% |
With triethylamine In dichloromethane at 0 - 20℃; Inert atmosphere; |
1-(2-hydroxy-5-methoxyphenyl)ethan-1-one
oxalyl dichloride
N,N-dimethyl-formamide
6-methoxy-4-oxo-4H-chromene-3-carbaldehyde
Conditions | Yield |
---|---|
Stage #1: 1-(2-hydroxy-5-methoxyphenyl)ethan-1-one; N,N-dimethyl-formamide In tetrahydrofuran at 0℃; Inert atmosphere; Stage #2: oxalyl dichloride In tetrahydrofuran at 0 - 20℃; for 12h; Inert atmosphere; | 95% |
1-(2-hydroxy-5-methoxyphenyl)ethan-1-one
trimethylsilyl cyanide
ethylamine
Conditions | Yield |
---|---|
Stage #1: 1-(2-hydroxy-5-methoxyphenyl)ethan-1-one; ethylamine With zinc(II) oxide In neat (no solvent) at 20℃; for 0.166667h; Green chemistry; Stage #2: trimethylsilyl cyanide In neat (no solvent) at 20℃; Green chemistry; | 95% |
isoquinoline
1-(2-hydroxy-5-methoxyphenyl)ethan-1-one
4-(bromoacetyl)toluene
Conditions | Yield |
---|---|
Stage #1: isoquinoline; 4-(bromoacetyl)toluene In water at 80℃; for 0.5h; Green chemistry; Stage #2: 1-(2-hydroxy-5-methoxyphenyl)ethan-1-one With carbonic acid dimethyl ester In water at 80℃; for 3h; Green chemistry; | 95% |
isoquinoline
1-(2-hydroxy-5-methoxyphenyl)ethan-1-one
2-Bromo-4'-methoxyacetophenone
Conditions | Yield |
---|---|
Stage #1: isoquinoline; 2-Bromo-4'-methoxyacetophenone In water at 80℃; for 0.5h; Green chemistry; Stage #2: 1-(2-hydroxy-5-methoxyphenyl)ethan-1-one With carbonic acid dimethyl ester In water at 80℃; for 3h; Green chemistry; | 95% |
1-(2-hydroxy-5-methoxyphenyl)ethan-1-one
4-methoxy-benzaldehyde
4-Methoxyphenyl isothiocyanate
carbonic acid dimethyl ester
malononitrile
Conditions | Yield |
---|---|
Stage #1: 1-(2-hydroxy-5-methoxyphenyl)ethan-1-one; carbonic acid dimethyl ester With magnetic Fe3O4 nanoparticles and ZnO nanoparticles on multiwalled carbon nanotubes at 20℃; for 0.333333h; Stage #2: 4-methoxy-benzaldehyde; malononitrile With magnetic Fe3O4 nanoparticles and ZnO nanoparticles on multiwalled carbon nanotubes at 20℃; for 1h; Stage #3: 4-Methoxyphenyl isothiocyanate at 20℃; for 2h; | 95% |
1-(2-hydroxy-5-methoxyphenyl)ethan-1-one
4-fluorobenzoyl chloride
1-(4-fluorophenyl)-3-(2-hydroxy-5-methoxyphenyl)propane-1,3-dione
Conditions | Yield |
---|---|
Stage #1: 1-(2-hydroxy-5-methoxyphenyl)ethan-1-one With lithium hexamethyldisilazane In tetrahydrofuran; hexane at -78 - 20℃; Inert atmosphere; Stage #2: 4-fluorobenzoyl chloride In tetrahydrofuran; hexane at -78 - 20℃; Inert atmosphere; | 94.9% |
1-(2-hydroxy-5-methoxyphenyl)ethan-1-one
Diethyl carbonate
4-hydroxy-6-methoxycoumarin
Conditions | Yield |
---|---|
With sodium hydride In mineral oil at 0 - 100℃; | 94% |
With sodium hydride In toluene at 0℃; for 4.5h; Reflux; | 90% |
Stage #1: 1-(2-hydroxy-5-methoxyphenyl)ethan-1-one With sodium hydride In toluene for 0.25h; Inert atmosphere; Cooling with ice; Stage #2: Diethyl carbonate In toluene at 20℃; for 5.5h; Inert atmosphere; Reflux; | 82% |
Conditions | Yield |
---|---|
94% |
1-(2-hydroxy-5-methoxyphenyl)ethan-1-one
N,N-Dimethylthiocarbamoyl chloride
O-2-acetyl-4-methoxyphenyl N,N-dimethylcarbamothioate
Conditions | Yield |
---|---|
With 1,4-diaza-bicyclo[2.2.2]octane In N,N-dimethyl-formamide at 50℃; for 5h; Inert atmosphere; | 94% |
Conditions | Yield |
---|---|
With N,N-dimethyl-aniline; 1,1'-carbonyldiimidazole In acetonitrile at 20℃; for 12h; Inert atmosphere; | 93% |
1-(2-hydroxy-5-methoxyphenyl)ethan-1-one
ethyl bromoacetate
ethyl 2-(2-acetyl-4-methoxyphenoxy)acetate
Conditions | Yield |
---|---|
With potassium carbonate In acetone | 92% |
With potassium carbonate In butanone for 10h; Heating / reflux; | 40% |
With potassium carbonate; acetone |
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