1. We integrate research and development, production, and sales. A 1800 square meter research and development center,The company has conducted over 50 research and development and technical service projects annually, applied for more than 10 patents,
Cas:61-76-7
Min.Order:1 Kilogram
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Type:Trading Company
inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
Cas:61-76-7
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inquiryCAS No.: 61-76-7 Other Names: Phenylephrine HCL MF: C9H13NO2.HCl EINECS No.: 200-517-3, 200-517-3 Place of Origin: Shaanxi, China (Mainland) Type: nutrition
Cas:61-76-7
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inquiry1. Guaranteed purity; 2. Large quantity in stock; 3. Largest manufacturer; 4. Best service after shipment with email; 5. High quality & competitive price; ...... Appearance:White or almost white crystalline powder Storage:Store at RT.
Cas:61-76-7
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Type:Trading Company
inquiryGood quality Competitive price On time delivery Our Advantages: Full experience of large numbers containers loading in main Chinese seaports Packing with pallet as buyer's special request Best service after shipment with e-mail
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Min.Order:1 Kilogram
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
Cas:61-76-7
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inquiry(R)-Phenylephrine Hydrochlorid Mol Download Chemical properties CAS: 61-76-7 MF: C9H13NO2.ClH MW: 203.67 EINECS: 200-517-3 MDL No.: MFCD00012605 Properties Melting point: 143-145 °C(lit.) alpha -47 º (c=2, H2O) refractive
Cas:61-76-7
Min.Order:1 Kilogram
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Type:Trading Company
inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Cas:61-76-7
Min.Order:5 Kiloliter
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Type:Manufacturers
inquiryWhy is SINOWAY: 1) Specialized in pharmaceutical and healthcare industrial for 34 years. 2) ISO 9001:2015 & SGS audited supplier . 3) Accept various payment terms : T.T 30-60 days. 4) We have warehouse in USA with quickly shipment . 5) We c
Cas:61-76-7
Min.Order:1 Kilogram
FOB Price: $500.0
Type:Trading Company
inquiryName:(R)-Phenylephrine Hydrochlorid CAS NO: 61-76-7 Grade:Medical scientific research and export Molecular formula: C9H15Cl2NO2 Molecular weight:240.1269 Product Quality 12 years of chemical raw materials Mature operation of the industry
Cas:61-76-7
Min.Order:25 Kilogram
FOB Price: $2.0 / 3.0
Type:Other
inquiryOur company was built in 2009 with an ISO certificate.In the past 6 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O
Cas:61-76-7
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Type:Lab/Research institutions
inquiryWith our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin
Cas:61-76-7
Min.Order:1 Kilogram
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Type:Trading Company
inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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Type:Trading Company
inquiryOur Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
Cas:61-76-7
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Type:Trading Company
inquiryAdvantage : LIDE PHARMACEUTICALS LTD. is a mid-small manufacturing-type enterprise, engaged in pharmaceutical intermediates of R&D, custom-made and production, and also involving trading chemicals for export. We have established the R&
Cas:61-76-7
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Type:Lab/Research institutions
inquiryPhenylephrine Hydrochloride CAS 61-76-7 Phenylephrine Hydrochloride CAS 61-76-7 CAS 61-76-7 Brand: Sinotech MF C9H13NO2 · HCl MSDS: Aviable
Appearance:White to almost white crystalline powder Storage:R.T Package:25kg/drum Application:API Transportation:Express/Sea/Air Port:Any port in China
Cas:61-76-7
Min.Order:1 Kilogram
FOB Price: $510.0 / 580.0
Type:Lab/Research institutions
inquiryAdvantages: Hubei XinRunde Chemical Co., Ltd is a renowned pharmaceutical manufacturer. We can offer high quality products at competitive price in quick delivery with 100% custom pass guaranteed. Never stop striving to offer our best service is
Cas:61-76-7
Min.Order:10 Gram
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Type:Other
inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
Cas:61-76-7
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryWuhan hanweishi Pharmchem Co., Ltd(Hanways chempharm) is a specialized company concentrating on the R&D, production, marketing and technical service of APIs and pharmaceutical intermediates. The leading products range are APIs, Hormones, Peptides
Cas:61-76-7
Min.Order:100 Kilogram
FOB Price: $1.0 / 5.0
Type:Trading Company
inquiryPacking: According to customer requirements Delivery time: In stock or depands Port of shipment: Ningbo/Shanghai/Qingdao OEM/ODM:Welcome Sample:We can offer our existing samples at once Appearance:white crystalline powder Storage:Store in dry,
Cas:61-76-7
Min.Order:10 Gram
Negotiable
Type:Trading Company
inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At present
Cas:61-76-7
Min.Order:1 Kilogram
FOB Price: $246.0 / 298.0
Type:Trading Company
inquiry(R)-Phenylephrine Hydrochlorid CAS:61-76-7 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organ
Cas:61-76-7
Min.Order:1 Gram
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Type:Lab/Research institutions
inquiryWe generally use secure shipping methods that do not require you to do any customs clearance. Free shipping to your address without worrying about any customs issues. We have a professional customs clearance team to 100% guarantee the safe delivery o
Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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inquiryWe can provide GMP validation service that complies with SFDA, FDA, WHO and EU EMPA.Excellent registration team could help us easlily to register our products in different countries.If you and your customer are interested in some products or need C
Cas:61-76-7
Min.Order:1 Gram
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Type:Trading Company
inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Cas:61-76-7
Min.Order:0
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Type:Lab/Research institutions
inquiryAppearance:white crystalline powder Storage:Store in a cool,dry place and keep away from direct strong light Package:As customer request Application:Used for research and industrial manufacture. Transportation:Common products:Se
Cas:61-76-7
Min.Order:100 Metric Ton
Negotiable
Type:Lab/Research institutions
inquiryOur Services 1. New Molecules R&D 2. Own test center HPLC NMR GC LC-MS 3. API and Intermediates from China reputed manufacturers 4. Documents support COA MOA MSDS DMF open part Our advantages 1. Government awarded company. Top 100 enter
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Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquirymethylamine
3-((R)-1-Hydroxy-2-iodo-ethyl)-phenol
phenylephrine hydrochloride
Conditions | Yield |
---|---|
Stage #1: methylamine; 3-((R)-1-Hydroxy-2-iodo-ethyl)-phenol In tetrahydrofuran; water at 20℃; for 3h; Stage #2: With hydrogenchloride at 20℃; | 90% |
phenylephrine hydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride In methanol for 1h; Reflux; | 90% |
3-Hydroxyphenyl-ω-methylaminoacetophenone hydrochloride
phenylephrine hydrochloride
Conditions | Yield |
---|---|
With hydrogen; [Rh(cod)(R-Binapine)]BF4 In methanol at 65℃; under 21752.2 - 24752.5 Torr; for 18.25h; Product distribution / selectivity; | 85% |
Conditions | Yield |
---|---|
With hydrogenchloride In isopropyl alcohol at 55 - 65℃; for 0.5h; Product distribution / selectivity; | 84.5% |
With hydrogenchloride In water; isopropyl alcohol pH=7 - 8; enantioselective reaction; | 3.35 g |
Conditions | Yield |
---|---|
Stage #1: (1R)-2-bromo-1-(3-hydroxylphenyl)ethanol; methylamine In methanol for 6h; Inert atmosphere; Stage #2: With hydrogenchloride In methanol for 0.5h; Inert atmosphere; | 74.8% |
(R)-2-(Benzyl-methyl-amino)-1-(3-benzyloxy-phenyl)-ethanol; hydrochloride
phenylephrine hydrochloride
Conditions | Yield |
---|---|
With hydrogen; palladium on activated charcoal at 3℃; under 7600 Torr; for 3h; Yield given; | |
With hydrogen; palladium on activated charcoal In ethanol at 50℃; under 7600 Torr; for 3h; Yield given; |
3-(tert-butyl-dimethyl-sylanyloxy)benzaldehyde
phenylephrine hydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 6 steps 1.1: 90 percent / tetrahydrofuran / 6 h / 20 °C 2.1: 97 percent / (DHQD)2PHAL; K3Fe(CH)6; K2CO3 / OsO4 / 2-methyl-propan-2-ol; H2O / 24 h / 0 °C 3.1: 98 percent / dibutyltin oxide; NEt3 / CH2Cl2 / 0.75 h / 20 °C 4.1: 90 percent / AcOH / H2O; tetrahydrofuran / 10 h / 60 °C 5.1: 98 percent / NaI / acetone / 6 h / Heating 6.1: H2O; tetrahydrofuran / 3 h / 20 °C 6.2: 90 percent / methanolic HCl / 20 °C View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 7 steps 1.1: 90 percent / imidazole / CH2Cl2 / 5 h / 0 - 20 °C 2.1: 90 percent / tetrahydrofuran / 6 h / 20 °C 3.1: 97 percent / (DHQD)2PHAL; K3Fe(CH)6; K2CO3 / OsO4 / 2-methyl-propan-2-ol; H2O / 24 h / 0 °C 4.1: 98 percent / dibutyltin oxide; NEt3 / CH2Cl2 / 0.75 h / 20 °C 5.1: 90 percent / AcOH / H2O; tetrahydrofuran / 10 h / 60 °C 6.1: 98 percent / NaI / acetone / 6 h / Heating 7.1: H2O; tetrahydrofuran / 3 h / 20 °C 7.2: 90 percent / methanolic HCl / 20 °C View Scheme | |
Multi-step reaction with 5 steps 1.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 3 h / 0 °C 2.1: sodium hydride / dimethyl sulfoxide; mineral oil / 0.25 h / 0 °C 2.2: 0.5 h / 20 °C 3.1: (R,R)-Jacobsen catalyst / water / 61 h / 0 - 20 °C / Resolution of racemate 4.1: methanol / 2 h / 20 °C 5.1: hydrogenchloride / methanol / 1 h / Reflux View Scheme |
tert-butyldimethyl-(3-vinylphenoxy)silane
phenylephrine hydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1.1: 97 percent / (DHQD)2PHAL; K3Fe(CH)6; K2CO3 / OsO4 / 2-methyl-propan-2-ol; H2O / 24 h / 0 °C 2.1: 98 percent / dibutyltin oxide; NEt3 / CH2Cl2 / 0.75 h / 20 °C 3.1: 90 percent / AcOH / H2O; tetrahydrofuran / 10 h / 60 °C 4.1: 98 percent / NaI / acetone / 6 h / Heating 5.1: H2O; tetrahydrofuran / 3 h / 20 °C 5.2: 90 percent / methanolic HCl / 20 °C View Scheme |
1-[3-(tert-butyl-dimethyl-silanyloxy)-phenyl]-ethane-1,2-diol
phenylephrine hydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: 98 percent / dibutyltin oxide; NEt3 / CH2Cl2 / 0.75 h / 20 °C 2.1: 90 percent / AcOH / H2O; tetrahydrofuran / 10 h / 60 °C 3.1: 98 percent / NaI / acetone / 6 h / Heating 4.1: H2O; tetrahydrofuran / 3 h / 20 °C 4.2: 90 percent / methanolic HCl / 20 °C View Scheme |
Toluene-4-sulfonic acid (R)-2-hydroxy-2-(3-hydroxy-phenyl)-ethyl ester
phenylephrine hydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: 98 percent / NaI / acetone / 6 h / Heating 2.1: H2O; tetrahydrofuran / 3 h / 20 °C 2.2: 90 percent / methanolic HCl / 20 °C View Scheme |
toluene-4-sulfonic acid 2-[3-(tert-butyl-dimethyl-silanyloxy)-phenyl]-2-hydroxy-ethyl ester
phenylephrine hydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: 90 percent / AcOH / H2O; tetrahydrofuran / 10 h / 60 °C 2.1: 98 percent / NaI / acetone / 6 h / Heating 3.1: H2O; tetrahydrofuran / 3 h / 20 °C 3.2: 90 percent / methanolic HCl / 20 °C View Scheme |
3'-benzyloxy-2-(N-benzyl-N-methyl)aminoacetophenone hydrochloride
phenylephrine hydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: H2, 2, (2R,4R)-N-(methylcarbamoyl)-4-(dicyclohexylphosphino)-2-<(diphenylphosphino)methyl>pyrrolidine, triethylamine / methanol / 20 h / 50 °C / 15200 Torr 2: H2 / 10percent Pd/C / ethanol / 3 h / 50 °C / 7600 Torr View Scheme | |
Multi-step reaction with 2 steps 1: 100 percent / H2, triethylamine / <(Rh(COD)Cl>2, (2R,4R)-MCCPM / CH2Cl2 / 20 h / 50 °C / 15200 Torr 2: H2 / 10percent Pd/C / 3 h / 3 °C / 7600 Torr View Scheme |
2-(benzyl(methyl)amino)-1-(3'-hydroxyphenyl)ethanol
2-(benzyl(methyl)amino)-1-(3'-hydroxyphenyl)ethanone hydrochloride
phenylephrine hydrochloride
Conditions | Yield |
---|---|
With hydrogen; triethylamine In methanol |
3-Hydroxyphenyl-ω-methylaminoacetophenone hydrochloride
A
phenylephrine hydrochloride
B
(+)-Phenylephrine hydrochloride
Conditions | Yield |
---|---|
With hydrogen; [(S)-Xyl-P-Phos RuCl(p-cymene)]Cl In methanol at 80 - 85℃; under 18751.9 - 23252.3 Torr; for 21h; Product distribution / selectivity; | A n/a B n/a |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: sodium hydroxide / methanol / 0.5 h / 20 °C 1.2: 1.5 h / 25 - 60 °C / Resolution of racemate 2.1: hydrogenchloride / toluene; water / 0.5 h / 75 - 80 °C / pH < 2 2.2: 1 - 15 °C / pH ~ 9 3.1: hydrogenchloride / isopropyl alcohol / 0.5 h / 55 - 65 °C View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: methanol / 2 h / 20 - 65 °C / Resolution of racemate 2.1: hydrogenchloride / toluene; water / 0.5 h / 75 - 80 °C / pH < 2 2.2: 1 - 15 °C / pH ~ 9 3.1: hydrogenchloride / isopropyl alcohol / 0.5 h / 55 - 65 °C View Scheme |
(R)-phenylephrine-(R)-naproxen
phenylephrine hydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: hydrogenchloride / toluene; water / 0.5 h / 75 - 80 °C / pH < 2 1.2: 1 - 15 °C / pH ~ 9 2.1: hydrogenchloride / isopropyl alcohol / 0.5 h / 55 - 65 °C View Scheme |
(3-methoxyethoxymethyloxy)benzaldehyde
phenylephrine hydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: sodium hydride / dimethyl sulfoxide; mineral oil / 0.25 h / 0 °C 1.2: 0.5 h / 20 °C 2.1: (R,R)-Jacobsen catalyst / water / 61 h / 0 - 20 °C / Resolution of racemate 3.1: methanol / 2 h / 20 °C 4.1: hydrogenchloride / methanol / 1 h / Reflux View Scheme |
phenylephrine hydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: (R,R)-Jacobsen catalyst / water / 61 h / 0 - 20 °C / Resolution of racemate 2: methanol / 2 h / 20 °C 3: hydrogenchloride / methanol / 1 h / Reflux View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: bromine; aluminum (III) chloride / diethyl ether / -10 °C 2.1: borane-THF; (3aR)-1-methyl-3,3-diphenyl-tetrahydro-pyrrolo[1,2-c][1,3,2]oxazaborole / toluene; tetrahydrofuran / 20 °C / Inert atmosphere 2.2: 0 °C / Inert atmosphere 3.1: methanol / 6 h / Inert atmosphere 3.2: 0.5 h / Inert atmosphere View Scheme | |
Multi-step reaction with 3 steps 1.1: bromine; aluminum (III) chloride / diethyl ether / -10 °C 2.1: borane-THF; (3aR)-1-methyl-3,3-diphenyl-tetrahydro-pyrrolo[1,2-c][1,3,2]oxazaborole / toluene; tetrahydrofuran / 20 °C / Inert atmosphere 2.2: 0 °C / Inert atmosphere 3.1: methanol / 6 h / Inert atmosphere 3.2: 0.5 h / Inert atmosphere View Scheme | |
Multi-step reaction with 4 steps 1.1: bromine; aluminum (III) chloride / diethyl ether / -10 °C 2.1: sodium hydrogencarbonate / methanol 3.1: borane-THF; (3aR)-1-methyl-3,3-diphenyl-tetrahydro-pyrrolo[1,2-c][1,3,2]oxazaborole / toluene; tetrahydrofuran / 20 °C / Inert atmosphere 3.2: 0 °C / Inert atmosphere 4.1: methanol / 6 h / Inert atmosphere 4.2: 0.5 h / Inert atmosphere View Scheme |
2-bromo-3-acetyloxylacetophenone
phenylephrine hydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: borane-THF; (3aR)-1-methyl-3,3-diphenyl-tetrahydro-pyrrolo[1,2-c][1,3,2]oxazaborole / toluene; tetrahydrofuran / 20 °C / Inert atmosphere 1.2: 0 °C / Inert atmosphere 2.1: methanol / 6 h / Inert atmosphere 2.2: 0.5 h / Inert atmosphere View Scheme | |
Multi-step reaction with 2 steps 1.1: borane-THF; (3aR)-1-methyl-3,3-diphenyl-tetrahydro-pyrrolo[1,2-c][1,3,2]oxazaborole / toluene; tetrahydrofuran / 20 °C / Inert atmosphere 1.2: 0 °C / Inert atmosphere 2.1: methanol / 6 h / Inert atmosphere 2.2: 0.5 h / Inert atmosphere View Scheme | |
Multi-step reaction with 3 steps 1.1: sodium hydrogencarbonate / methanol 2.1: borane-THF; (3aR)-1-methyl-3,3-diphenyl-tetrahydro-pyrrolo[1,2-c][1,3,2]oxazaborole / toluene; tetrahydrofuran / 20 °C / Inert atmosphere 2.2: 0 °C / Inert atmosphere 3.1: methanol / 6 h / Inert atmosphere 3.2: 0.5 h / Inert atmosphere View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: sodium hydroxide / water / 1.5 h / 0 °C / pH 7 - 8 2.1: bromine; aluminum (III) chloride / diethyl ether / -10 °C 3.1: borane-THF; (3aR)-1-methyl-3,3-diphenyl-tetrahydro-pyrrolo[1,2-c][1,3,2]oxazaborole / toluene; tetrahydrofuran / 20 °C / Inert atmosphere 3.2: 0 °C / Inert atmosphere 4.1: methanol / 6 h / Inert atmosphere 4.2: 0.5 h / Inert atmosphere View Scheme | |
Multi-step reaction with 4 steps 1.1: sodium hydroxide / water / 1.5 h / 0 °C / pH 7 - 8 2.1: bromine; aluminum (III) chloride / diethyl ether / -10 °C 3.1: borane-THF; (3aR)-1-methyl-3,3-diphenyl-tetrahydro-pyrrolo[1,2-c][1,3,2]oxazaborole / toluene; tetrahydrofuran / 20 °C / Inert atmosphere 3.2: 0 °C / Inert atmosphere 4.1: methanol / 6 h / Inert atmosphere 4.2: 0.5 h / Inert atmosphere View Scheme | |
Multi-step reaction with 5 steps 1.1: sodium hydroxide / water / 1.5 h / 0 °C / pH 7 - 8 2.1: bromine; aluminum (III) chloride / diethyl ether / -10 °C 3.1: sodium hydrogencarbonate / methanol 4.1: borane-THF; (3aR)-1-methyl-3,3-diphenyl-tetrahydro-pyrrolo[1,2-c][1,3,2]oxazaborole / toluene; tetrahydrofuran / 20 °C / Inert atmosphere 4.2: 0 °C / Inert atmosphere 5.1: methanol / 6 h / Inert atmosphere 5.2: 0.5 h / Inert atmosphere View Scheme | |
Multi-step reaction with 3 steps 1.1: sulfuryl dichloride / dichloromethane / 2 h / 5 - 25 °C 2.1: (1R,2S)-1-Amino-2-indanol; borane-THF / tetrahydrofuran / 0.5 h / 20 - 25 °C 3.1: water; methanol / 30 - 40 °C 3.2: 0.5 h / 0 - 50 °C View Scheme |
methylamine
(R)-2-chloro-1-(3-hydroxyphenyl)ethanol
phenylephrine hydrochloride
Conditions | Yield |
---|---|
Stage #1: methylamine; (R)-2-chloro-1-(3-hydroxyphenyl)ethanol In methanol; water at 30 - 40℃; Stage #2: With hydrogenchloride In methanol; water at 0 - 50℃; for 0.5h; |
phenylephrine hydrochloride
sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate
Conditions | Yield |
---|---|
In chloroform at 20℃; for 1h; | 97% |
Conditions | Yield |
---|---|
for 9h; Irradiation; | 96.1% |
phenylephrine hydrochloride
N,N-diethylcarbamyl chloride
(1R)-1-(3-hydroxyphenyl)-2-ethanol
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran for 1h; | 76% |
phenylephrine hydrochloride
propargyl bromide
(R)-3-hydroxy-α-<(methyl-2-propanoylamino)methyl>benzenemethanol
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran; toluene for 16h; | 64% |
phenylephrine hydrochloride
Diethyl carbonate
(R)-5-(3-hydroxyphenyl)-3-methyl-2-oxazolidone
Conditions | Yield |
---|---|
With potassium carbonate for 4h; Heating; | 51% |
phenylephrine hydrochloride
Diethyl carbonate
5-(3-hydroxyphenyl)-3-methyl-2-oxazolidone
Conditions | Yield |
---|---|
With potassium carbonate In acetone | 51% |
phenylephrine hydrochloride
N,N-Dimethylthiocarbamoyl chloride
(R)-1-(3-hydroxyphenyl)-2-ethanol
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran for 2h; | 47% |
phenylephrine hydrochloride
N,N-Dimethylthiocarbamoyl chloride
1-(3-Hydroxyphenyl)-2-(N-methyl-N-dimethylthiocarbamoyl)amino ethanol
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran; hexane; dichloromethane | 47% |
sodium cyanide
phenylephrine hydrochloride
Conditions | Yield |
---|---|
With [4,4’-bis(1,1-dimethylethyl)-2,2’-bipyridine-N1,N1‘]bis [3,5-difluoro-2-[5-(trifluoromethyl)-2-pyridinyl-N]phenyl-C]iridium(III) hexafluorophosphate; acetic acid In acetonitrile at 20℃; for 24h; Irradiation; Sealed tube; | 26% |
phenylephrine hydrochloride
7α-hydroxyendesm-4-en-6,12-olide
(3aR,5aR,9bS)-3a-hydroxy-3-((((2R)-2-hydroxy-2-(3-hydroxyphenyl)ethyl)(methyl)amino)methyl)-5a,9-dimethyl-3,3a,4,5,5a,6,7,8-octahydronaphtho[1,2-b]furan-2(9bH)-one
Conditions | Yield |
---|---|
With triethylamine In ethanol at 25℃; for 15h; | 21.3% |
4-(chlorocarbonyl)pyridine
phenylephrine hydrochloride
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran for 1h; |
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran for 1h; |
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran for 1h; |
phenylephrine hydrochloride
(S)-methyl 1-(chlorocarbonyl)pyrrolidine-2-carboxylate
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran for 1h; |
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran for 1h; |
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran for 1h; |
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran for 1h; |
phenylephrine hydrochloride
phosphorous acid
butan-1-ol
2-(3-Hydroxyphenyl)-methylaminoethane
Conditions | Yield |
---|---|
With hydrogen iodide; sodium sulfate | 23.72 g (62.7%) |
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