CAS No.3333-13-9,1-ALLYL-4-METHYLBENZENE Suppliers,MSDS download

Dayang Chem (Hangzhou) Co.,Ltd.

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Benzene,1-methyl-4-(2-propen-1-yl)-

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Henan Wentao Chemical Product Co., Ltd.

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Henan Tianfu Chemical Co., Ltd.

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TAIZHOU ZHENYU BIOTECHNOLOGY CO., LTD

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1-ALLYL-4-METHYLBENZENE

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Shandong Mopai Biotechnology Co., LTD

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Antimex Chemical Limied

hight degree of purity Application:Fine chemical intermediates, used as the main raw material for he synthesis of various pesticides, medicines, surfactants, polymer monomers, Ond Ontifungal agents

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Hangzhou Fandachem Co.,Ltd

Benzene,1-methyl-4-(2-propen-1-yl)- cas 3333-13-9Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express

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Henan Kanbei Chemical Co.,LTD

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Chemlyte Solutions

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ZHEJIANG JIUZHOU CHEM CO.,LTD

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Nanjing Chemlin Chemical Co., Ltd.

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Finetech Industry Limited

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Sigma-Aldrich Chemie GmbH

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Synthetic route

: 591-87-7
Allyl acetate

: 937-12-2
4-tolyltrimethylstannane

: 3333-13-9
p-allyltoluene

Conditions

Conditions	Yield
With tetrakis(triphenylphosphine) palladium(0) In N,N,N,N,N,N-hexamethylphosphoric triamide for 6h;	100%
tetrakis(triphenylphosphine) palladium(0) In N,N,N,N,N,N-hexamethylphosphoric triamide at 20℃;	100 % Chromat.

: 1826-67-1
vinyl magnesium bromide

: 104-81-4
4-Methylbenzyl bromide

: 3333-13-9
p-allyltoluene

Conditions

Conditions	Yield
With copper(l) iodide In tetrahydrofuran at -30℃; for 1h;	93%

: 106-95-6
allyl bromide

pTolSnR3: pTolSnR3

: 3333-13-9
p-allyltoluene

Conditions

Conditions	Yield
Pd(phenylimino)acenaphthene dimethyl fumarate In N,N-dimethyl-formamide at 50℃; for 16h;	88%

: 72824-04-5
2-Allyl-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 100-44-7
benzyl chloride

: 3333-13-9
p-allyltoluene

Conditions

Conditions	Yield
Stage #1: 2-Allyl-4,4,5,5-tetramethyl-1,3,2-dioxaborolane; benzyl chloride With tris-(dibenzylideneacetone)dipalladium(0); triphenylphosphine; cesium fluoride In dichloromethane at 30℃; for 20h; Inert atmosphere; Stage #2: With toluene-4-sulfonic acid In dichloromethane at 30℃; for 10h; Inert atmosphere; regioselective reaction;	80%

: 937-12-2
4-tolyltrimethylstannane

: 106-95-6
allyl bromide

: 3333-13-9
p-allyltoluene

Conditions

Conditions	Yield
bis(η3-allyl-μ-chloropalladium(II)) In N,N-dimethyl-formamide at 70℃;	75%
With bis(η3-allyl-μ-chloropalladium(II)) In N,N-dimethyl-formamide at 70℃; for 3h;	75%

: 937-12-2
4-tolyltrimethylstannane

: 106-95-6
allyl bromide

A: 3333-13-9
p-allyltoluene

B: 1066-44-0
trimethyltin bromide

Conditions

Conditions	Yield
With ((π-C3H5)PdCl)2 In N,N-dimethyl-formamide 70°C;	A 75% B n/a
tetrakis(triphenylphosphine) palladium(0) In N,N,N,N,N,N-hexamethylphosphoric triamide at 20℃; for 6h;	A 18 % Chromat. B n/a

...Expand

: 106-38-7
para-bromotoluene

: 106-95-6
allyl bromide

: 3333-13-9
p-allyltoluene

Conditions

Conditions	Yield
With magnesium In tetrahydrofuran for 0.5h; Heating;	72%
(i) Mg, Et2O, (ii) /BRN= 605308/; Multistep reaction;
Stage #1: para-bromotoluene With iodine; magnesium In diethyl ether for 2h; Reflux; Inert atmosphere; Stage #2: allyl bromide In diethyl ether at 20℃; Cooling with ice; Inert atmosphere;

: 5720-05-8
4-methylphenylboronic acid

: 107-05-1
3-chloroprop-1-ene

: 3333-13-9
p-allyltoluene

Conditions

Conditions	Yield
With potassium tert-butylate In isopropyl alcohol at 50℃; for 12h; Inert atmosphere;	68%

: 5720-05-8
4-methylphenylboronic acid

: 106-95-6
allyl bromide

: 3333-13-9
p-allyltoluene

Conditions

Conditions	Yield
With tetrakis(triphenylphosphine) palladium(0); sodium carbonate In 1,2-dimethoxyethane; water for 6h; Reflux;	66%
With C25H19ClNOPPd; potassium carbonate In toluene at 90℃; for 24h;	56%
With potassium carbonate In toluene at 90℃; for 3h; regioselective reaction;	15%
With aluminum oxide; potassium fluoride; palladium at 100℃; for 4h; Suzuki reaction;	28 % Chromat.
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In tetrahydrofuran at 0 - 50℃; Schlenk technique; Inert atmosphere;

: 624-31-7
4-tolyl iodide

: 2551-83-9
allyltrimethoxysilane

: 3333-13-9
p-allyltoluene

Conditions

Conditions	Yield
With tetrabutyl ammonium fluoride; bis(dibenzylideneacetone)-palladium(0) In tetrahydrofuran; N,N-dimethyl-formamide at 85℃; for 2h;	60%

: 2550-04-1
allyltriethoxysilane

: 624-31-7
4-tolyl iodide

: 3333-13-9
p-allyltoluene

Conditions

Conditions	Yield
With palladium(II) acetylacetonate; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene; tetrabutylammonium triphenyldifluorosilicate In tetrahydrofuran-d8 at 80℃; Hiyama Coupling; Glovebox; Sealed tube;	58%

: 591-87-7
Allyl acetate

: 106-38-7
para-bromotoluene

: 3333-13-9
p-allyltoluene

Conditions

Conditions	Yield
With magnesium; triphenylphosphine; copper(I) bromide; lithium bromide In tetrahydrofuran at 80℃; for 6h; Sealed tube;	56%
Stage #1: para-bromotoluene With magnesium; lithium chloride In tetrahydrofuran at 20℃; for 2h; Inert atmosphere; Stage #2: With iron(III)-acetylacetonate In tetrahydrofuran for 0.0833333h; Inert atmosphere; Stage #3: Allyl acetate In tetrahydrofuran at 0℃; for 0.75h; Inert atmosphere;

: 6921-43-3
1-cyclopropyl-4-methyl-benzene

A: 3333-13-9
p-allyltoluene

B: 2077-29-4
(Z)-1-(4-tolyl)-1-propene

C: 2077-30-7
(E)-1-methyl-4-(prop-1-enyl)benzene

Conditions

Conditions	Yield
With n-butyllithium; potassium tert-butylate In tetrahydrofuran 1) RT, 24 h, 2) reflux;	A 8% B 35% C 53%

...Expand

: 106-43-4
para-chlorotoluene

: 762-72-1
allyl-trimethyl-silane

: 3333-13-9
p-allyltoluene

Conditions

Conditions	Yield
With caesium carbonate In 2,2,2-trifluoroethanol for 18h; Inert atmosphere; UV-irradiation;	53%

: 66222-29-5
tri-n-butylstannylmethyl iodide

: C15H15LiOS

: 3333-13-9
p-allyltoluene

Conditions

Conditions	Yield
In tetrahydrofuran Product distribution; investigation of reactions of allyl 2-pyridyl sulfides or allyl phenyl sulfones;	46%

: C15H15LiOS

: 3333-13-9
p-allyltoluene

Conditions

Conditions	Yield
With tri-n-butylstannylmethyl iodide In tetrahydrofuran	46%

: 556-56-9
allyl iodid

: 5720-05-8
4-methylphenylboronic acid

: 3333-13-9
p-allyltoluene

Conditions

Conditions	Yield
With aluminum oxide; potassium fluoride; palladium at 100℃; for 4h; Suzuki reaction;	39%

: 624-31-7
4-tolyl iodide

: 72824-04-5
2-Allyl-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 3333-13-9
p-allyltoluene

Conditions

Conditions	Yield
With bis-triphenylphosphine-palladium(II) chloride; potassium carbonate In tetrahydrofuran at 80℃; for 48h; Suzuki-Miyaura coupling; Inert atmosphere;	35%

: C28H28In(1-)*Mg(2+)*Cl(1-)

: 106-95-6
allyl bromide

: 3333-13-9
p-allyltoluene

Conditions

Conditions	Yield
With [FeCl2(dpbz)2] at 85℃; for 4h;	21%

: 106-95-6
allyl bromide

: 4294-57-9
para-methylphenylmagnesium bromide

: 3333-13-9
p-allyltoluene

Conditions

Conditions	Yield
With diethyl ether

: 106-38-7
para-bromotoluene

: 24850-33-7
allyltributylstanane

: 3333-13-9
p-allyltoluene

Conditions

Conditions	Yield
Heating;

: 556-56-9
allyl iodid

: 937-12-2
4-tolyltrimethylstannane

: 3333-13-9
p-allyltoluene

Conditions

Conditions	Yield
With <η3-C3H5Pd(PPh3)2>+*Cl- In N,N,N,N,N,N-hexamethylphosphoric triamide at 20℃; for 4h;	64 % Chromat.

: 556-56-9
allyl iodid

: 937-12-2
4-tolyltrimethylstannane

A: 3333-13-9
p-allyltoluene

B: 811-73-4
trimethylstannyl iodide

Conditions

Conditions	Yield
tetrakis(triphenylphosphine) palladium(0) In N,N,N,N,N,N-hexamethylphosphoric triamide at 20℃; for 6h;	A 56 % Chromat. B n/a

...Expand

: 591-87-7
Allyl acetate

: 937-12-2
4-tolyltrimethylstannane

A: 3333-13-9
p-allyltoluene

B: 1118-14-5
trimethyltin acetate

Conditions

Conditions	Yield
tetrakis(triphenylphosphine) palladium(0) In N,N,N,N,N,N-hexamethylphosphoric triamide at 20℃; for 6h;	A 100 % Chromat. B n/a

...Expand

: 937-12-2
4-tolyltrimethylstannane

A: 3333-13-9
p-allyltoluene

B: 613-33-2
(4,4'-dimethyl-1,1'-biphenyl)

C: 1118-14-5
trimethyltin acetate

Conditions

Conditions	Yield
With Allyl acetate; tetrakis(triphenylphosphine) palladium(0) In tetrahydrofuran at 68℃; for 2.5h;	A 59 % Chromat. B 32 % Chromat. C n/a

...Expand

: 84648-35-1
C18H17ClO4

A: 3333-13-9
p-allyltoluene

B: 1074-55-1
p-n-propyltoluene

C: 84648-45-3
C16H17Cl

D: 84648-39-5
3-Chloro-benzoic acid 3-p-tolyl-propyl ester

E: 108-90-7
chlorobenzene

Conditions

Conditions	Yield
In cyclohexanone at 100℃; Mechanism; CIDNP, thermolyse;

...Expand

: 84648-35-1
C18H17ClO4

A: 3333-13-9
p-allyltoluene

B: 77975-31-6
1-(3-chloropropyl)-4-methylbenzene

C: 84648-45-3
C16H17Cl

D: 84648-39-5
3-Chloro-benzoic acid 3-p-tolyl-propyl ester

E: 541-73-1
1,3-Dichlorobenzene

Conditions

Conditions	Yield
In various solvent(s) at 100℃; Mechanism; CIDNP, thermolyse;

...Expand

: 107-18-6
allyl alcohol

: 108-88-3
toluene

A: 3333-13-9
p-allyltoluene

B: 1587-04-8
1-methyl-2-(2-propenyl)-benzene

C: 3333-20-8
1-allyl-3-methylbenzene

D: 187737-37-7
propene

E: 74-85-1
ethene

F: 557-40-4
Allyl ether

Conditions

Conditions	Yield
HUSY26 at 149.9℃; Product distribution; other catalysts, other temp., also allylation with 3-buten-1-ol and allyl chloride;

...Expand

: 112176-19-9
(4-MeC6H4)Ti(O-i-Pr)3

: 106-95-6
allyl bromide

: 3333-13-9
p-allyltoluene

Conditions

Conditions	Yield
With bis(η3-allyl-μ-chloropalladium(II)) In diethyl ether; benzene for 0.5h;	98 % Chromat.

: 3333-13-9
p-allyltoluene

: 62-53-3
aniline

: C15H15N

Conditions

Conditions	Yield
With sodium sulfate In diethyl ether at 20℃; for 24h;	100%

: 3333-13-9
p-allyltoluene

: 783-08-4
[4-(benzylideneamino)phenyl]methanol

: (E)-N-[4-(4-methylphenyl)-1-phenylbut-3-enyl]-4-methoxyaniline

Conditions

Conditions	Yield
With sodium hexamethyldisilazane In 1,4-dioxane at 25℃; for 20h; Inert atmosphere; regioselective reaction;	99%

: 3333-13-9
p-allyltoluene

: 74-93-1
methylthiol

: methyl(3-(p-tolyl)propyl)sulfane

Conditions

Conditions	Yield
With C38H28Au2F12FeN2O8P2S4 In 1,4-dioxane at 45℃; for 20h; Inert atmosphere; Glovebox; Sealed tube;	98%

: 3333-13-9
p-allyltoluene

: 74-85-1
ethene

: 622-97-9
1-ethenyl-4-methylbenzene

Conditions

Conditions	Yield
With Hoveyda-Grubbs catalyst second generation; di-μ-bromobis-(tritert-butylphosphine)dipalladium(I) In tetrahydrofuran at 60℃; under 7500.75 Torr; for 16h; Autoclave;	94%

: 3333-13-9
p-allyltoluene

: 5838-00-6
methyl dimethyl 2-(trifluoromethyl)propanedioate

: 1455396-80-1
(E)-dimethyl 2-(3-(p-tolyl)allyl)-2-(trifluoromethyl)malonate

Conditions

Conditions	Yield
With 2,6-dimethoxy-p-quinone; palladium diacetate; triphenylphosphine In 1-methyl-pyrrolidin-2-one at 20℃; for 12h; Inert atmosphere; Schlenk technique;	94%

: 3333-13-9
p-allyltoluene

: 7648-30-8
ethyl 2,2-difluoro-2-iodoacetate

: 2,2-difluoro-4-iodo-5-(p-tolyl) pentanoate

Conditions

Conditions	Yield
With 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; bis-diphenylphosphinomethane In tetrahydrofuran at 80℃; for 20h; Catalytic behavior; Reagent/catalyst; Solvent; Inert atmosphere; Schlenk technique;	94%
With 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; bis-diphenylphosphinomethane In tetrahydrofuran at 80℃; for 20h; Reagent/catalyst; Temperature; Inert atmosphere;	90%
With o-phenylenebis(diphenylphosphine); cobalt(II) bromide; zinc In water; acetone at 20℃; for 3h; Inert atmosphere; stereoselective reaction;	84%

: 3333-13-9
p-allyltoluene

: 2096-86-8
p-Tolylaceton

Conditions

Conditions	Yield
With iron(III) sulfate; palladium(II) trifluoroacetate; sodium 2,2,2-trifluoroacetate In water; acetonitrile at 30℃; Wacker-Tsuji Olefin Oxidation; Inert atmosphere; Darkness;	94%

: 3333-13-9
p-allyltoluene

: 13081-18-0
ethyl-3,3,3-trifluoropyruvate

: ethyl (2R,E)-2-(trifluoromethyl)-2-hydroxy-5-p-tolylpent-4-enoate

Conditions

Conditions	Yield
With cis-Pd(S(-)-BINAP)(OTf)2 In dichloromethane at 20℃; for 0.166667h; Inert atmosphere; optical yield given as %ee; enantioselective reaction;	93%
With silver hexafluoroantimonate; chiral PtCl2 based NU-BIPHEP-type catalyst In dichloromethane for 60h;
silver hexafluoroantimonate; δ-dichloro[3,3'-bis(diphenylphosphanyl)-5,6,7,8,5',6',7',8'-octahydro[2,2']binaphthalene]platinum In dichloromethane at 20℃; for 1h; Product distribution / selectivity;	n/a

: 3333-13-9
p-allyltoluene

: 5337-93-9
4'-methylpropiophenone

Conditions

Conditions	Yield
With tert.-butylhydroperoxide; palladium diacetate; toluene-4-sulfonic acid In water; acetonitrile at 20℃; for 6h; Wacker Oxidation; chemoselective reaction;	93%

: 3333-13-9
p-allyltoluene

: 555-16-8
4-nitrobenzaldehdye

: (1R,2S)-1-(4-nitrophenyl)-2-(p-tolyl)but-3-en-1-ol

Conditions

Conditions	Yield
Stage #1: p-allyltoluene With N-fluorobis(benzenesulfon)imide; triphenylphosphine; bis(dibenzylideneacetone)-palladium(0); bis((+)-pinanediolato)diboron In toluene at 50℃; for 24h; Inert atmosphere; Stage #2: 4-nitrobenzaldehdye With C34H21O4P In toluene at 25℃; for 24h; Inert atmosphere; enantioselective reaction;	91%

: 3333-13-9
p-allyltoluene

: 56578-35-9
4-methyl-cinnamaldehyde

Conditions

Conditions	Yield
With water; 2,3-dicyano-5,6-dichloro-p-benzoquinone; palladium dichloride In 1,2-dichloro-ethane at 50℃; for 2h; stereoselective reaction;	90%
With 2,3-dicyano-5,6-dichloro-p-benzoquinone; palladium dichloride In water; 1,2-dichloro-ethane at 50℃;	90%
With water; 2,3-dicyano-5,6-dichloro-p-benzoquinone In 1,2-dichloro-ethane at 60℃; for 10h;	80%
With water; oxygen; palladium diacetate In dimethyl sulfoxide at 100℃; under 760.051 Torr; for 24h; Green chemistry; regioselective reaction;	78%

: 3333-13-9
p-allyltoluene

: (E)-1-(3-azidoprop-1-enyl)-4-methylbenzene

Conditions

Conditions	Yield
With sodium azide; oxygen; palladium diacetate In dimethyl sulfoxide at 100℃; for 24h; regioselective reaction;	90%
Multi-step reaction with 2 steps 1: bromine / chloroform / 0.17 h / 0 °C 2: sodium azide; 1,8-diazabicyclo[5.4.0]undec-7-ene; sodium iodide / dimethyl sulfoxide / 2 h / 22 °C / Sealed tube View Scheme

: 3333-13-9
p-allyltoluene

: C12H13NO4

: (E)-3-methyl-3-(4-nitrophenyl)-6-(p-tolyl)hex-5-en-2-one

Conditions

Conditions	Yield
With palladium diacetate; caesium carbonate; triphenylphosphine; tert-butyl alcohol In tetrahydrofuran at 80℃; for 22h; Schlenk technique; Inert atmosphere;	90%

: 3333-13-9
p-allyltoluene

: 2.5-Dimethyl-N.N.N'.N'-tetramethyl-p-phenylendiamin

: C22H32N2

Conditions

Conditions	Yield
With C32H53N2OScSi2; N,N'-dimethylaniliniumtetrakis(pentafluorophenyl)borate In toluene at 80℃; for 12h; Inert atmosphere; regioselective reaction;	90%

: 3333-13-9
p-allyltoluene

: 104-09-6
4-methylphenylacetaldehyde

Conditions

Conditions	Yield
Stage #1: p-allyltoluene With ozone In dichloromethane at -78℃; Stage #2: With (Z,Z,Z)-4,4'-bis[4-(diphenylphosphino)styryl]stilbene In dichloromethane at -78 - 23℃; for 0.5h; Stage #3: With erythrosine B In tetrahydrofuran for 1h; Irradiation;	89%
With ozone In methanol at -78℃; for 0.75h;	13%

: 3333-13-9
p-allyltoluene

: 694-53-1
phenylsilane

: phenyl(1-p-tolylpropan-2-yl)silane

Conditions

Conditions	Yield
Stage #1: phenylsilane With C22H31Cl2CoN2P In tetrahydrofuran for 0.166667h; Inert atmosphere; Glovebox; Stage #2: p-allyltoluene In tetrahydrofuran at 60℃; for 24h; Inert atmosphere; Sealed tube; regioselective reaction;	89%

: 3333-13-9
p-allyltoluene

: 78782-17-9
4,4,5,5-tetramethyl-2-[(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)methyl]-1,3,2-dioxaborolane

: 1375536-65-4
(E)-4,4,5,5-tetramethyl-2-(4-(p-tolyl)but-3-en-1-yl)-1,3,2-dioxaborolane

Conditions

Conditions	Yield
With potassium dihydrogenphosphate; silver tetrafluoroborate; 1,2-Bis(phenylsulfinyl)ethane; palladium diacetate; [1,4]naphthoquinone In 1,4-dioxane at 50℃; for 24h; Sealed tube; Schlenk technique;	88%

: 3333-13-9
p-allyltoluene

: 67-68-5
dimethyl sulfoxide

: 1-(methylthio)-3-p-tolylpropan-2-ol

Conditions

Conditions	Yield
With ammonium iodide; water at 130℃; for 24h; Schlenk technique;	88%

: 3333-13-9
p-allyltoluene

: 491-36-1
4-Hydroxyquinazoline

: 3-(3-(p-tolyl)allyl)quinazolin-4(3H)-one

Conditions

Conditions	Yield
With 2,6-dimethyl-1,4-benzoquinone; palladium dichloride In dimethyl sulfoxide at 100℃; for 24h; chemoselective reaction;	88%

: 3333-13-9
p-allyltoluene

: 127427-45-6
2-bromo-2,2-difluoro-N-phenyl-acetamide

: 2,2-difluoro-4-hydroxy-N-phenyl-5-(p-tolyl)pentanamide

Conditions

Conditions	Yield
With N,N,N',N'',N'''-pentamethyldiethylenetriamine; rhodamine 6G at 25℃; for 22h; Irradiation;	88%

: 3333-13-9
p-allyltoluene

: 1632-83-3
1-Methylbenzimidazole

A: 1-methyl-2-(3-(p-tolyl)propyl)-1H-benzo[d]imidazole

B: 1-methyl-2-(1-(p-tolyl)propyl)-1H-benzo[d]imidazole

Conditions

Conditions	Yield
With bis(1,5-cyclooctadiene)nickel(0); [1,3-bis(2,4,6-trimethylphenyl)imidazol]-2-ylidene In toluene at 130℃; for 16h; Overall yield = 94 %; regioselective reaction;	A n/a B 87%
With bis(1,5-cyclooctadiene)nickel(0); trimethylaluminum; 1,3-bis-(2,6-diisopropylphenyl)-imidazol-2-ylidene In toluene at 130℃; for 16h; Overall yield = 89 %; regioselective reaction;	A 85% B n/a

...Expand

: 3333-13-9
p-allyltoluene

: 7511-27-5
1-bromo-7-methylnaphthalene

Conditions

Conditions	Yield
With carbon tetrabromide; iron In ethanol at 20℃; for 2h; Irradiation;	87%

: 3333-13-9
p-allyltoluene

: 122058-30-4
p-methylcinnamyl alcohol

Conditions

Conditions	Yield
With palladium(II) trifluoroacetate; water; p-benzoquinone In dimethyl sulfoxide at 20℃; for 22h; Sealed tube; Green chemistry; regioselective reaction;	86%
With hydrogenchloride; water; oxygen; palladium dichloride In dimethyl sulfoxide at 100℃; under 760.051 Torr; for 24h; Green chemistry; regioselective reaction;	81%

: 3333-13-9
p-allyltoluene

: 1-(((dimethyl(oxo)- λ6-sulfanylidene)methyl)sulfonyl)-4-methylbenzene

: (2E,4E)-1,5-di-p-tolylpenta-2,4-dien-1-one

Conditions

Conditions	Yield
With 2,6-dimethyl-1,4-benzoquinone; palladium diacetate; triphenylphosphine In dimethyl sulfoxide at 65℃; for 24h; regioselective reaction;	85%

: 3333-13-9
p-allyltoluene

: 6066-82-6
1-hydroxy-pyrrolidine-2,5-dione

: (E)-1-((3-(p-tolyl)allyl)oxy)pyrrolidine-2,5-dione

Conditions

Conditions	Yield
With oxygen; palladium diacetate; copper(II) acetate monohydrate; acetic acid In acetonitrile at 75℃;	85%

: 3333-13-9
p-allyltoluene

: 421-83-0
trifluoromethane sulfonyl chloride

: 4,4,4-trifluoro-1-(p-tolyl)butane-2-sulfonyl chloride

Conditions

Conditions	Yield
With dipotassium hydrogenphosphate; [Cu(2,9-bis(4-methoxyphenyl)-1,10-phenanthroline)2]Cl In acetonitrile at 20℃; for 24h; Inert atmosphere; Irradiation;	82%

: 3333-13-9
p-allyltoluene

: 71-36-3
butan-1-ol

: 123248-21-5
(E)-n-butyl 3-(p-tolyl)acrylate

Conditions

Conditions	Yield
With water; oxygen; palladium diacetate In N,N-dimethyl acetamide at 100℃; under 760.051 Torr; for 24h; Schlenk technique; chemoselective reaction;	82%

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