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titanium trichloride CAS NO.7705-07-9 Application:titanium trichloride CAS NO.7705-07-9
titanium trichloride CAS NO.7705-07-9Appearance:contact Crystal Song for details Storage:Shading, sealed, dry place. Package:foil bags, drums or bottles Application:Pharmaceutical Intermediates / Active Pharmaceutical Ingredients / For Chemical Resea
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inquiryTitanous chloride Basic information Product Name: Titanous chloride Synonyms: ALUMINUM TITANIUM CHLORIDE;ALUMINIUM CHLORIDE-TITANIUM TRICHLORIDE COMPLEX;TITANOU
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inquiryBest price Titanium(III) chloride CAS 7705-07-9 1.Professional manufacturer 2.Best price 3.Fast delivery 4.Prompt before and after sale service 5.Quality guarantee 6.Reliable and truthworthy supplier Appearance:Crystallized solid St
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titanium trichloride CAS#7705-07-9 Storage:Keep container tightly closed in a dry, cool and well-ventilated place. Package:25Kg/drum, 150Kg/drum, 200kg/drum, According to request. Transportation:By sea, by air.
bis(η6-toluene)titanium(0)
titanium tetrachloride
titanium(III) chloride
Conditions | Yield |
---|---|
In n-heptane byproducts: CH3C6H5; under purified Ar atm.; soln. of TiCl4 in heptane added to soln. of Ti(η6-MeC6H5)2 in heptane; mixt. stirred for 18 h at room temp.; solid filtered; washed (heptane); dried (vac.); elem. anal.; | 62% |
titanium tetrachloride
magnesium
A
titanium
C
titanium(III) chloride
D
magnesium chloride
Conditions | Yield |
---|---|
In neat (no solvent) Mg film exposing to TiCl4 at 1E-7 and 1E-6 Torr; monitoring by XPS; |
Conditions | Yield |
---|---|
reaction is vigorous below red heat;; | |
reaction is vigorous below red heat;; |
titanium
titanium tetrachloride
aluminium
A
aluminium trichloride
E
titanium(III) chloride
Conditions | Yield |
---|---|
In neat (no solvent) at 1100 K; further product TiAlCl5; identification by mass spectrometry; |
titanium
titanium tetrachloride
aluminium
A
aluminium trichloride
C
titanium(III) chloride
Conditions | Yield |
---|---|
In neat (no solvent) at 900 K; identification by mass spectrometry; |
titanium
titanium tetrachloride
aluminium
A
aluminium trichloride
D
titanium(III) chloride
Conditions | Yield |
---|---|
In neat (no solvent) at 1000 K; identification by mass spectrometry; |
titanium tetrachloride
copper
A
titanium(III) chloride
Conditions | Yield |
---|---|
In water room temp., exclusion of air;; |
Conditions | Yield |
---|---|
In gas Kinetics; |
Conditions | Yield |
---|---|
react. in closed tube at 890/440 K; | |
In neat (no solvent) 1100 K; | |
250 °C in tube; |
Conditions | Yield |
---|---|
In water | |
In hydrogenchloride metal dissoln. in concd. acid for 7 d; | |
In hydrogenchloride dissoln. of metallic titanium in distilled HCl under inert atmosphere; stored air-proof; |
Conditions | Yield |
---|---|
With tin In hydrogenchloride strong aq. HCl-soln.; | |
With C6H5CHOHCO2H byproducts: C6H5CHO, HCl, CO2; Irradiation (UV/VIS); | |
With sodium dithionite In not given byproducts: NaCl, SO2; in dild. acids; |
triethylaluminum
titanium tetrachloride
A
titanium
B
EtTiCl2
C
titanium(III) chloride
D
magnesium chloride
Conditions | Yield |
---|---|
In neat (no solvent) sample exposition to Al-compd. layer at 300 K for 10 min; monitoring by XPS; |
Conditions | Yield |
---|---|
With chlorine burning a flame of Cl2 and TiCl4-vapor in hydrogen atmosphere; |
hydrogen
titanium tetrachloride
B
chlorine
C
titanium(III) chloride
Conditions | Yield |
---|---|
In gas Kinetics; byproducts: HCl; Irradiation (UV/VIS); stationary photolysis in a sealed quartz cell at 210°C; vac.distn.; |
titanium(III) chloride
Conditions | Yield |
---|---|
With C; alkali chlorides; Cl2 In neat (no solvent) byproducts: CO2; Electrochem. Process; at 700 - 930°C;; |
Conditions | Yield |
---|---|
In gas Irradiation (UV/VIS); in a laser powder synthesis cell; 1330-1530°C; various yields for various conditions; X-ray diffraction; transmission electron microscopy; single point BET surface area analysis; thermal gravimetric analysis; differential thermalanalysis; atomic absorption spectroscopy; | A 50-70 B n/a |
Conditions | Yield |
---|---|
With hydrogenchloride byproducts: H2; | A 10-18 B n/a |
With HCl |
Conditions | Yield |
---|---|
With hydrogenchloride dry HCl gas, room temp., then 350-400°C for 18h; | |
With hydrogenchloride hot 20% HCl, under H2-stream; | A 0% B n/a |
With hydrogenchloride In water byproducts: H2; 300°C; |
Conditions | Yield |
---|---|
cooling, in vac., quartz tube, 800-900°C, 24h; 4-5 days, 600-700°C; |
Conditions | Yield |
---|---|
With chlorine |
Conditions | Yield |
---|---|
hydrolysis, heating in a bomb tube, 120°C; | |
hydrolysis, heating in a bomb tube, 120°C; |
Conditions | Yield |
---|---|
With hydrogen In gas byproducts: HCl; Irradiation (UV/VIS); in a laser powder synthesis cell; 1100°C; X-ray diffraction; transmission electron microscopy; single point BET surface area analysis; thermal gravimetric analysis; differential thermalanalysis; atomic absorption spectroscopy; | A 0% B n/a |
Conditions | Yield |
---|---|
In neat (no solvent) TiCl4 and Et2AlCl were reacted, solid was succesively treated with diisopropylether and TiCl4; |
Conditions | Yield |
---|---|
With nitrogen; hydrogen byproducts: HCl; glowing W-thread, TiCl3 precitipate on the vesselwall, thread temp. 1400-2000 K; | |
With N2; H2 byproducts: HCl; glowing W-thread, TiCl3 precitipate on the vesselwall, thread temp. 1400-2000 K; |
Conditions | Yield |
---|---|
In not given Electrolysis; | A 0% B n/a |
titanium tetrachloride
A
sulfur dioxide
B
titanium(III) chloride
C
sodium chloride
Conditions | Yield |
---|---|
In water reaction of TiCl4 with aq. Na2S2O4 forming TiCl3, NaCl and SO2; equilibrium reaction; forward reaction preferenced in an acidic soln. with an excess of Na2S2O4; reverse reaction preferenced in an alkaline soln.;; | |
In water reaction of TiCl4 with aq. Na2S2O4 forming TiCl3, NaCl and SO2; equilibrium reaction; forward reaction preferenced in an acidic soln. with an excess of Na2S2O4; reverse reaction preferenced in an alkaline soln.;; |
titanium(III) chloride
Conditions | Yield |
---|---|
In not given Electrolysis; |
2,2-bis(trifluoromethyl)-4,5-dichloro-4,5-difluoro-1,3-dioxolane
titanium(III) chloride
Conditions | Yield |
---|---|
In tetrahydrofuran | 100% |
TiCl3 In tetrahydrofuran |
Conditions | Yield |
---|---|
In further solvent(s) byproducts: MeCl; slow heating in neat Ph(Me)P(O)OMe until complete pptn.; particle size and polymerization degree depending on heating rate; | 100% |
tricyclo[5.2.1.0(2,6)]deca-2,4-dien-6-yllithium
titanium(III) chloride
Conditions | Yield |
---|---|
In tetrahydrofuran (Ar), added at -78°C, temp. quickly increased to 25°C, stirred for 14 h; treated with hydrochloric acid, extracted with chloroform, dried, evapd., recrystd. from dichloromethane/hexane; | A 2% B 98% C n/a |
1,4-dioxane
2-Adamantanone
titanium(III) chloride
adamantylidene-adamantane
Conditions | Yield |
---|---|
TiCl3 In argon | 97% |
thionyl chloride
titanium(III) chloride
bis(triphenylphosphine)iminium chloride
Conditions | Yield |
---|---|
In thionyl chloride (Ar), TiCl3 and ligand mixed (Ti:L=0.64:1.29), slowly treated with SOCl2under stirring, stirred for 4 h at room temp.; pptd.(pentane), filtered, washed (pentane), dried (vac.) for 3 h, elem. anal.; | 96% |
Conditions | Yield |
---|---|
In tetrahydrofuran | 95% |
titanium(III) chloride
Conditions | Yield |
---|---|
In tetrahydrofuran; dichloromethane byproducts: TiCl4; under N2 or Ar; TiCl3 soln. was added to a stirred slurry of equimolar amt. of CpMoCl4; pptn. over 1-2 min, filtered;; the ppt. was washed with CH2Cl2 and dried in vac.; elem. anal.;; | 95% |
N,N,N,N,N,N-hexamethylphosphoric triamide
titanium(III) chloride
TiCl3(((CH3)2N)3PO)3
Conditions | Yield |
---|---|
In tetrahydrofuran (N2), TiCl3 extracted into dry THF, organic compound added; collected, washed with n-hexane, pumped in vac. at room temp. for several hours; elem. anal.; | 95% |
niobium pentachloride
titanium(III) chloride
Conditions | Yield |
---|---|
In neat (no solvent, solid phase) byproducts: Nb3Cl8; Ar atmosphere, TlCl, TiCl3, Nb, NbCl5 in sealed quartz tube at 720 °C for 3 d, heating and cooling rates: 50 °/h; | 95% |
niobium pentachloride
titanium(III) chloride
Conditions | Yield |
---|---|
In neat (no solvent, solid phase) byproducts: Nb3Cl8; Ar atmosphere, RbCl, TiCl3, Nb, NbCl5 in sealed quartz tube at 720 °C for 3 d, heating and cooling rates: 50 °/h; | 95% |
niobium pentachloride
titanium(III) chloride
Conditions | Yield |
---|---|
In neat (no solvent, solid phase) byproducts: Nb3Cl8; Ar atmosphere, KCl, TiCl3, Nb, NbCl5 in sealed quartz tube at 720 °C for 3 d, heating and cooling rates: 50 °/h; | 95% |
niobium pentachloride
titanium(III) chloride
Conditions | Yield |
---|---|
In neat (no solvent, solid phase) byproducts: Nb3Cl8; Ar atmosphere, InCl, TiCl3, Nb, NbCl5 in sealed quartz tube at 720 °C for 3 d, heating and cooling rates: 50 °/h; | 95% |
niobium pentachloride
titanium(III) chloride
Conditions | Yield |
---|---|
In neat (no solvent, solid phase) byproducts: Nb3Cl8; Ar atmosphere, CsCl, TiCl3, Nb, NbCl5 in sealed quartz tube at 720 °C for 3 d, heating and cooling rates: 50 °/h; | 95% |
titanium(III) chloride
2-(3-nitrophenylamino)-3-oxobutanoic acid ethyl ester
Conditions | Yield |
---|---|
In hydrogenchloride; water; ethyl acetate; acetone | 95% |
thionyl chloride
hafnium tetrachloride
titanium(III) chloride
bis(triphenylphosphine)iminium chloride
Conditions | Yield |
---|---|
In neat (no solvent) (Ar), HfCl4, TiCl3, bis(triphenylphosphanyl)iminium chloride (1:1:2) treated dropwise under stirring with SOCl2, refluxed for 1 h, cooled to room temp., stirred for 2 h; concd.(vac.), pptd.(pentane), filtered, washed (pentane), dried (vac.) for 2 h, elem. anal.; | 94% |
thionyl chloride
N-benzyl-N,N,N-triethylammonium chloride
hafnium tetrachloride
titanium(III) chloride
Conditions | Yield |
---|---|
In neat (no solvent) (Ar), HfCl4, TiCl3, (Et3NBz)Cl (1:1:2) treated dropwise under stirring with SOCl2, refluxed for 1 h, cooled to room temp., stirred for 2 h; concd.(vac.), pptd.(pentane), filtered, washed (pentane), dried (vac.) for 2 h, elem. anal.; | 94% |
thionyl chloride
titanium(III) chloride
bis(triphenylphosphine)iminium chloride
Conditions | Yield |
---|---|
In thionyl chloride (Ar), TiCl3 and ligand mixed (Ti:L=0.73:1.09), slowly treated with SOCl2under stirring, stirred for 4 h at room temp.; pptd.(pentane), filtered, washed (pentane), dried (vac.) for 3 h, elem. anal.; | 93% |
titanium(III) chloride
Conditions | Yield |
---|---|
In chloroform; water; argon | 92% |
Conditions | Yield |
---|---|
In tetrahydrofuran the mixt. was refluxed for 22 h, ccoled to room temp. (Ar); ppt. was washed with pentane; | 92% |
titanium(III) chloride
N,N',N''-trimethyl-1,4,7-triazacyclononane
Conditions | Yield |
---|---|
In acetonitrile Under Ar, dissolving of TiCl3 under reflux, dropwise addn. of triazacyclononane, stirring (30 min, 20°C).; Filtn.; | 92% |
titanium(III) chloride
N,N',N''-trimethyl-1,4,7-triazacyclononane
TiCl3(C6H12N3(CH3)3)
Conditions | Yield |
---|---|
In acetonitrile Ar-purged soln. of TiCl3 in CH3CN refluxed for 30 min, cooled to room temp., dropwise addn. of ligand in CH3CN, stirred at 20°C for 30 min under Ar, blue pptn.; filtered, washed with dry Et2O, air dried; elem. anal.; | 92% |
Conditions | Yield |
---|---|
In tetrahydrofuran Ar-atmosphere; mixing indene derivative and slight excess of TiCl3, cooling to -78°C, dropwise addn. of THF, warming to room temp., refluxing for 4 h; concn. (vac.), extn. into CHCl3, addn. of 6 M HCl, stirring for 1 h, extn. of water layer with CH2Cl2, drying (MgSO4), concn.; isomer mixt. (dl:meso=1:1) not sepd., detd. by (1)H- and (13)C-NMR spectroscopy; | 92% |
1-(2-fluoro-3-methoxy-6-nitrophenyl)propan-2-one
titanium(III) chloride
2-methyl-4-fluoro-5-methoxy-1H-indole
Conditions | Yield |
---|---|
In water; acetone | 90% |
In water; acetone | 90% |
C5(CH3)4P(C6H5)2Li
titanium(III) chloride
Conditions | Yield |
---|---|
In tetrahydrofuran Ar atmosphere; addn. of org. ligand soln. to stirred suspn. of TiCl3; refluxing overnight; solvent removal (vac.); toluene addn. to residue; ppt. removal (filtration, frit, vac.-line); CCl4 addn. to filtrate; stirring (room temp., 1 h); solvent evapn. (reduced pressure); residue washing (pentane); elem. anal.; | 90% |
[2,2]bipyridinyl
titanium(III) chloride
tris-bipyridyl-(2,2') titanium (0)
Conditions | Yield |
---|---|
With sodium amalgam In tetrahydrofuran under oxygen-free nitrogen or argon or vac.; 2,2'-bpyridin was added toa suspn. of TiCl3 and sodium amalgam in THF; after stirring for 24 h atroom temp. and filtering, the soln. was reduced under vac.; diethylether was slowly added; ppt. was collected, washed with petroleum (b.p.40-60°C) and recrystd. from THF-diethylether; | 89% |
With Li In tetrahydrofuran all operations under N2 and Ar atm.; TiCl3 reacted with 3 equiv. amt. ofbipy and excess of Li in THF; purity checked by elem. anal., 1H and 13C NMR spectra; |
hydrogenchloride
titanium(III) chloride
1,2-bis(1-indenyl)benzene
(1,2-bis(1-indenyl)benzene)dichlorotitanium
Conditions | Yield |
---|---|
With N-BuLi In tetrahydrofuran; hexane N2-atmosphere; addn. of excess BuLi (in hexanes) to indene derivative (in THF) at -78°C, addn. to TiCl3 (in THF) at -78°C, warmingto room temp., refluxing for 6 h, concn., extn. into CHCl3, stirring wi th 6 M HCl for 1.5 h; extn. of water layer with CH2Cl2, drying (MgSO4), concn., filtration, washing (hexanes), drying (vac.); isomer mixt. (dl:meso=1:1) not sepd., detd. by (1)H- and (13)C-NMR spectroscopy; | 89% |
titanium(III) chloride
sodium hydrogencarbonate
methanesulfonyl chloride
Conditions | Yield |
---|---|
With pyridine In HCl-H2 O; dichloromethane; acetic acid; ethyl acetate | 88% |
thionyl chloride
N-benzyl-N,N,N-triethylammonium chloride
titanium(III) chloride
Conditions | Yield |
---|---|
In thionyl chloride (Ar), TiCl3 and ligand mixed (Ti:L=1.24:1.25), slowly treated with SOCl2under stirring, stirred for 4 h at room temp.; pptd.(pentane), filtered, washed (pentane), dried (vac.) for 3 h, elem. anal.; | 88% |
(CH3C5H3NNHC6H3CH3)2
titanium(III) chloride
Conditions | Yield |
---|---|
With KH In tetrahydrofuran (Ar); using Schlenk techniques; stirring of soln. of (MeC5H3NNHC6H3Me)2 and KH in THF for 12 h; filtration, addn. to soln. of TiCl3 in toluene at -60°C; warming to room temp., stirring for 12 h, filtration, addn. of PbCl2, stirring for 15 h; concn., extn. with toluene, filtration, concn., washing with pentane, drying under reduced pressure; | 87% |
titanium(III) chloride
bis(triphenylphosphine)iminium chloride
bis[bis(triphenylphosphanyl)iminium] ennachlorodititanate(IV)
Conditions | Yield |
---|---|
In thionyl chloride (Ar), TiCl3 and ligand mixed (Ti:L=3.67:1.83), slowly treated with SOCl2under stirring, stirred for 4 h at room temp.; pptd.(pentane), filtered, washed (pentane), dried (vac.), elem. anal.; | 87% |
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