sodium nitrite
nitrogen(II) oxide
Conditions | Yield |
---|---|
With acetic acid; potassium iodide In water Product distribution / selectivity; | 100% |
With sulfuric acid; water at 10℃; under 375.038 Torr; for 1.38889E-05h; Reagent/catalyst; Temperature; Pressure; Time; | 99.99% |
With maleic acid; ascorbic acid In water Product distribution / selectivity; |
Conditions | Yield |
---|---|
In neat (no solvent) introduction of NO2 into an rapid streaming mixture of H-He;; spectrometric determination of OH concentration;; | A 100% B n/a |
In gaseous matrix Kinetics; in argon carrier under 0.7 torr; followed by infrared chemiluminescence spectroscopy; | |
In gas crossed molecular beam experiment; Laser fluorescence spectroscopy; |
ammonia
oxygen
A
nitrogen
B
nitrogen(II) oxide
C
dinitrogen monoxide
Conditions | Yield |
---|---|
With oxygen In neat (no solvent) Fe-ZSM-5 catalyst prepared by ion exchange and heat-treated at 400, 425or 450 °C, 100 % NH3 conversion, 100 % N2 selectivity, 1000 ppm NH3 in 2 % O2-contg. He; | A 100% B 0% C 0% |
With catalyst:Fe-mordenite In neat (no solvent) Fe-mordenite catalyst prepared by ion exchange and heat-treated at 425 °C, 92 % NH3 conversion, 99 % N2 selectivity, 1000 ppm NH3 in 2 %O2-contg. He; | A 92% B n/a C 0% |
With catalyst:Fe-ZSM-5 In neat (no solvent) Fe-ZSM-5 catalyst prepared by ion exchange and heat-treated at 375 °C, 90 % NH3 conversion, 99 % N2 selectivity, 1000 ppm NH3 in 2 % O2-contg. He; | A 90% B n/a C 0% |
nitrogen(II) oxide
Conditions | Yield |
---|---|
With cobaltocene In fluorobenzene for 5h; Inert atmosphere; | 100% |
nitrogen(II) oxide
Conditions | Yield |
---|---|
With water; nitric acid at 20℃; under 75.0075 Torr; for 2.77778E-05h; | 99.99% |
In water decompn. in concd. soln. already at cool; | |
In water decompn. in concd. soln. already at cool; |
potassium nitrite
nitrogen(II) oxide
Conditions | Yield |
---|---|
With sulfuric acid; water at 20℃; under 375.038 Torr; for 2.22222E-05h; Pressure; Reagent/catalyst; Temperature; Time; | 99.98% |
With sulfuric acid; potassium iodide In not given byproducts: H2O, I2; washing with NaOH soln.; | |
above 500 °C, based on spect. results; |
ammonia
A
nitrogen
B
nitrogen(II) oxide
C
dinitrogen monoxide
Conditions | Yield |
---|---|
With oxygen In neat (no solvent) Fe-mordenite catalyst prepared by ion exchange and heat-treated at 450 °C, 99 % NH3 conversion, 100 % N2 selectivity, 1000 ppm NH3 in 2 % O2-contg. He; | A 99% B 0% C 0% |
With oxygen; platinum high excess O2,500 °C; | A <1 B n/a C n/a |
With oxygen; platinum at 300 °C; | A n/a B <9 C n/a |
ammonia
nitrogen(II) oxide
Conditions | Yield |
---|---|
With oxygen; platinum react. with air adding O2; | 99% |
With oxygen; platinum optimal time of contact at very high temp.:some E-6 s; | 97% |
With oxygen; Pt(90),Rh(10) (X%) 8 atm,high temp.; | 96% |
methyl nitrite
carbon monoxide
A
Dimethyl oxalate
B
nitrogen(II) oxide
Conditions | Yield |
---|---|
With 0.5% Pd/C at 100℃; under 375.038 Torr; for 0.000555556h; Pressure; Reagent/catalyst; Temperature; Time; | A 98.9% B n/a |
Conditions | Yield |
---|---|
Sr0.22La0.78CoO2.843 In neat (no solvent) byproducts: H2O; 800°C; | A n/a B 98.6% |
Sr0.42La0.68CoO2.80 In neat (no solvent) byproducts: H2O; 800°C; | A n/a B 98.1% |
Sr0.46La0.54CoO2.79 In neat (no solvent) byproducts: H2O; 800°C; | A n/a B 98% |
chloro(N,N'-ethylenebis(salicylideneiminato))iron(III)
A
(μ-oxo)bis[(1,2-ethanediamino-N,N'-bis(salicylidene))iron(III)]
B
nitrogen(II) oxide
Conditions | Yield |
---|---|
In acetonitrile under vac., equimolar mixt.; chromy.; | A n/a B 98% |
With water In acetonitrile under vac., equimolar mixt.; chromy.; | A n/a B 63% |
A
nitrogen
B
nitrogen(II) oxide
C
Nitrogen dioxide
D
dinitrogen monoxide
Conditions | Yield |
---|---|
at 220-260°C, nearly 98% N2O, 2% N2; troces of NO and NO2 (0.001%); | A 2% B n/a C n/a D 98% |
nitrosyl hexafluorophosphate
niobocene dichloride
B
nitrogen(II) oxide
Conditions | Yield |
---|---|
In liquid sulphur dioxide Reaction of Cp2NbCl2 with NOSbF6 in 1/1 molar ratio at room temp. under Ar.; sepn. of solvent and NO under vac., recrystn. (SO2), elem. anal.; | A 98% B n/a |
Conditions | Yield |
---|---|
In acetonitrile Pd sponge (1.0 g) and NOBF4 (2.2 g) stirred in MeCN (50 mL) under vac. for 12 h with periodical removing of NO generated during the react.; filtration; anhydrous ether added to the filtrate; resulting ppt. washed (anhydrous ether) and dried (vac.); elem. anal.; | A 98% B n/a |
(N,N'-ethylenebis(salicylideneiminato))iron(III) nitrate
A
(μ-oxo)bis[(1,2-ethanediamino-N,N'-bis(salicylidene))iron(III)]
B
nitrogen(II) oxide
Conditions | Yield |
---|---|
In acetonitrile under vac., equimolar mixt.; chromy.; | A n/a B 97% |
Conditions | Yield |
---|---|
In gas Kinetics; High Pressure; the reagent ions were generated in an electron impact high-pressure ion source contg. NO2; the reagent ions were selected using a quadrupole mass filter before being injected into a drift region contg. helium carriergas; at 298 K; monitoring by quadrupole mass spectrometer at the end of the flow tube; | A 97% B 3% C n/a D n/a |
Conditions | Yield |
---|---|
With tert.-butylnitrite; trifluoroacetic acid In chloroform Inert atmosphere; | A 95% B 97% |
A
nitrogen(II) oxide
B
gold
Conditions | Yield |
---|---|
With [NO(1+),HMB]BF4(1-) In acetonitrile byproducts: CH4, C2H6; | A 96% B n/a |
niobocene dichloride
B
nitrogen(II) oxide
Conditions | Yield |
---|---|
In liquid sulphur dioxide Reaction of Cp2NbCl2 with NOBF4 in 1/1 molar ratio at room temp. under Ar.; sepn. of solvent and NO under vac., recrystn. (SO2), elem. anal.; | A 96% B n/a |
triphenylphosphine
B
nitrogen(II) oxide
Conditions | Yield |
---|---|
With [NO(1+),HMB]BF4(1-) In acetonitrile | A 94% B 96% |
silver(I) nitrite
(N,N'-ethylenebis(salicylideneiminato))iron(III) nitrate
A
(μ-oxo)bis[(1,2-ethanediamino-N,N'-bis(salicylidene))iron(III)]
B
nitrogen(II) oxide
Conditions | Yield |
---|---|
In acetonitrile under vac., equimolar mixt.; chromy.; | A n/a B 95% |
trifluoroacetic acid
B
nitrogen(II) oxide
Conditions | Yield |
---|---|
In dichloromethane Kinetics; CF3COOH soln. added; UV; | A n/a B 95% |
acetic acid
B
nitrogen(II) oxide
Conditions | Yield |
---|---|
In dichloromethane gas chromy.; | A n/a B 95% |
1-Adamantanethiol
B
nitrogen(II) oxide
Conditions | Yield |
---|---|
In diethyl ether at 20℃; for 0.25h; Solvent; | A 95% B n/a |
ferrocenium(III) tetrafluoroborate
triphenylmethanethiol
B
nitrogen(II) oxide
Conditions | Yield |
---|---|
With [PPN]2[S5Fe(μ-S)2FeS5] In tetrahydrofuran; acetonitrile at 20℃; for 12h; Inert atmosphere; Schlenk technique; | A 92% B n/a |
vanadium
dinitrogen tetroxide
A
vanadium nitrate
B
nitrogen(II) oxide
Conditions | Yield |
---|---|
In acetonitrile acceleration with acetonitrile at o°C;; | A 91% B n/a |
Conditions | Yield |
---|---|
In perchloric acid byproducts: H2O; nitric acid soln. addn. to Ag suspn. at 30-40°C, mixt. keeping at tis temp. for 15 min; | A n/a B 90% |
(N,N'-ethylenebis(salicylideneiminato))iron(III) nitrate
sodium nitrite
A
(μ-oxo)bis[(1,2-ethanediamino-N,N'-bis(salicylidene))iron(III)]
B
nitrogen(II) oxide
Conditions | Yield |
---|---|
In acetonitrile under vac., equimolar mixt.; chromy.; | A n/a B 90% |
bis{octakis(dodecyloxy)phthalocyaninato}lutetium
A
2(C12H25O)8C32H8N8(2-)*Lu(5+)*BF4(1-)={(C12H25O)8C32H8N8}2LuBF4
B
nitrogen(II) oxide
Conditions | Yield |
---|---|
In dichloromethane evapn., dissolved in heptane, filtered, recrystn. (ethyl acetate); elem. anal.; | A 90% B n/a |
Conditions | Yield |
---|---|
In neat (no solvent) decompn. at 225-230°C;; | A 2-6 B 3-5 C n/a D 90% |
In neat (no solvent) decompn. at 225-230°C;; | A 2-6 B 3-5 C n/a D 90% |
nitrogen(II) oxide
nitrogen
Conditions | Yield |
---|---|
With Pd supported ZrO2-CeO2 catalyst at 175 - 400℃; for 1h; Reagent/catalyst; Temperature; Inert atmosphere; | 100% |
With H2; O2; catalyst: 0.1 wtpercent Pt/La0.7Sr0.2Ce0.1FeO3 In neat (no solvent, gas phase) Kinetics; NO:H2:O2 = 1:0.25:5% gas mixt. with 5% H2O added in feed stream; at 140°C for 20 h; H2O as reagent; detd. by mass spectrometry, gas chromy.; | 93% |
With (Y0.90Pr0.10)2O(3+x) at 900℃; Temperature; Inert atmosphere; | 79% |
carbon monoxide
nitrogen(II) oxide
Conditions | Yield |
---|---|
In neat (no solvent) 85 atm CO, 15 atm NO, 200°C;; | 100% |
Conditions | Yield |
---|---|
In neat (no solvent) 105°C, humidity as catalyst;; sublimation in N2-stream at 115°C;; | 100% |
In neat (no solvent) 105°C, humidity as catalyst;; sublimation in N2-stream at 115°C;; | 100% |
In ethanol | |
In ethanol |
carbon monoxide
nitrogen(II) oxide
Conditions | Yield |
---|---|
In neat (no solvent) 85 atm CO, 15 atm NO, 200°C;; | 100% |
Conditions | Yield |
---|---|
1.5h, 250°C; at room temp. slowly; | 100% |
1.5h, 250°C; at room temp. slowly; | 100% |
With oxygen In water | |
With oxygen In water |
Conditions | Yield |
---|---|
In neat (no solvent) 2g dried CoI2 at 105°C reacts with NO gas during 15-20 h;; sublimation in N2 stream at 115°C;; | 100% |
In neat (no solvent) byproducts: I2; 70-80°C;; | |
With copper In neat (no solvent) at 140°C;; | 0% |
With nickel In neat (no solvent) |
Fe(tetraphenylporphyrinate)C6H5
nitrogen(II) oxide
{(C20H8(C6H5)4N4)Fe(C6H5)(NO)}
Conditions | Yield |
---|---|
reaction of a solid complex in NO atm. or a soln. of complex in toluenesaturated with NO at -28°C; | 100% |
In neat (no solvent) exposure of degassed solid ((C20H8(C6H5)4N4)Fe(C6H5)) to 1 atm of nitric oxide;; elem. anal.;; | >99 |
nitrogen(II) oxide
B
benzonitrile
Conditions | Yield |
---|---|
With NaClO4; CH2Cl2 In dichloromethane room temp., 15 min; | A 80% B 100% |
With CH2Cl2 In dichloromethane room temp., 15 min; | A n/a B 73% |
Conditions | Yield |
---|---|
In neat (no solvent) under 760.051 Torr; for 0.166667h; | 100% |
Conditions | Yield |
---|---|
In benzene Inert atmosphere; | 100% |
[(1,3-bis[(di-tert-butylphosphino)methyl)-4,6-dimethylbenzene(-1H))Rh(N2)]
nitrogen(II) oxide
Conditions | Yield |
---|---|
In tetrahydrofuran Inert atmosphere; | 100% |
Conditions | Yield |
---|---|
With catalyst: Ni(2+)Y zeolite In neat (no solvent) reduction of very dild. mixt. of NO/NO2 in gas mixt. of N2/H2 on zeolite catalyst (300°C reaction temp.); gas chromy. (dimethylsulfolane coated diatomite); | 99% |
With catalyst: industrial nickel methanation catalyst In neat (no solvent) reduction of very dild. mixt. of NO/NO2 in gas mixt. of N2/H2 on zeolite catalyst (300°C reaction temp.); gas chromy. (dimethylsulfolane coated diatomite); | 99% |
With catalyst: phthalocyanineNiY zeolite In neat (no solvent) reduction of very dild. mixt. of NO/NO2 in gas mixt. of N2/H2 on zeolite catalyst (230°C reaction temp.); gas chromy. (dimethylsulfolane coated diatomite); | 94% |
With catalyst: NiY zeolite In neat (no solvent) reduction of very dild. mixt. of NO/NO2 in gas mixt. of N2/H2 on zeolite catalyst (450°C reaction temp.); gas chromy. (dimethylsulfolane coated diatomite); | 84% |
nitrogen(II) oxide
[(1,1',2,2'-bisdiphenylphosphinoethylene)Pt(CF3)(NO2)]
Conditions | Yield |
---|---|
In tetrahydrofuran byproducts: HNO2; | 99% |
In tetrahydrofuran; diethyl ether suspended in THF/Et2O mixture, evacuated and saturated with NO, stirredat 25°C for 1.5 h, N2 bubbled; filtered, washed with Et2O, dried, recrystd. from CH2Cl2/MeOH; |
Conditions | Yield |
---|---|
With perchloric acid; sodium perchlorate In water Kinetics; byproducts: H2O; HClO4 was added to soln. of Fe complex in aq. NaClO4 to pH 3; soln. was deoxygenated with N2; NO was bubbled; UV monitoring; | 99% |
With perchloric acid; sodium perchlorate; sodium thiocyanide In perchloric acid; water Kinetics; deoxygenated soln. of NaSCN in aq. HClO4 was satd. with NO and mixed with deoxygenated soln. of Fe complex in aq. NaClO4 (pH 3) at 25°C; UV monitoring; | |
With 1,4-pyrazine; perchloric acid; sodium perchlorate In perchloric acid; water Kinetics; deoxygenated soln. of pyrazine in aq. HClO4 was satd. with NO and mixed with deoxygenated soln. of Fe complex in aq. NaClO4 (pH 3) at 25°C; UV monitoring; |
[CuI(tris(2-pyridylmethyl)amine)(CH3CN)]2+
nitrogen(II) oxide
A
[Cu(tris(2-pyridylmethyl)amine)(H2O)](2+)
B
dinitrogen monoxide
Conditions | Yield |
---|---|
In water room temp., pH = 7.0; reaction followed by gas chromy.; | A 99% B n/a |
nitrogen(II) oxide
Conditions | Yield |
---|---|
In tetrahydrofuran byproducts: HNO2; | 99% |
Conditions | Yield |
---|---|
In tetrahydrofuran byproducts: HNO2; | 99% |
Conditions | Yield |
---|---|
In diethyl ether reaction at 25°C; | 99% |
[(η(3)-cyclooctenyl)Co(Pr(i)2PCH2CH2PPr(i)2)](+)BF4(-)
nitrogen(II) oxide
[(η(3)-cyclooctenyl)Co(Pr(i)2PCH2CH2PPr(i)2)NO](+)BF4(-)
Conditions | Yield |
---|---|
In acetone Ar-atmosphere; excess NO, 4 h; collection (filtration), washing (Et2O), drying (vac.); elem. anal.; | 99% |
nitrogen(II) oxide
Conditions | Yield |
---|---|
In further solvent(s) NO passed for 30 min through a CH2Cl2/tetra-n-butylammonium perchlorate soln. of Ru complex; the soln. purged with N2 until dry, washed (acetone); elem. anal.; | 99% |
Conditions | Yield |
---|---|
In diethyl ether reaction at 25°C; | 99% |
Conditions | Yield |
---|---|
In diethyl ether reaction at 25°C; | 99% |
Molecular Structure:
Molecular Formula: NO
Molecular Weight: 30.0061
IUPAC Name: Nitric oxide
Synonyms of Nitric oxide (CAS NO.10102-43-9): Amidogen, oxo- ; Bioxyde d'azote ; Bioxyde d'azote [French] ; CCRIS 4319 ; EINECS 233-271-0 ; HSDB 1246 ; INOmax ; Mononitrogen monoxide ; Nitric oxide ; Nitrogen monoxide ; Nitrogen oxide (NO) ; Oxyde nitrique ; Oxyde nitrique [French] ; RCRA waste number P076 ; Stickmonoxyd ; Stickmonoxyd [German] ; UN 1660 ; UNII-31C4KY9ESH ; Nitric oxide 10% by volume or more ; Nitric oxide, compressed ; Nitric oxide, compressed [UN1660] [Poison gas] ; Nitrogen oxide ; UN1660
CAS NO: 10102-43-9
Classification Code: Anti-Asthmatic Agents ; Antioxidants ; Autonomic Agents ; Bronchodilator agents ; Cardiovascular Agents ; Endothelium-Dependent Relaxing Factors ; Free radical scavengers ; Mutation data ; Neurotransmitter Agents ; Peripheral Nervous System Agents ; Respiratory System Agents ; Vasodilator agents
Melting point: −163.6 °C
Boiling Point: −151.7 °C
Vapor density: 1.05 (vs air)
Nitric oxide (CAS NO.10102-43-9) can be used for detecting surface radicals on polymers.
Commercially:4 NH3 + 5 O2 → 4 NO + 6 H2O (at 750°C to 900°C (normally at 850°C)
In the laboratory:8 HNO3 + 3 Cu → 3 Cu(NO3)2 + 4 H2O + 2 NO
Organism | Test Type | Route | Reported Dose (Normalized Dose) | Effect | Source |
---|---|---|---|---|---|
dog | LCLo | inhalation | 5000ppm/25M (5000ppm) | LUNGS, THORAX, OR RESPIRATION: ACUTE PULMONARY EDEMA BLOOD: METHEMOGLOBINEMIA-CARBOXYHEMOGLOBIN | British Journal of Anesthesia. Vol. 39, Pg. 393, 1967. |
mouse | LCLo | inhalation | 320ppm (320ppm) | BEHAVIORAL: CONVULSIONS OR EFFECT ON SEIZURE THRESHOLD LUNGS, THORAX, OR RESPIRATION: CYANOSIS BLOOD: METHEMOGLOBINEMIA-CARBOXYHEMOGLOBIN | Naunyn-Schmiedeberg's Archiv fuer Experimentelle Pathologie und Pharmakologie. Vol. 181, Pg. 145, 1936. |
rat | LC50 | inhalation | 1068mg/m3/4H (1068mg/m3) | Gigiena Truda i Professional'nye Zabolevaniya. Labor Hygiene and Occupational Diseases. Vol. 19(4), Pg. 52, 1975. |
Reported in EPA TSCA Inventory. EPA Extremely Hazardous Substances List.
Hazard Codes of Nitric oxide (CAS NO.10102-43-9): O,T
Risk Statements: 8-23-34-44
R8: Contact with combustible material may cause fire.
R23: Toxic by inhalation.
R34: Causes burns.
R44: Risk of explosion if heated under confinement.
Safety Statements: 17-23-36/37/39-45
S17: Keep away from combustible material.
S23: Do not breathe vapour.
S36/37/39: Wear suitable protective clothing, gloves and eye/face protection.
S45: In case of accident or if you feel unwell, seek medical advice immediately (show the label whenever possible.)
RIDADR: UN 1660 2.3
WGK Germany: 1
RTECS: QX0525000
HazardClass: 2.3
A poison gas. A severe eye, skin, and mucous membrane irritant. A systemic irritant by inhalation. Mutation data reported. Exposure may occur whenever nitric acid acts upon organic material, such as wood, sawdust, and refuse; it occurs when nitric acid is heated, and when organic nitro compounds are burned, for example, celluloid, cellulose nitrate (guncotton), and dynamite. The action of nitric acid upon metals, as in metal etching and pickling, also liberates the fumes. In high-temperature welding, as with the oxyacetylene or electric torch, the nitrogen and oxygen of the air unite to form oxides of nitrogen. Automobile exhaust and power plant emissions are also sources of NOx. Exposure occurs in many manufacturing processes when nitric acid is made or used. Oxides of nitrogen have been implicated as a cause of acid rain.
The oxides of nitrogen are somewhat soluble in water, reacting with it to form nitric and nitrous acids. This is the action that takes place deep in the respiratory system. The acids formed are irritating and can cause congestion in the throat and bronchi and edema of the lungs. The acids are neutralized by the alkalies present in the tissues, with the formation of nitrates and nitrites. The latter may cause some arterial dilation, fall in blood pressure, headache, and dizziness, and there may be some formation of methemoglobin. However, the nitrite effect is of secondary importance.
Because of their relatively low solubility in water, the nitrogen oxides are initially only slightly irritating to the mucous membranes of the upper respiratory tract. Their warning power is therefore low, and dangerous amounts of the fumes may be breathed before the worker notices any real discomfort. Higher concentrations (60–150 ppm) cause immediate irritation of the nose and throat, with coughing and burning in the throat and chest. These symptoms often clear upon breathing fresh air, and the worker may feel well for several hours. Some 6–24 hours after exposure, a sensation of tightness and burning in the chest develops, followed by shortness of breath, sleeplessness, and restlessness. Dyspnea and air hunger may increase rapidly with development of cyanosis and loss of consciousness followed by death. In cases that recover from the pulmonary edema, there is usually no permanent disability, but pneumonia may develop later. Concentrations of 100–150 ppm are dangerous for short exposures of 30–60 minutes. Concentrations of 200–700 ppm may be fatal after even very short exposures.
Continued exposure to low concentrations of the fumes, insufficient to cause pulmonary edema, is said to result in chronic irritation of the respiratory tract, with cough, headache, loss of appetite, dyspepsia, corrosion of the teeth, and gradual loss of strength.
Exposure to NOx is always potentially serious, and persons so exposed should be kept under close observation for at least 48 hours.
An oxidizer. The liquid is a sensitive explosive. Explosive reaction with carbon disulfide (when ignited), methanol (when ignited), pentacarbonyl iron (at 50°C), phosphine + oxygen, sodium diphenylketyl, dichlorine oxide, fluorine, nitrogen trichloride, ozone, perchloryl fluoride (at 100–300°C), vinyl chloride. Reacts to form explosive products with dienes (e.g., 1,3-butadiene, cyclopentadiene, propadiene).
Can react violently with acetic anhydride, Al, amorphous boron, BaO, BCl3, CsHC2, calcium, carbon + potassium hydrogen tartrate, charcoal, ClO, pyrophoric chromium, 1,2-dichloroethane, dichloroethylene, ethylene, fuels, hydrocarbons, hydrogen + oxygen, Na2O, uns-dimethyl hydrazine, NH3, CHCl3, Fe, Mg, Mn, CH2Cl2, olefins, phosphorus, PNH2, PH3, potassium, potassium sulfide, propylene, rubidium acetylide, Na, S, tungsten carbide, trichloroethylene, 1,1,1-trichloroethane, uns-tetrachloroethane, uranium, uranium dicarbide. Will react with water or steam to produce heat and corrosive fumes; can react vigorously with reducing materials.
OSHA PEL: TWA 25 ppm
ACGIH TLV: TWA 25 ppm
NIOSH REL: (Oxides of Nitrogen) TWA 25 ppm
DOT Classification: 2.3; Label: Poison Gas
For occupational chemical analysis use OSHA: #ID-109.
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