Appearance:YELLOW TO SLIGHT YELLOW CRYSTALLINE POWDER Application:Zuclopenthixol
Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities
Cas:86-39-5
Min.Order:1 Kilogram
FOB Price: $3.0
Type:Lab/Research institutions
inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
Cas:86-39-5
Min.Order:1 Kilogram
Negotiable
Type:Manufacturers
inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Cangzhou Enke Pharma Tech Co.,ltd. is located in Cangzhou City, Hebei province ,where is a famous petroleum chemical industry city in China. Enke Pharma a high-tech enterprise ,and we are dedicated to developing and manufacturing new ap
Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Cas:86-39-5
Min.Order:5 Kiloliter
FOB Price: $1.2 / 5.0
Type:Manufacturers
inquiry2-Chlorothioxanthone Basic information Product Name: 2-Chlorothioxanthone Synonyms: 2-chloro-9h-thioxanthen-9-on;2-chloro-9H-Thioxanthen-9-one;KayacureCTX;NissoCureCTX;QuantacureCTX;Sand
Our advantages: 1. High quality and competitive price: 1) Standard: BP/USP/EP/ enterprise standard 2) All purity ≥99% 3) We are manufacturers and can provide high quality products at factory prices. 2. Fast and safe delivery 1) The package c
Cas:86-39-5
Min.Order:1 Kilogram
FOB Price: $1.0 / 10.0
Type:Trading Company
inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:86-39-5
Min.Order:1 Kilogram
FOB Price: $139.0 / 210.0
Type:Trading Company
inquiryProduct name: 2-Chlorothioxanthone CAS No.: 86-39-5 Molecular formula C13H7ClOS Appearance: light yellow crystalline powder Melting point: ≥151℃
1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
Cas:86-39-5
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At prese
Cas:86-39-5
Min.Order:1 Kilogram
FOB Price: $76.0 / 85.0
Type:Trading Company
inquiry2-Chlorothioxanthone CAS:86-39-5 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic interme
Cas:86-39-5
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Our advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We have s
Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:86-39-5
Min.Order:0 Metric Ton
Negotiable
Type:Lab/Research institutions
inquiryCompany Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments
Cas:86-39-5
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Massive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and
Cas:86-39-5
Min.Order:1 Gram
FOB Price: $1.0
Type:Lab/Research institutions
inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:86-39-5
Min.Order:10 Gram
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Type:Lab/Research institutions
inquiry2-ChlorothioxanthoneAppearance:Beige powder Storage:keep in dry and ventilated place Package:according to customers' requirements Application:intermediates Transportation:By air(EMS or EUB or FedEx or TNT ect...) or by sea(FOB or CIF or CNF ect...)or
supplier in China Appearance:Beige powder Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package: 1g/bag, 5g/bag, 10g/bag, 100g/bag, 1kg/bag or as per your request Application:Used as a drug chloride thiamethoxam ton
Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
GMP standard, high purity, competitive price, in stock 1. Quick Response: within 6 hours after receiving your email. 2. Quality Guarantee: All products are strictly tested by our QC, confirmed by QA, and approved by a third-party lab in China, USA,
2-Chlorothioxanthone Basic information Product Name: 2-Chlorothioxanthone Synonyms: 2-chloro-9h-thioxanthen-9-on;2-chloro-9H-Thioxanthen-9-one;2-Chlorothoxanthone;2-CHLOROTHIAXANTHONE;2-CHLOROTHIOXANTHEN-9-ONE;2-CHLOROTHIOXANTHENE-9-ONE;2-CHLO
factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
Cas:86-39-5
Min.Order:1 Kilogram
FOB Price: $18.0 / 20.0
Type:Trading Company
inquiryProduct name: 2-Chlorothioxanthen-9-one CAS No,: 86-39-5 Molecule Formula:C13H7ClOS Molecule Weight:246.71 Purity: 99.0% Package: 25kg/drum Description:Ginger yellow powder Manufacture Standards:Enterprise Standard
Cas:86-39-5
Min.Order:1 Kilogram
Negotiable
Type:Trading Company
inquiryWe Huarong Pharm can provide Customized Synthesis & Process R&D & APIs and intermediates Production & Quality Research & Registration Application, especially our GMP validation service which complies with SFDA, FDA, WHO and EU EMPA. O
Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
Cas:86-39-5
Min.Order:1 Metric Ton
FOB Price: $1.5
Type:Trading Company
inquiryConditions | Yield |
---|---|
With tert.-butylnitrite; oxygen; acetic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone In 1,2-dichloro-ethane at 20℃; for 12h; Irradiation; | 98% |
With potassium hexafluorophosphate; iron(III) nitrate monohydrate; oxygen In acetonitrile at 80℃; for 12h; Reagent/catalyst; Temperature; Concentration; | 96% |
In 1,2-dichloro-ethane at 20℃; for 4h; UV-irradiation; | 70% |
With air In 1,2-dichloro-ethane at 20℃; for 4h; UV-irradiation; | 70% |
With tert.-butylnitrite; oxygen; acetic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone In 1,2-dichloro-ethane at 20℃; for 12h; Sealed tube; Irradiation; |
(2-bromo-5-chlorophenyl)(2-fluorophenyl)methanone
2-Chlorothioxanthone
Conditions | Yield |
---|---|
With sodiumsulfide nonahydrate In N,N-dimethyl-formamide at 60℃; | 95% |
Conditions | Yield |
---|---|
With sulfuric acid at 60℃; for 3h; Temperature; | 89.3% |
With sulfuric acid Reflux; | 68% |
With sulfuric acid | |
With sulfuric acid | |
With sulfuric acid at 100℃; for 12h; Inert atmosphere; | 8.1mg |
Conditions | Yield |
---|---|
With 1-hydroxy-pyrrolidine-2,5-dione; graphitic carbon nitride; oxygen In acetonitrile at 20℃; Inert atmosphere; Irradiation; | 62% |
9-bromo-2-chloro-9-(1-hydroxy-3-dimethylaminopropyl)thioxanthene
A
2-Chlorothioxanthone
B
1-(2-Chloro-9H-thioxanthen-9-yl)-3-dimethylamino-propan-1-one; hydrobromide
C
9-amino-2-chloro-9-(1-hydroxy-3-dimethylaminopropyl)thioxanthene dihydrochloride
D
Chlorprothixen
Conditions | Yield |
---|---|
at 130℃; for 2h; | A 30 mg B 36% C 0.66 g D 0.26 g |
2-<5-Chloro-2-(2-fluorophenylthio)phenyl>-5-dimethylaminopentan-2-ol
A
2-Chlorothioxanthone
B
8-Chloro-6-methyl-6-(3-dimethylaminopropyl)-6H-dibenz-1,4-oxathiepin
Conditions | Yield |
---|---|
With sodium hydride In N,N-dimethyl-formamide at 70℃; for 8h; | A 0.17 g B 35% |
5-Chloro-2-(2-fluorophenylthio)acetophenone
2-Chlorothioxanthone
Conditions | Yield |
---|---|
With sodium hydride In N,N-dimethyl-formamide at 70℃; for 8h; | 12% |
Multi-step reaction with 2 steps 1: 1) Mg / 1) THF, reflux, 3 h; 2) THF, reflux, 3 h 2: 1.88 g / NaH / dimethylformamide / 8 h / 70 °C View Scheme | |
Multi-step reaction with 2 steps 1: 1) Mg / 1) THF, reflux, 2 h; 2) THF, reflux, 4 h 2: 0.17 g / NaH / dimethylformamide / 8 h / 70 °C View Scheme |
1-[5-Chloro-2-(2-fluoro-phenylsulfanyl)-phenyl]-1-(1-methyl-piperidin-4-yl)-ethanol
A
2-Chlorothioxanthone
B
8-Chloro-6-methyl-6-(1-methyl-4-piperidyl)-6H-dibenz-1,4-oxathiepin
Conditions | Yield |
---|---|
With sodium hydride In N,N-dimethyl-formamide at 70℃; for 8h; | A 1.88 g B 8% |
2-amino-9H-thioxanthen-9-one
2-Chlorothioxanthone
Conditions | Yield |
---|---|
ueber die Diazonium-Verbindung; |
3-(Dimethylamino)propyl chloride
A
2-Chlorothioxanthone
B
Dihydrochlorprothixene
Conditions | Yield |
---|---|
With hydrogenchloride; methanol; alkaline aqueous potassium borate solution Vor der Umsetzung mit <3-Chlor-propyl>-dimethyl-amin unter Stickstoff wurde das Reaktionsprodukt mit Butyllithium in Aether behandelt; |
Conditions | Yield |
---|---|
With sulfuric acid | |
With sulfuric acid at 75℃; for 2h; | |
With sulfuric acid at 75℃; for 2h; | |
With sulfuric acid at 75℃; for 2h; | |
With sulfuric acid at 75℃; for 2h; |
Conditions | Yield |
---|---|
With potassium permanganate; 18-crown-6 ether In benzene |
2-methyl-1,2,3,4,10,14b-hexahydrodibenzo[c,f]pyrazino[1,2-a]azepine hydrochloride
2-Chlorothioxanthone
Conditions | Yield |
---|---|
With potassium permanganate In water |
Conditions | Yield |
---|---|
In methanol at 22℃; for 480h; Product distribution; Irradiation; degradation, various conditions; | A 32 % Chromat. B n/a |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 2: H2SO4 View Scheme | |
Multi-step reaction with 2 steps 1: potassium hydroxide; copper / water / 12 h / Reflux 2: sulfuric acid / Reflux View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 2: H2SO4 View Scheme | |
Multi-step reaction with 2 steps 1: potassium hydroxide; copper / water / 12 h / Reflux 2: sulfuric acid / Reflux View Scheme |
2-chlorosulfenylbenzoyl chloride
chlorobenzene
A
4-chlorothioxanthen-9-one
B
2-Chlorothioxanthone
Conditions | Yield |
---|---|
aluminum (III) chloride In 1,2-dichloro-ethane at 40 - 45℃; for 1h; Friedel Crafts Acylation; |
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: (1,5-cyclooctadiene)(methoxy)iridium(I) dimer / hexane / 14 h / 20 °C / Inert atmosphere 2: copper(II) sulfate; sodium hydrogencarbonate / methanol / 24 h / 20 °C / Inert atmosphere 3: potassium hydroxide; water / methanol / 1 h / 80 °C / Inert atmosphere 4: sulfuric acid / 12 h / 100 °C / Inert atmosphere View Scheme |
4-chlorophenyl 2-methoxycarbonylphenyl sulfide
2-Chlorothioxanthone
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: potassium hydroxide; water / methanol / 1 h / 80 °C / Inert atmosphere 2: sulfuric acid / 12 h / 100 °C / Inert atmosphere View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: copper(II) sulfate; sodium hydrogencarbonate / methanol / 24 h / 20 °C / Inert atmosphere 2: potassium hydroxide; water / methanol / 1 h / 80 °C / Inert atmosphere 3: sulfuric acid / 12 h / 100 °C / Inert atmosphere View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: acetic acid; dihydrogen peroxide / water / 50 h / 0 - 20 °C / Inert atmosphere 2: copper(II) sulfate; sodium hydrogencarbonate / methanol / 24 h / 20 °C / Inert atmosphere 3: potassium hydroxide; water / methanol / 1 h / 80 °C / Inert atmosphere 4: sulfuric acid / 12 h / 100 °C / Inert atmosphere View Scheme |
2-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)benzoic acid methyl ester
2-Chlorothioxanthone
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: copper(II) sulfate; sodium hydrogencarbonate / methanol / 24 h / 20 °C / Inert atmosphere 2: potassium hydroxide; water / methanol / 1 h / 80 °C / Inert atmosphere 3: sulfuric acid / 12 h / 100 °C / Inert atmosphere View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: hydrogen sulfide / 300 °C / Flow reactor 2: lithium hydroxide monohydrate; sodium hydroxide / toluene / 12 h / 120 °C 3: sulfuric acid / 3 h / 60 °C View Scheme |
Conditions | Yield |
---|---|
In toluene at 25℃; for 42h; Large scale; | 99% |
Conditions | Yield |
---|---|
Stage #1: triallyl(phenyl)silane With tetrabutyl ammonium fluoride In tetrahydrofuran; water at 20℃; for 1h; Stage #2: 2-Chlorothioxanthone With XPhos; bis(η3-allyl-μ-chloropalladium(II)) In tetrahydrofuran; water at 80℃; for 12h; | 98% |
2-Chlorothioxanthone
2-hydroxy thioxanthone
Conditions | Yield |
---|---|
With t-BuBrettPhos; C44H62NO5PPdS; water; potassium hydroxide In 1,4-dioxane at 80℃; for 18h; Inert atmosphere; | 98% |
With tris-(dibenzylideneacetone)dipalladium(0); C39H57O3P; potassium hydroxide In 1,4-dioxane at 80℃; | 98% |
With tris-(dibenzylideneacetone)dipalladium(0); potassium hydroxide; tert-butyl XPhos In 1,4-dioxane; water at 100℃; for 16h; Schlenk technique; Inert atmosphere; Reflux; | 85% |
With copper acetylacetonate; N1-(4-hydroxy-2,6-dimethylphenyl)-N2-(4-hydroxy-3,5-dimethylphenyl)oxalamide; water In water; dimethyl sulfoxide at 130℃; for 24h; Schlenk technique; Inert atmosphere; | 76% |
With tris-(dibenzylideneacetone)dipalladium(0); potassium hydroxide; tert-butyl XPhos In 1,4-dioxane; water at 100℃; for 16h; Inert atmosphere; |
Conditions | Yield |
---|---|
With 4,4'-(phenylphosphinediyl)bis(2,6-dimethylmorpholine); caesium carbonate; tris(dibenzylideneacetone)dipalladium (0) In 1,4-dioxane for 8h; Suzuki-Miyaura coupling; Heating; | 95% |
2-Chlorothioxanthone
d(4)-methanol
2-trideuteriomethoxy-9H-thioxanthen-9-one
Conditions | Yield |
---|---|
With t-BuBrettPhos; [(2-di-tert-butylphosphino-3,6-dimethoxy-2’,4’,6’-triisopropyl-1,1’-biphenyl)-2-(2’-amino-1,1‘-biphenyl)]palladium(II) methanesulfonate; sodium t-butanolate In 1,4-dioxane at 20℃; for 20h; Sealed tube; Inert atmosphere; | 94% |
Conditions | Yield |
---|---|
With dimethylsulfide borane complex In tetrahydrofuran for 2h; Reflux; | 93% |
With borane In tetrahydrofuran 1) 0 - 5 deg C, 0.5 h, 2) 1 h, rt; | 90% |
Conditions | Yield |
---|---|
With C26H33N2P; C39H46N3O3PPdS; sodium t-butanolate In 1,4-dioxane at 80℃; for 12h; Inert atmosphere; | 93% |
Conditions | Yield |
---|---|
With potassium phosphate; 2-(2,6-dimethoxyphenyl)-1-methyl-3-(diphenylphosphino)-1H-indole; palladium diacetate at 90℃; for 18h; Inert atmosphere; Schlenk technique; | 88% |
With bis[chloro(1,2,3-trihapto-allylbenzene)palladium(II)]; 2-methoxy-6-(N-methyl-N-phenyl-amino)phenyl(dicyclohexyl)phosphine; caesium carbonate at 90℃; for 16h; Inert atmosphere; Schlenk technique; Sealed tube; | 87% |
Conditions | Yield |
---|---|
Stage #1: 2-Chlorothioxanthone; Chloroiodomethane With methyllithium lithium bromide In tetrahydrofuran at -78℃; for 0.75h; Inert atmosphere; Stage #2: With hexylsilane; tris(pentafluorophenyl)borate In dichloromethane at 20℃; for 1h; Inert atmosphere; chemoselective reaction; | 87% |
Conditions | Yield |
---|---|
With 2-(2,6-dimethoxyphenyl)-1-methyl-3-(diphenylphosphino)-1H-indole; palladium diacetate; lithium tert-butoxide In 1,4-dioxane at 100℃; for 1h; Schlenk technique; Inert atmosphere; | 87% |
Conditions | Yield |
---|---|
With (2-dicyclohexylphosphino-2’,4’,6’-triisopropyl-1,1'-biphenyl)[2-(2-amino-1,1’-biphenyl)]palladium(II)methanesulfonate; XPhos In toluene at 100℃; Inert atmosphere; Schlenk technique; | 86% |
Conditions | Yield |
---|---|
Stage #1: bromobenzene With magnesium; ethylene dibromide In tetrahydrofuran Heating; Stage #2: 2-Chlorothioxanthone In tetrahydrofuran for 0.5h; Grignard reaction; Further stages.; | 83% |
2-Chlorothioxanthone
N-Methyl-N-phenethylamine
2-(methyl(phenethyl)amino)-9H-thioxanthen-9-one
Conditions | Yield |
---|---|
With 1,1'-bis-(diphenylphosphino)ferrocene; cis-[1,1'-bis(diphenylphosphino)ferrocene](2-methylphenyl)nickel(II) chloride; acetonitrile; lithium tert-butoxide at 100℃; for 1h; Inert atmosphere; | 83% |
Conditions | Yield |
---|---|
Stage #1: 2-Bromobiphenyl With n-butyllithium In tetrahydrofuran at -78℃; for 0.5h; Inert atmosphere; Stage #2: 2-Chlorothioxanthone In tetrahydrofuran at -78 - 20℃; Inert atmosphere; | 83% |
2-Chlorothioxanthone
tetramethylammonium trifluoromethylselenate(0)
Conditions | Yield |
---|---|
With 1,1'-bis-(diphenylphosphino)ferrocene; bis(1,5-cyclooctadiene)nickel (0) In toluene at 50℃; for 12h; Inert atmosphere; | 82% |
2-Chlorothioxanthone
1-Dimethylaminomethyl-vinylmagnesiumbromid
Conditions | Yield |
---|---|
In tetrahydrofuran | 80% |
2-Chlorothioxanthone
2-amino-9H-thioxanthen-9-one
Conditions | Yield |
---|---|
With dicyclohexyl(2',4',6'-triisopropyl-5-methoxy-3,4,6-trimethyl-[1,1'-biphenyl]-2-yl)phosphine; C50H70NO4PPdS; C50H70NO4PPdS; dicyclohexyl(2',4',6'-triisopropyl-4-methoxy-3,5,6-trimethyl-[1,1'-biphenyl]-2-yl)phosphine; ammonia; sodium t-butanolate In 1,4-dioxane at 80℃; for 24h; Inert atmosphere; | 80% |
With ammonium hydroxide; potassium phosphate; copper(l) iodide; N1,N2-bis(5-methyl-[1,1'-biphenyl]-2-yl)oxalamide In water; dimethyl sulfoxide at 110℃; for 24h; Inert atmosphere; | 70% |
Conditions | Yield |
---|---|
With potassium phosphate; copper(l) iodide; N1,N2-bis(2,4,6-trimethoxyphenyl)oxalamide In dimethyl sulfoxide at 120℃; for 24h; Inert atmosphere; Schlenk technique; | 78% |
Conditions | Yield |
---|---|
With C12H10N(1-)*CH3O3S(1-)*Pd(2+)*C39H57O2P; sodium t-butanolate In 1,4-dioxane at 40℃; for 15h; Reagent/catalyst; Sealed tube; Schlenk technique; Inert atmosphere; | 78% |
2-Chlorothioxanthone
dimethyl diazomalonate
2-chlorothioxanthonium bis(carbomethoxy)methylide
Conditions | Yield |
---|---|
With copper(II) sulfate In toluene at 95 - 100℃; for 5h; | 77% |
With copper(II) sulfate In toluene Yield given; |
2-Chlorothioxanthone
2-chloro-3-nitrothioxanth-9-one-10,10-dioxide
Conditions | Yield |
---|---|
With sulfuric acid; nitric acid at 0℃; for 0.5h; | 77% |
2-Chlorothioxanthone
sodium methansulfinate
Conditions | Yield |
---|---|
With potassium phosphate; copper(l) iodide; (2S,4R)-4-hydroxy-N-(2-methylnaphthalen-1-yl)pyrrolidine-2-carboxamide In dimethyl sulfoxide at 120℃; Sealed tube; Inert atmosphere; | 75% |
Conditions | Yield |
---|---|
With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate; bis(η3-allyl-μ-chloropalladium(II)) In toluene at 100℃; for 4h; | 70% |
Conditions | Yield |
---|---|
With ammonium cerium(IV) nitrate In water; acetonitrile at 65℃; for 1.5h; | 67.3% |
Conditions | Yield |
---|---|
With silver hexafluoroantimonate; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; Trimethylacetic acid In 1,2-dichloro-ethane at 80℃; for 20h; Sealed tube; | 64% |
2-(2-Hydroxyethyl)pyridine
2-Chlorothioxanthone
2-[2-(pyridin-2-yl)ethoxy]-9H-thioxanthen-9-one
Conditions | Yield |
---|---|
With tris-(dibenzylideneacetone)dipalladium(0); (R)-(-)-1-[(SP)-2-(dicyclohexylphosphino)ferrocenyl]ethyldi-tert-butylphosphine; caesium carbonate In toluene at 80℃; for 16h; Catalytic behavior; Inert atmosphere; | 58% |
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