Dayangchem鈥檚 R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities of
Cas:108-69-0
Min.Order:1 Kilogram
FOB Price: $3.0
Type:Lab/Research institutions
inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
Cas:108-69-0
Min.Order:1 Metric Ton
Negotiable
Type:Manufacturers
inquiryhigh quality Appearance:Colorless liquid Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea Port:shanghai
The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Cas:108-69-0
Min.Order:5 Kiloliter
FOB Price: $1.2 / 5.0
Type:Manufacturers
inquiryHebei Yanxi Chemical Co., Ltd. is a professional research, development and production of lead acetate benzene acetamide enterprise backbone members by local well-known entrepreneurs and professional senior engineers in the party's "low car
Cas:108-69-0
Min.Order:1 Metric Ton
FOB Price: $1.0 / 2.0
Type:Trading Company
inquiryOur company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so
Cas:108-69-0
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryOur Services 1. New Molecules R&D 2. Own test center HPLC NMR GC LC-MS 3. API and Intermediates from China reputed manufacturers 4. Documents support COA MOA MSDS DMF open part Our advantages 1. Government awarded company. Top 100 enter
Cas:108-69-0
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryTriumph has the complete production of G- KG - MT service chain,we can make the new technology into productivity quickly in the research and development of new products. Main Business Custom Synthesis: Trading(Raw Mater
Cas:108-69-0
Min.Order:0 Metric Ton
FOB Price: $18.0 / 20.0
Type:Lab/Research institutions
inquirysuperior quality Appearance:Dark brown liquid. Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:1kg/bag, 1kg/drum or 25kg/drum or as per your request. Application:Used as Pharmaceutical Intermediates Transportation
Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:108-69-0
Min.Order:0 Metric Ton
Negotiable
Type:Lab/Research institutions
inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
We are leading fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.Our main business covers the fields below: 1.Noble Metal Catalysts (Pt.Pd...)
Cas:108-69-0
Min.Order:1 Kilogram
FOB Price: $5.0
Type:Lab/Research institutions
inquiryProductName:3,5-Dimethylaniline CAS:108-69-0 Molecular Formula:C8H11N Molecular Weight:121.18000 Appearance:Colorless to reddish brown liquid Assay:≥99.0% Water content:≤0.20% Appearance:brown liquid Storage:keep sealed an
Cas:108-69-0
Min.Order:10 Gram
Negotiable
Type:Lab/Research institutions
inquiryAppearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea
SAGECHEM is a chemical R&D, manufacturing and distribution company in China since 2009, including pharmaceutical intermediates, agrochemical, dyestuff intermediates, organosilicone, API and etc. We also offer a full range of services in custom synthe
Cas:108-69-0
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryCapability on chemical synthesis1. Beijing High-Tech Enterprises2. Strong R&D Team3. 8 years of experiences in R & D of high-tech Catalyst;4. 5000 production techniques, 69 items of national patents, and 360 kinds of products on sales;5. The producti
3,5-DimethylanilineAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air
ISO/factory/goodqualityAppearance:off white Storage:Dry,cool place Package:drum Application:active pharmaceutical ingredients Transportation:by air/sea/express Port:shenzhen/shanghai
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
R & D enterprises have their own stock in stockAppearance:To be subject to the object Package:Customized Application:pharmaceutical intermediates Transportation:Air Port:Shanghai;Guangzhou
high purity,in stock Package:25kg/drum,or as per customers'demand Application:API,Pharmaceutical intermediates Transportation:air,sea,courier
1.High quality : the purity is 99% min . through multiple producing procedures. 2.Competitive price : low price because of our skilled production technolpgy ,save the production cost at most , and give big profit room to our customers330.Safe and fa
Our clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS
Product Description Description & Specification Category Pharmaceutical Raw Materials, Fine Chemicals, Bulk drug Standard Medical standard
Cas:108-69-0
Min.Order:1 Kilogram
FOB Price: $112.0
Type:Trading Company
inquiryAnsciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
★.Best quality according to requirement ★.Competitive price in China market ★.Mature Technical support ★.Professional logistic support
3,5-Dimethylaniline, 98% Application:3,5-Dimethylaniline, 98%
3,5-Dimethylaniline, 98%Appearance:White powder Storage:Room temperature Package:25KG/drum Application:Organic chemicals Transportation:By express (Door to door) such as FEDEX, DHL, EMS for small amount. By air(airport to airport) or by sea LCL/FCL f
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:any port in China
Conditions | Yield |
---|---|
With copper(I) oxide; ammonium hydroxide In 1-methyl-pyrrolidin-2-one at 80℃; for 15h; | 100% |
With copper(l) iodide; 2-carboxyquinoline N-oxide; potassium carbonate; ammonium hydroxide In dimethyl sulfoxide at 80℃; for 23h; Inert atmosphere; | 91% |
With copper(l) iodide; ammonia; sodium phosphate In water at 100℃; for 24h; | 86% |
With diethylenetriaminopentaacetic acid; ammonia; copper(II) oxide; potassium hydroxide In water at 100℃; for 6h; | 74% |
Stage #1: 5-bromo-1,3-xylene With magnesium In tetrahydrofuran Inert atmosphere; Stage #2: With C10H17NO In tetrahydrofuran; toluene at -78℃; for 2h; Inert atmosphere; Stage #3: With ammonium chloride In tetrahydrofuran; water; toluene Inert atmosphere; | 74% |
Conditions | Yield |
---|---|
With borane-ammonia complex In methanol; water at 49.84℃; for 0.166667h; Catalytic behavior; | 99% |
With sodium tetrahydroborate In water at 60℃; for 0.0166667h; | 96% |
Stage #1: 5-nitro-m-xylene With Cu(OH)x impregnated on Fe3O4 In water for 0.0833333h; Green chemistry; Stage #2: With sodium tetrahydroborate In water at 55 - 60℃; for 0.116667h; Green chemistry; | 95% |
3,5-dimethylphenyl iodide
3,5-dimethylaminoaniline
Conditions | Yield |
---|---|
With copper(I) oxide; ammonium hydroxide In 1-methyl-pyrrolidin-2-one at 80℃; for 15h; | 99% |
With potassium phosphate; copper(l) iodide; N-((1-oxy-pyridin-2-yl)methyl)oxalamic acid; ammonia In water; dimethyl sulfoxide at 25℃; Schlenk technique; Inert atmosphere; Sealed tube; chemoselective reaction; | 95% |
With copper(l) iodide; 2-carboxyquinoline N-oxide; potassium carbonate; ammonium hydroxide In dimethyl sulfoxide at 50℃; for 23h; Inert atmosphere; | 92% |
Conditions | Yield |
---|---|
With ammonium hydroxide; potassium phosphate In dimethyl sulfoxide at 80℃; UV-irradiation; | 99% |
Multi-step reaction with 2 steps 1.1: sulfuric acid; nitric acid / 30 °C / Cooling with ice 2.1: palladium on activated charcoal / ethanol / 0.5 h / 50 °C / Autoclave 2.2: 0.83 h / 65 °C / 2250.23 Torr / Autoclave View Scheme |
N-hydroxy-3,5-dimethylbenzamide
3,5-dimethylaminoaniline
Conditions | Yield |
---|---|
With potassium carbonate In dimethyl sulfoxide at 90℃; for 4h; Lossen Rearrangement; | 97% |
Conditions | Yield |
---|---|
With palladium/alumina; ammonia; hydrogen In toluene at 250℃; under 2250.23 Torr; Temperature; Pressure; Solvent; | 95% |
With 5%-palladium/activated carbon; hydrazine hydrate; lithium hydroxide In 1,4-dioxane at 170℃; for 16h; Molecular sieve; Inert atmosphere; | 71% |
With ammonia at 350℃; under 117681 - 183877 Torr; | |
With aluminum oxide; nitrogen; ammonia; hydrogen at 450℃; under 147102 Torr; |
3,5-dimethyl-cyclohexanone oxime
3,5-dimethylaminoaniline
Conditions | Yield |
---|---|
With Pd(OH)x/LDH In N,N-dimethyl acetamide at 130℃; for 11h; Schlenk technique; Inert atmosphere; | 91% |
3,5-dimethylaminoaniline
Conditions | Yield |
---|---|
With 2,2'-azobis(isobutyronitrile); tris-(trimethylsilyl)silane In toluene at 100℃; Sealed tube; | 88% |
1,2,3,4-tetrahydroisoquinoline
5-nitro-m-xylene
A
quinoline
B
3,5-dimethylaminoaniline
Conditions | Yield |
---|---|
With nickel-nitrogen-doped carbon framework In water at 145℃; for 18h; Inert atmosphere; Sealed tube; Green chemistry; | A 73% B 76% |
5-nitro-m-xylene
2-methyl indoline
A
2-methyl-1H-indole
B
3,5-dimethylaminoaniline
Conditions | Yield |
---|---|
With nickel-nitrogen-doped carbon framework In water at 145℃; for 18h; Inert atmosphere; Sealed tube; Green chemistry; | A 74% B 76% |
Conditions | Yield |
---|---|
With ethene; 5%-palladium/activated carbon; ammonium acetate In acetonitrile at 90℃; under 760.051 Torr; for 15h; Schlenk technique; | 71% |
ethanol
5-nitro-m-xylene
A
2,5,7-trimethylquinoline
B
3,5-dimethylaminoaniline
Conditions | Yield |
---|---|
With platinum-loaded TiO2 at 30℃; for 5h; UV-irradiation; | A 68% B 16% |
Conditions | Yield |
---|---|
Stage #1: 2,4-Xylenol With Nonafluorobutanesulfonyl fluoride; tris(trimethylsilyl)amine; potassium hexamethylsilazane In tetrahydrofuran at 60℃; for 5h; Schlenk technique; Inert atmosphere; Stage #2: With hydrogenchloride In water at 20℃; for 0.0833333h; pH=3 - 4; | 67% |
5-methoxyindoline
5-nitro-m-xylene
A
5-methoxylindole
B
3,5-dimethylaminoaniline
Conditions | Yield |
---|---|
With nickel-nitrogen-doped carbon framework In water at 145℃; for 18h; Inert atmosphere; Sealed tube; Green chemistry; | A 62% B 61% |
m-xylene
A
3,5-dimethylaminoaniline
B
2,4-Xylidine
C
2,6-dimethylaniline
Conditions | Yield |
---|---|
With tris-(2-chloro-ethyl)-amine; trifluorormethanesulfonic acid; trifluoroacetic acid In chloroform at 25℃; for 1h; | A 2% B 58% C 15% |
With hydrogenchloride; aluminium trichloride; sodium azide In various solvent(s) at 20℃; | |
With sodium azide; trifluorormethanesulfonic acid at 20℃; Ultrasonic irradiation; | |
Stage #1: m-xylene With sulfuric acid; hydroxylamine hydrochloride In acetonitrile at 25℃; for 0.166667h; Stage #2: With hydrogenchloride; titanium(III) chloride In water; acetonitrile at 25℃; Inert atmosphere; Sealed tube; Overall yield = 60 percent; Overall yield = 72 mg; |
Conditions | Yield |
---|---|
With hydrogenchloride; PPA; hydroxylamine |
Conditions | Yield |
---|---|
With alkaline sodium hypobromite |
2-amino-4,6-dimethylbenzene-1,3-dicarbonitrile
A
2-amino-4,6-dimethyl benzamide
B
3,5-dimethylaminoaniline
Conditions | Yield |
---|---|
With sulfuric acid |
3,5-dimethyl-cyclohex-2-enone oxime
3,5-dimethylaminoaniline
Conditions | Yield |
---|---|
With hydrogenchloride at 170℃; |
3,5-Dimethylphenol
A
bis-(3,5-dimethylphenyl)-amine
B
3,5-dimethylaminoaniline
Conditions | Yield |
---|---|
With ammonium chloride at 350℃; under 36775.4 Torr; |
3,5-dimethylaminoaniline
Conditions | Yield |
---|---|
With hydrogenchloride; tin(ll) chloride | |
With iron; acetic acid | |
With hydrogenchloride; tin |
Conditions | Yield |
---|---|
at 350℃; under 117681 Torr; |
3,5-Dimethylphenol
A
bis-(3,5-dimethylphenyl)-amine
B
3,5-dimethylaminoaniline
Conditions | Yield |
---|---|
at 350℃; under 36775.4 - 44130.5 Torr; |
1,2,3-triethylbenzene
bis-(3,5-dimethyl-cyclohex-2-enylidene)-hydrazine
3,5-dimethylaminoaniline
hydrogenchloride
4-(3,5-dimethyl-phenylazo)-3,5-dimethyl-aniline
A
3,5-dimethylaminoaniline
B
3,5-dimethylaminoaniline
Conditions | Yield |
---|---|
In chloroform-d1 not isolated; detected by NMR; |
3,5-dimethylaminoaniline
Conditions | Yield |
---|---|
With 3,6-dimethyl-1,2,4,5-tetrazine; formic acid In acetonitrile at 20℃; for 1h; Reagent/catalyst; Solvent; | |
With 3,6-dimethyl-1,2,4,5-tetrazine; formic acid In acetonitrile at 20℃; for 1h; Reagent/catalyst; Solvent; |
Conditions | Yield |
---|---|
With pyridine In acetonitrile at 20℃; for 1h; Reagent/catalyst; |
3,5-dimethylaminoaniline
p-toluenesulfonyl chloride
N-(3,5-dimethylphenyl)-4-methyl-benzenesulfonamide
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 4℃; | 100% |
With silica gel at 20℃; | 95% |
With triethylamine In dichloromethane at 0 - 20℃; | 82% |
3,5-dimethylaminoaniline
Trimethylacetic acid
N-(3,5-dimethylphenyl)pivalamide
Conditions | Yield |
---|---|
With diphosphorus tetraiodide In tetrachloromethane; dichloromethane Heating; | 100% |
3,5-dimethylaminoaniline
dimethyl acetylenedicarboxylate
dimethyl (Z)-N-(3,5-dimethylphenyl)aminofumarate
Conditions | Yield |
---|---|
at 20℃; for 0.133333h; Michael addition; | 100% |
In diethyl ether at 0℃; | 75% |
4-methoxy-benzaldehyde
3,5-dimethylaminoaniline
3,5-dimethyl-N-(4-methoxybenzylidene)aniline
Conditions | Yield |
---|---|
at 20℃; | 100% |
With acetic acid In methanol at 20℃; |
Ethyl oxalyl chloride
3,5-dimethylaminoaniline
2-(3,5-dimethylphenylamino)-2-oxoacetic acidethyl ester
Conditions | Yield |
---|---|
With pyridine at 20℃; for 1.5h; Inert atmosphere; | 100% |
With triethylamine In tetrahydrofuran at 0 - 20℃; | 68% |
3,5-dimethylaminoaniline
3-(3,5-dimethyl-phenylamino)-propionamide
Conditions | Yield |
---|---|
With ammonia In methanol at 80℃; | 100% |
2-(2-tert-butoxycarbonylaminopyridin-4-ylmethylthio)pyridine-3-carboxylic acid
3,5-dimethylaminoaniline
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine; HATU In N,N-dimethyl-formamide at 20℃; for 12h; | 100% |
{4-[6-formyl-1-(3-hydroxy-6-methylpyridin-2-ylmethyl)-1H-benzoimidazol-2-ylamino]piperidin-1-yl}acetic acid ethyl ester
3,5-dimethylaminoaniline
{4-[6-[(3,5-dimethylphenylamino)methyl]-1-(3-hydroxy-6-methylpyridin-2-ylmethyl)-1H-benzoimidazol-2-ylamino]piperidin-1-yl}acetic acid ethyl ester
Conditions | Yield |
---|---|
With sodium cyanoborohydride; acetic acid In acetonitrile at 20℃; for 12h; | 100% |
3,5-dimethylaminoaniline
1,2-dibromobenzene
N,N'-di(3,5-dimethylphenyl)benzene-1,2-diamine
Conditions | Yield |
---|---|
With ammonium chloride; sodium t-butanolate; palladium diacetate In water; argon; toluene | 100% |
With tri-tert-butyl phosphine; palladium diacetate; sodium t-butanolate In toluene at 110℃; for 14h; Inert atmosphere; | 100 %Chromat. |
β-(1-naphthyl)nitroethylene
3,5-dimethylaminoaniline
C20H20N2O2
Conditions | Yield |
---|---|
at 20℃; for 0.1h; Michael addition; neat (no solvent); | 100% |
1-nitro-2-(2-nitrovinyl)benzene
3,5-dimethylaminoaniline
C16H17N3O4
Conditions | Yield |
---|---|
at 20℃; for 0.1h; Michael addition; neat (no solvent); | 100% |
Conditions | Yield |
---|---|
at 20℃; for 0.1h; Michael addition; neat (no solvent); | 100% |
3-nitro-β-nitrostyrene
3,5-dimethylaminoaniline
3,5-dimethyl-N-[2-nitro-1-(3-nitro-phenyl)-ethyl]-aniline
Conditions | Yield |
---|---|
at 20℃; for 0.1h; Michael addition; neat (no solvent); | 100% |
1-chloro-4-(2-nitrovinyl)benzene
3,5-dimethylaminoaniline
C16H17ClN2O2
Conditions | Yield |
---|---|
at 20℃; for 0.1h; Michael addition; neat (no solvent); | 100% |
3,5-dimethylaminoaniline
acetylenedicarboxylic acid diethyl ester
diethyl (Z)-N-(3,5-dimethylphenyl)aminofumarate
Conditions | Yield |
---|---|
at 20℃; for 0.15h; Michael addition; | 100% |
benzaldehyde
3,5-dimethylaminoaniline
3,5-dimethyl-N-benzylideneaniline
Conditions | Yield |
---|---|
at 20℃; | 100% |
In methanol | 99% |
In ethanol for 3h; Reflux; |
4-methyl-benzaldehyde
3,5-dimethylaminoaniline
3,5-dimethyl-N-(4-methylbenzylidene)aniline
Conditions | Yield |
---|---|
at 20℃; | 100% |
4-chlorobenzaldehyde
3,5-dimethylaminoaniline
3,5-dimethyl-N-(4-chlorobenzylidene)aniline
Conditions | Yield |
---|---|
at 20℃; | 100% |
In neat (no solvent) at 20℃; for 0.5h; Schlenk technique; Molecular sieve; Inert atmosphere; |
3,5-dimethylaminoaniline
4-bromo-benzaldehyde
3,5-dimethyl-N-(4-bromobenzylidene)aniline
Conditions | Yield |
---|---|
at 20℃; | 100% |
Conditions | Yield |
---|---|
at 20℃; | 100% |
2-bromo-butyryl bromide
3,5-dimethylaminoaniline
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0 - 20℃; | 100% |
Conditions | Yield |
---|---|
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 14h; | 100% |
Conditions | Yield |
---|---|
In tetrahydrofuran at 0 - 20℃; Inert atmosphere; | 99% |
Stage #1: acetic anhydride; 3,5-dimethylaminoaniline In tetrahydrofuran at 0 - 20℃; Inert atmosphere; Stage #2: With sodium hydroxide In tetrahydrofuran; water pH=12 - 14; Cooling with ice; | 99% |
Stage #1: acetic anhydride; 3,5-dimethylaminoaniline In tetrahydrofuran at 20℃; for 1h; Inert atmosphere; Stage #2: With sodium hydroxide In tetrahydrofuran; water pH=12 - 14; Cooling with ice; | 99% |
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 201℃; for 1h; | 99% |
Stage #1: 3,5-dimethylaminoaniline With potassium carbonate In dichloromethane at 0℃; for 0.5h; Inert atmosphere; Stage #2: acetyl chloride for 2h; Inert atmosphere; | 99% |
With potassium carbonate In dichloromethane at 20℃; for 2.5h; Cooling with ice; | 98.8% |
4-hydroxyphenylacetate
3,5-dimethylaminoaniline
N-(3,5-dimethylphenyl)-4-hydroxyphenylacetamide
Conditions | Yield |
---|---|
With fluorosulfonyl fluoride; N-ethyl-N,N-diisopropylamine In acetonitrile at 20℃; for 5h; | 99% |
With boric acid In toluene for 18h; Heating; | 95% |
With pyridine; FI-750-M; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In water at 60℃; for 0.75h; Sealed tube; | 86% |
2-dimethylaminomethylene-1,3-bis(dimethylimonio)propane diperchlorate
3,5-dimethylaminoaniline
Conditions | Yield |
---|---|
With perchloric acid In ethanol at 105℃; for 1.5h; | 99% |
1-(tert-butoxycarbonyl)-L-proline
3,5-dimethylaminoaniline
(S)-tert-butyl 2-((3,5-dimethylphenyl)carbamoyl)pyrrolidine-1-carboxylate
Conditions | Yield |
---|---|
With chloroformic acid ethyl ester; triethylamine In dichloromethane at 20℃; for 1h; | 99% |
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine In dichloromethane at 0 - 20℃; for 12h; | 85% |
With benzotriazol-1-ol; dicyclohexyl-carbodiimide In dichloromethane for 12h; Ambient temperature; | 65% |
para-chlorotoluene
3,5-dimethylaminoaniline
3,5-dimethyl-N-p-tolylbenzenamine
Conditions | Yield |
---|---|
With bis(η3-allyl-μ-chloropalladium(II)); potassium tert-butylate; 1,3-bis[(2,6-diisopropyl)phenyl]imidazolinium chloride In 1,4-dioxane at 100℃; for 1.5h; Inert atmosphere; | 99% |
With bis[chloro(1,2,3-trihapto-allylbenzene)palladium(II)]; N-[2-(di(1-adamantyl)phosphino)phenyl]morpholine; potassium hydroxide; sodium t-butanolate In water at 110℃; for 22h; Buchwald-Hartwig amination; Inert atmosphere; chemoselective reaction; | 95% |
With sodium t-butanolate; [Na2PdCl4]; dicyclohexyl-(9-ethyl-9H-fluoren-9-yl)phosphane*HBF4 In toluene at 120℃; for 12h; Buchwald-Hartwig coupling reaction; | |
With sodium t-butanolate; palladium diacetate; dicyclohexyl(9-ethyl-9H-fluorene-9-yl)-phosphine·HBF4 In toluene at 120℃; for 12h; Product distribution / selectivity; Buchwald-Hartwig Amination; |
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