Diglycolic acid supplier | CasNO.110-99-6

Name
Diglycolic acid
EINECS 203-823-5
CAS No. 110-99-6
Article Data44
CAS DataBase
Density 1.486
Solubility soluble
Melting Point 140-144
Formula C4H6 O5
Boiling Point 445.2°Cat760mmHg
Molecular Weight 134.089
Flash Point 201.7°C
Transport Information
Appearance white to light beige crystalline powder
Safety Moderately toxic by ingestion. When heated to decomposition it emits acrid smoke and irritating vapors.
Risk Codes R22;R34
Molecular Structure
Hazard Symbols
Synonyms Aceticacid, oxydi- (8CI); Diglycolic acid (6CI); 2,2'-Oxydiacetic acid;3-Oxapentane-1,5-dioic acid; 3-Oxapentanedioic acid; Bis(carboxymethyl) ether;NSC 8651; Oxodiacetic acid; Oxybisacetic acid; Oxydiacetic acid; Oxydiethanolicacid
PSA 83.83000
LogP -0.82780

Synthetic route

: 111-46-6
diethylene glycol

: 110-99-6
2,2'-oxybis-acetic acid

Conditions

Conditions	Yield
With nitric acid at 45 - 80℃; for 2.16667h;	92%
With nitric acid	90%
With C24H33IrN4O3; water; sodium hydroxide for 18h; Reflux;	90%

: 3041-16-5
p-dioxanone

: 110-99-6
2,2'-oxybis-acetic acid

Conditions

Conditions	Yield
With dinitrogen tetraoxide In chloroform	75%

: 112-60-7
Tetraethylene glycol

A: 110-99-6
2,2'-oxybis-acetic acid

B: 23243-68-7
3,6-dioxasuberic acid

C: 13887-98-4
tetraglycolic acid

Conditions

Conditions	Yield
at 5℃; for 8h; electrolysis: nickel net anode, cylindrical stainless steel cathode; electrolyte: 1M NaOH/H2O; Title compound not separated from byproducts;	A 3% B 16% C 50%

...Expand

: 4358-64-9
cis-1,4-anhydroerythritol

A: 110-99-6
2,2'-oxybis-acetic acid

B: 2-(formyloxymethoxy)acetic acid

Conditions

Conditions	Yield
With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; tetrabutylammomium bromide; 3-chloro-benzenecarboperoxoic acid In dichloromethane at 20℃; for 0.75h; Time; Inert atmosphere;	A n/a B 29%

: 79-14-1
glycolic Acid

: 110-99-6
2,2'-oxybis-acetic acid

Conditions

Conditions	Yield
at 200 - 240℃;

: 79-08-3
bromoacetic acid

A: 110-99-6
2,2'-oxybis-acetic acid

B: 79-14-1
glycolic Acid

Conditions

Conditions	Yield
With water quantitativer Verlauf der Bildung mit verschiedenen Basen;

: 79-11-8
chloroacetic acid

: 110-99-6
2,2'-oxybis-acetic acid

Conditions

Conditions	Yield
With calcium hydroxide; water
With barium dihydroxide; water
With strontium hydroxide; water
With barium dihydroxide Darstellung; ueber mehrere Stufen;

: 79-11-8
chloroacetic acid

A: 110-99-6
2,2'-oxybis-acetic acid

B: 79-14-1
glycolic Acid

Conditions

Conditions	Yield
With water; lead(II) oxide
With water; magnesium oxide

: 123-91-1
1,4-dioxane

: 110-99-6
2,2'-oxybis-acetic acid

Conditions

Conditions	Yield
With hydrogenchloride; sodium hypochlorite

: 111-96-6
diethylene glycol dimethyl ether

: 110-99-6
2,2'-oxybis-acetic acid

Conditions

Conditions	Yield
With hydrogenchloride; sodium hypochlorite

: 4480-83-5
1,4-dioxane-2,6-dione

: 7732-18-5
water

: 110-99-6
2,2'-oxybis-acetic acid

: 4430-05-1
morpholine-3,5-dione

KOH-solution: KOH-solution

: 110-99-6
2,2'-oxybis-acetic acid

: 462110-57-2
4-ethyltetrahydro-1,4-oxazine-3,5-dione

: 7732-18-5
water

A: 110-99-6
2,2'-oxybis-acetic acid

B: 75-04-7
ethylamine

...Expand

: 57503-67-0
4-methyltetrahydro-1,4-oxazine-3,5-dione

: 7732-18-5
water

A: 110-99-6
2,2'-oxybis-acetic acid

B: 74-89-5
methylamine

...Expand

: 7732-18-5
water

: 79-08-3
bromoacetic acid

A: 110-99-6
2,2'-oxybis-acetic acid

B: 79-14-1
glycolic Acid

Conditions

Conditions	Yield
Geschwindigkeit und Verlauf der Reaktionen;

...Expand

: 79-08-3
bromoacetic acid

-base: -base

A: 110-99-6
2,2'-oxybis-acetic acid

B: 79-14-1
glycolic Acid

Conditions

Conditions	Yield
Geschwindigkeit und Verlauf der Reaktionen;

...Expand

: 79-11-8
chloroacetic acid

-base: -base

A: 110-99-6
2,2'-oxybis-acetic acid

B: 79-14-1
glycolic Acid

...Expand

dimethyl ester of/the/ diglycolic acid: dimethyl ester of/the/ diglycolic acid

: 110-99-6
2,2'-oxybis-acetic acid

Conditions

Conditions	Yield
With sulfuric acid; water
With water
With phosphoric acid; water

: 79-11-8
chloroacetic acid

lithium hydroxide: lithium hydroxide

: 110-99-6
2,2'-oxybis-acetic acid

Conditions

Conditions	Yield
With water

: 105-39-5
chloroacetic acid ethyl ester

sodium glycolic acid ester: sodium glycolic acid ester

: 110-99-6
2,2'-oxybis-acetic acid

Conditions

Conditions	Yield
und Verseifung des entstehenden Diaethylesters;

: 7697-37-2
nitric acid

: 111-46-6
diethylene glycol

A: 110-99-6
2,2'-oxybis-acetic acid

B: 79-14-1
glycolic Acid

C: 144-62-7
oxalic acid

...Expand

: 111-46-6
diethylene glycol

A: 110-99-6
2,2'-oxybis-acetic acid

B glycolic acid and oxalic acid: glycolic acid and oxalic acid

Conditions

Conditions	Yield
With nitric acid

: 79-14-1
glycolic Acid

A: 110-99-6
2,2'-oxybis-acetic acid

B poly glycolide: poly glycolide

C polyoxymethylene: polyoxymethylene

Conditions

Conditions	Yield
at 200 - 240℃;

...Expand

: 7647-01-0
hydrogenchloride

: 22064-41-1
diglycolamide

A: 110-99-6
2,2'-oxybis-acetic acid

B: ammonium chloride

Conditions

Conditions	Yield
und Behandeln mit Wasser;

...Expand

: 22064-41-1
diglycolamide

alkali: alkali

A: 110-99-6
2,2'-oxybis-acetic acid

B: 7664-41-7
ammonia

...Expand

: 4480-83-5
1,4-dioxane-2,6-dione

: 23288-49-5
(4,4'-isopropylidenedithio)bis[2,6-di-tert-butylphenol]

A: 110-99-6
2,2'-oxybis-acetic acid

B diglycolic acid, mono[4-[[1-[[3,5-bis(1,1-dimethylethyl)-4-hydroxyphenyl]thio]-1-methylethyl]thio]-2,6-bis(1,1-dimethylethyl)phenyl]ester: diglycolic acid, mono[4-[[1-[[3,5-bis(1,1-dimethylethyl)-4-hydroxyphenyl]thio]-1-methylethyl]thio]-2,6-bis(1,1-dimethylethyl)phenyl]ester

Conditions

Conditions	Yield
In tetrahydrofuran

...Expand

: dipotassium salt of diglycolic acid

: 110-99-6
2,2'-oxybis-acetic acid

Conditions

Conditions	Yield
In carbon dioxide
In carbon dioxide

: 4480-83-5
1,4-dioxane-2,6-dione

: 60-29-7
diethyl ether

: 110-99-6
2,2'-oxybis-acetic acid

Conditions

Conditions	Yield
With dmap In pyridine

: 110-99-6
2,2'-oxybis-acetic acid

: 67-56-1
methanol

: 7040-23-5
dimethyl diglycolate

Conditions

Conditions	Yield
With thionyl chloride at 0 - 20℃;	100%
Stage #1: 2,2'-oxybis-acetic acid With thionyl chloride at 20℃; for 8h; Stage #2: methanol	98%
With sulfuric acid for 24h; Heating;	90%

: 110-99-6
2,2'-oxybis-acetic acid

: 21062-20-4
diglycolyl chloride

Conditions

Conditions	Yield
With oxalyl dichloride In benzene	100%
With oxalyl dichloride; N,N-dimethyl-formamide In dichloromethane at 20℃; Cooling with ice;	88%
With thionyl chloride for 5h; Reflux;	86.2%

: 110-99-6
2,2'-oxybis-acetic acid

: thorium(IV) nitrate hexahydrate

: [Th(oxydiacetate)2]n

Conditions

Conditions	Yield
In methanol stoich. amts. (pptn.);	99%
In not given addn. of >= 2 equiv. of ligand to Th salt; crystn. (several days), filtration, washing (H2O, MeOH); elem. anal.;

: 110-99-6
2,2'-oxybis-acetic acid

: 5856-63-3
(2R)-2-aminobutan-1-ol

: 850410-75-2
(-)-bis{[4-(R)-ethyloxazolin-2-yl]methyl} ether

Conditions

Conditions	Yield
In toluene for 23h; Reflux;	98%

: 571190-30-2
PD 0332991

: 110-99-6
2,2'-oxybis-acetic acid

: 2-(2-(4-(6-((6-acetyl-8-cyclopentyl-5-methyl-7-oxo-7,8-dihydropyrido[2,3-d]pyrimidin-2-yl)amino)pyridin-3-yl)piperazin-1-yl)-2-oxoethoxy)acetic acid

Conditions

Conditions	Yield
With 4-methyl-morpholine; 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane; dimethyl sulfoxide at 20℃;	96%

: 110-99-6
2,2'-oxybis-acetic acid

: terbium(III) perchlorate hexahydrate

: cadmium(II) perchlorate dihydrate

: 7732-18-5
water

: {[Tb2(oxydiacetate)6Cd3(H2O)6]·6H2O}n

Conditions

Conditions	Yield
Stage #1: 2,2'-oxybis-acetic acid; terbium(III) perchlorate hexahydrate; water With sodium hydroxide at 20℃; for 1h; pH=6.0; Stage #2: cadmium(II) perchlorate dihydrate With sodium hydroxide at 60℃; for 4h; pH=6.5;	95%

...Expand

: 110-99-6
2,2'-oxybis-acetic acid

: praseodymium perchlorate hexahydrate

: cadmium(II) perchlorate dihydrate

: 7732-18-5
water

: {[Pr2((oxydiacetate))6Cd3(H2O)6]·9H2O}n

Conditions

Conditions	Yield
Stage #1: 2,2'-oxybis-acetic acid; praseodymium perchlorate hexahydrate; water With sodium hydroxide at 20℃; for 1h; pH=6; Stage #2: cadmium(II) perchlorate dihydrate With sodium hydroxide at 60℃; for 4h; pH=6.5;	95%

...Expand

: 110-99-6
2,2'-oxybis-acetic acid

: neodymium(III) perchlorate hexahydrate

: cadmium(II) perchlorate dihydrate

: 7732-18-5
water

: {[Nd2((oxydiacetate))6Cd3(H2O)6]·6H2O}n

Conditions

Conditions	Yield
Stage #1: 2,2'-oxybis-acetic acid; neodymium(III) perchlorate hexahydrate; water With sodium hydroxide at 20℃; for 1h; pH=6; Stage #2: cadmium(II) perchlorate dihydrate With sodium hydroxide at 60℃; for 4h; pH=6.5;	95%

...Expand

: 110-99-6
2,2'-oxybis-acetic acid

: samarium(III) perchlorate hexahydrate

: cadmium(II) perchlorate dihydrate

: 7732-18-5
water

: {[Sm2((oxydiacetate))6Cd3(H2O)6]·6H2O}n

Conditions

Conditions	Yield
Stage #1: 2,2'-oxybis-acetic acid; samarium(III) perchlorate hexahydrate; water With sodium hydroxide at 20℃; for 1h; pH=6; Stage #2: cadmium(II) perchlorate dihydrate With sodium hydroxide at 60℃; for 4h; pH=6.5;	95%

...Expand

: 110-99-6
2,2'-oxybis-acetic acid

: europium(III) perchlorate hexahydrate

: cadmium(II) perchlorate dihydrate

: 7732-18-5
water

: {[Eu2((oxydiacetate))6Cd3(H2O)6]·6H2O}n

Conditions

Conditions	Yield
Stage #1: 2,2'-oxybis-acetic acid; europium(III) perchlorate hexahydrate; water With sodium hydroxide at 20℃; for 1h; pH=6; Stage #2: cadmium(II) perchlorate dihydrate With sodium hydroxide at 60℃; for 4h; pH=6.5;	95%

...Expand

: 110-99-6
2,2'-oxybis-acetic acid

: dysprosium(III) perchlorate hexahydrate

: cadmium(II) perchlorate dihydrate

: 7732-18-5
water

: {[Dy2((oxydiacetate))6Cd3(H2O)6]·3H2O}n

Conditions

Conditions	Yield
Stage #1: 2,2'-oxybis-acetic acid; dysprosium(III) perchlorate hexahydrate; water With sodium hydroxide at 20℃; for 1h; pH=6; Stage #2: cadmium(II) perchlorate dihydrate With sodium hydroxide at 60℃; for 4h; pH=6.5;	95%

...Expand

: 110-99-6
2,2'-oxybis-acetic acid

: 109-89-7
diethylamine

: 77077-06-6
N,N,N′,N′-tetraethyl diglycolamide

Conditions

Conditions	Yield
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In chloroform at 20℃; for 18h;	95%

: 110-99-6
2,2'-oxybis-acetic acid

: (3S,4S)-N3,N4-bis(((1S,2R)-2-phenylcyclopropyl)carbamoyl)pyrrolidine-3,4-dicarboxamide hydrochloride

: (3S,3’S,4S,4’S)-1,1’-(2,2’-oxybis(acetyl))bis-(N3,N4-bis((1S,2R)-2-phenylcyclopropyl)pyrrolidine-3,4-dicarboxamide)

Conditions

Conditions	Yield
With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 23℃; for 18h;	94%

: 110-99-6
2,2'-oxybis-acetic acid

: 4480-83-5
1,4-dioxane-2,6-dione

Conditions

Conditions	Yield
With oxalyl dichloride; N,N-dimethyl-formamide In toluene for 3h; Inert atmosphere; Reflux;	93%
With phosphoric acid; acetic anhydride at 145℃; for 2h; Temperature;	90%
With niobium(V) oxide hydrate In o-xylene at 160℃; for 72h; Inert atmosphere; Molecular sieve;	86%

: 110-99-6
2,2'-oxybis-acetic acid

: gadolinium(III) perchlorate hexahydrate

: cadmium(II) perchlorate dihydrate

: 7732-18-5
water

: {[Gd2(oxydiacetate)6Cd3(H2O)6]·6H2O}n

Conditions

Conditions	Yield
Stage #1: 2,2'-oxybis-acetic acid; gadolinium(III) perchlorate hexahydrate; water With sodium hydroxide at 20℃; for 1h; pH=6.0; Stage #2: cadmium(II) perchlorate dihydrate With sodium hydroxide at 60℃; for 4h; pH=6.5;	92%

...Expand

: 110-99-6
2,2'-oxybis-acetic acid

: 5-[2-([3-(2-amino-ethoxy)-5-([(4-benzyloxycarbonyl-butylcarbamoyl)-methyl]-{[2-(4-fluoro-phenyl)-ethylcarbamoyl]-methyl}-carbamoyl)-benzoyl]-{[2-(4-fluoro-phenyl)-ethylcarbamoyl]-methyl}-amino)-acetylamino]-pentanoic acid benzyl ester; hydrochloride

: C120H136F4N14O25

Conditions

Conditions	Yield
With N-ethyl-N,N-diisopropylamine; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate In N,N-dimethyl-formamide at 25℃; for 12h; Condensation;	90%

: 110-99-6
2,2'-oxybis-acetic acid

: cobalt(II) nitrate hexahydrate

: 7803-57-8
hydrazine hydrate

: Co(2+)*CO2CH2OCH2CO2(2-)*2N2H4=Co(CO2CH2OCH2CO2)*2N2H4

Conditions

Conditions	Yield
In water oxiacetic acid and hydrazine hydrate in water were added to the aq. soln. of metal nitrate hydrate; ppt. was washed with water, alcohol and ther and dried in air; elem. anal.;	90%

...Expand

: 110-99-6
2,2'-oxybis-acetic acid

: nickel(II) nitrate hydrate

: 7803-57-8
hydrazine hydrate

: Ni(2+)*CO2CH2OCH2CO2(2-)*2N2H4=Ni(CO2CH2OCH2CO2)*2N2H4

Conditions

Conditions	Yield
In water oxiacetic acid and hydrazine hydrate in water were added to the aq. soln. of metal nitrate hydrate; ppt. was washed with water, alcohol and ther and dried in air; elem. anal.;	90%

...Expand

: 110-99-6
2,2'-oxybis-acetic acid

: zinc(II) nitrate hydrate

: 7803-57-8
hydrazine hydrate

: 332397-36-1
Zn(2+)*CO2CH2OCH2CO2(2-)*N2H4*H2O=Zn(CO2CH2OCH2CO2)*N2H4*H2O

Conditions

Conditions	Yield
In water oxiacetic acid and hydrazine hydrate in water were added to the aq. soln. of metal nitrate hydrate; ppt. was washed with water, alcohol and ther and dried in air; elem. anal.;	90%

...Expand

: 110-99-6
2,2'-oxybis-acetic acid

: dysprosium hydroxide

: cadmium(II) perchlorate dihydrate

: 7732-18-5
water

: {[Cd(H2O)6]·[Dy2(oxydiacetate)6Cd2]·6H2O}n

Conditions

Conditions	Yield
at 170℃; for 168h; High pressure;	90%

...Expand

: 110-99-6
2,2'-oxybis-acetic acid

: erbium hydroxide

: cadmium(II) perchlorate dihydrate

: 7732-18-5
water

: {[Cd(H2O)6]·[Er2(oxydiacetate)6Cd2]·12H2O}n

Conditions

Conditions	Yield
at 170℃; for 168h; High pressure;	90%

...Expand

: 110-99-6
2,2'-oxybis-acetic acid

: holmium(III) hydroxide

: cadmium(II) perchlorate dihydrate

: 7732-18-5
water

: {[Cd(H2O)6]·[Ho2(oxydiacetate)6Cd2]·12H2O}n

Conditions

Conditions	Yield
at 170℃; for 168h; High pressure;	90%

...Expand

: 110-99-6
2,2'-oxybis-acetic acid

: thulium(III) hydroxide

: cadmium(II) perchlorate dihydrate

: 7732-18-5
water

: {[Cd(H2O)6]·[Tm2(oxydiacetate)6Cd2]·12H2O}n

Conditions

Conditions	Yield
at 170℃; for 168h; High pressure;	90%

...Expand

: 110-99-6
2,2'-oxybis-acetic acid

: lutetium(III) hydroxide

: cadmium(II) perchlorate dihydrate

: 7732-18-5
water

: {[Cd(H2O)6]·[Lu2(oxydiacetate)6Cd2]·12H2O}n

Conditions

Conditions	Yield
at 170℃; for 168h; High pressure;	90%

...Expand

: 110-99-6
2,2'-oxybis-acetic acid

azido-PEG24-CO[N(PN)2][Lys]4[(α-NH2*TFA)(ε-NHPEG1100)]4: azido-PEG24-CO[N(PN)2][Lys]4[(α-NH2*TFA)(ε-NHPEG1100)]4

: (8S,10S)-10-(4-Amino-5-hydroxy-6-methyl-tetrahydro-pyran-2-yloxy)-6,8,11-trihydroxy-8-(2-hydroxy-acetyl)-1-methoxy-7,8,9,10-tetrahydro-naphthacene-5,12-dione

azido-PEG24-CO[N(PN)2][Lys]4[(α-NH-DGA-3'-NH-dox)(ε-NH-COPEG1100)]4: azido-PEG24-CO[N(PN)2][Lys]4[(α-NH-DGA-3'-NH-dox)(ε-NH-COPEG1100)]4

Conditions

Conditions	Yield
Stage #1: (8S,10S)-10-(4-Amino-5-hydroxy-6-methyl-tetrahydro-pyran-2-yloxy)-6,8,11-trihydroxy-8-(2-hydroxy-acetyl)-1-methoxy-7,8,9,10-tetrahydro-naphthacene-5,12-dione With dmap In N,N-dimethyl-formamide at 20℃; for 0.0833333h; Stage #2: 2,2'-oxybis-acetic acid In N,N-dimethyl-formamide for 3h; Stage #3: azido-PEG24-CO[N(PN)2][Lys]4[(α-NH2*TFA)(ε-NHPEG1100)]4 With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃;	89%

Yield

Stage #1: (8S,10S)-10-(4-Amino-5-hydroxy-6-methyl-tetrahydro-pyran-2-yloxy)-6,8,11-trihydroxy-8-(2-hydroxy-acetyl)-1-methoxy-7,8,9,10-tetrahydro-naphthacene-5,12-dione With dmap In N,N-dimethyl-formamide at 20℃; for 0.0833333h;
Stage #2: 2,2'-oxybis-acetic acid In N,N-dimethyl-formamide for 3h;
Stage #3: azido-PEG24-CO[N(PN)2][Lys]4[(α-NH2*TFA)(ε-NHPEG1100)]4 With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃;

89%

...Expand

: 110-99-6
2,2'-oxybis-acetic acid

azido-PEG24-CO[N(PN)2][Lys]4[(α-NH2*TFA)(ε-NHPEG1100)]4: azido-PEG24-CO[N(PN)2][Lys]4[(α-NH2*TFA)(ε-NHPEG1100)]4

: Nemorubicin

azido-PEG24CO-[N(PN)2][Lys]4[(α-NH-DGA-14-O-nemo)(ε-NH-COPEG1100) ]4: azido-PEG24CO-[N(PN)2][Lys]4[(α-NH-DGA-14-O-nemo)(ε-NH-COPEG1100) ]4

Conditions

Conditions	Yield
Stage #1: Nemorubicin With dmap In N,N-dimethyl-formamide at 20℃; for 0.0833333h; Stage #2: 2,2'-oxybis-acetic acid In N,N-dimethyl-formamide for 3h; Stage #3: azido-PEG24-CO[N(PN)2][Lys]4[(α-NH2*TFA)(ε-NHPEG1100)]4 With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃;	89%

...Expand

: 110-99-6
2,2'-oxybis-acetic acid

: 183133-96-2
carbazitaxel

: 1375468-21-5
diglycolyl-cabazitaxel

Conditions

Conditions	Yield
With triethylamine In dichloromethane at 20℃; for 1.5h;	88.5%

: 110-99-6
2,2'-oxybis-acetic acid

: 95-54-5
1,2-diamino-benzene

: 94665-42-6
1,3-bis(1H-benzimidazol-2-yl)-2-oxapropane

Conditions

Conditions	Yield
With silphox [POCl3-n(SiO2)n, silica phosphinoxide] In N,N-dimethyl-formamide for 0.25h; Microwave irradiation;	87%
With hydrogenchloride; water for 14h; Heating;	72%
With polyphosphoric acid at 180℃;	70%

: 110-99-6
2,2'-oxybis-acetic acid

: uranyl nirate hexahydrate

: 45979-40-6, 48122-12-9
oxydiacetatodioxouranium(VI)

Conditions

Conditions	Yield
With sodium bicarbonate In water diglycolic acid and sodium bicarbonate dissolved in H2O, uranyl nitrate hexahydrate in H2O added, heated to reflux, cooled to ambient temp.; filtered, washed with H2O and acetone, dried by suction;	87%

Diglycolic acid Chemical Properties

MF: C₄H₆O₅

MW: 134.09
mp: 140-144 ^°C(lit.)
Physical State: Crystalline powder
Color of OXODIACETIC ACID: clear slight yellow
Solubility : soluble in water and soluble in alcohol

Diglycolic acid Toxicity Data With Reference

orl-rat LD50:500 mg/kg

ACIEAY Angewandte Chemie, International Edition in English. 14 (1975),94.

Diglycolic acid Consensus Reports

Reported in EPA TSCA Inventory.

Diglycolic acid Safety Profile

Hazard Codes: Xn
Risk Statements: 22-36/37/38-34
Safety Statements: 26-36-45-36/37/39
RIDADR: 2811
WGK Germany: 3
RTECS: AJ1530000
HazardClass: 8
PackingGroup: III
Moderately toxic by ingestion. When heated to decomposition it emits acrid smoke and irritating vapors.

Diglycolic acid Specification

Handling of OXODIACETIC ACID: Avoid contact with eyes, skin, and clothing. Avoid ingestion and inhalation. Keep container tightly closed. Wash thoroughly after handling. Remove contaminated clothing and wash before reuse. Use with adequate ventilation.
Storage of OXODIACETIC ACID: Store in a cool, dry, well-ventilated area away from incompatible substances. Store in a tightly closed container. Keep container closed when not in use.

Product Name

Diglycolic acid

Synthetic route

Diglycolic acid Chemical Properties

Diglycolic acid Toxicity Data With Reference

Diglycolic acid Consensus Reports

Diglycolic acid Safety Profile

Diglycolic acid Specification

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